CN102896267A - Isothermal forging method of TC17 titanium alloy disc-shaped forge piece - Google Patents

Isothermal forging method of TC17 titanium alloy disc-shaped forge piece Download PDF

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CN102896267A
CN102896267A CN2012103696218A CN201210369621A CN102896267A CN 102896267 A CN102896267 A CN 102896267A CN 2012103696218 A CN2012103696218 A CN 2012103696218A CN 201210369621 A CN201210369621 A CN 201210369621A CN 102896267 A CN102896267 A CN 102896267A
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titanium alloy
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陈由红
王淑云
东赟鹏
张敏聪
李金栋
孙兴
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BEIJING INSTITUTE OF AERONAUTICAL MATERIALS CHINA AVIATION INDUSTRY GROUP Corp
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Abstract

本发明涉及一种钛合金盘形锻件的锻造方法,特别涉及一种TC17钛合金盘形锻件的等温锻造方法。其工艺为:将钛合金棒锭加热到相变点以下40℃~50℃,加热上、下平模到相变点以下40℃~50℃,上平模下行使得棒锭以0.001s-1~0.01s-1的应变速率进行第一火等温镦粗成一次饼坯,然后再以0.001s-1~0.01s-1的应变速率进行第二火等温镦粗成二次饼坯,变形量30~50%;加热二次饼坯到相变点以下20℃~30℃,加热上、下型腔模到相变点以下20℃~30℃,压机锻压二次饼坯使其以0.001s-1~0.01s-1的应变速率在型腔模内变形量达到30~50%后成形锻件;锻后锻件热处理采用固溶+时效处理。采用该方法锻造的盘形锻件具有较理想的等轴组织和高性能,适用于制造航空发动机的压气机盘和涡轮盘等锻件。

Figure 201210369621

The invention relates to a forging method of a titanium alloy disc forging, in particular to an isothermal forging method of a TC17 titanium alloy disc forging. The process is as follows: heating the titanium alloy ingot to 40°C to 50°C below the phase transition point, heating the upper and lower flat dies to 40°C to 50°C below the phase transition point, and moving the upper flat die down so that the ingot can be heated at a temperature of 0.001s -1 ~ The strain rate of 0.01s -1 is subjected to the first fire isothermal upsetting to form a primary cake base, and then the second fire isothermal upsetting is performed at a strain rate of 0.001s -1 to 0.01s -1 to form a secondary cake base, with a deformation of 30 ~50%; heat the secondary cake base to 20°C-30°C below the phase transition point, heat the upper and lower cavity molds to 20°C-30°C below the phase transition point, press the secondary cake base to forge it in 0.001s The strain rate of -1 ~ 0.01s -1 forms the forging after the deformation in the cavity mold reaches 30 ~ 50%; the heat treatment of the forging after forging adopts solid solution + aging treatment. The disk-shaped forgings forged by this method have ideal equiaxed structure and high performance, and are suitable for manufacturing forgings such as compressor disks and turbine disks of aero-engines.

Figure 201210369621

Description

一种TC17钛合金盘形锻件的等温锻造方法A kind of isothermal forging method of TC17 titanium alloy disc forging

技术领域 technical field

本发明涉及一种钛合金盘形锻件的锻造方法,特别涉及一种TC17钛合金盘形锻件的等温锻造方法。The invention relates to a forging method of a titanium alloy disc forging, in particular to an isothermal forging method of a TC17 titanium alloy disc forging.

背景技术 Background technique

钛合金具有强度高、质量轻和良好的抗腐蚀等特性,在航空、航天领域有着重要的应用,尤其是航空发动机的压气机盘、涡轮盘等盘件由于工作环境恶劣,受力复杂,往往采用综合性能优异的α+β型两相钛合金锻造成形。采用α+β型两相钛合金锻造的盘件具有高强度、断裂韧度好、淬透性高和锻造温度范围宽等一系列优点,能够满足损失容限设计的需要和高结构、高可靠性及低制造成本的要求。显微组织的变化对机械性能影响较为显著,而上述的优异综合性能须靠理想的锻件微观组织来保证。Titanium alloy has the characteristics of high strength, light weight and good corrosion resistance. It has important applications in the field of aviation and aerospace, especially the compressor discs and turbine discs of aero-engines. Due to the harsh working environment and complex stress, they are often It is formed by forging α+β type two-phase titanium alloy with excellent comprehensive performance. The disc forged with α+β two-phase titanium alloy has a series of advantages such as high strength, good fracture toughness, high hardenability and wide forging temperature range, which can meet the needs of loss tolerance design and high structure, high reliability and low manufacturing cost requirements. The change of microstructure has a significant impact on mechanical properties, and the above-mentioned excellent comprehensive properties must be guaranteed by the ideal microstructure of forgings.

