CN102873739A - Improved production method for vacuum insulated panel - Google Patents

Improved production method for vacuum insulated panel Download PDF

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Publication number
CN102873739A
CN102873739A CN2012101871157A CN201210187115A CN102873739A CN 102873739 A CN102873739 A CN 102873739A CN 2012101871157 A CN2012101871157 A CN 2012101871157A CN 201210187115 A CN201210187115 A CN 201210187115A CN 102873739 A CN102873739 A CN 102873739A
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production method
film
insulating plate
vacuum heat
plate according
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CN2012101871157A
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CN102873739B (en
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翟传伟
李壮贤
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Qingdao Kerui new environmental protection materials Group Co. Ltd.
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Qingdao Creek New Environmental Materials Co Ltd
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Abstract

The invention relates to an improved production method for a vacuum insulated panel, which comprises the following technical steps: dosing: inputting pumice stones, diatomaceous earth, calcium silicate, aerosil, inorganic fiber and vacuum stabilizer in proportion to a mixer to be mixed adequately; drying: drying the mixed materials which are agitated uniformly; core forming: inputting the dried materials and a degasser into a mould, and placing the mould into a press to be pressurized for forming; wrapping: taking a press-formed core plate out of the mould and wrapping the core plate in non-woven fabric to obtain a vacuum insulated panel core plate for buildings; placing the core plate in a high gas resistant film bag and vacuumizing, wherein the vacuum degree is 0.02-20 Pa; and then sealing. The invention has the advantages that the strength of the insulated panel is increased by mixing fiber, pumice stones, diatomaceous earth, calcium silicate and aerosol, and the insulating performance is improved. The core has a lower coefficient of heat conductivity and is an inorganic material which is not easy to combust. The raw materials are low in cost, the cost of the raw materials is lowered, and the environmental pollution is reduced.

