CN103006509B - Emulsion compositions and apply its wet tissue - Google Patents
Emulsion compositions and apply its wet tissue Download PDFInfo
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- CN103006509B CN103006509B CN201210543740.0A CN201210543740A CN103006509B CN 103006509 B CN103006509 B CN 103006509B CN 201210543740 A CN201210543740 A CN 201210543740A CN 103006509 B CN103006509 B CN 103006509B
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Abstract
A kind of emulsion compositions, it contains cool feeling agent, heat sensitizer and water, and the mass ratio of wherein cool feeling agent, both heat sensitizers is 1:0.01-100; This cool feeling agent comprises at least one in menthol, menthol ester, hydrogenation of six carbocyclic amide derivatives, non-carbon Cydic amide derivatives, raw peppermint oil, Oleum menthae, Peppermint essential oil, mentha leave extracting solution, water solublity Mentholum, water solublity Oleum menthae; This heat sensitizer comprises at least one in cephrol butyl ether, vanillyl alcohol n-propyl ether, vanillyl alcohol isopropyl ether, vanillyl alcohol isobutyl ether, vanillyl alcohol n-amino ether, vanillyl alcohol isoamyl ether, cephrol n-hexyl ether, vanillyl alcohol methyl ether, vanillyl alcohol ethyl ether, zingiberol, shogaol, (4-hydroxy-3-methoxyphenyl)ethyl methyl ketone, capsaicin, capsaicin.Emulsion compositions of the present invention and apply the wet tissue of this emulsion compositions, processing technology is simple, with low cost, and can stimulate multiple sensory organ of human body skin, and the refreshment time compared with the single sensory product of human body is longer with only stimulating.
Description
Technical field
The present invention relates to a kind of emulsion compositions and apply the wet tissue of this emulsion compositions.
Background technology
Modern society's rhythm of life is accelerated, dog-eat-dog causes people to live and operating pressure increases, spirit emotion is often in high-pressure and excitedly state, easy appearance is tired, sleepy, the problems such as distractibility, impact study, work efficiency, even threat to life safety, as the driver time pass for a long time or open night shift bus time, there will be tired, doze unavoidably, easily cause vehicle accident, jeopardize individual and autre vie safety.To this, people are typically employed in the skin surface wiping material different from skin temperature or volatile material and change skin surface temperature, thus stimulate cerebral nervous system, inspire enthusiasm the fatigue that occurs when improving or eliminate work and study and sleepy sense.
Traditional mode normally adopts cold/warm water to wash one's face, to produce thermal stimulation thus inspire enthusiasm on skin, but the comparatively inconvenience out of doors of this mode.A lot of portable external preparation is as aerosol or smear series products, and these products mainly comprise following two kinds: (1) is using the composite plant liquid extract of many compositions as main refreshment composition; (2) using pennyroyal composition as main refreshment composition.The complicated process of preparation of (1) series products, cost is high, and normal using ethanol as the extractant of product, because ethanol content is higher, also can stimulate eyes and user be done not feel like oneself.(2) series products mainly allows people produce refrigerant sensation by the cold sensation organ or olfactory sensation that stimulate human body, thus plays the effect of refreshment, but the time that the usual cool feeling of this series products continues is shorter, and the effect of refreshment is unsatisfactory.
Summary of the invention
In view of this, be necessary to provide a kind of emulsion compositions, its preparation technology is simple, with low cost, and not containing ethanol, easy to use, refreshment effect is lasting.
In addition, there is a need to provide a kind of wet tissue containing above-mentioned emulsion compositions.
A kind of emulsion compositions, it contains cool feeling agent, heat sensitizer and water, and the mass ratio of wherein cool feeling agent, both heat sensitizers is 1:0.01-100, this cool feeling agent comprises at least one in menthol, menthol ester, hydrogenation of six carbocyclic amide derivatives, non-carbon Cydic amide derivatives, raw peppermint oil, Oleum menthae, Peppermint essential oil, mentha leave extracting solution, water solublity Mentholum, water solublity Oleum menthae, this heat sensitizer comprises cephrol butyl ether, vanillyl alcohol n-propyl ether, vanillyl alcohol isopropyl ether, vanillyl alcohol isobutyl ether, vanillyl alcohol n-amino ether, vanillyl alcohol isoamyl ether, cephrol n-hexyl ether, vanillyl alcohol methyl ether, vanillyl alcohol ethyl ether, zingiberol, shogaol, (4-hydroxy-3-methoxyphenyl)ethyl methyl ketone, capsaicin, capsaicin (N-(4-hydroxyl-3-methoxybenzy)-8-methyl pelargonamide, (6E)-N-(4-hydroxyl-3-methoxybenzy)-8-methyl-6-nonenamide), at least one in capsaicin analog.
