CN102973747A - Bath fumigating liquid and preparation process thereof - Google Patents
Bath fumigating liquid and preparation process thereof Download PDFInfo
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Abstract
The present invention relates to a bath fumigating drug liquid prepared by adopting Hmong medicinal plants as raw materials. The bath fumigating drug liquid comprises, by weight, 2.5-5.0 parts of sargenrgloryvine, 1.0-2.0 parts of tatarinow sweetflag rhizome, 1.5-3.0 parts of polygonum perfoliatum, 1.5-3.0 parts of tasselblower, 2.0-4.0 parts of rose glorybower twig and leaf, 2.5-5.0 parts of moxa, 2.5-5.0 parts of Chinese ivy herb (variant), and 3.0-4.0 parts of szechwan lovage rhizome. The bath fumigating drug liquid is applicable for leisure, skin cleaning, fatigue eliminating, recovery promoting after recovery from illness of health bath, medicine bath treatment methods of subhealth (fatigue syndrome), common cold, skin pruritus, chronic gastroenteritis (yang deficiency cold type), lumbar vertebrae hyperosteogeny, soft tissue strain, anchylosis, muscle adhesion and joint swelling and pain, fumigating treatment methods, hot compress treatment methods and cold compress treatment methods.
Description
Technical field
The present invention relates to Miao ethnic group's medicinal plants is the shower of raw material making, the medicinal liquid of stifling usefulness.
Background technology
Having a lot of synthetic compounds or synthetic compound to add the animals and plants extract in the prior art is the bath foam that effective ingredient is made, and can play the effect of cleaning skin, and what have has certain skin protection, a skin moistening effect.
For example: Shiseido favour profit bath gel, mainly contain Aloe, vitamin E moisturizing elite composition, form moist protecting film on the skin top layer, play the problem of the rear scaly dry skin that prevents from taking a shower.
The elegant bath gel of L'Oreal's crystal, mainly contain Flos Rosae Rugosae, Magnolia denudata Desr., ten thousand longevity Fructus Citri tangerinaes, Flos Jasmini Sambac, five pulse conditions of ZANG-organs Cortex Melaleucae leucadendrae, Herba Menthae, Herba pyrolae japonicae, obtain 28 kinds of fresh fruit flowers and plants quintessence oils such as reed grass and natural honey, the hot spring mineral salt is formulated, the special long-acting plant moisturizing elite effective ingredient that adds, play cleaning, Glycerin, the clean demodicid mite of degerming, anophelifuge, itching-relieving action.
The Amway bath gel mainly contains glycerol, natural honey, mandarin orange elite, plays gentle moistening, and helps skin to resist the infringement of free radical etc., makes the tender children of skin sliding moist.
Occurred also afterwards that some have will be with the bathing product of function, such as " huoxue Tongluo Tang, contains Flos Carthami, Olibanum, Myrrha, Radix Paeoniae Rubra etc. and fries in shallow oil the soup bathing, can blood circulation promoting and blood stasis dispelling, and removing obstruction in the collateral to relieve pain is controlled wound or acute sprain causes lumbago.
The effect of present existing bathing product or fumigation product is more single.Although current bath shampoo, fumigant have all allowed consumer too plenty for the eye to take it all in, dazzled on brand and function.But the Product Safety of bath shampoo, fumigant that contains the synthetic chemical constituent is troubling.
Therefore, research and develop a kind of nontoxic, efficient, external and have easily the effects such as antipruritic and antibiotic, allaying tiredness concurrently, be daily bath shampoo, the pharmaceutical preparation that fumigant is again health, therapeutic type be very necessary and suitable.We have scientifically analyzed the market demand that each consumer of stratum of various places has nothing in common with each other for understanding and the expectation of bath shampoo, extract elite from Miao ethnic group's medicinal plants, have developed this functional Miao Ethnomedicine bathing fumigation liquid formulation.
Summary of the invention
Main purpose of the present invention provides and a kind ofly can be used for daily bathing, stifling bathing fumigation liquid and the preparation technology who has again the disease treatment function concurrently.
