CN102964885B - Core-shell organic silicon durable paint and preparation method thereof - Google Patents
Core-shell organic silicon durable paint and preparation method thereof Download PDFInfo
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- CN102964885B CN102964885B CN201210491373.4A CN201210491373A CN102964885B CN 102964885 B CN102964885 B CN 102964885B CN 201210491373 A CN201210491373 A CN 201210491373A CN 102964885 B CN102964885 B CN 102964885B
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Abstract
The invention discloses Core-shell organic silicon durable paint and preparation method thereof, in airtight pressure vessel, adding the water of above-mentioned weight portion, cellulose etc. 50 70 DEG C utilizes hydro-thermal method to mix core processed, response time is no less than 30min, then add the dispersant DP270 of above-mentioned weight ratio, antibacterial XG 405, paint antifoaming agent NXZ etc. in continuous dropping mode and be simultaneously introduced polymerization, uniform stirring, ripening, levelling viscosity, through technical specification metering packing after the assay was approved.The invention has the beneficial effects as follows: manufacturing process is simple, low cost of manufacture is suitable for industrialization, it it is the optimal representative of a new generation's water paint, gather environmental protection guarantor's light with oil paint of water paint, protect color, anti-pollution characteristic extra-weather-proof, super, it is functional that film has acidproof, alkaline-resisting, chemicals-resistant pollution etc., it is adaptable to the new construction of the buildings such as various houses, office building, hotel, Factory Building, school and engineering.
Description
Technical field
The present invention relates to Core-shell organic silicon durable paint and preparation method thereof, belong to technical field of coatings.
Background technology
It is that the one that surface covers in method of modifying is important by the method changing powder body at nano powder surface peplos
Method, shell both can be Organic substance or inorganic matter.Make it have thing thing compatibility as required or improve its thermomechanical and change
Learning stability, change light, magnetic, electrical and service life, the surface chemistry composition controlling nano-powder is to improve added value nanometer
The key of powder body.
Core-shell polymers is a kind of polymer composite particle with unique texture, it than common emulsion blending thing or
Random copolymer has more preferable stability, cohesive and mechanical property, thus at adhesive, preservative, decorative paint, and sense
The fields such as luminescent material have a wide range of applications.
Due to the preparation technology of existing core-shell type nano powder body material, substantially use and first prepare nanometer karyosome and enter again
The process route of row peplos, the later stage is through crystallization and thermal treatment, and technological process is complicated, and the production cycle is long, make make high, it is achieved
Industrialization has limitation.
Summary of the invention
It is an object of the invention to provide Core-shell organic silicon durable paint and preparation method thereof, a kind of manufacture work can be made
Skill is simple, low cost of manufacture is suitable for industrialization and has the coating of good stability, cohesive and mechanical property.
It is an object of the invention to be achieved through the following technical solutions: Core-shell organic silicon durable paint, it is by following
The raw material of weight portion is made:
The manufacture method of Core-shell organic silicon durable paint, in airtight pressure vessel, add above-mentioned weight portion water,
Cellulose, rutile, calcined kaolin, blanc fixe, mica powder, triple superphosphate and ethylene glycol utilize hydro-thermal method at 50～70 DEG C
Mixing core processed, the response time is no less than 30min, then adds the dispersant DP270 of above-mentioned weight ratio in continuous dropping mode, kills
Microbial inoculum XG-405, paint antifoaming agent NXZ, function additive AMP-95, function additive 2100, coalescents, thickening agent TT-936, stream
Flat agent HEUR-D and preservative are simultaneously introduced polymerization, uniform stirring, ripening, levelling viscosity, and it is qualified to check through technical specification
Rear metering packing.
The beneficial effects of the present invention is: manufacturing process is simple, low cost of manufacture is suitable for industrialization, prepared coating has
Good stability, cohesive and mechanical property, the soft grace of coating film gloss so that film chemical stability is high, thus reaches
The most durable super-durable performance, use Core-shell technology formed densification and tough and tensile film, there is good hydrophobic breathability
With high self-cleaning, it is the optimal representative of a new generation's water paint, has gathered environmental protection and guarantor's light of oil paint, the guarantor of water paint
Color, anti-pollution characteristic extra-weather-proof, super, it is functional that film has acidproof, alkaline-resisting, chemicals-resistant pollution etc., it is adaptable to various houses,
The new construction of the buildings such as office building, hotel, Factory Building, school and engineering.