A wet tissue containing above-mentioned emulsion compositions, it comprises base material and is absorbed in the emulsion compositions in base material, and wherein the mass ratio of emulsion compositions and base material is 1-5:1; Described base material is the material with water suction, water holding capacity.
Emulsion compositions of the present invention and apply the wet tissue of this emulsion compositions, processing technology is simple, with low cost, and esy to use, safe and reliable.The generation of usual heat sensitizer hotness is guided by cool feeling, therefore, when using this emulsion compositions, the existence of heat sensitizer can be strengthened sensation that refrigerant or ice that emulsion compositions produces feels well and intensity at product and contact skin initial stage and extend the cool feeling lasting time.In cool feeling close to disappear or when disappearing completely, the warmth sensation that the heat sensitizer in emulsion compositions provides, by the cool feeling before taking over, stimulates human body further thus extends effect of the refreshment that mixed liquor produces.In addition, this emulsion compositions, using water as solvent, avoids the skin irritation problem produced using ethanol as solvent.
Detailed description of the invention
Emulsion compositions of the present invention contains cool feeling agent, heat sensitizer and appropriate water, the mass ratio of wherein cool feeling agent, both heat sensitizers is 1:0.01-100, wherein the mass percentage of cool feeling agent in emulsion compositions is 0.05%-15%, and the mass percentage of heat sensitizer in emulsion compositions is 0.001%-5%.
After this cool feeling agent and contact skin can directly and the effect of human body skin cold sensation receptor teleneuron produce physiological action thus produce the refreshing sensation of refrigerant/ice.Produce physiological reaction with human thermal sensation's organ teleneuron after this heat sensitizer and contact skin thus produce warm sensation.
In this emulsion compositions, also alternative is added with fragrant atmosphere composition, and the mass ratio of wherein cool feeling agent, heat sensitizer and fragrant atmosphere composition three is 1:0.01-100:0.01-50, and the mass percentage of fragrant atmosphere composition in emulsion compositions is 0.001%-5%.This fragrant atmosphere composition is have the essence of or same characteristic features abnormal smells from the patient similar with at least one in Herba Menthae, Citrua paradiai, green tea, coffee, Fructus Citri Limoniae, Fructus Cucumidis sativi, lavandula angustifolia, spice, quintessence oil or extracting solution.This fragrant atmosphere composition can stimulate the olfactory sensation of human body to make people produce refrigerant, ice to feel well or clearly pleasant sensation, and then feels spirit and QI cleaning.
The generation of usual heat sensitizer hotness is guided by cool feeling, therefore, when using this emulsion compositions, the existence of heat sensitizer can be strengthened sensation that refrigerant or ice that emulsion compositions produces feels well and intensity at product and contact skin initial stage and extend the cool feeling lasting time.In cool feeling close to disappearance or when disappearing completely, the warmth sensation that heat sensitizer in emulsion compositions provides is by the cool feeling before taking over, further stimulation human body thus the effect extending the refreshment that produces of mixed liquor are (after heat sensitizer and contact human skin, the stimulation of similar cool feeling that what first human body was experienced is, then just hotness can be experienced, so this emulsion compositions first allow human feeling to be cool feeling, be then only hotness).The existence of fragrant atmosphere composition can strengthen refreshment effect while cool feeling agent and heat sensitizer performance function in emulsion compositions.Ternary exist simultaneously, can stimulate multiple sensory receptor officials of human body skin in use, and avoiding stimulates feeling fatigue or benumbing caused by same human body skin sensory organ separately, improves the effect of refreshing oneself of product.In addition, this emulsion compositions, using water as solvent, avoids the skin irritation problem produced using ethanol as solvent.