For achieving the above object, the technical solution adopted in the present invention is: a kind of bathing fumigation liquid is comprised of the component of following weight ratio:
Caulis Sargentodoxae (Latin name: Sargentodoxa cuneata (Oliv.) Rehd.Et Wils; Miao: Bas hlat hsongd hab(stops La Shanghai)) 2.5～5.0 parts;
Rhizoma Acori Graminei (Latin name: Acorus tatarinowii Schott; Miao: good group of Jab box()) 1.0～2.0 part;
Herba Polygoni cymosi (Latin name: Polygonum perfoliatum; Miao: Jab gangb eb wal nangb(Jia Gang Europe is bright)) 1.5～3.0 parts;
Herba Duchesneae Indicae (Latin name: Emilia sonchifolia (L.) DC; Miao: Jab vilbes(is good not)) 1.5～3.0 parts;
Caulis et folium clerodendri bungei (Latin name: Clerodendrum bungei Steud; Miao: Vob hmangd bangd(nest Hong list)) 2.0～4.0 part;
Chinese mugwort (Latin name: Artemisia argyi L é vl.et Vant; Miao: Vob hvid(nest)) 2.5～5.0 parts;
Caulis Hederae Sinensis (mutation) (Latin name: Hedera nepalensis K.Koch var.sinensis (Tobl.) Rehd; Miao: it is new for Vob tad hxid(nest)) 2.5～5.0 parts;
Rhizoma Chuanxiong (Latin name: Ligusticum chuanxiong Hort; Miao: Vob xiangd qinx(nest Apium graveolens)) 3.0～4.0 part.
Further preferred: 5 parts of described Caulis Sargentodoxae, 2 parts of Rhizoma Acori Graminei, 3 parts of Herba Polygoni cymosis, 3 parts of Herba Duchesneae Indicae, 4 parts of Caulis et folium clerodendri bungeis, 5 parts of Chinese mugworts, 4 parts of Caulis Hederae Sinensiies (mutation), 4 parts of Rhizoma Chuanxiongs.
Miao ethnic group's medicinal plants of composition the present invention prescription is loaded " Chinese Plants will " or " Plants From Guizhou will " all.Wherein " Pharmacopoeia of People's Republic of China 2010 version one one " record has: one one the 19th page of Caulis Sargentodoxae Sargentodoxa cuneata (Oliv.) Rehd.Et Wils(Pharmacopoeia of People's Republic of China version in 2010), one one the 85th page of Rhizoma Acori Graminei Acorus tatarinowii Schott(Pharmacopoeia of People's Republic of China version in 2010), one one the 155th page of Herba Polygoni cymosi Polygonum perfoliatum L(Pharmacopoeia of People's Republic of China version in 2010), the 21st page of appendix of Herba Duchesneae Indicae Emilia sonchifolia (L.) DC(Pharmacopoeia of People's Republic of China version in 2010), one one the 82nd page of Chinese mugwort Artemisia argyi L é vl.et Vant(Pharmacopoeia of People's Republic of China version in 2010), Rhizoma Chuanxiong Ligusticum chuanxiong Hort(Pharmacopoeia of People's Republic of China version in 2010 is one one the 38th page); Be not written into " Pharmacopoeia of People's Republic of China 2010 version one one " but be written into having of " Plants From Guizhou will ": the 1889th page of the 128th page of Chinese medicine voluminous dictionary volume two of Caulis et folium clerodendri bungei Clerodendrum bungei Steud(Plants From Guizhou will the tenth volume), the 2103rd page of the 314th page of Chinese medicine voluminous dictionary volume two in Caulis Hederae Sinensis (mutation) Hedera nepalensis K.Koch var.sinensis (Tobl.) Rehd(Plants From Guizhou will Volume Four).
