CN102873739B - Improved production method for vacuum insulated panel - Google Patents

Improved production method for vacuum insulated panel Download PDF

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Publication number
CN102873739B
CN102873739B CN201210187115.7A CN201210187115A CN102873739B CN 102873739 B CN102873739 B CN 102873739B CN 201210187115 A CN201210187115 A CN 201210187115A CN 102873739 B CN102873739 B CN 102873739B
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film
production method
insulating plate
vacuum
vacuum heat
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CN102873739A (en
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何奕
侯钦鹏
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Qingdao Kerui new environmental protection materials Group Co. Ltd.
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Qingdao Creek New Environmental Materials Co Ltd
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Abstract

The invention relates to an improved production method for a vacuum insulated panel, which comprises the following technical steps: dosing: inputting pumice stones, diatomaceous earth, calcium silicate, aerosil, inorganic fiber and vacuum stabilizer in proportion to a mixer to be mixed adequately; drying: drying the mixed materials which are agitated uniformly; core forming: inputting the dried materials and a degasser into a mould, and placing the mould into a press to be pressurized for forming; wrapping: taking a press-formed core plate out of the mould and wrapping the core plate in non-woven fabric to obtain a vacuum insulated panel core plate for buildings; placing the core plate in a high gas resistant film bag and vacuumizing, wherein the vacuum degree is 0.02-20 Pa; and then sealing. The invention has the advantages that the strength of the insulated panel is increased by mixing fiber, pumice stones, diatomaceous earth, calcium silicate and aerosol, and the insulating performance is improved. The core has a lower coefficient of heat conductivity and is an inorganic material which is not easy to combust. The raw materials are low in cost, the cost of the raw materials is lowered, and the environmental pollution is reduced.