This cool feeling agent comprises at least one in menthol, menthol ester, hydrogenation of six carbocyclic amide derivatives, non-carbon Cydic amide derivatives, raw peppermint oil, Oleum menthae, Peppermint essential oil, mentha leave extracting solution, water solublity Mentholum, water solublity Herba Menthae wet goods.The freshener eutectic that this cool feeling agent is preferably made up of menthol ester, hydrogenation of six carbocyclic amide derivatives and non-carbon Cydic amide derivatives.
This menthol ester comprises at least one in Herba Menthae lactate, menthyl pyrrolidone carboxylate, menthyl succinate, 3-hydroxybutyrate menthyl ester, monomethyl succinate, p-menthyl-3-hydroxy acid-1-vinyl glyceride (WS-4), p-menthyl-3-hydroxy acid-1-glyceride (WS-30), 1,3-propanedicarboxylic acid-menthyl ester, 3-citraconic acid-menthyl ester, 2-citraconic acid ester group menthyl monomenthyl glutarate.
This hydrogenation of six carbocyclic amide derivatives comprises terpane formyl ethamine, N-(4-methoxyphenyl)-to menthyl-3-carboxylic acid amides (WS-12), the N-tert-butyl group-to menthyl-3-carboxylic acid amides (WS-14), N-(glycine ethyl ester base)-2-isopropyl-5-methyl-cyclohexyl alkane amide (WS-5), N-(2-(2-pyridine radicals) ethyl)-2-isopropyl-5-methyl-cyclohexyl alkane amide, N-(4-acetylphenyl)-to amide of mint, N-(4-hydroxymethyl phenyl)-to amide of mint and N-(3-hydroxy-4-methoxyphenyl)-to amide of mint, at least one in N-((5-methyl-2-(1-Methylethyl) cyclohexyl) carbonyl) alanine ethyl ester.
This non-carbon Cydic amide derivatives comprises at least one in methyl diisopropyl propionic acid amide., N, N-diethyl 2,2-dimethylpropionamide, N, N-diethyl 2-ethyl butyramide, heptane-2-carboxylic acid amides.
This heat sensitizer comprises at least one in cephrol butyl ether, vanillyl alcohol n-propyl ether, vanillyl alcohol isopropyl ether, vanillyl alcohol isobutyl ether, vanillyl alcohol n-amino ether, vanillyl alcohol isoamyl ether, cephrol n-hexyl ether, vanillyl alcohol methyl ether, vanillyl alcohol ethyl ether, zingiberol, shogaol, (4-hydroxy-3-methoxyphenyl)ethyl methyl ketone, capsaicin, capsaicin (N-(4-hydroxyl-3-methoxybenzy)-8-methyl pelargonamide and/or (6E)-N-(4-hydroxyl-3-methoxybenzy)-8-methyl-6-nonenamide), capsaicin analog, preferably cephrol butyl ether.
Further, be present in wet tissue in order to what make that emulsion compositions can be stable, emulsifying solubiliser can be added emulsion compositions is dispersed in wet tissue uniformly.This emulsifying solubiliser is that hydrophilic-hydrophobic balance value (Hydrophile-LipophileBalanceNumber, HLB) is greater than the single emulsifying solubiliser of hydrophilic of 10 or compound emulsifying solubiliser.Emulsifying solubiliser specifically comprises tween 20, Tween-60, tween 80, tween 20, tween 80, Tween-60, alkyl polyglucoside and derivant thereof, PEG-20 sucrose stearate, PEG-5 glyceryl stearate, Cremophor RH40, PEG-60 castor oil hydrogenated, ceteareth-6, ceteareth-25, stereth-2, stereth-21, laureth-4, laureth-23, single or the compound emulsifying solubiliser that PEG-40 tristerin forms.
Further, in order to improve the skin protection performance of this emulsion compositions, in emulsion compositions, also skin protectant can be added.This skin protectant comprises alcohols skin protectant, natural plants skin protectant, skin moistening oils and fats.Alcohols skin protectant comprises 1,3 butylene glycol, glycerol, propylene glycol, pentanediol etc.; Natural plants skin protectant comprises hyaluronate sodium, Aloe, collagen protein, oat beta-glucan, hydrolyzed wheat protein, Herba Lysimachiae foenum-graeci quintessence oil, Flos Rosae Rugosae quintessence oil, Semen pruni armeniacae oil, olive oil, Jojoba wet goods.Skin moistening oils and fats comprises isopropyl myristate, polydimethylsiloxane, Polyethylene Glycol-7 glyceryl cocoate, Polyethylene Glycol-6 caprylic/capric glyceride type, dicaprylyl carbonate, caprylic/capric triglyceride, isopropyl palmitate, octyl palmitate, Vitamin E acetate etc.
