CN102972865A - Preparation method of flavoring particles for cigarette filter tip by coating method, obtained product and use - Google Patents
Preparation method of flavoring particles for cigarette filter tip by coating method, obtained product and use Download PDFInfo
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- CN102972865A CN102972865A CN2012105673969A CN201210567396A CN102972865A CN 102972865 A CN102972865 A CN 102972865A CN 2012105673969 A CN2012105673969 A CN 2012105673969A CN 201210567396 A CN201210567396 A CN 201210567396A CN 102972865 A CN102972865 A CN 102972865A
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- perfuming
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- curing agent
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Abstract
The invention relates to a preparation method of flavoring particles for a cigarette filter tip by a coating method, an obtained product and a use. According to the preparation method, a release base material and an organic polymer skeleton are used as main raw materials, and active release type cigarette flavoring particles are formed by processes including mixing, coating, granulating, curing, drying and the like, wherein the release base material is made from an organic acid and a release backing material; a flavoring curing agent is made from an anhydrous solvent, the organic polymer skeleton and a flavor; and the flavoring particles are obtained by rotary coating, drying and screening. According to the invention, the flavoring particles actively release flavoring materials and produce water after meeting a mainstream smoke, the reaction is sustained and stable, the cigarette style and the smoking quality can be enhanced, and the moisturizing effect is realized.
Description
[technical field]
The invention belongs to the cigarette material technical field, the fragrant material of the benefit of particularly adding in the cigarette filter and this material preparation method.
[background technology]
The lowering harm and decreasing coking problem is one of countries tobacco sixty-four dollar question.The first half of the year in 2011 whole nation cigarette list props up the weighted average tar content and drops to below 11 milligrams, and part cigarette product tar content has dropped to below 10 milligrams.Also not rare on 5 milligrams the cigarette market, the cigarette of 1 milligram even 0.1 milligram also comes out.
For reaching the purpose of reducing tar and reducing harm, the technology industries such as filter tip, the fine composite filter of paper/vinegar, natural permeable degree tipping paper, online laser boring have been introduced.In the time of their effective harmful components that reduce in the cigarette smoke, also can be so that corresponding reduction be followed in the aspects such as original suction flavor of cigarette, mouthfeel, physiological strength.Especially the loss of fragrance matter and perfume quantity in the cigarette, easily make taste lose original style, this just need to carry out part and remedy by adding other spices, and one of effect of perfuming is when reducing cigarette harm, remedy the loss of fragrance, provide satisfied product to the consumer.
Chinese invention patent 201010239046.0 discloses a kind of novel flavoring filter tip, choose diameter and cause fragrant particle in the 20-40 purpose, by the mouth rod forming machine, in every millimeter mouth rod tow, add equably 3 milligrams and describedly cause fragrant particle, make function mouth rod, described function mouth rod and the excellent Length Ratio by 10: 15 of base are rolled into flavoring filter tip by composite molding machine; Describedly cause fragrant particle and formed in comminutor take aluminosilicate as carrier by weight by following component: 4 parts of cloud and mist absolute oil; 1.5 parts of oak moss absolutes; 0.5 part of tree orchid essential oil; 4 parts of maltols; 15 parts of caramel colorants; 65 parts of propane diols; 10 parts in water.Yet find that through smokeing panel test its flavouring effect is not ideal, it is natural not to inhale flavor, and comparatively significantly artificial fragrance breath is arranged.
[summary of the invention]
The inventor utilizes organic acid acid and carbonate mixture to meet water reaction Heat of Formation or CO through research
2With the mechanism of water, set up flue gas Active Compensation system; Heat and CO
2Can take the essence that is added in the soda acid particle out of reach flavor compensating effect when overflowing, the generation of water has then increased the effect that the moisture in the flue gas reaches humectation; Because the aerosol that the fragrance that overflows and moisture form and the similitude of flue gas make compensation effect more obvious.
For this reason, the invention provides a kind of coating method and prepare the method that cigarette filter is used the perfuming particle, step is as follows:
A, preparation discharge base-material: get respectively organic acid and in 50-60 ℃ of baking oven, be heated to drying with discharging bed material, in weight ratio take by weighing 1:2 ~ 3:2 through the organic acid of oven dry with discharge bed material, mix, obtain discharging base-material;
B, preparation perfuming curing agent: the anhydrous solvent and the organic polymer skeleton that take by weighing 4:1 ~ 19:1 in weight ratio, mix, obtain curing agent, take by weighing again curing agent and the Zimbabwe's tobacco extract of 6:1 ~ 50:1 in weight ratio, mix and obtain the perfuming curing agent;
C, dressing: take by weighing 7:30 ~ 1:2 perfuming curing agent and discharge base-material in weight ratio, to discharge base-material and pour in the coating pan rotation into and mix behind the 10min and according to aforementioned proportion the perfuming curing agent slowly to be sprayed into until sprayed fully, and continue to make wet granular behind the rotation dressing 1h;
D, described wet granular is dried in 50-60 ℃ baking oven, cross 100 mesh sieves, obtain described cigarette filter perfuming particle.