Useful technique effect of the present invention:
This prescription be used for to take a shower, the prescription of the medicinal plants preparation of stifling other is completely different, this prescription is used theory, experience and the Therapeutic Method that these medicinal plants are based on Seedling medicine, with regard to the function and usage of single medicinal plants, all function and the usage with contained these medicinal plants of state-promulgated pharmacopoeia and medicine monograph is very different.It is new such as the medicinal plants Vob tad hxid(of Miao ethnic group nest in this prescription), Miao ethnic group is that function take this plant is as its name, the meaning of Vob tad hxid Miao be have the good logical muscle arteries and veins that relaxes (it is new for tad hxid--(and tad--it, the meaning of relaxing and leading to), (hxid--is new, the muscle arteries and veins that refers to the people) the dish class plant of effect (Vob--nest (the edible plant of " dish " general reference of dish class plant--Miao ethnic group's medicinal plants, be not only that the people eats, also comprise domestic animal, insecticide, the edible plant of animal) the medicinal plants name reflects the function of this medicinal plants.Therefore, this prescription has obvious uniqueness.
Preparation is daily bath foam, is again fumigant, the drug fever application with treatment, health-care effect; Of many uses, easy to use.Its contained bioactive substance all comes from natural plants; volatile oil wherein; glycoside; phenol; flavone; phenolic substance; anthraquinone; alkaloid; carotene; bioactive substances such as organic acid or directly act on body surface; or through skin; mucosa absorbs and enters in the body; has cleaning skin; promote skin metabolism; the effect of protection capillary vascular toughness; have antibiotic and antivirus action; has the blood of regulating the flow of vital energy; by cold-damp; pain relieving; warming the meridian; collateral dredging; anti-allergic effects; blood vessel with expansion part or whole skin; promote the blood circulation of skin; the benefiting action of allaying tiredness is to subhealth state (fatigue syndrome); soft-tissue strain; ankylosis; muscle adhesion; myalgia; arthralgia; lumbar vertebra hyperosteogeny; the chronic gastroenteritis asthenic cold type; common cold has certain therapeutical effect.
Below the further openly preparation technology of preparation of the present invention so that those skilled in the art can repeat to implement.
In view of the chemical constituent of Miao Ethnomedicine compound recipe is very complicated, and the physical and chemical reaction that occurs in processing and making process might cause the chemical constituent that has to disappear or produces novel compound.Therefore, the proper method that finds this Miao Ethnomedicine compound recipe to extract makes its elaboration products become " natural combination chemical combination storehouse " and produces the effect of " multiple target effect ", has definite curative effect, is the basic ideas of this prescription Miao Ethnomedicine separation and Extraction.From these basic ideas, the inventor carries out the preparation process design according to the character of this prescription Miao ethnic group medicinal plants and this composing prescription preparation application target, application approach.Obtained application safety, definite effect, stable in properties, controlled, and the processing technique of good economy performance and product.
A kind of preparation technology of bathing fumigation liquid, step comprises:
A, this prescription medical material is pulverized respectively;
B, Herba Polygoni cymosi, Herba Duchesneae Indicae, Caulis Hederae Sinensis (mutation) medicated powder 2%(V/V) acidic ethanol dipping, dip time and ethanol consumption are with medicated powder fully evenly moistening and degree of being expanded to; 2%(V/V) acidic ethanol compound method: 11.74mol/L concentrated hydrochloric acid solution 2ml adds the ethanol of mass fraction 95% to 100ml;
C, Rhizoma Acori Graminei, Chinese mugwort, the Rhizoma Chuanxiong medicated powder alcohol dipping of mass fraction 95%; Dipping is with medicated powder fully evenly moistening and degree of being expanded to;
D, Caulis Sargentodoxae, Caulis et folium clerodendri bungei 75% alcohol dipping; Dipping is with medicated powder fully evenly moistening and degree of being expanded to;
E, with the medical material among step b, c, the d by successively from lower to upper layering be positioned in the percolator, after adding 95% alcohol dipping 48h of 3 times of medical material amounts, flow out the filter percolation speed percolation of liquid of l～3mL with 1000g medical material per minute, synchronized 70% ethanol that adds 2 times of medical material amounts in the percolator, when the liquid for the treatment of just to filter reaches 2.5 times of medical material medical material amount, get the liquid of just filtering;
F, synchronized 50% ethanol that adds 2 times of medical material amounts in the percolator again, continuous filtering when regathering the liquid of filtering and reaching again 2 times of medical material medical material amounts, must continue the liquid 1 of filtering;
G, the synchronized purified water that adds 3 times of medical material amounts in the percolator again, continuous filtering when the liquid of filtering of collecting reaches again 2 times of medical material medical material amounts again, must continue the liquid 2 of filtering; Add again continuous the filtering of purified water and end to percolate is colourless, must continue the liquid 3 of filtering;
H, merge just filter liquid and continuous filter liquid 1,2 Recycled ethanols, just filter liquid and all are continuous filters that liquid is concentrated, water precipitating, separate, make with extra care and to get finished product.
