CN102993936B - Anticorrosive quick-drying orange-figured paint with high third dimension and preparation method thereof - Google Patents
Anticorrosive quick-drying orange-figured paint with high third dimension and preparation method thereof Download PDFInfo
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- CN102993936B CN102993936B CN201210508552.4A CN201210508552A CN102993936B CN 102993936 B CN102993936 B CN 102993936B CN 201210508552 A CN201210508552 A CN 201210508552A CN 102993936 B CN102993936 B CN 102993936B
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Abstract
The invention discloses an anticorrosive quick-drying orange-figured paint with a high third dimension and a preparation method thereof. The anticorrosive quick-drying orange-figured paint comprises the following components in percentage by weight: A components consisting of resin with active hydroxyl, dispersing agent, pigment, mixed organic solvent, bentonite, dibutyltin dilaurate and ore-figured agent; B components consisting of butyl acetate, dehydrating agent and condensate, wherein in a using process, the mixing ratio by weight of A components to the B components is (3-5) to 1. The anticorrosive quick-drying orange-figured paint with the high third dimension provided by the invention is proportioned and mixed according to a specified ratio in a construction process and then directly sprayed once; moreover, compared with the prior art, the thickness of the dry film can be reduced by about 20 microns (the thickness of the dry film being 45 plus or minus 5 microns), so that the third dimension effect of figures can be doubled, and the drying time is short.
Description
Technical field
This product belongs to chemical technology field, relates to a kind of decorative paints of protection against corrosion class patterned effect, is specifically related to a kind of protection against corrosion high stereoscopic sensation quick-dry type tangerine line paint and preparation method thereof.Be applicable to the protection decoration applications such as all kinds of machinery, equipment, lathe, the hackly flaw in various metallic surface can be covered up and play art decorative effect.
Background technology
The product tangerine line coating construction process of prior art is loaded down with trivial details, and effect of decorative patterns is not obvious, the defect (needing just can be delivered for use after application for seven days) that the drying varniss time is slow.What adopt is long oil Synolac and cobalt, manganese, plumbous class siccative, color stuffing, 200 ﹟ solvent oils, dimethylbenzene make.General application twice: first working viscosity is adjusted rarer a little, are advisable to hide the end; After 15-30 minute, spraying second, now working viscosity is larger than first, and adopt continuously, interval, the gimmicks such as specking, make salient point even.Build 65 ± 5um.The tangerine line coating construction process of prior art is loaded down with trivial details, and effect of decorative patterns stereoscopic sensation is not enough, the defect that time of drying is slow.
Summary of the invention
The object of the present invention is to provide a kind of protection against corrosion high stereoscopic sensation quick-dry type tangerine line paint.
Another object of the present invention is to the preparation method that a kind of protection against corrosion high stereoscopic sensation quick-dry type tangerine line paint is provided.
Object of the present invention can be achieved through the following technical solutions:
A kind of protection against corrosion high stereoscopic sensation quick-dry type tangerine line paint, weight percentage, it comprises following component:
Component A
Containing the resin 50% ~ 75% of activity hydroxy
Dispersion agent 0.5% ~ 1.5%
Pigment 3% ~ 26%
Mixed organic solvents 15% ~ 20%
Wilkinite 0.1% ~ 2%
Dibutyl tin laurate 0.1% ~ 1%
In tangerine line agent 0.1% ~ 2%(A component, the weight percentage sum of each component is 100%)
B component
N-BUTYL ACETATE 20% ~ 49.9%
Dewatering agent 0.1% ~ 0.3%
In solidifying agent 50% ~ 79.9%(B component, the weight percentage sum of each component is 100%)
During use, the Mixing ratio by weight of component A and B component is 3 ~ 5:1.
Preferably, the weight percentage of each component is:
Component A
Containing the resin 60% ~ 70% of activity hydroxy
Dispersion agent 0.5% ~ 1.5%
Pigment 5% ~ 20%
Mixed organic solvents 15% ~ 20%
Wilkinite 0.1% ~ 0.5%
Dibutyl tin laurate 0.1% ~ 0.5%
Tangerine line agent 0.5% ~ 1%
B component
N-BUTYL ACETATE 30% ~ 39.9%
Dewatering agent 0.1% ~ 0.3%
Solidifying agent 60% ~ 69.9%
During use, the Mixing ratio by weight of component A and B component is 4:1.
The described resin containing activity hydroxy is preferably Hydroxylated acrylic resin.
Described solidifying agent is isocyanate prepolymer.