In the present invention, Zimbabwe's tobacco extract is the product that can buy acquisition on the market, for example Zimbabwe's tobacco extract of Huabao Edible Essence ﹠ Condiment's sale.
In the present invention, the dressing of step c is undertaken by sugar coating machine, the BY-Chufa-type sugarcoating machine of for example selecting Jiangyin City's health and machine-building Co., Ltd to manufacture.
In the present invention, described organic acid is selected from one or more organic acids in citric acid, citric acid, tartaric acid and/or the malic acid.
Described release bed material is selected from one or more release bed materials of sodium acid carbonate, saleratus, sodium carbonate, lithium carbonate and/or potash.
Among the step a gained is discharged base-material and sieve, choose the above particle of particle diameter 40 orders as discharging base-material, as the raw material of step c.
Described anhydrous solvent is selected from ethanol, propane diols and/or acetone.
Described organic polymer skeleton is selected from lac, acetate fiber and/or PLA.
The invention still further relates to the cigarette filter application of perfuming particle in cigarette filter that above-mentioned preparation method obtains, preferably with the cigarette-filter tow length gauge, the addition of described perfuming particle is 0.5-35mg/mm.
Similarly, the perfuming particle for preparing of the present invention can also be applied to that binary is compound, in the tri compound, cavity composite filter.
Method of the present invention is simple, cost of manufacture is lower, and gained perfuming particle has consolidation homogeneous, the mellow and full advantage such as smooth.The cigarette filter that utilizes the inventive method to prepare has nontoxic with material.Slowly disintegration after particle and the main flume effect produces CO
2Can carry out the active perfuming, can guarantee that fragrance uniformity, acid-base reaction stable and the suction flavor produce water and reach the humectation effect as the perfuming carrier with water.
[specific embodiment]
Can understand better the present invention by following embodiment.
Embodiment 1
Make the perfuming particle:
Take by weighing the citric acid 100g of having dried, tartaric acid 30g and saleratus 20g, sodium acid carbonate 100g, sodium carbonate 50g mixing obtains discharging base-material perfuming curing agent.
With acetone 135g and acetate fiber 12g, PLA 3g, Zimbabwe tobacco extract 3g, the dissolving mixing obtains the perfuming curing agent.
The perfuming curing agent sprayed in the release base-material prepare rotate dressing, then 50 ℃ of oven dry of baking oven, screening is chosen grade and is mended fragrant particle at 40 to 60 order particles as cigarette.
Cigarette is mended fragrant particle be applied to the composite particles filter stick formation by addition 25mg/mm, make ternary cavity composite filter.Select the finished cigarettes of quality between 0.880-0.900g, remove original filter stick, the active release type particle filter stick that the tipping preparation is complete.
Cigarette is placed 22 ℃, the balance 48h of thermostatic constant wet chamber of 60% humidity.In the spacious environment of smoothness, 22 ℃ of room temperatures, humidity 60% that ventilates, estimate under the environment.
Embodiment 2
Make the perfuming particle:
Take by weighing the citric acid 60g of having dried, tartaric acid 100g and saleratus 140g mixing obtain discharging base-material perfuming curing agent.
With absolute ethyl alcohol 48g and shellac 12g Zimbabwe tobacco extract 10g, the dissolving mixing obtains the perfuming curing agent.
The perfuming curing agent sprayed in the release base-material prepare rotate dressing, 50 ℃ of oven dry of gained particle baking oven are sieved at last, choose grade and namely get described cigarette and mend fragrant particle with interior at 20 to 40 orders.
The gained particle is applied to the composite particles filter stick formation by addition 2mg/mm, makes ternary cavity composite filter.Select the finished cigarettes of quality between 0.880-0.900g, produce red plum board such as Yunnan Yuxi Cigarette Factory, remove original filter stick, the active release type particle filter stick that the tipping preparation is complete.
Cigarette is placed 22 ℃, the balance 48h of thermostatic constant wet chamber of 60% humidity.In the spacious environment of smoothness, 22 ℃ of room temperatures, humidity 60% that ventilates, estimate under the environment again.