Description

The production method of improved vacuum heat-insulating plate
Technical field
The present invention relates to a kind of production method of improved vacuum heat-insulating plate, for the production of vacuum heat-insulating plate, this vacuum heat-insulating plate is as building or industrial heat preservation material.
Background technology
Existing vacuum heat-insulating plate is mainly by inner insulated core material with cover the high-gas resistance film outward and consist of, wherein insulated core material generally adopts conventional insulation material (such as foamed plastic), glass fibre or/and the materials such as aeroge are made, its shortcoming is that material cost is high, and energy consumption is high, not environmental protection.
Summary of the invention
The present invention aims to provide a kind of production method of improved vacuum heat-insulating plate, and the material cost that exists with the solution prior art is high, and energy consumption is high, the problem of not environmental protection.
Technical scheme of the present invention is: a kind of production method of improved vacuum heat-insulating plate, core is packed in the high resistant air film bag, vacuumize rear sealing, it is characterized in that, described core composition and parts by weight are: float stone 20-30, diatomite 10-15, calcium silicates 15-20, aerosil 10-15, inorfil 8-12, vacuum stabilizing agent 2-3;
Manufacture craft comprises the steps:
(1) batching: the material input mixer of described prescription is fully mixed;
(2) oven dry: the compound that stirs is dried, and bake out temperature is controlled at 100-120 ℃, until the moisture content of compound reaches below 0.5%, stops oven dry;
(3) non-woven fabric bag: nonwoven is made three banding sacks, or make three banding sacks with limb;
(4) core material can: the mixture of oven dry is dropped in the nonwoven sack of three bandings, and then the one side with opening seals;
(5) Bag Material shakeouts: the mixture integral body that will seal is shakeout:
(6) compressing: the packed mixture that will shakeout, put under the press together with the nonwoven sack of outside, carry out compression forming, obtain being incubated central layer;
(7) will be incubated central layer and insert in the high resistant air film bag and vacuumize, vacuum is 0.02-20Pa, then sealing.
The drying course of step (2) also can carry out in the process of step (1) simultaneously.
In the step (4), the filling speed of automatic filling machine be the 8-25 bag/minute, mixture is by measuring cup or Auger feeding and metering.
Used nonwoven is flame-retardant non-woven in step (3) and the step (6), and mass area ratio is 35-100g/m 2
In the step (5), the mixture that has sealed is by manually shakeouing, or flattens by roll shaft.
The decrease speed of press is controlled at 3-7 cm/s in the step (6), and pressure is controlled at 20-280T/m 2
Compressing technique is progressively suppressed continuously shaped by the belt that up and down several pair of rollers drive continuously in the step (6).
Described inorfil comprises more than one in rock wool, glass, lignin fibre and the glass-ceramic fibre, mixes with arbitrary proportion; Fibre length is 3-12mm, and diameter is the 0.2-13 micron.
Described high resistant air film bag is by the overcoat in the outside and inboard compound composition of sealant, and the sealing layer comprises that aluminium foil, polyester film, nylon film, polyethylene film, polyvinyl chloride film, polystyrene film, polyvinylidene chloride, polyvinyl alcohol film, ethylene-vinyl acetate copolymer film, polyvinyl alcohol film, nylon film, ethylene/vinyl alcohol copolymer film, polycarbonate film, polyacrylic one or more are composited; The outermost protective layer of this high resistant air film bag is composited by one or more of glass-fiber-fabric, nonwoven, carbon-fiber cloth, basalt fiber cloth, ceramic fiber cloth.
Two ends at described high resistant air film bag are provided with edge sealing, and this edge sealing is located at the relative one side at the two ends of this high resistant air film bag, are provided with the occlusal crib that coincide with this edge sealing at the another side relative with this edge sealing.
Advantage of the present invention is: fiber mixes the intensity that has increased warming plate with float stone, diatomite, calcium silicates and aerosil, and has improved heat-insulating property.The vacuum stabilizing agent has improved the durability that vacuum keeps.Core can reach lower thermal conductivity factor, is again inorganic material, and is nonflammable, can satisfy the needs of country's six or five energy conservation plans.Cost of material is cheap, guarantees certain low thermal conductivity, reduces cost of material; Reduced the pollution to environment.
Description of drawings
Fig. 1 is the side structure schematic diagram of one embodiment of the invention;
Fig. 2 is another embodiment of the present invention side structure schematic diagram;
Fig. 3 is the top view of Fig. 1;
Fig. 4 is the docking schematic diagram of the present invention when using.
The specific embodiment
The production method of a kind of improved vacuum heat-insulating plate of the present invention, core is packed in the high resistant air film bag, vacuumize rear sealing, it is characterized in that, described core composition and parts by weight are: float stone 20-30, diatomite 10-15, calcium silicates 15-20, aerosil 10-15, inorfil 8-12 and vacuum stabilizing agent 2-3;
Manufacture craft comprises the steps:
(1) batching: the material input mixer of described prescription is fully mixed;
(2) oven dry: the compound that stirs is dried, and bake out temperature is controlled at 100-120 ℃, until the moisture content of compound reaches below 0.5%, stops oven dry;
(3) non-woven fabric bag: nonwoven is made three banding sacks, or make three banding sacks with limb;
(4) core material can: drop in the nonwoven sack of three bandings with the mixture of automatic filling machine with oven dry, then the one side with opening seals.The filling speed of automatic filling machine be the 8-25 bag/minute, mixture is by measuring cup or Auger feeding and metering.
 
(5) Bag Material shakeouts: the mixture integral body that will seal is shakeout.The mixture that has sealed is by manually shakeouing, or flattens by roll shaft.
(6) compressing: the packed mixture that will shakeout, put under the press together with the nonwoven sack of outside, carry out compression forming, obtain being incubated central layer.The decrease speed of press is controlled at 3-7 cm/s, and pressure is controlled at 20-280T/m 2
Compressing technique also can be continuously shaped, and is progressively compressing continuously by the belt that up and down several pair of rollers drive.
(7) will be incubated central layer and insert in the high resistant air film bag and vacuumize, vacuum is 0.02-20Pa, then sealing.
The drying course of step (2) also can carry out in the process of step (1) simultaneously.
Used nonwoven is flame-retardant non-woven in step (3) and the step (6), and mass area ratio is 35-100g/m 2
Described vacuum active stabilizing agent is by active carbon, and one or more arbitrary proportion mixtures in barium lithium alloy activator, calcium oxide, magnesia and the silica gel consist of.
Described inorfil comprises a kind of in rock wool, glass, lignin fibre and the glass-ceramic fibre, or the two or more above-mentioned fiber that mixes with arbitrary proportion.Described fibre length is 3-12mm, and diameter is the 0.2-13 micron.
Described high resistant air film bag is by the overcoat in the outside and inboard compound composition of sealant.
Described sealant comprises that aluminium foil, polyester film, nylon film, polyethylene film, polyvinyl chloride film, polystyrene film, polyvinylidene chloride, polyvinyl alcohol film, ethylene-vinyl acetate copolymer film, polyvinyl alcohol film, nylon film, ethylene/vinyl alcohol copolymer film, polycarbonate film, polyacrylic one or more are composited.
The outermost protective layer of described high resistant air film bag is composited by one or more of glass-fiber-fabric, nonwoven, carbon-fiber cloth, basalt fiber cloth, ceramic fiber cloth.
Described high resistant air film bag also can adopt the material of any existing routine to make.Getter also is conventional material, adopts scattering device or adopts layer structure to be arranged on the surface of central layer.
Referring to Fig. 1-Fig. 4, the vacuum heat-insulating plate contour structures that the present invention makes can be conventional shape, is provided with sealing strip 3(referring to Fig. 1 at the two ends of high resistant air film bag 1).Also the sealing strip 3 at high resistant air film bag 1 two ends can be located at the relative one side at the two ends of this high resistant air film bag 1, be provided with the occlusal crib 4 that coincide with this edge sealing at the another side relative with sealing limit 3.Adjacent two warming plate A1 and A2 edge sealing 3 are placed in the other side's the occlusal crib 4 (as shown in Figure 4) in when construction, have reduced the heat bridge thickness between adjacent two warming plates, improved heat insulation effect and efficiency of construction.