Detailed description of the invention
Further describe technical scheme below in conjunction with embodiment, but claimed scope is not limited to institute
State.
Embodiment 1
Core-shell organic silicon durable paint, it is made up of the raw material of following weight portion:
The manufacture method of Core-shell organic silicon durable paint, in airtight pressure vessel, add above-mentioned weight portion water,
Cellulose, rutile, calcined kaolin, blanc fixe, mica powder, triple superphosphate and ethylene glycol utilize hydro-thermal method to mix at 70 DEG C
Core processed, response time 30min, then add the dispersant DP270 of above-mentioned weight ratio, antibacterial XG-in continuous dropping mode
405, paint antifoaming agent NXZ, function additive AMP-95, function additive 2100, coalescents, thickening agent TT-936, levelling agent
HEUR-D and preservative are simultaneously introduced polymerization, uniform stirring, ripening, levelling viscosity, count after the assay was approved through technical specification
Amount packaging.
Embodiment 2
Core-shell organic silicon durable paint, it is made up of the raw material of following weight portion:
The manufacture method of Core-shell organic silicon durable paint, in airtight pressure vessel, add above-mentioned weight portion water,
Cellulose, rutile, calcined kaolin, blanc fixe, mica powder, triple superphosphate and ethylene glycol utilize hydro-thermal method to mix at 70 DEG C
Core processed, response time 60min, then add the dispersant DP270 of above-mentioned weight ratio, antibacterial XG-in continuous dropping mode
405, paint antifoaming agent NXZ, function additive AMP-95, function additive 2100, coalescents, thickening agent TT-936, levelling agent
HEUR-D and preservative are simultaneously introduced polymerization, uniform stirring, ripening, levelling viscosity, count after the assay was approved through technical specification
Amount packaging.
Embodiment 3
The manufacture method of Core-shell organic silicon durable paint, in airtight pressure vessel, add above-mentioned weight portion water,
Cellulose, rutile, calcined kaolin, blanc fixe, mica powder, triple superphosphate and ethylene glycol utilize hydro-thermal method to mix at 60 DEG C
Core processed, response time 50min, then add the dispersant DP270 of above-mentioned weight ratio, antibacterial XG-in continuous dropping mode
405, paint antifoaming agent NXZ, function additive AMP-95, function additive 2100, coalescents, thickening agent TT-936, levelling agent
HEUR-D and preservative are simultaneously introduced polymerization, uniform stirring, ripening, levelling viscosity, count after the assay was approved through technical specification
Amount packaging.
Embodiment 4
The manufacture method of Core-shell organic silicon durable paint, in airtight pressure vessel, add above-mentioned weight portion water,
Cellulose, rutile, calcined kaolin, blanc fixe, mica powder, triple superphosphate and ethylene glycol utilize hydro-thermal method to mix at 55 DEG C
Core processed, response time 40min, then add the dispersant DP270 of above-mentioned weight ratio, antibacterial XG-in continuous dropping mode
405, paint antifoaming agent NXZ, function additive AMP-95, function additive 2100, coalescents, thickening agent TT-936, levelling agent
HEUR-D and preservative are simultaneously introduced polymerization, uniform stirring, ripening, levelling viscosity, count after the assay was approved through technical specification
Amount packaging.
Embodiment 5
The manufacture method of Core-shell organic silicon durable paint, in airtight pressure vessel, add above-mentioned weight portion water,
Cellulose, rutile, calcined kaolin, blanc fixe, mica powder, triple superphosphate and ethylene glycol utilize hydro-thermal method to mix at 65 DEG C
Core processed, response time 45min, then add the dispersant DP270 of above-mentioned weight ratio, antibacterial XG-in continuous dropping mode
405, paint antifoaming agent NXZ, function additive AMP-95, function additive 2100, coalescents, thickening agent TT-936, levelling agent
HEUR-D and preservative are simultaneously introduced polymerization, uniform stirring, ripening, levelling viscosity, count after the assay was approved through technical specification
Amount packaging.