《上海钢研》2006年02期刊登一篇名为钛合金整体叶盘等温锻造技术文章,该文章对TC17合金整体叶盘的锻件图、锻造毛坯的形状和模具结构及等温锻造工艺进行了研究,并通过等温锻造工艺生产出钛合金整体叶盘等温锻件。该文章所述TC17盘件等温锻造与本专利所述为同一类材料盘件等温锻造,但是该文章没有对所述锻件的成形工艺方法进行描述。不用的成形工艺方法有着不同的效果及经济效益。"Shanghai Iron and Steel Research" published an article titled "Titanium Alloy Blisk Isothermal Forging Technology" in February 2006. The article studied the forging diagram of the TC17 alloy blisk, the shape of the forging blank, the mold structure and the isothermal forging process. , and produce titanium alloy blisk isothermal forgings through isothermal forging process. The isothermal forging of the TC17 disc described in this article is the same type of material disc isothermal forging as described in this patent, but the article does not describe the forming process of the forging. Different forming process methods have different effects and economic benefits.

在α+β型钛合金锻造的研究上,因热变形工艺不同可以获得四种类型的显微组织,随着对发动机性能越来越高的要求,各项性能设计指标不断提高,许多研究工作投入到获得网篮组织,CN1403622A公开了一种钛合金准β锻造工艺,采用该工艺对α+β型钛合金进行准β锻时,是把钛合金坯料加热到β相变点温度附近的区域,即相变点温度以下10℃至相变点温度以上10℃的范围进行锻造,在这一区域加热时,由于坯料在出炉后的降温,锻件的变形实际上是在α+β区进行的,该网篮组织的初生α相在15以内。但是该方法是通过热模锻进行锻造,不能有效的控制锻造变形温度,因此对锻件组织的控制没有稳定性。In the research of α + β titanium alloy forging, four types of microstructures can be obtained due to different hot deformation processes. With the increasingly higher requirements for engine performance, various performance design indicators continue to improve, and a lot of research work has been invested in To obtain the basket structure, CN1403622A discloses a titanium alloy quasi-β forging process. When using this process to perform quasi-β forging on α+β-type titanium alloys, the titanium alloy blank is heated to a region near the temperature of the β phase transition point, that is, the phase transition Forging is carried out in the range of 10°C below the transformation point temperature to 10°C above the transformation point temperature. When heating in this area, due to the cooling of the billet after it is released from the furnace, the deformation of the forging is actually carried out in the α+β area. The structure of the basket structure The primary alpha phase is within 15. However, this method is forging by hot die forging, which cannot effectively control the forging deformation temperature, so there is no stability in the control of the structure of the forging.

专利CN101804441A《TC17两相钛合金盘形锻件的近等温锻造方法》,该方法采用“低-高-低”工艺制坯,即把TC17钛合金棒锭加热到相变点以下30℃~75℃,镦粗;再加热到相变点以上20℃~60℃,拔长;再加热到相变点以下30℃~75℃,镦粗冲孔后得到α等轴化分布的环形坯料,再把环形坯料加热到相变点以上20℃~60℃,把锻模加热到相变点以下10℃~20℃后制备全网篮状组织的锻件。该方法虽然也是TC17钛合金盘形锻件的锻造方法,但是制备出的是全网篮状组织的锻件,若要得到双态组织的锻件,该方法则不可实现。Patent CN101804441A "Near-isothermal Forging Method of TC17 Two-phase Titanium Alloy Disc Forging", the method adopts the "low-high-low" process to make billets, that is, the TC17 titanium alloy ingot is heated to 30°C to 75°C below the phase transition point , upsetting; reheating to 20°C-60°C above the phase transition point, elongated; reheating to 30°C-75°C below the phase transition point, upsetting and punching to obtain a circular blank with α equiaxed distribution, and then The ring blank is heated to 20°C to 60°C above the phase transition point, and the forging die is heated to 10°C to 20°C below the phase transition point to prepare a forging with a full mesh and basket structure. Although this method is also a forging method for TC17 titanium alloy disc forgings, it produces a forging with a full mesh and basket structure. If a forging with a two-state structure is to be obtained, this method cannot be realized.