Preferably: among described step b, c, the d, dip time is 1～2 hour; The ethanol consumption is enough to flood medicated powder;
Further, among the described step h, refining that finished product 1ml is equivalent to former medicinal plants medical material 1～1.5g.
Further, among the described step h, refining that finished product 1ml is equivalent to former medicinal plants medical material 1.3g.
Process selection of the present invention is large to the active component dissolubility, to not needing the little solvent of dissolved element dissolubility, the solvent extraction method that effective ingredient is dissolved out in the medical material tissue, adopt accurate, easy, representative, quantifiable comprehensive evaluation index, this Miao Ethnomedicine prescription is carried out compound recipe extract.In the extraction process, pay attention to solvent, the concentration of solvent, acid-base value, and the conditions such as temperature, time are on extracting the impact that separates, designed with opposed polarity solvent, variable concentrations solvent, different pH values solvent and at normal temperatures in the same container, extracted the extraction scheme of this prescription medicinal plants composition.
The product that preparation technology of the present invention makes does not contain any surfactant, cosolvent, penetrating agent, antiseptic; Liquid is not stratified, no suspended substance or precipitation; Transparent brownish red, color and luster is even, without obvious mechanical admixture and stain; The peat-reek of tool plant, free from extraneous odour; In-5 ± 2 ℃ to 40 ± 1 ℃ environment, place 24h, observe when returning to room temperature, transparent haze-free, without layering and metachromatism, free from extraneous odour, good stability.The bathing fumigation liquid of making by this technique shows this extraction scheme craft science, reasonable, novel after using, and bathing fumigation liquid safety is remarkably productive without sensitization to mucocutaneous nonirritant, without toxicity, is convenient to produce, is subject to the user welcome.
The below further introduces the using method of product of the present invention.
Being applicable to of this Miao Ethnomedicine composing prescription preparation lain fallow, " cleaning skin ", " allaying tiredness ", " recovery after promotion is recovered " and " medicinal bath therapy of subhealth state (fatigue syndrome), common cold, skin pruritus, chronic gastroenteritis asthenic cold type, lumbar vertebra hyperosteogeny, soft-tissue strain, ankylosis, muscle adhesion, myalgia, arthralgia, fumigation and steaming therapy, hot compress therapy, the cold compress therapy of health body-wash.
The application of this Miao Ethnomedicine composing prescription preparation is similar to using method, the points for attention of the medicinal bath therapy of Chinese medicine, fumigation and steaming therapy.Specific as follows:
The bathing method:
A. the first clean health of bathing person.
B. clean bathing implement, be ready to drinking-water, sucrose solution or other liquid food, in order to bathing person's need.
C. according to bathing person's needs; get bathing fumigation liquid of the present invention in clean shower; add a certain amount of shower and dilute with warm water; can dilute according to the personal like; but be no more than 100 times, according to bathing person's heat-resisting custom, adjust water temperature; and in the bathing process, suitably adjust temperature, generally between the 39-42 degree.