Further, in order to improve the antiinflammatory antiallergic performance of emulsion compositions, natural antiinflammatory anti-allergic agent can be added in emulsion compositions, improving the irritation of skin environment to external world.This antiinflammatory anti-allergic agent comprises Flos Matricariae chamomillae extracting solution, bisabolol, Flos Lonicerae extractive solution, tea tree ethereal oil, Flos Inulae extracting solution, Radix Glycyrrhizae and derivant, Rhizoma Zingiberis Recens extracting solution, Herba Portulacae extract etc.
Further, in order to make the acid-base value of emulsion compositions close to the acid-base balance value of skin, also appropriate pH adjusting agent can be added in emulsion compositions, as citric acid, sodium citrate, triethanolamine etc.
Further, in order to improve the storage time of emulsion compositions, appropriate antiseptic can be added in emulsion compositions.
Further, the actual demand to meet emulsion compositions such as film former, thickening agent, other surfactant can also be added in emulsion compositions.
Wet tissue of the present invention comprises base material and is absorbed in the emulsion compositions in base material, and wherein the mass ratio of emulsion compositions and base material is 1-5:1.Described base material is the material with water suction, water holding capacity, concrete non-woven fabrics, cotton, gauze, towel, wet-strength paper etc.
Emulsion compositions of the present invention and apply the wet tissue of this emulsion compositions, processing technology is simple, with low cost, and can stimulate multiple sensory organ of human body skin, and the refreshment time compared with the single sensory product of human body is longer with only stimulating.In addition due to using water as solvent, with ethanol as solvent refreshment product compared with skin irritation reduce, and esy to use, safe and reliable.
Below by embodiment, the present invention is specifically described.
Embodiment 1
Prepared by emulsion compositions: about 70% water adds in allotment bucket by (1), adds in keg by the tween 20 of cephrol butyl ether and 0.5%, after being uniformly mixed, adding after appropriate water continues stirring and emulsifying (emulsion should be creamy white) and adds in allotment bucket; (2) tween 20 of freshener eutectic and 2.0% is added in keg, after being uniformly mixed, adding after appropriate water continues stirring and emulsifying (emulsion should be creamy white) and add in allotment bucket; (3) Aloe, Flos Matricariae chamomillae extracting solution, glycerol, cucumber extract, antiseptic are added in allotment bucket, stir, finally add pH adjusting agent by about the pH regulator to 6.0 of mixed emulsion.
The formula of emulsion compositions is specifically joined shown in table one.
Wet tissue makes: be that 3:1 adds on base material (addition manner is soak) by emulsion compositions according to the mass ratio of emulsion compositions and base material, then cuts into required size and can obtain required wet tissue.
Table one
Embodiment 2
Prepared by emulsion compositions: about 70% water adds in allotment bucket by (1), adds in keg by the tween 20 of cephrol butyl ether and 1.5%, after being uniformly mixed, adding after appropriate water continues stirring and emulsifying (emulsion should be creamy white) and adds in allotment bucket; (2) Citrua paradiai essence and Cremophor RH40 are added in keg, after being uniformly mixed, adding after appropriate water continues stirring and emulsifying (emulsion should be creamy white) and add in allotment bucket; (3) tween 20 of tea tree ethereal oil and 0.5% is added in keg, after being uniformly mixed, adding after appropriate water continues stirring and emulsifying and add in allotment bucket; (4) successively 1,3 butylene glycol, water solublity Oleum menthae, mentha leave extracting solution, Flos Lonicerae extractive solution, antiseptic are added in allotment bucket, stir, finally add pH adjusting agent by about the pH regulator to 6.0 of mixed emulsion.
The formula of emulsion compositions is specifically joined shown in table two.
Wet tissue makes: be that 3.5:1 adds (addition manner is spray) on base material to by emulsion compositions according to the mass ratio of Emulsion combination and base material, then cuts into required size and can obtain required wet tissue.