发明内容 Contents of the invention

本发明要解决的技术问题是提供一种使盘形锻件内部显微组织为含量约20%等轴α相且均匀分布的双态组织的TC17钛合金盘形锻件的等温锻造方法。本发明的技术解决方案是,The technical problem to be solved by the present invention is to provide an isothermal forging method for a TC17 titanium alloy disc forging whose internal microstructure is about 20% equiaxed α-phase and uniformly distributed bimodal structure. Technical solution of the present invention is,

把TC17钛合金棒材按规格下料成棒锭,加热该棒锭到合金相变点以下40℃~50℃,按该棒锭有效厚度0.6~1min/mm保温;加热上、下平模到相变点以下40℃~50℃后把所述棒锭装入平模,压机锻压棒锭使其以0.001s-1~0.01s-1的应变速率在平模内变形量达到30%~50%成形为一次饼坯,从平模内取出一次饼坯,趁热回炉加热保温;Cut the TC17 titanium alloy bar into an ingot according to the specifications, heat the ingot to 40°C-50°C below the phase transition point of the alloy, and keep it warm according to the effective thickness of the ingot at 0.6-1min/mm; heat the upper and lower flat dies to phase Put the ingot into the flat die at 40°C-50°C below the change point, and press the ingot to forge the ingot to make it deform in the flat die at a strain rate of 0.001s - 1-0.01s -1 to 30%-50 %Formed into a primary cake base, take out the primary cake base from the flat mold, return to the furnace while it is hot to heat and keep it warm;

回炉保温时间按到温后计算,保温时间按第一次保温时间减半;保温结束后,再次把一次饼坯装入平模进行第二火次镦粗,压机锻压一次饼坯使其以0.001s-1~0.01s-1的应变速率在平模内变形量达到30%~50%成形为二次饼坯,从平模内取出二次饼坯空冷;The heat preservation time of returning to the furnace is calculated according to the temperature after reaching the temperature, and the heat preservation time is halved according to the first heat preservation time; With a strain rate of 0.001s -1 ~0.01s -1 , the deformation in the flat die reaches 30% to 50% to form a secondary cake base, and the secondary cake base is taken out from the flat die and air-cooled;

加热上述的二次饼坯到相变点以下20℃~30℃,按该二次饼坯有效厚度0.6~1min/mm保温;加热上、下型腔模到相变点以下20℃~30℃后把二次饼坯装入型腔模,压机锻压二次饼坯使其以0.001s-1~0.01s-1的应变速率在型腔模内变形量达到30%~50%后成形锻件,从型腔模内取出锻件空冷;Heat the above-mentioned secondary cake base to 20°C-30°C below the phase transition point, and keep warm according to the effective thickness of the secondary cake base of 0.6-1min/mm; heat the upper and lower cavity molds to 20°C-30°C below the phase transition point Finally, put the secondary cake blank into the cavity mold, press the secondary cake blank to forge the secondary cake blank at a strain rate of 0.001s -1 ~ 0.01s -1 in the cavity mold, and then form the forging after the deformation reaches 30% ~ 50%. , take out the forging from the cavity mold and air cool;

锻后对锻件进行热处理,锻后锻件进行热处理,其热处理制度为为780℃~820℃×4小时,水冷;590℃~650℃×8小时,空冷。After forging, the forgings are heat treated, and the forgings are heat treated after forging. The heat treatment system is 780℃~820℃×4 hours, water cooling; 590℃~650℃×8 hours, air cooling.

所述的锻件热处理制度为800℃±10℃×4小时,水冷;620℃±10℃×8小时,空冷。The heat treatment system of the forging is 800°C±10°C×4 hours, water cooling; 620°C±10°C×8 hours, air cooling.