D. require to set the bathing time according to bathing person, be generally 30min.
When e. the whole body hot bath was just bathed, water level should be below heart, and behind about 3～5 minutes body adaptationes, slowly bubble is extremely takeed on the position again.The bathing time can not be oversize, especially.Because sweating is too much, the body fluid amount lost is large; Skin heart is fully expanded, and the body surface blood flow volume increases, and causes the head ischemia and occurs dizzy or faint.In a single day as fainting, should in time hold up out bathtub, flat crouching on the bed of lobby drunk a little boiled water or sucrose solution to patient simultaneously, replenishes body fluid and energy.Or use the cold water foot bath, and lower limb vascular is shunk, the head blood supply is sufficient.
When f. bathing finished, bathing person will stand up from bathtub at leisure, need not in addition again flushing, and the bath foam that only dips on the dried health with towel gets final product.
The bathing points for attention:
But a right and left balneation in a hour after meal.
B soaks the place should note the well-ventilated, but can not catch cold.
C does not carry out the puerpera of operative delivery, can be in beginning in 7 days puerperal bathing.
D has slight high hypopiesi history, the slightly poor person of cardiac function to answer the layman to accompany lower use bathing, and notice that the place ventilates, each soak time is unsuitable oversize, as in immersion process, not feeling well, should stand up slightly to fit rest in the well-ventilated place, after recovering, again soak, generally divide two to three immersions to get final product.
E physical weakness person answers the layman to accompany lower use bathing.
F skin has larger area wound person, Severe Asthma patient, the above high and low blood pressure trouble of moderate, cardiac should avoid using bathing.
The g drunken person is forbidden bathing.
In a single day h whole body hot bath person should in time notify the health doctor and hold up out bathtub as fainting, flat crouching on the bed of lobby drunk a little G/Ws to him simultaneously, uses the cold water foot bath.
Stifling points for attention:
When a. fumigating, loose for avoiding liquid medicine steaming to make leave with rage, cover affected part and the vessel of containing medicinal liquid.
B. to make the steam temperature moderate, and grasp affected part and the distance of containing the medicinal liquid vessel, in order to avoid scald or the affected part of burning, but medicinal liquid also can not be supercool.
C. some needs stifling disease of time expand, the available iron sliding weight of steelyard, or the cobblestone of cleaning burning is red, puts into basin, strengthens evaporation.
When d. fumigating, winter should be warming, and should tremble with fear summer in wind sheltering, in order to avoid flu increases the weight of the state of an illness.Behind the fumigation and wash method lower limb, wipe away immediately driedly, cover is warming.
E. hemorrhagic disease patient, purulence limitation focus patient, malignant tumor patient, severe cardiovascular disease patient, serious anemia patient, active tuberculosis patient, anemia of pregnant woman, elderly and infirm etc. avoid with whole body stifling.
This Miao Ethnomedicine composing prescription preparation safety in prolonged application, to stingless the paying property of skin, without sensitization, nontoxic, have no side effect.Have uniqueness, significant effect.
1, is used for general shower (dipping bath)
To 430 multi-users statistics, use this composing prescription preparation and do to take a shower (behind the dipping bath) at random, " after this liquid medicine was bathed, the people was very comfortable, and aftersensation is light, spirit has been howed than bathing with common bath gel at common bathing pool (chamber) in all reflections.Sleep quality obviously improves after using a week, and is easily sleeping, and sleep is dull, dreaminess, the situations such as Yi Xing disappear ".
2, be used for work, rear take a shower (dipping bath) of motion
To 100 user statistics, this composing prescription preparation of application after the above physical work of 4h or the above sports of 4h is done to take a shower (behind the dipping bath) at random, all reflections " after this liquid medicine was bathed, people's sense tired out and full Shen Acid pain had been eliminated, and feeling relaxed is comfortable ".
3, the cutaneous pruritus patient is used for take a shower (dipping bath)
According to the middle-aged and elderly people of 23 trouble " skin pruritus " with do to take a shower the readme after (dipping bath) of this composing prescription preparation, after the shower (dipping bath) once, all sensation " skin pruritus " alleviates a lot, continuous 3 times (1 day 1 time) " skin pruritus " transference cures, and the vestige of scratching of leaving over because of pruritus on the skin also disappears, and following the tracks of all not have more than three months to recur.