Embodiment 3
Make the perfuming particle:
Take by weighing the citric acid 50g of having dried, citric acid 90g, sodium carbonate 60g, lithium carbonate 100g mixing obtains discharging base-material perfuming curing agent.
With absolute ethyl alcohol 108g and shellac 12g Zimbabwe tobacco extract (alcohol extracting part) 6g, the dissolving mixing obtains the perfuming curing agent.
The perfuming curing agent sprayed in the release base-material prepare rotate dressing.60 ℃ in gained particle baking oven baking 1 hour is sieved at last, chooses grade and namely gets described cigarette and mend fragrant particle with interior at 20 to 40 orders.
The gained particle is applied to the composite particles filter stick formation by addition 20mg/mm, makes ternary cavity composite filter.Select the finished cigarettes of quality between 0.880-0.900g, remove original filter stick, the active release type particle filter stick that the tipping preparation is complete.
Cigarette is placed 22 ℃, the balance 48h of thermostatic constant wet chamber of 60% humidity.In the spacious environment of smoothness, 22 ℃ of room temperatures, humidity 60% that ventilates, estimate under the environment again.
Embodiment 4
Make the perfuming particle:
Take by weighing the tartaric acid 180g of having dried, sodium acid carbonate 120g mixing obtains discharging base-material perfuming curing agent.
With acetone 114g and acetate fiber 6g Zimbabwe tobacco extract (alcohol extracting part) 10g, the dissolving mixing obtains the perfuming curing agent.
The perfuming curing agent sprayed in the release base-material prepare rotate dressing;
With 60 ℃ of oven dry of gained particle baking oven, sieve at last, choose grade and namely get described cigarette and mend fragrant material with interior at 20 to 40 orders.
The gained particle is applied to the composite particles filter stick formation by addition 2mg/mm, makes ternary cavity composite filter.
Select the finished cigarettes of quality between 0.880-0.900g, remove original filter stick, the active release type particle filter stick that the tipping preparation is complete.
Then cigarette is placed 22 ℃, the balance 48h of thermostatic constant wet chamber of 60% humidity.In the spacious environment of smoothness, 22 ℃ of room temperatures, humidity 60% that ventilates, estimate under the environment again.
Embodiment 5
Make the perfuming particle:
Take by weighing the tartaric acid 130g of having dried, sodium acid carbonate 130g, sodium carbonate 60g mixing obtains discharging base-material perfuming curing agent.
Ethanol 114g and shellac 6g Zimbabwe tobacco extract (alcohol extracting part) 6g are dissolved also, and the dissolving mixing obtains the perfuming curing agent.
The perfuming curing agent sprayed in the release base-material prepare rotate dressing;
With 50 ℃ in gained particle baking oven baking 2 hours, sieve at last, choose grade and namely get described cigarette and mend fragrant particle with interior at 20 to 40 orders.
The gained particle is applied to the composite particles filter stick formation by addition 20mg/mm, makes ternary cavity composite filter.
Select the finished cigarettes of quality between 0.880-0.900g, remove original filter stick, the active release type particle filter stick that the tipping preparation is complete.
Cigarette is placed 22 ℃, the balance 48h of thermostatic constant wet chamber of 60% humidity.In the spacious environment of smoothness, 22 ℃ of room temperatures, humidity 60% that ventilates, estimate under the environment again.Smoking result sees Table 1.
Table 1
Claims (8)
1. coating method prepares the method that cigarette filter is used the perfuming particle, it is characterized in that step is as follows:
A, preparation discharge base-material: get respectively organic acid and in 50-60 ℃ of baking oven, be heated to drying with discharging bed material, in weight ratio take by weighing 1:2 ~ 3:2 through the organic acid of oven dry with discharge bed material, mix, obtain discharging base-material;
B, preparation perfuming curing agent: the anhydrous solvent and the organic polymer skeleton that take by weighing 4:1 ~ 19:1 in weight ratio, mix, obtain curing agent, take by weighing again curing agent and the Zimbabwe's tobacco extract of 6:1 ~ 50:1 in weight ratio, mix and obtain the perfuming curing agent;
C, dressing: take by weighing 7:30 ~ 1:2 perfuming curing agent and discharge base-material in weight ratio, to discharge base-material and pour in the coating pan rotation into and mix behind the 10min and according to aforementioned proportion the perfuming curing agent slowly to be sprayed into until sprayed fully, and continue to make wet granular behind the rotation dressing 1h;
D, described wet granular is dried in 50-60 ℃ baking oven, cross 100 mesh sieves, obtain described cigarette filter perfuming particle.