Table two
Through verification experimental verification: use the wet tissue scrape skin of embodiment 1-2 can produce lasting effect of refreshing oneself.
In addition, those skilled in the art also can make various amendments in other form and details, interpolation and replacement in the claims in the present invention scope of disclosure and spirit.Certainly, the changes such as these various amendments made according to the present invention's spirit, interpolation and replacement, all should be included within the present invention's scope required for protection.
Claims (7)
1. an emulsion compositions, is characterized in that: this emulsion compositions contains cool feeling agent, heat sensitizer, fragrant atmosphere composition and water, and the mass ratio of wherein cool feeling agent, heat sensitizer and fragrant atmosphere composition three is 1:0.01-0.3:0.01-50; The mass percentage of cool feeling agent in emulsion compositions is 0.05%-15%, and the mass percentage of heat sensitizer in emulsion compositions is 0.001%-5%, and the mass percentage of fragrant atmosphere composition in emulsion compositions is 0.001%-5%;
The freshener eutectic that this cool feeling agent is made up of menthol ester, hydrogenation of six carbocyclic amide derivatives and non-carbon Cydic amide derivatives, wherein, menthol ester is selected from least one in Herba Menthae lactate, menthyl pyrrolidone carboxylate, menthyl succinate, 3-hydroxybutyrate menthyl ester, monomethyl succinate, p-menthyl-3-hydroxy acid-1-vinyl glyceride (WS-4), p-menthyl-3-hydroxy acid-1-glyceride (WS-30), 1,3-propanedicarboxylic acid-menthyl ester, 3-citraconic acid-menthyl ester, 2-citraconic acid ester group menthyl monomenthyl glutarate, hydrogenation of six carbocyclic amide derivatives is selected from terpane formyl ethamine, N-(4-methoxyphenyl)-to menthyl-3-carboxylic acid amides (WS-12), the N-tert-butyl group-to menthyl-3-carboxylic acid amides (WS-14), N-(glycine ethyl ester base)-2-isopropyl-5-methyl-cyclohexyl alkane amide (WS-5), N-(2-(2-pyridine radicals) ethyl)-2-isopropyl-5-methyl-cyclohexyl alkane amide, N-(4-acetylphenyl)-to amide of mint, N-(4-hydroxymethyl phenyl)-to amide of mint and N-(3-hydroxy-4-methoxyphenyl)-to amide of mint, at least one in N-((5-methyl-2-(1-Methylethyl) cyclohexyl) carbonyl) alanine ethyl ester, non-carbon Cydic amide derivatives is selected from least one in methyl diisopropyl propionic acid amide., N, N-diethyl 2,2-dimethylpropionamide, N, N-diethyl 2-ethyl butyramide, heptane-2-carboxylic acid amides,
This heat sensitizer is selected from least one in cephrol butyl ether, vanillyl alcohol n-propyl ether, vanillyl alcohol isopropyl ether, vanillyl alcohol isobutyl ether, vanillyl alcohol n-amino ether, vanillyl alcohol isoamyl ether, cephrol n-hexyl ether, vanillyl alcohol methyl ether, vanillyl alcohol ethyl ether, zingiberol, shogaol, (4-hydroxy-3-methoxyphenyl)ethyl methyl ketone, capsaicin, N-(4-hydroxyl-3-methoxybenzy)-8-methyl pelargonamide, (6E)-N-(4-hydroxyl-3-methoxybenzy)-8-methyl-6-nonenamide;
This fragrant atmosphere composition is have the essence of or same characteristic features abnormal smells from the patient similar with at least one in Herba Menthae, Citrua paradiai, green tea, coffee, Fructus Citri Limoniae, Fructus Cucumidis sativi, lavandula angustifolia, spice, quintessence oil or extracting solution;
Cool feeling is first provided to reoffer hotness when this emulsion compositions and contact skin.
2. emulsion compositions as claimed in claim 1, is characterized in that: this emulsion compositions is also containing emulsifying solubiliser, and this emulsifying solubiliser is that hydrophilic-hydrophobic balance value is greater than the single emulsifying solubiliser of hydrophilic of 10 or compound emulsifying solubiliser.