Described dispersion agent is preferably BYK-163 or the dispersion agent of the same type with BYK-163.
Described mixed organic solvent is that toluene and N-BUTYL ACETATE are mixed to get by the weight ratio of 1:1.
Can need to select suitable pigment according to client, as white paint selects titanium dioxide as pigment.
The preparation method of above-mentioned protection against corrosion high stereoscopic sensation quick-dry type tangerine line paint comprises the following steps:
(1) component A is prepared: take containing after the mixing of the resin of activity hydroxy, dispersion agent, pigment, mixed organic solvents and wilkinite in proportion, first 800 ~ 1200r/min disperses 20 ~ 30min in a kettle., and then be ground to fineness≤20 μm, after finally adding dibutyl tin laurate and the agent of tangerine line again, 800 ~ 1200r/min disperses 5 ~ 10min to make component A in a kettle.; Temperature in twice dispersion process controls at 25 ~ 35 DEG C;
(2) B component is prepared: in proportion N-BUTYL ACETATE and dewatering agent are mixed rear standing 30 ~ 50min, add solidifying agent again and stir and make B component (the whole production process of B component is carried out under air dried condition, relative air humidity < 85 ﹪).
Beneficial effect of the present invention:
It is loaded down with trivial details that protection against corrosion high stereoscopic sensation quick-dry type tangerine line paint prepared by the present invention mainly solves prior art construction technology, and effect of decorative patterns stereoscopic sensation is not enough, the defect that time of drying is slow.After allocating according to the specified ratio in construction process, direct spraying together, and paint film build can reduce about 20 μm (builds 45 ± 5 μm) than prior art, third dimension of patterns effect can up to prior art one times, time of drying is (surface drying < 30 minutes soon, do solid work < 24 hours, i.e. application all referable uses one day after).
Embodiment
Reaction raw materials
Resin containing activity hydroxy: brilliant same moral Chemical Co., Ltd. of Hydroxylated acrylic resin (AC1010-C) Foshan City
Dispersion agent: BYK-163, German BYK company.
Pigment: Rutile type Titanium Dioxide (R-996, Sichuan Long Mang group)
Mixed organic solvents: toluene and N-BUTYL ACETATE press the mixed solvent of 1:1 weight ratio.
Dewatering agent: F-180, German Lyar company
Solidifying agent: isocyanate prepolymer: three wooden 775K
Wilkinite, dibutyl tin laurate, the agent of tangerine line, the commercially available conventional products of N-BUTYL ACETATE.
Embodiment 1
A kind of protection against corrosion high stereoscopic sensation quick-dry type tangerine line paint, weight percentage, it comprises following component:
Component A
Containing the resin 65% of activity hydroxy
Dispersion agent 1%
Pigment 15%
Mixed organic solvents 18%
Wilkinite 0.2%
Dibutyl tin laurate 0.2%
Tangerine line agent 0.6%
B component
N-BUTYL ACETATE 35%
Dewatering agent 0.2%
Solidifying agent 64.8%
During use, the Mixing ratio by weight of component A and B component is 4:1.
Preparation technology:
(1) component A is prepared: take containing after the mixing of the resin of activity hydroxy, dispersion agent, pigment, mixed organic solvents and wilkinite in proportion, first 1000r/min disperses 25min in a kettle., and then be ground to fineness≤20 μm, after finally adding dibutyl tin laurate and the agent of tangerine line again, 1000r/min disperses 8min to make component A in a kettle.; Temperature in twice dispersion process controls at 25 ~ 35 DEG C;
(2) B component is prepared: in proportion N-BUTYL ACETATE and dewatering agent are mixed rear standing 40min, add solidifying agent again and stir and make B component (the whole production process of B component is carried out under air dried condition, relative air humidity < 85 ﹪).
Embodiment 2
A kind of protection against corrosion high stereoscopic sensation quick-dry type tangerine line paint, weight percentage, it comprises following component:
Component A
Containing the resin 60% of activity hydroxy
Dispersion agent 1%
Pigment 18%
Mixed organic solvents 20%
Wilkinite 0.2%
Dibutyl tin laurate 0.2%
Tangerine line agent 0.6%
B component
N-BUTYL ACETATE 30%
Dewatering agent 0.3%
Solidifying agent 69.7%
During use, the Mixing ratio by weight of component A and B component is 4:1.
Preparation technology is with embodiment 1.