4, with this composing prescription preparation in stifling
According to suffering from because 21 adults of myalgia, arthralgia or chronic gastroenteritis asthenic cold type that rheumatism causes or common cold or lumbar vertebra hyperosteogeny do readme after stifling (stifling part or health) with this composing prescription preparation, stifling once after the subjective symptomss such as discomfort of pain and health all be eased even disappear.The subjective symptomss such as discomfort of pain and health all are eased even disappear behind the continuous fumigation 7 days (once a day).
The specific embodiment
The below provides preferred prescription and the preparation technology embodiment of bathing fumigation liquid of the present invention.
Embodiment one
5 parts of Caulis Sargentodoxae, 2 parts of Rhizoma Acori Graminei, 3 parts of Herba Polygoni cymosis, 3 parts of Herba Duchesneae Indicae, 4 parts of Caulis et folium clerodendri bungeis, 5 parts of Chinese mugworts, 4 parts of Caulis Hederae Sinensiies (mutation), 4 parts of Rhizoma Chuanxiongs, total amount 1kg.
Preparation process:
A, medical material is pulverized respectively;
B, Herba Polygoni cymosi, Herba Duchesneae Indicae, Caulis Hederae Sinensis (mutation) medicated powder 2%(V/V) the acidic ethanol dipping, dipping ethanol consumption is enough to flood whole medicines, the abundant moistening of medicated powder, expansion after 1 hour time; 2%(V/V) acidic ethanol compound method: 11.74mol/L concentrated hydrochloric acid solution 2ml adds the ethanol of mass fraction 95% to 100ml;
C, Rhizoma Acori Graminei, Chinese mugwort, the Rhizoma Chuanxiong medicated powder alcohol dipping of mass fraction 95%; Dipping ethanol consumption is enough to flood whole medicines, the abundant moistening of medicated powder, expansion after 1 hour time;
D, Caulis Sargentodoxae, Caulis et folium clerodendri bungei 75% alcohol dipping; Dipping ethanol consumption is enough to flood whole medicines, the abundant moistening of medicated powder, expansion after 1 hour time;
E, Herba Polygoni cymosi, Herba Duchesneae Indicae, Caulis Hederae Sinensis (mutation) medicated powder after will flooding are positioned over orlop in the percolator, and Rhizoma Acori Graminei, Chinese mugwort, Rhizoma Chuanxiong layer and Caulis Sargentodoxae, Caulis et folium clerodendri bungei layer are placed in layering from lower to upper successively; After adding the 95% alcohol dipping 48h of 3kg, flow out the filter percolation speed percolation of liquid of 2mL with 1000g medical material per minute, synchronizedly in percolator, add 2kg70% ethanol, when the liquid for the treatment of just to filter reaches 2.5kg, get the liquid of just filtering;
F, synchronized 50% ethanol that adds 2kg in the percolator again, continuous filtering when regathering the liquid of filtering and reaching 2kg again, must continue the liquid 1 of filtering;
G, the synchronized purified water that adds 3kg in the percolator again, continuous filtering when the liquid of filtering of collecting reaches 2kg again again, must continue the liquid 2 of filtering; Add again continuous the filtering of purified water and end to percolate is colourless, must continue the liquid 3 of filtering;
H, merge just filter liquid and continuous filter liquid 1,2 Recycled ethanols, merge that just filter liquid and all continuously filter that liquid is concentrated, water precipitating, separate, make with extra care and to get finished product; Finished product 1ml is equivalent to former medicinal plants medical material 1.3g.
Embodiment two
5 parts of Caulis Sargentodoxae, 2 parts of Rhizoma Acori Graminei, 3 parts of Herba Polygoni cymosis, 3 parts of Herba Duchesneae Indicae, 3 parts of Caulis et folium clerodendri bungeis, 4 parts of Chinese mugworts, 5 parts of Caulis Hederae Sinensiies (mutation), 4 parts of Rhizoma Chuanxiongs, total amount 1kg.