Claims (10)

1. the production method of an improved vacuum heat-insulating plate, core is packed in the high resistant air film bag, vacuumize rear sealing, it is characterized in that, described core composition and parts by weight are: float stone 20-30, diatomite 10-15, calcium silicates 15-20, aerosil 10-15, inorfil 8-12, vacuum stabilizing agent 2-3;
Manufacture craft comprises the steps:
(1) batching: the material input mixer of described prescription is fully mixed;
(2) oven dry: the compound that stirs is dried, and bake out temperature is controlled at 100-120 ℃, until the moisture content of compound reaches below 0.5%, stops oven dry;
(3) non-woven fabric bag: nonwoven is made three banding sacks, or make three banding sacks with limb;
(4) core material can: the mixture of oven dry is dropped in the nonwoven sack of three bandings, and then the one side with opening seals;
(5) Bag Material shakeouts: the mixture integral body that will seal is shakeout:
(6) compressing: the packed mixture that will shakeout, put under the press together with the nonwoven sack of outside, carry out compression forming, obtain being incubated central layer;
(7) will be incubated central layer and insert in the high resistant air film bag and vacuumize, vacuum is 0.02-20Pa, then sealing.
2. the production method of improved vacuum heat-insulating plate according to claim 1, it is characterized in that: the drying course of step (2) also can carry out in the process of step (1) simultaneously.
3. the production method of improved vacuum heat-insulating plate according to claim 1 is characterized in that: in the step (4), the filling speed of automatic filling machine be the 8-25 bag/minute, mixture is by measuring cup or Auger feeding and metering.
4. the production method of improved vacuum heat-insulating plate according to claim 1, it is characterized in that: used nonwoven is flame-retardant non-woven in step (3) and the step (6), and mass area ratio is 35-100g/m 2
5. the production method of improved vacuum heat-insulating plate according to claim 1 is characterized in that: in the step (5), the mixture that has sealed is by manually shakeouing, or flattens by roll shaft.
6. the production method of improved vacuum heat-insulating plate according to claim 1 is characterized in that: the decrease speed of press is controlled at 3-7 cm/s in the step (6), and pressure is controlled at 20-280T/m 2
7. the production method of improved vacuum heat-insulating plate according to claim 1 is characterized in that: compressing technique is progressively suppressed continuously shaped by the belt that up and down several pair of rollers drive continuously in the step (6).
8. the production method of improved vacuum heat-insulating plate according to claim 1 is characterized in that, described inorfil comprises more than one in rock wool, glass, lignin fibre and the glass-ceramic fibre, mixes with arbitrary proportion; Fibre length is 3-12mm, and diameter is the 0.2-13 micron.
9. the production method of improved vacuum heat-insulating plate according to claim 1, it is characterized in that, described high resistant air film bag is by the overcoat in the outside and inboard compound composition of sealant, and the sealing layer comprises that aluminium foil, polyester film, nylon film, polyethylene film, polyvinyl chloride film, polystyrene film, polyvinylidene chloride, polyvinyl alcohol film, ethylene-vinyl acetate copolymer film, polyvinyl alcohol film, nylon film, ethylene/vinyl alcohol copolymer film, polycarbonate film, polyacrylic one or more are composited; The outermost protective layer of this high resistant air film bag is composited by one or more of glass-fiber-fabric, nonwoven, carbon-fiber cloth, basalt fiber cloth, ceramic fiber cloth.
10. the production method of improved vacuum heat-insulating plate according to claim 1, it is characterized in that, two ends at described high resistant air film bag are provided with edge sealing, this edge sealing is located at the relative one side at the two ends of this high resistant air film bag, is provided with the occlusal crib that coincide with this edge sealing at the another side relative with this edge sealing.
CN201210187115.7A 2012-06-08 2012-06-08 Improved production method for vacuum insulated panel Active CN102873739B (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103672300A (en) * 2013-11-07 2014-03-26 苏州市君悦新材料科技有限公司 Novel heat-insulating coldness-preserving material
CN104100012A (en) * 2014-08-04 2014-10-15 天津市建筑科学研究院有限公司 Vacuum inorganic insulation outer external wall board, manufacturing method thereof and external wall insulation system
CN104631634A (en) * 2014-12-29 2015-05-20 中国科学院合肥物质科学研究院 Powder core vacuum insulation panel for building and preparing method thereof
CN106317700A (en) * 2016-08-30 2017-01-11 江苏爱富希新型建材股份有限公司 Silicon-plastic plate and manufacturing method thereof