3. emulsion compositions as claimed in claim 2, is characterized in that: the single or compound emulsifying solubiliser that this emulsifying solubiliser is selected from tween 20, Tween-60, tween 80, alkyl polyglucoside, PEG-20 sucrose stearate, PEG-5 glyceryl stearate, Cremophor RH40, PEG-60 castor oil hydrogenated, ceteareth-6, ceteareth-25, stereth-2, stereth-21, laureth-4, laureth-23, PEG-40 tristerin form.
4. emulsion compositions as claimed in claim 1, is characterized in that: be also added with at least one in skin protectant, antiinflammatory anti-allergic agent, pH adjusting agent, antiseptic, film former, thickening agent, surfactant in this emulsion compositions.
5. emulsion compositions as claimed in claim 4, it is characterized in that: this skin protectant is selected from alcohols skin protectant, natural plants skin protectant, skin moistening oils and fats, this alcohols skin protectant is selected from glycerol, 1,3 butylene glycol, propylene glycol, pentanediol, Polyethylene Glycol; This natural plants skin protectant is selected from Aloe, collagen protein, oat beta-glucan, hydrolyzed wheat protein, transparent sodium phytate, Herba Lysimachiae foenum-graeci quintessence oil, Flos Rosae Rugosae quintessence oil, Semen pruni armeniacae oil, olive oil; This skin moistening oils and fats is selected from caprylic/capric triglyceride, octyl palmitate, polydimethylsiloxane, dicaprylyl carbonate, isopropyl myristate, isopropyl palmitate, white mineral oil, Vitamin E acetate.
6. emulsion compositions as claimed in claim 4, is characterized in that: this antiinflammatory anti-allergic agent is selected from Flos Matricariae chamomillae extracting solution, bisabolol, Flos Lonicerae extractive solution, tea tree ethereal oil, Flos Inulae, Radix Glycyrrhizae, Rhizoma Zingiberis Recens extracting solution, Herba Portulacae extract; This pH adjusting agent is selected from citric acid, sodium citrate, triethanolamine.
7. the wet tissue containing emulsion compositions described in any one in claim 1-6, it comprises base material and is absorbed in the emulsion compositions in base material, and wherein the mass ratio of emulsion compositions and base material is 1-5:1; Described base material is non-woven fabrics, cotton, gauze, towel or wet-strength paper.
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| CN103315930A (en) * | 2013-05-31 | 2013-09-25 | 花之町（厦门）日用品有限公司 | Special wet tissue for blowing one's nose |
| CN103432029B (en) * | 2013-08-15 | 2016-02-17 | 金红叶纸业集团有限公司 | Compositions and apply its napkin |
| CN103479921A (en) * | 2013-09-29 | 2014-01-01 | 李宏江 | Acne herb tea and acne removal wet tissue combined acne treatment partner |
| CN104138349B (en) * | 2014-07-25 | 2017-01-11 | 嘉兴市蝶柔化妆品有限公司 | Mask achieving skin ruddiness, face dark removal and moisture preservation functions and production method thereof |
| CN104473836A (en) * | 2014-11-20 | 2015-04-01 | 柳江县联华纸制品厂 | Cleansing wet tissue |
| CN105411913A (en) * | 2015-12-01 | 2016-03-23 | 赵雅珺 | Makeup removal wet tissue |
| CN105662982B (en) * | 2016-03-31 | 2018-07-31 | 广州皙泉品牌管理有限公司 | A kind of cold and hot SPA eye essences breast and the preparation method and application thereof |
| CN108338938A (en) * | 2017-11-10 | 2018-07-31 | 李斌 | A kind of preparation method of hygenic towelette |
| CN108125797A (en) * | 2018-01-02 | 2018-06-08 | 深圳市芭格美生物科技有限公司 | A kind of hand mouth wet tissue and preparation method thereof |
| EP3810078A1 (en) * | 2018-06-22 | 2021-04-28 | The Procter & Gamble Company | Dentifrice compositions |
| CN108771640B (en) * | 2018-09-07 | 2020-06-09 | 广州立白企业集团有限公司 | Ethanol-free anti-mosquito composition capable of improving efficacy of menthyl-3, 8-diol |
| CN113133950A (en) * | 2021-03-24 | 2021-07-20 | 深圳全棉时代科技有限公司 | Composition and solution for refreshing and relieving fatigue and application thereof |
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