Preparation process:
A, medical material is pulverized respectively;
B, Herba Polygoni cymosi, Herba Duchesneae Indicae, Caulis Hederae Sinensis (mutation) medicated powder 2%(V/V) acidic ethanol dipping, dip time and ethanol consumption are with medicated powder fully evenly moistening and degree of being expanded to; 2%(V/V) acidic ethanol compound method: 11.74mol/L concentrated hydrochloric acid solution 2ml adds the ethanol of mass fraction 95% to 100ml;
C, Rhizoma Acori Graminei, Chinese mugwort, the Rhizoma Chuanxiong medicated powder alcohol dipping of mass fraction 95%; Dip time and ethanol consumption are with medicated powder fully evenly moistening and degree of being expanded to;
D, Caulis Sargentodoxae, Caulis et folium clerodendri bungei 75% alcohol dipping; Dip time and ethanol consumption are with medicated powder fully evenly moistening and degree of being expanded to;
E, Herba Polygoni cymosi, Herba Duchesneae Indicae, Caulis Hederae Sinensis (mutation) medicated powder after will flooding are positioned over orlop in the percolator, and Rhizoma Acori Graminei, Chinese mugwort, Rhizoma Chuanxiong layer and Caulis Sargentodoxae, Caulis et folium clerodendri bungei layer are placed in layering from lower to upper successively; After adding the 95% alcohol dipping 48h of 3kg, flow out the filter percolation speed percolation of liquid of 2mL with 1000g medical material per minute, synchronizedly in percolator, add 2kg70% ethanol, when the liquid for the treatment of just to filter reaches 2.5kg, get the liquid of just filtering;
F, synchronized 50% ethanol that adds 2kg in the percolator again, continuous filtering when regathering the liquid of filtering and reaching 2kg again, must continue the liquid 1 of filtering;
G, the synchronized purified water that adds 3kg in the percolator again, continuous filtering when the liquid of filtering of collecting reaches 2kg again again, must continue the liquid 2 of filtering; Add again continuous the filtering of purified water and end to percolate is colourless, must continue the liquid 3 of filtering;
H, merge just filter liquid and continuous filter liquid 1,2 Recycled ethanols, merge that just filter liquid and all continuously filter that liquid is concentrated, water precipitating, separate, make with extra care and to get finished product; Finished product 1ml is equivalent to former medicinal plants medical material 1.3g.
Claims (6)
1. bathing fumigation liquid is comprised of the component of following weight ratio:
2.5～5.0 parts of Caulis Sargentodoxae;
1.0～2.0 parts of Rhizoma Acori Graminei;
1.5～3.0 parts of Herba Polygoni cymosis;
1.5～3.0 parts of Herba Duchesneae Indicae;
2.0～4.0 parts of Caulis et folium clerodendri bungeis;
End 2.5～5.0 parts;
2.5～5.0 parts of Caulis Hederae Sinensiies (mutation);
3.0～4.0 parts of Rhizoma Chuanxiongs.
2. a kind of bathing fumigation liquid according to claim 1 is characterized in that: 5 parts of described Caulis Sargentodoxae, 2 parts of Rhizoma Acori Graminei, 3 parts of Herba Polygoni cymosis, 3 parts of Herba Duchesneae Indicae, 4 parts of Caulis et folium clerodendri bungeis, 5 parts of Chinese mugworts, 4 parts of Caulis Hederae Sinensiies (mutation), 4 parts of Rhizoma Chuanxiongs.