Embodiment 3
A kind of protection against corrosion high stereoscopic sensation quick-dry type tangerine line paint, weight percentage, it comprises following component:
Component A
Containing the resin 70% of activity hydroxy
Dispersion agent 1%
Pigment 13%
Mixed organic solvents 15%
Wilkinite 0.2%
Dibutyl tin laurate 0.2%
Tangerine line agent 0.6%
B component
N-BUTYL ACETATE 39%
Dewatering agent 0.2%
Solidifying agent 60.8%
During use, the Mixing ratio by weight of component A and B component is 4:1.
Preparation technology is with embodiment 1.
Embodiment 4
A kind of protection against corrosion high stereoscopic sensation quick-dry type tangerine line paint, weight percentage, it comprises following component:
Component A
Containing the resin 50% of activity hydroxy
Dispersion agent 1%
Pigment 25%
Mixed organic solvents 20%
Wilkinite 2%
Dibutyl tin laurate 0.5%
Tangerine line agent 1.5%
B component
N-BUTYL ACETATE 20%
Dewatering agent 0.3%
Cured article 79.7%
During use, the Mixing ratio by weight of component A and B component is 4:1.
Preparation technology is with embodiment 1.
Embodiment 5
A kind of protection against corrosion high stereoscopic sensation quick-dry type tangerine line paint, weight percentage, it comprises following component:
Component A
Containing the resin 75% of activity hydroxy
Dispersion agent 0.5%
Pigment 7.5%
Mixed organic solvents 16%
Wilkinite 0.2%
Dibutyl tin laurate 0.2%
Tangerine line agent 0.6%
B component
N-BUTYL ACETATE 20% ~ 49.9%
Dewatering agent 0.1% ~ 0.3%
Cured article 50% ~ 79.9%
During use, the Mixing ratio by weight of component A and B component is 4:1.
Preparation technology is with embodiment 1.
The performance test results of protection against corrosion high stereoscopic sensation quick-dry type tangerine line paint prepared by table 1 embodiment 1-5
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Hardness | 2H | 2H | 2H | 2H | 2H |
| The h of resistance to lubricating oil | 96 | 95 | 90 | 88 | 85 |
| Sticking power | 5B | 5B | 5B | 5B | 5B |
| Solid content % | 56 | 56 | 58 | 60 | 54 |
Conclusion: after allocating according to the specified ratio in construction process, direct spraying together, sticking power is high, hardness is large, resistance to lubricating oil, and paint film build can reduce about 20 μm (builds 45 ± 5 μm) than prior art, third dimension of patterns effect reaches 1 times than prior art raising, and time of drying is (surface drying < 30 minutes soon, do solid work < 24 hours, i.e. application all referable uses one day after).
Claims (5)
1. a protection against corrosion high stereoscopic sensation quick-dry type tangerine line paint, it is characterized in that weight percentage, it is made up of following component:
Component A
Containing the resin 50% ~ 75% of activity hydroxy
Dispersion agent 0.5% ~ 1.5%
Pigment 3% ~ 26%
Mixed organic solvents 15% ~ 20%
Wilkinite 0.1% ~ 2%
Dibutyl tin laurate 0.1% ~ 1%
Tangerine line agent 0.1% ~ 2%
B component
N-BUTYL ACETATE 20% ~ 49.9%
Dewatering agent 0.1% ~ 0.3%
Solidifying agent 50% ~ 79.9%
During use, the Mixing ratio by weight of component A and B component is 3 ~ 5:1;
In component A and B component, the weight percentage sum of each component is 100%;
The described resin containing activity hydroxy is Hydroxylated acrylic resin;
Described solidifying agent is isocyanate prepolymer.
2. protection against corrosion high stereoscopic sensation quick-dry type tangerine line paint according to claim 1, is characterized in that composed of the following components:
Component A
Containing the resin 60% ~ 70% of activity hydroxy
Dispersion agent 0.5% ~ 1.5%
Pigment 5% ~ 20%
Mixed organic solvents 15% ~ 20%
Wilkinite 0.1% ~ 0.5%
Dibutyl tin laurate 0.1% ~ 0.5%
Tangerine line agent 0.5% ~ 1%
B component
N-BUTYL ACETATE 30% ~ 39.9%
Dewatering agent 0.1% ~ 0.3%
Solidifying agent 60% ~ 69.9%
During use, the Mixing ratio by weight of component A and B component is 4:1;
In component A and B component, the weight percentage sum of each component is 100%.
3. protection against corrosion high stereoscopic sensation quick-dry type tangerine line paint according to claim 1, is characterized in that described mixed organic solvents is that toluene and N-BUTYL ACETATE are mixed to get by the weight ratio of 1:1.