为方便取模,所述棒锭及饼坯在加热装模前先预热到200℃~300℃后在其表面喷涂玻璃润滑剂;所述平模及型腔模在所述棒锭装模前在模具表面喷涂玻璃润滑剂。For the convenience of taking molds, the ingot and cake base are preheated to 200°C-300°C before heating and loading, and then spray glass lubricant on the surface; the flat mold and cavity mold are molded on the ingot Before spraying glass lubricant on the surface of the mold.

与现有技术相比,本发明的有益效果如下:Compared with the prior art, the beneficial effects of the present invention are as follows:

本发明采用棒锭两火次等温镦粗工艺制坯,即把TC17钛合金棒锭加热到相变点以下40℃~50℃,把平模加热到相变点以下40℃~50℃后,使棒锭在平模内以应变速率0.001s-1~0.01s-1范围内、变形量达到30%~50%范围内进行两火次镦粗,保证棒锭在两相区内进行,得到细小且分布均匀的等轴α组织的饼坯,为后续锻件成形打下了基础。The present invention adopts the ingot two-firing isothermal upsetting process to make the billet, that is, the TC17 titanium alloy ingot is heated to 40°C-50°C below the phase transition point, and the flat die is heated to 40°C-50°C below the phase transition point. In the flat die, the ingot is subjected to two-fire upsetting with a strain rate of 0.001s -1 to 0.01s -1 and a deformation of 30% to 50%, so as to ensure that the ingot is carried out in the two-phase region, and the obtained The fine and evenly distributed equiaxed α-structure cake lays the foundation for subsequent forging forming.

把饼坯加热到相变点以下20℃~30℃,把型腔模加热到相变点以下20℃~30℃后,使饼坯在型腔模内以应变速率0.001s-1~0.01s-1范围内、变形量达到30%~50%范围内成形锻件,保证锻坯在两相区内进行,得到等轴α含量约为20%的双态组织,从而获得最佳的断裂韧性和塑性的匹配,充分满足损失容限设计的需要。Heat the cake base to 20°C to 30°C below the phase transition point, heat the cavity mold to 20°C to 30°C below the phase transition point, and make the cake base in the cavity mold at a strain rate of 0.001s -1 to 0.01s In the range of -1 , the deformation reaches 30% to 50% to form forgings, to ensure that the forging blank is carried out in the two-phase region, and to obtain a two-state structure with an equiaxed α content of about 20%, so as to obtain the best fracture toughness and Plastic matching fully meets the needs of loss tolerance design.

本发明的优点是通过常规的α+β两相锻造区等温锻造,即等温镦粗+等温模锻,变形抗力小,容易成形,稳定性好、成品率高,且避免了现行工艺中多火次自由锻改锻制坯所带来的高成本、长周期,在满足设计要求的同时大大增加了经济效益。The invention has the advantages of isothermal forging in the conventional α+β two-phase forging zone, that is, isothermal upsetting + isothermal die forging, small deformation resistance, easy forming, good stability, high yield, and avoiding the excessive fire in the current process The high cost and long period brought about by the secondary free forging to forging billet greatly increase the economic benefits while meeting the design requirements.

采用该方法锻造的锻件经热处理后具有较理想的综合性能,并且实现150mm厚锻件超声波检测杂波水平满足0.8-12DB要求。The forgings forged by this method have ideal comprehensive properties after heat treatment, and the ultrasonic detection clutter level of 150mm thick forgings can meet the requirements of 0.8-12DB.

附图说明 Description of drawings

图1是钛合金两火次等温镦粗制坯及一火次等温锻造成形盘形锻件工艺流程图。Figure 1 is a process flow chart of forming a disc forging by two times of isothermal upsetting and one time of isothermal forging of titanium alloy.

图2是采用TC17钛合金等温锻造成形锻件沿中心线剖开的纵截面R/2位置处的金相组织照片。Figure 2 is a photo of the metallographic structure at the R/2 position of the longitudinal section cut along the center line of the forging formed by isothermal forging of TC17 titanium alloy.

具体实施方式 Detailed ways

α+β型两相钛合金,例如:中国材料牌号为TC17的钛合金。α+β type two-phase titanium alloy, for example: titanium alloy with Chinese material designation TC17.