3. the preparation technology of bathing fumigation liquid according to claim 1 and 2, step comprises:
A, this prescription medical material is pulverized respectively;
B, Herba Polygoni cymosi, Herba Duchesneae Indicae, Caulis Hederae Sinensis (mutation) medicated powder 2%(V/V) acidic ethanol dipping, dip time and ethanol consumption are with medicated powder fully evenly moistening and degree of being expanded to; 2%(V/V) acidic ethanol compound method: 11.74mol/L concentrated hydrochloric acid solution 2ml adds the ethanol of mass fraction 95% to 100ml;
C, Rhizoma Acori Graminei, Chinese mugwort, the Rhizoma Chuanxiong medicated powder alcohol dipping of mass fraction 95%; Dipping is with medicated powder fully evenly moistening and degree of being expanded to;
D, Caulis Sargentodoxae, Caulis et folium clerodendri bungei 75% alcohol dipping; Dipping is with medicated powder fully evenly moistening and degree of being expanded to;
E, with the medical material among step b, c, the d by successively from lower to upper layering be positioned in the percolator, after adding 95% alcohol dipping 48h of 3 times of medical material amounts, flow out the filter percolation speed percolation of liquid of l～3mL with 1000g medical material per minute, synchronized 70% ethanol that adds 2 times of medical material amounts in the percolator, when the liquid for the treatment of just to filter reaches 2.5 times of medical material medical material amount, get the liquid of just filtering;
F, synchronized 50% ethanol that adds 2 times of medical material amounts in the percolator again, continuous filtering when regathering the liquid of filtering and reaching again 2 times of medical material medical material amounts, must continue the liquid 1 of filtering;
G, the synchronized purified water that adds 3 times of medical material amounts in the percolator again, continuous filtering when the liquid of filtering of collecting reaches again 2 times of medical material medical material amounts again, must continue the liquid 2 of filtering; Add again continuous the filtering of purified water and end to percolate is colourless, must continue the liquid 3 of filtering;
H, merge just filter liquid and continuous filter liquid 1,2 Recycled ethanols, just filter liquid and all are continuous filters that liquid is concentrated, water precipitating, separate, make with extra care and to get finished product.
4. the preparation technology of bathing fumigation liquid according to claim 3, it is characterized in that: among described step b, c, the d, dip time is 1～2 hour; The ethanol consumption is enough to flood medicated powder.
5. the preparation technology of bathing fumigation liquid according to claim 4 is characterized in that: among the described step h, refining that finished product 1ml is equivalent to former medicinal plants medical material 1～1.5g.
6. the preparation technology of bathing fumigation liquid according to claim 5 is characterized in that: among the described step h, refining that finished product 1ml is equivalent to former medicinal plants medical material 1.3g.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210273821.3A CN102973747B (en) | 2012-08-02 | 2012-08-02 | Bath fumigating liquid and preparation process thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210273821.3A CN102973747B (en) | 2012-08-02 | 2012-08-02 | Bath fumigating liquid and preparation process thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107375813A (en) * | 2017-09-14 | 2017-11-24 | 贵州云上苗家康养有限公司 | A kind of Miao ethnic group's external application bath foam |
| CN109125210A (en) * | 2018-10-08 | 2019-01-04 | 广东云瑶生物医药科技有限公司 | borneol milk foam bath lotion and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101590004A (en) * | 2009-06-22 | 2009-12-02 | 杨平 | The Chinese medicine bath foam |
| CN102145140A (en) * | 2011-03-11 | 2011-08-10 | 苏永生 | Traditional Chinese medicine fumigant for treating psoriasis |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101590004A (en) * | 2009-06-22 | 2009-12-02 | 杨平 | The Chinese medicine bath foam |
| CN102145140A (en) * | 2011-03-11 | 2011-08-10 | 苏永生 | Traditional Chinese medicine fumigant for treating psoriasis |
Non-Patent Citations (2)
| Title |
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| 《湖北中医杂志》 20110131 梁建文 "中药配方颗粒熏蒸浴配伍组方的实践探讨" 第33卷, 第1期 * |
| 梁建文: ""中药配方颗粒熏蒸浴配伍组方的实践探讨"", 《湖北中医杂志》, vol. 33, no. 1, 31 January 2011 (2011-01-31) * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107375813A (en) * | 2017-09-14 | 2017-11-24 | 贵州云上苗家康养有限公司 | A kind of Miao ethnic group's external application bath foam |
| CN109125210A (en) * | 2018-10-08 | 2019-01-04 | 广东云瑶生物医药科技有限公司 | borneol milk foam bath lotion and preparation method thereof |
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| CN102973747B (en) | 2014-05-14 |
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