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1057659A (en) * 1990-06-23 1992-01-08 龙昂 Composite heat insulatant thermal insulation material
EP1340728A1 (en) * 2000-11-10 2003-09-03 Mitsubishi Shoji Construction Materials Corporation Composition for building material and building material
JP3783734B2 (en) * 1995-05-30 2006-06-07 株式会社エーアンドエーマテリアル Calcium silicate plate manufacturing method
WO2007033836A1 (en) * 2005-09-23 2007-03-29 Va-Q-Tec Ag Method for the production of a vacuum insulation element wrapped in a film, filled with powder
CN101691899A (en) * 2009-10-01 2010-04-07 福建赛特新材料有限公司 Composite core material vacuum insulation panel and preparation method thereof
CN101734903A (en) * 2008-11-14 2010-06-16 中国电力科学研究院 Nano silica dioxide heat-insulating material and preparation method thereof
CN102173714A (en) * 2011-01-19 2011-09-07 河北辽原硅藻材料有限公司 Environment-friendly calcium silicate heat insulation product and preparation method thereof

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1057659A (en) * 1990-06-23 1992-01-08 龙昂 Composite heat insulatant thermal insulation material
JP3783734B2 (en) * 1995-05-30 2006-06-07 株式会社エーアンドエーマテリアル Calcium silicate plate manufacturing method
EP1340728A1 (en) * 2000-11-10 2003-09-03 Mitsubishi Shoji Construction Materials Corporation Composition for building material and building material
WO2007033836A1 (en) * 2005-09-23 2007-03-29 Va-Q-Tec Ag Method for the production of a vacuum insulation element wrapped in a film, filled with powder
CN101310137A (en) * 2005-09-23 2008-11-19 瓦克技术股份公司 Method for the production of a vacuum insulation element wrapped in a film, filled with powder
CN101734903A (en) * 2008-11-14 2010-06-16 中国电力科学研究院 Nano silica dioxide heat-insulating material and preparation method thereof
CN101691899A (en) * 2009-10-01 2010-04-07 福建赛特新材料有限公司 Composite core material vacuum insulation panel and preparation method thereof
CN102173714A (en) * 2011-01-19 2011-09-07 河北辽原硅藻材料有限公司 Environment-friendly calcium silicate heat insulation product and preparation method thereof

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103672300A (en) * 2013-11-07 2014-03-26 苏州市君悦新材料科技有限公司 Novel heat-insulating coldness-preserving material
CN104100012A (en) * 2014-08-04 2014-10-15 天津市建筑科学研究院有限公司 Vacuum inorganic insulation outer external wall board, manufacturing method thereof and external wall insulation system
CN104100012B (en) * 2014-08-04 2016-09-07 天津市建筑科学研究院有限公司 A kind of vacuum inorganic heat preservation Side fascia and preparation method thereof and exterior wall heat-preserving system
CN104631634A (en) * 2014-12-29 2015-05-20 中国科学院合肥物质科学研究院 Powder core vacuum insulation panel for building and preparing method thereof
CN104631634B (en) * 2014-12-29 2017-07-11 中国科学院合肥物质科学研究院 A kind of powder core material vacuum heat-insulation board for building and preparation method thereof
CN106317700A (en) * 2016-08-30 2017-01-11 江苏爱富希新型建材股份有限公司 Silicon-plastic plate and manufacturing method thereof

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