Claims (1)
1. Core-shell organic silicon durable paint, it is characterised in that: it is made up of the raw material of following weight portion:
The manufacture method of described Core-shell organic silicon durable paint: in airtight pressure vessel, add above-mentioned weight portion water,
Cellulose, rutile, calcined kaolin, blanc fixe, mica powder, triple superphosphate and ethylene glycol utilize hydro-thermal method at 50～70 DEG C
Mixing core processed, the response time is no less than 30min, then adds the dispersant DP270 of above-mentioned weight portion in continuous dropping mode, kills
Microbial inoculum XG-405, paint antifoaming agent NXZ, function additive AMP-95, function additive 2100, coalescents, thickening agent TT-936, stream
Flat agent HEUR-D and preservative are simultaneously introduced polymerization, uniform stirring, ripening, adjustment viscosity, and it is qualified to check through technical specification
Rear metering packing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210491373.4A CN102964885B (en) | 2012-11-27 | 2012-11-27 | Core-shell organic silicon durable paint and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210491373.4A CN102964885B (en) | 2012-11-27 | 2012-11-27 | Core-shell organic silicon durable paint and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102964885A CN102964885A (en) | 2013-03-13 |
| CN102964885B true CN102964885B (en) | 2016-12-21 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210491373.4A Expired - Fee Related CN102964885B (en) | 2012-11-27 | 2012-11-27 | Core-shell organic silicon durable paint and preparation method thereof |
Country Status (1)
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107815198A (en) * | 2017-10-26 | 2018-03-20 | 宁波甬波新材料科技有限公司 | A kind of water paint for floor chamfer site and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1152329A (en) * | 1994-07-08 | 1997-06-18 | 纳幕尔杜邦公司 | Durable coating compositions |
| EP0820961A1 (en) * | 1996-07-24 | 1998-01-28 | Nissan Chemical Industries, Limited | Process for producing an acidic aqueous alumina sol |
| CN1850724A (en) * | 2006-05-16 | 2006-10-25 | 广东工业大学 | Preparation method for synthesizing nucleocapsid TiO2/Al2O3 nano powder by one-step hydrothermal process |
| CN101041758A (en) * | 2007-03-21 | 2007-09-26 | 邓天宁 | Crylic acid emulsion coating having three-in-one functions of decoration, thermal insulation and water resistance |
| JP2008037961A (en) * | 2006-08-03 | 2008-02-21 | National Institute Of Advanced Industrial & Technology | Sheet-like fluorescent particle and method for producing the same |
| CN101168640A (en) * | 2007-11-26 | 2008-04-30 | 北京京卫宏远工贸有限公司 | Environment-friendly type antifreeze emulsion paint and preparation method thereof |
-
2012
- 2012-11-27 CN CN201210491373.4A patent/CN102964885B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1152329A (en) * | 1994-07-08 | 1997-06-18 | 纳幕尔杜邦公司 | Durable coating compositions |
| EP0820961A1 (en) * | 1996-07-24 | 1998-01-28 | Nissan Chemical Industries, Limited | Process for producing an acidic aqueous alumina sol |
| CN1850724A (en) * | 2006-05-16 | 2006-10-25 | 广东工业大学 | Preparation method for synthesizing nucleocapsid TiO2/Al2O3 nano powder by one-step hydrothermal process |
| JP2008037961A (en) * | 2006-08-03 | 2008-02-21 | National Institute Of Advanced Industrial & Technology | Sheet-like fluorescent particle and method for producing the same |
| CN101041758A (en) * | 2007-03-21 | 2007-09-26 | 邓天宁 | Crylic acid emulsion coating having three-in-one functions of decoration, thermal insulation and water resistance |
| CN101168640A (en) * | 2007-11-26 | 2008-04-30 | 北京京卫宏远工贸有限公司 | Environment-friendly type antifreeze emulsion paint and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN102964885A (en) | 2013-03-13 |
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Granted publication date: 20161221 Termination date: 20211127 |