Description

The production method of the vacuum heat-insulating plate improved
Technical field
The present invention relates to a kind of production method of vacuum heat-insulating plate of improvement, for the production of vacuum heat-insulating plate, this vacuum heat-insulating plate is used as building or industrial heat preservation material.
Background technology
Existing vacuum heat-insulating plate is primarily of inner insulated core material and cover high-gas resistance film formation outward, wherein insulated core material generally adopts conventional insulation material (as foamed plastic), glass fibre or/and the materials such as aeroge are made, its shortcoming is that material cost is high, and energy consumption is high, not environmentally.
Summary of the invention
The present invention aims to provide a kind of production method of vacuum heat-insulating plate of improvement, and high with the material cost solving prior art existence, energy consumption is high, problem not environmentally.
Technical scheme of the present invention is: a kind of production method of vacuum heat-insulating plate of improvement, core is loaded in high resistant air film bag, vacuumize rear sealing, it is characterized in that, described core composition and parts by weight are: float stone 20-30, diatomite 10-15, calcium silicates 15-20, aerosil 10-15, inorfil 8-12, vacuum stabilizer 2-3;
Manufacture craft comprises the steps:
(1) prepare burden: the material of described formula is dropped into mixer and fully mixes;
(2) dry: dried by the compound stirred, bake out temperature controls at 100-120 DEG C, until the moisture content of compound reaches less than 0.5%, stop drying;
(3) non-woven fabric bag: non-woven fabrics is made three banding sacks, or the three banding sacks making band limb;
(4) core material is filling: dropped into by the mixture of oven dry in the non-woven fabrics sack of three bandings, then by the heat-sealing of opening;
(5) Bag Material shakeouts: the mixture entirety of having sealed shakeout:
(6) compressing: by the packed mixture shakeout, under putting into press together with the non-woven fabrics sack of outside, carry out compression forming, obtain heat preservation core plate;
(7) heat preservation core plate inserted in high resistant air film bag and vacuumize, vacuum is 0.02-20Pa, then seals.
The drying course of step (2) also can carry out in the process of step (1) simultaneously.
In step (4), the filling speed of automatic filling machine be 8-25 bag/point, mixture is by measuring cup or Auger feeding and measure.
In step (3) and step (6), non-woven fabrics used is flame-retardant non-woven, and mass area ratio is 35-100g/m 2.
In step (5), the mixture sealed by manually shakeouing, or is flattened by roll shaft.
In step (6), the decrease speed of press controls at 3-7 cm/s, and Stress control is at 20-280T/m 2.
In step (6), compressing technique is progressively suppressed continuously shaped by the belt that upper and lower a few pair roller subband is dynamic continuously.
Described inorfil comprise in rock wool, glass, lignin fibre and glass-ceramic fibre more than one, mix with arbitrary proportion; Fibre length is 3-12mm, and diameter is 0.2-13 micron.
Described high resistant air film bag is made up of the overcoat in outside and the sealant compound of inner side, and sealing layer comprises aluminium foil, polyester film, nylon film, polyethylene film, polyvinyl chloride film, polystyrene film, polyvinylidene chloride, polyvinyl alcohol film, ethylene-vinyl acetate copolymer film, polyvinyl alcohol film, nylon film, ethylene/vinyl alcohol copolymer film, polycarbonate film, polyacrylic one or more are composited; The outermost protective layer of this high resistant air film bag by glass-fiber-fabric, non-woven fabrics, carbon-fiber cloth, basalt fiber cloth, ceramic fiber cloth one or more be composited.
Be provided with edge sealing at the two ends of described high resistant air film bag, this edge sealing is located at the relative of the two ends of this high resistant air film bag, is provided with the occlusal crib coincide with this edge sealing at the another side relative with this edge sealing.
Advantage of the present invention is: fiber mixes with float stone, diatomite, calcium silicates and aerosil the intensity adding warming plate, and improves heat-insulating property.Vacuum stabilizer improves the durability that vacuum keeps.Core can reach lower thermal conductivity factor, is again inorganic material, nonflammable, can meet the needs of country's six or five energy conservation plans.Low in raw material price, ensures certain low thermal conductivity, reduces cost of material; Decrease the pollution to environment.
Accompanying drawing explanation
Fig. 1 is the side structure schematic diagram of one embodiment of the invention;
Fig. 2 is another embodiment of the present invention side structure schematic diagram;
Fig. 3 is the top view of Fig. 1;
Fig. 4 is the docking schematic diagram of the present invention when applying.
Detailed description of the invention
The production method of the vacuum heat-insulating plate of a kind of improvement of the present invention, core is loaded in high resistant air film bag, vacuumize rear sealing, it is characterized in that, described core composition and parts by weight are: float stone 20-30, diatomite 10-15, calcium silicates 15-20, aerosil 10-15, inorfil 8-12 and vacuum stabilizer 2-3;
Manufacture craft comprises the steps:
(1) prepare burden: the material of described formula is dropped into mixer and fully mixes;
(2) dry: dried by the compound stirred, bake out temperature controls at 100-120 DEG C, until the moisture content of compound reaches less than 0.5%, stop drying;
(3) non-woven fabric bag: non-woven fabrics is made three banding sacks, or the three banding sacks making band limb;
(4) core material is filling: drop in the non-woven fabrics sack of three bandings with automatic filling machine by the mixture of oven dry, then by the heat-sealing of opening.The filling speed of automatic filling machine be 8-25 bag/point, mixture is by measuring cup or Auger feeding and measure.
(5) Bag Material shakeouts: the mixture entirety of having sealed shakeout.The mixture sealed by manually shakeouing, or is flattened by roll shaft.
(6) compressing: by the packed mixture shakeout, under putting into press together with the non-woven fabrics sack of outside, carry out compression forming, obtain heat preservation core plate.The decrease speed of press controls at 3-7 cm/s, and Stress control is at 20-280T/m 2.
Compressing technique also can be continuously shaped, and the belt dynamic by upper and lower a few pair roller subband is progressively compressing continuously.
(7) heat preservation core plate inserted in high resistant air film bag and vacuumize, vacuum is 0.02-20Pa, then seals.
The drying course of step (2) also can carry out in the process of step (1) simultaneously.
In step (3) and step (6), non-woven fabrics used is flame-retardant non-woven, and mass area ratio is 35-100g/m 2.
Described vacuum active stabilizing agent is by active carbon, and one or more arbitrary proportion mixtures in barium lithium alloy activator, calcium oxide, magnesia and silica gel are formed.
Described inorfil comprises the one in rock wool, glass, lignin fibre and glass-ceramic fibre, or with the two or more above-mentioned fiber of arbitrary proportion mixing.Described fibre length is 3-12mm, and diameter is 0.2-13 micron.
Described high resistant air film bag is made up of the overcoat in outside and the sealant compound of inner side.
Described sealant comprises aluminium foil, polyester film, nylon film, polyethylene film, polyvinyl chloride film, polystyrene film, polyvinylidene chloride, polyvinyl alcohol film, ethylene-vinyl acetate copolymer film, polyvinyl alcohol film, nylon film, ethylene/vinyl alcohol copolymer film, polycarbonate film, polyacrylic one or more are composited.
The outermost protective layer of described high resistant air film bag by glass-fiber-fabric, non-woven fabrics, carbon-fiber cloth, basalt fiber cloth, ceramic fiber cloth one or more be composited.
Described high resistant air film bag also can adopt the material of any existing routine to make.Getter is also conventional material, adopts scattering device or adopts Rotating fields to be arranged on the surface of central layer.
See Fig. 1-Fig. 4, the vacuum heat-insulating plate contour structures that the present invention makes can be conventional shape, is provided with sealing strip 3(see Fig. 1 at the two ends of high resistant air film bag 1).Also the sealing strip 3 at high resistant air film bag 1 two ends can be located at the relative one side at the two ends of this high resistant air film bag 1, be provided with the occlusal crib 4 coincide with this edge sealing at the another side relative with sealing limit 3.When constructing, adjacent two pieces of warming plate A1 and A2 edge sealing 3 being placed on (as shown in Figure 4) in the occlusal crib 4 of the other side, reducing the heat bridge thickness between adjacent two pieces of warming plates, improve heat insulation effect and efficiency of construction.