4. protection against corrosion high stereoscopic sensation quick-dry type tangerine line paint according to claim 1, is characterized in that adopting following steps preparation:
(1) component A is prepared: take containing after the mixing of the resin of activity hydroxy, dispersion agent, pigment, mixed organic solvents and wilkinite in proportion, first 800 ~ 1200r/min disperses 20 ~ 30min in a kettle., and then be ground to fineness≤20 μm, after finally adding dibutyl tin laurate and the agent of tangerine line again, 800 ~ 1200r/min disperses 5 ~ 10min to make component A in a kettle.; Temperature in twice dispersion process controls at 25 ~ 35 DEG C;
(2) B component is prepared: N-BUTYL ACETATE and dewatering agent are mixed in proportion and leave standstill 30 ~ 50min afterwards, then add solidifying agent and stir and make B component.
5. the preparation method of protection against corrosion high stereoscopic sensation quick-dry type tangerine line paint according to claim 1, is characterized in that comprising the following steps:
(1) component A is prepared: take containing after the mixing of the resin of activity hydroxy, dispersion agent, pigment, mixed organic solvents and wilkinite in proportion, first 800 ~ 1200r/min disperses 20 ~ 30min in a kettle., and then be ground to fineness≤20 μm, after finally adding dibutyl tin laurate and the agent of tangerine line again, 800 ~ 1200r/min disperses 5 ~ 10min to make component A in a kettle.; Temperature in twice dispersion process controls at 25 ~ 35 DEG C;
(2) B component is prepared: N-BUTYL ACETATE and dewatering agent are mixed in proportion and leave standstill 30 ~ 50min afterwards, then add solidifying agent and stir and make B component.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210508552.4A CN102993936B (en) | 2012-12-03 | 2012-12-03 | Anticorrosive quick-drying orange-figured paint with high third dimension and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210508552.4A CN102993936B (en) | 2012-12-03 | 2012-12-03 | Anticorrosive quick-drying orange-figured paint with high third dimension and preparation method thereof |
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| Publication Number | Publication Date |
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| CN102993936A CN102993936A (en) | 2013-03-27 |
| CN102993936B true CN102993936B (en) | 2015-06-10 |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104861842A (en) * | 2015-06-08 | 2015-08-26 | 成都拜迪新材料有限公司 | Method for preparing highly weather-resistant and three-dimension orange-peel finish |
| CN105219260B (en) * | 2015-11-05 | 2018-02-16 | 单华俊 | Double-layer polyester modified organic silicon tangerine line coating and its production and use |
| CN109468040A (en) * | 2018-10-11 | 2019-03-15 | 河北晨阳工贸集团有限公司 | A kind of superpower three-dimensional hydronasty orange-peel paint |
| CN114907758A (en) * | 2022-05-17 | 2022-08-16 | 浙江伟星实业发展股份有限公司 | Napagi dermatoglyph paint and preparation method and application thereof |
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|---|---|---|---|---|
| CN102140305A (en) * | 2011-03-07 | 2011-08-03 | 中国海洋石油总公司 | Polyurethane orange-peel coating |
| CN102220078A (en) * | 2011-05-10 | 2011-10-19 | 深圳市天健涂料科技开发有限公司 | Orangefigured paint, preparation method and construction process thereof |
| CN102796438A (en) * | 2012-08-16 | 2012-11-28 | 广州立邦涂料有限公司 | Orange peel pattern wrinkled epoxy floor paint and its preparation method |
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2012
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102140305A (en) * | 2011-03-07 | 2011-08-03 | 中国海洋石油总公司 | Polyurethane orange-peel coating |
| CN102220078A (en) * | 2011-05-10 | 2011-10-19 | 深圳市天健涂料科技开发有限公司 | Orangefigured paint, preparation method and construction process thereof |
| CN102796438A (en) * | 2012-08-16 | 2012-11-28 | 广州立邦涂料有限公司 | Orange peel pattern wrinkled epoxy floor paint and its preparation method |
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Address after: No.888, Huhuang Avenue, Fangqiao Town Industrial Zone, Yixing City, Wuxi City, Jiangsu Province Patentee after: Huhuang New Material Technology Group Co.,Ltd. Address before: No.888, Huhuang Avenue, Fangqiao Town Industrial Zone, Yixing City, Wuxi City, Jiangsu Province Patentee before: WUXI HUHUANG PAINT Co.,Ltd. |
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