下面给出了TC17钛合金的近等温锻造工艺步骤:The near-isothermal forging process steps of TC17 titanium alloy are given below:

步骤1:检测所采用的TC17钛合金材料相变点温度为895℃。Step 1: Detect that the phase transition point temperature of the TC17 titanium alloy material used is 895°C.

步骤2:如图1所示,把TC17钛合金圆形棒材按锻件规格下料成棒锭1,把棒锭1预热到300℃后在其表面喷涂专用润滑剂,再把该棒锭1放到锻造加热炉内加热到钛合金相变点以下855℃,保温,保温时间按棒锭有效厚度0.6min/mm计算。Step 2: As shown in Figure 1, the TC17 titanium alloy round bar is cut into the ingot 1 according to the forging specification, and the ingot 1 is preheated to 300°C and then sprayed with a special lubricant on its surface, and then the ingot 1 Put it in the forging heating furnace and heat it to 855°C below the phase transition point of the titanium alloy, and keep it warm. The holding time is calculated based on the effective thickness of the ingot of 0.6min/mm.

步骤3:把上平模2和下平模3加热到该钛合金相变点以下855℃,若要在取模时更加方便,可以在上平模2和下平模3的表面喷涂玻璃润滑剂,加热时通过安装在锻压机上的环形模具加热炉8进行加热,再把经步骤1加热后的棒锭1装入平模,通过上平模下行对棒锭1进行等温镦粗成一次饼坯4。一次饼坯4趁热回炉。一次饼坯4的变形量为33%,一次饼坯4在锻压过程中的锻造应变速率为0.001s- 1~0.01s-1Step 3: Heat the upper flat die 2 and the lower flat die 3 to 855°C below the phase transition point of the titanium alloy. If it is more convenient to take the die, you can spray glass lubricant on the surface of the upper flat die 2 and the lower flat die 3. Heating is carried out through the ring mold heating furnace 8 installed on the forging press, and then the ingot 1 heated in step 1 is loaded into the flat die, and the ingot 1 is subjected to isothermal upsetting through the upper flat die to form a cake base 4 . Once the cake base 4 is returned to the furnace while it is hot. The deformation of the primary cake base 4 is 33%, and the forging strain rate of the primary cake base 4 in the forging process is 0.001s - 1 ~0.01s -1 .

步骤4:把上述趁热回炉的一次饼坯4加热到该钛合金相变点以下855℃,保温,保温时间按步骤2的保温时间减半。Step 4: heat the above-mentioned primary cake blank 4 returned to the furnace while it is hot to 855° C. below the phase transition point of the titanium alloy, keep it warm, and keep the keep time halved by step 2.

步骤5:从锻造加热炉内取出一次饼坯4,放到锻压机上再进行第二火次镦粗得到二次饼坯5,锻后空冷。二次饼坯5的变形量为36%,二次饼坯5在锻压过程中的锻造应变速率为0.001s-1~0.01s-1Step 5: Take out the primary cake blank 4 from the forging heating furnace, put it on the forging press and perform the second fire upsetting to obtain the secondary cake blank 5, and air cool after forging. The deformation of the secondary cake base 5 is 36%, and the forging strain rate of the secondary cake base 5 in the forging process is 0.001s -1 ~0.01s -1 .

步骤6:把二次饼坯5预热到300℃后在其表面喷涂玻璃润滑剂,再把该饼坯加热到该钛合金相变点以下865℃,保温,保温时间按该饼坯有效厚度0.6min/mm计算。Step 6: Preheat the secondary cake base 5 to 300°C, spray glass lubricant on its surface, then heat the cake base to 865°C below the phase transition point of the titanium alloy, keep it warm, and keep the heat preservation time according to the effective thickness of the cake base 0.6min/mm calculation.