Claims (9)

1. the production method of the vacuum heat-insulating plate improved, core is loaded in high resistant air film bag, vacuumize rear sealing, it is characterized in that, described core composition and parts by weight are: float stone 20-30, diatomite 10-15, calcium silicates 15-20, aerosil 10-15, inorfil 8-12, vacuum stabilizer 2-3; Described inorfil comprise in rock wool, glass, lignin fibre and glass-ceramic fibre more than one, mix with arbitrary proportion; Fibre length is 3-12mm, and diameter is 0.2-13 micron; Described vacuum stabilizer is made up of one or more arbitrary proportion mixtures in active carbon, barium lithium alloy activator, calcium oxide, magnesia and silica gel;
Manufacture craft comprises the steps:
(1) prepare burden: the material of described formula is dropped into mixer and fully mixes;
(2) dry: dried by the compound stirred, bake out temperature controls at 100-120 DEG C, until the moisture content of compound reaches less than 0.5%, stop drying;
(3) non-woven fabric bag: non-woven fabrics is made three banding sacks, or the three banding sacks making band limb;
(4) core material is filling: dropped into by the mixture of oven dry in the non-woven fabrics sack of three bandings, then by the heat-sealing of opening;
(5) Bag Material shakeouts: the mixture entirety of having sealed shakeout:
(6) compressing: by the packed mixture shakeout, under putting into press together with the non-woven fabrics sack of outside, carry out compression forming, obtain heat preservation core plate;
(7) heat preservation core plate inserted in high resistant air film bag and vacuumize, vacuum is 0.02-20Pa, then seals.
2. the production method of the vacuum heat-insulating plate of improvement according to claim 1, is characterized in that: the drying course of step (2) also can carry out in the process of step (1) simultaneously.
3. the production method of the vacuum heat-insulating plate of improvement according to claim 1, is characterized in that: in step (4), the filling speed of automatic filling machine be 8-25 bag/point, mixture is by measuring cup or Auger feeding and measure.
4. the production method of the vacuum heat-insulating plate of improvement according to claim 1, is characterized in that: in step (3) and step (6), non-woven fabrics used is flame-retardant non-woven, and mass area ratio is 35-100g/m 2.
5. the production method of the vacuum heat-insulating plate of improvement according to claim 1, is characterized in that: in step (5), and the mixture sealed by manually shakeouing, or is flattened by roll shaft.
6. the production method of the vacuum heat-insulating plate of improvement according to claim 1, is characterized in that: in step (6), the decrease speed of press controls at 3-7 cm/s, and Stress control is at 20-280T/m 2.
7. the production method of the vacuum heat-insulating plate of improvement according to claim 1, is characterized in that: in step (6), compressing technique is progressively suppressed continuously shaped by the belt that upper and lower a few pair roller subband is dynamic continuously.
8. the production method of the vacuum heat-insulating plate of improvement according to claim 1, it is characterized in that, described high resistant air film bag is made up of the overcoat in outside and the sealant compound of inner side, and sealing layer comprises aluminium foil, polyester film, nylon film, polyethylene film, polyvinyl chloride film, polystyrene film, polyvinylidene chloride, polyvinyl alcohol film, ethylene-vinyl acetate copolymer film, polyvinyl alcohol film, nylon film, ethylene/vinyl alcohol copolymer film, polycarbonate film, polyacrylic one or more are composited; The outermost protective layer of this high resistant air film bag by glass-fiber-fabric, non-woven fabrics, carbon-fiber cloth, basalt fiber cloth, ceramic fiber cloth one or more be composited.
9. the production method of the vacuum heat-insulating plate of improvement according to claim 1, it is characterized in that, edge sealing is provided with at the two ends of described high resistant air film bag, this edge sealing is located at the relative one side at the two ends of this high resistant air film bag, is provided with the occlusal crib coincide with this edge sealing at the another side relative with this edge sealing.
CN201210187115.7A 2012-06-08 2012-06-08 Improved production method for vacuum insulated panel Active CN102873739B (en)