2. method according to claim 1 is characterized in that described organic acid is selected from one or more organic acids in citric acid, citric acid, tartaric acid and/or the malic acid.
3. method according to claim 1 is characterized in that described release bed material is selected from one or more release bed materials of sodium acid carbonate, saleratus, sodium carbonate, lithium carbonate and/or potash.
4. method according to claim 1 is characterized in that among the step a gained being discharged base-material sieves, and chooses the above particle of particle diameter 40 orders as discharging base-material, as the raw material of step c.
5. method according to claim 1 is characterized in that described anhydrous solvent is selected from ethanol, propane diols and/or acetone.
6. method according to claim 1 is characterized in that described organic polymer skeleton is selected from lac, shellac, acetate fiber and/or PLA.
7. the cigarette filter that obtains of the described method of claim 1-6 is with the application of perfuming particle in cigarette filter.
8. the cigarette filter that obtains of the described method of claim 1-6 is characterized in that with the cigarette filter length gauge that with the application of perfuming particle in cigarette filter the addition of described perfuming particle is 0.5-35mg/mm.
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| CN201210567396.9A CN102972865B (en) | 2012-12-24 | 2012-12-24 | Preparation method of flavoring particles for cigarette filter tip by coating method, obtained product and use |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109497612A (en) * | 2018-12-12 | 2019-03-22 | 湖北中烟工业有限责任公司 | A kind of heating with tea perfume is not burnt cigarette filter tip |
| CN109588774A (en) * | 2018-12-07 | 2019-04-09 | 云南中烟新材料科技有限公司 | A kind of tealeaves filter tip particle and preparation method thereof extending fragrance remaining time |
| CN110801049A (en) * | 2019-11-07 | 2020-02-18 | 云南中烟工业有限责任公司 | Cigarette filter tip aroma sustained-release particles and preparation method thereof |
| CN112772971A (en) * | 2019-11-11 | 2021-05-11 | 云南恩典科技产业发展有限公司 | Fragrant bead for hollow large-particle filter stick and preparation method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109588774A (en) * | 2018-12-07 | 2019-04-09 | 云南中烟新材料科技有限公司 | A kind of tealeaves filter tip particle and preparation method thereof extending fragrance remaining time |
| CN109588774B (en) * | 2018-12-07 | 2021-08-13 | 云南中烟新材料科技有限公司 | Tea filter tip particles capable of prolonging aroma retention time and preparation method thereof |
| CN109497612A (en) * | 2018-12-12 | 2019-03-22 | 湖北中烟工业有限责任公司 | A kind of heating with tea perfume is not burnt cigarette filter tip |
| CN109497612B (en) * | 2018-12-12 | 2021-03-16 | 湖北中烟工业有限责任公司 | Heating non-combustion cigarette holder rod with tea aroma |
| CN110801049A (en) * | 2019-11-07 | 2020-02-18 | 云南中烟工业有限责任公司 | Cigarette filter tip aroma sustained-release particles and preparation method thereof |
| CN112772971A (en) * | 2019-11-11 | 2021-05-11 | 云南恩典科技产业发展有限公司 | Fragrant bead for hollow large-particle filter stick and preparation method thereof |
| CN112772971B (en) * | 2019-11-11 | 2022-08-16 | 云南恩典科技产业发展有限公司 | Fragrant bead for hollow large-particle filter stick and preparation method thereof |
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| CN102972865B (en) | 2014-04-09 |
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Address after: 850000 Lhasa economic and Technological Development Zone, Tibet autonomous region, road, investment building, Patentee after: HUABAO FLAVOURS & FRAGRANCES CO.,LTD. Address before: 850000 Lhasa economic and Technological Development Zone, Tibet autonomous region, road, investment building, Patentee before: Huabao flavor Ltd. |
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Address after: 850000 Lhasa economic and Technological Development Zone, Tibet autonomous region, road, investment building, Patentee after: Huabao flavor Ltd. Address before: 201821 Yecheng Road, Shanghai, No. 1299, No. Patentee before: Huabao Flavours & Fragrances Co.,Ltd |
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Effective date of registration: 20170123 Address after: 650503 Yunnan province Kunming city Kunming high tech Zone Jinpu rural Metro high-tech industrial base A6-2 Patentee after: YUNNAN XINYUN TECHNOLOGY DEVELOPMENT Co.,Ltd. Address before: 850000 Lhasa economic and Technological Development Zone, Tibet autonomous region, road, investment building, Patentee before: HUABAO FLAVOURS & FRAGRANCES CO.,LTD. |