步骤7:把上型腔模6和下型腔模7加热到该钛合金相变点以下865℃,若要在取模时更加方便,可以在上型腔模6和下型腔模7的表面喷涂玻璃润滑剂,加热时通过安装在锻压机上的环形模具加热炉8进行加热,再把经步骤5加热后的饼坯5装入型腔模,通过锻压机施加压力使上型腔模6下行,与下型腔模7合模并一火次把饼坯5锻压成形锻件9,锻件9出模空冷。锻件9的变形量为33%,锻件9在锻压过程中的锻造应变速率为0.001s-1~0.01s-1Step 7: Heat the upper cavity mold 6 and the lower cavity mold 7 to 865°C below the titanium alloy phase transition point. If it is more convenient when taking the mold, you can heat the upper cavity mold 6 and the lower cavity mold 7. The surface is sprayed with glass lubricant, heated by the ring mold heating furnace 8 installed on the forging press, and then the cake base 5 heated in step 5 is loaded into the cavity mold, and the pressure is applied by the forging press to make the upper cavity mold 6 Descending, close the mold with the lower cavity mold 7 and forge and press the cake blank 5 to form the forging 9 at one time, and the forging 9 is released from the mold and air-cooled. The deformation of the forging 9 is 33%, and the forging strain rate of the forging 9 in the forging process is 0.001s −1 to 0.01s −1 .

步骤8:锻件9进行热处理,即固溶+时效处理,其中固溶处理是把锻件9加热到800℃±10℃,保温4h后放入水中迅速冷却(水淬);时效处理是把经固溶处理后的锻件9加热到620℃±10℃,保温8h后进行空冷。Step 8: The forging 9 is heat treated, that is, solution + aging treatment, wherein the solution treatment is to heat the forging 9 to 800°C±10°C, keep it warm for 4 hours, and then put it into water to cool it rapidly (water quenching); The forged piece 9 after the solution treatment is heated to 620° C.±10° C., held for 8 hours, and then air-cooled.

Claims (4)

1. the isothermal forging method of a TC17 titanium alloy disk forge piece is characterized in that, may further comprise the steps:
The TC17 titanium alloy rod bar is become excellent ingot by the specification blanking, heat this rod ingot to below the alloy phase height 40 ℃~50 ℃, by this rod ingot effective thickness 0.6~1min/mm insulation;
Heat upper and lower flat-die and after below the transformation temperature 40 ℃~50 ℃ described excellent ingot is put into flat-die, press forges and presses excellent ingot makes it with 0.001s -1~0.01s -1Strain rate after flat-die internal strain amount reaches 30%~50%, obtain one time biscuit, take out and to melt down while hot;
Biscuit melts down temperature retention time while hot by calculating after temperature, temperature retention time reduces by half, and after insulation finishes, biscuit flat-die of packing into is carried out the second fire and is upset as the secondary biscuit, and press forges and presses a biscuit makes it with 0.001s - 1~0.01s -1Strain rate reach 30%~50% rear taking-up air cooling in flat-die internal strain amount;
Heat described secondary biscuit to following 20 ℃~30 ℃ of transformation temperature, by this secondary biscuit effective thickness 0.6~1min/mm insulation; Heat upper and lower swaging die after below the transformation temperature 20 ℃~30 ℃ the described secondary biscuit swaging die of packing into, press forging and pressing secondary biscuit makes it with 0.001s -1~0.01s -1Strain rate reach 30%~50% postforming forging in swaging die internal strain amount;
Forging is heat-treated after forging, and its heat treating regime is for being 780 ℃~820 ℃ * 4 hours, water-cooled; 590 ℃~650 ℃ * 8 hours, air cooling.
2. according to the isothermal forging method of TC17 titanium alloy forging claimed in claim 1, it is characterized in that: described excellent ingot is preheating to 200 ℃~300 ℃ before adding the hot charging mould after at its surface spraying glass lubricant.
3. according to the isothermal forging method of TC17 titanium alloy forging claimed in claim 1, it is characterized in that: described flat-die and swaging die before described excellent ingot dress mould at the mould surface spraying glass lubricant.
4. according to the isothermal forging method of TC17 titanium alloy forging claimed in claim 1, it is characterized in that: described forging heat treating regime is 800 ℃ ± 10 ℃ * 4 hours, water-cooled; 620 ℃ ± 10 ℃ * 8 hours, air cooling.
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CN115194069A (en) * 2022-07-14 2022-10-18 中国科学院金属研究所 A kind of preparation method of Ti175 alloy large size integral blisk forging
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