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CN102873739B true CN102873739B (en) 2015-01-14

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Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103672300A (en) * 2013-11-07 2014-03-26 苏州市君悦新材料科技有限公司 Novel heat-insulating coldness-preserving material
CN104100012B (en) * 2014-08-04 2016-09-07 天津市建筑科学研究院有限公司 A kind of vacuum inorganic heat preservation Side fascia and preparation method thereof and exterior wall heat-preserving system
CN104631634B (en) * 2014-12-29 2017-07-11 中国科学院合肥物质科学研究院 A kind of powder core material vacuum heat-insulation board for building and preparation method thereof
CN106317700A (en) * 2016-08-30 2017-01-11 江苏爱富希新型建材股份有限公司 Silicon-plastic plate and manufacturing method thereof

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1057659A (en) * 1990-06-23 1992-01-08 龙昂 Composite heat insulatant thermal insulation material
EP1340728A1 (en) * 2000-11-10 2003-09-03 Mitsubishi Shoji Construction Materials Corporation Composition for building material and building material
JP3783734B2 (en) * 1995-05-30 2006-06-07 株式会社エーアンドエーマテリアル Calcium silicate plate manufacturing method
WO2007033836A1 (en) * 2005-09-23 2007-03-29 Va-Q-Tec Ag Method for the production of a vacuum insulation element wrapped in a film, filled with powder
CN101691899A (en) * 2009-10-01 2010-04-07 福建赛特新材料有限公司 Composite core material vacuum insulation panel and preparation method thereof
CN101734903A (en) * 2008-11-14 2010-06-16 中国电力科学研究院 Nano silica dioxide heat-insulating material and preparation method thereof
CN102173714A (en) * 2011-01-19 2011-09-07 河北辽原硅藻材料有限公司 Environment-friendly calcium silicate heat insulation product and preparation method thereof

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1057659A (en) * 1990-06-23 1992-01-08 龙昂 Composite heat insulatant thermal insulation material
JP3783734B2 (en) * 1995-05-30 2006-06-07 株式会社エーアンドエーマテリアル Calcium silicate plate manufacturing method
EP1340728A1 (en) * 2000-11-10 2003-09-03 Mitsubishi Shoji Construction Materials Corporation Composition for building material and building material
WO2007033836A1 (en) * 2005-09-23 2007-03-29 Va-Q-Tec Ag Method for the production of a vacuum insulation element wrapped in a film, filled with powder
CN101310137A (en) * 2005-09-23 2008-11-19 瓦克技术股份公司 Method for the production of a vacuum insulation element wrapped in a film, filled with powder
CN101734903A (en) * 2008-11-14 2010-06-16 中国电力科学研究院 Nano silica dioxide heat-insulating material and preparation method thereof
CN101691899A (en) * 2009-10-01 2010-04-07 福建赛特新材料有限公司 Composite core material vacuum insulation panel and preparation method thereof
CN102173714A (en) * 2011-01-19 2011-09-07 河北辽原硅藻材料有限公司 Environment-friendly calcium silicate heat insulation product and preparation method thereof

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Inventor after: He Yi

Inventor after: Hou Qinpeng

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Address after: 266112 Shandong City, Chengyang District, Qingdao, the streets of the streets of the Wangjiazhuang neighborhood of the community on the north side of the 500 meters

Patentee after: Qingdao Kerui new environmental protection materials Group Co. Ltd.

Address before: 266112 Shandong City, Chengyang District, Qingdao, the streets of the streets of the Wangjiazhuang neighborhood of the community on the north side of the 500 meters

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