CN102864175A - High-efficiency liquid-state alcohol preparation method by wild straw leaves - Google Patents
High-efficiency liquid-state alcohol preparation method by wild straw leaves Download PDFInfo
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- CN102864175A CN102864175A CN2012103736696A CN201210373669A CN102864175A CN 102864175 A CN102864175 A CN 102864175A CN 2012103736696 A CN2012103736696 A CN 2012103736696A CN 201210373669 A CN201210373669 A CN 201210373669A CN 102864175 A CN102864175 A CN 102864175A
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Abstract
The invention relates to a high-efficiency liquid-state alcohol preparation method by wild straw leaves and relates to a novel alcohol preparation technology. The high-efficiency liquid-state alcohol preparation method includes configuring equipment, finely preparing and fermenting, distilling efficiently, converting and packaging, specifically, firstly weighing green Chinese silvergrass, dried Chinese silvergrass, weeds and stem leaves according to the proportion of 4-3:2-3:2-1 and 3-2:2-1:2-3 respectively, then weighing the green raw materials, lime and purified water according to the proportion of 6-5:2-1:5-4 and disposing into a tank to soak for 13-15 days so that crude fibers of the dried raw materials are softened, weighing the dried raw materials, the lime and the purified water according to the proportion of 5-4:3-2:6-5, and disposing to the tank to soak for 16-18 days so that crude fibers of the dried raw materials are softened; and then filtering and washing the green raw materials and the dried raw materials to smash into raw material pulp, weighing the raw material pulp, alcohol yeast and purified water according to the proportion of 7-6:4-3:8-7 to feed into a fermenting tank to ferment for 15-17 days, pumping mash into distilling equipment when the color of the mash turns into brown black, heating and distilling to obtain alcohol.
Description
Technical field
The present invention relates to a kind of ethanol method for making, particularly the liquid efficient system alcohol of a kind of wild stalk leaf.
Background technology
The world today, the energy has become Major Strategic resource and the decision-making foundation of various countries' the economic and political development and competition, and combustion can become more important in Energy resources, very finite sum is easily exhausted but as reserves such as the Main Resources coal that fires energy, oil, Sweet natural gases, and the large and destructible ecotope of exploitation use cost, thereby the further strong and resource of research and utilization regenerative power stalk leaf waste resources such as wild plant Chinese silvergrass, weeds, cauline leaf widely, through retrofit fermented soy ethanol with develop new forms of energy and seem particularly important and urgent.
Summary of the invention
The objective of the invention is for the brewage shortage of wild stalk leaf liquid ethanol and energy development problem, provide that a kind of complex art is leading, the batching fermentation is simplified, practical strong easily popularizations, wild stalk leaf raw material processed, refinement liquid state fermentation, quickness and high efficiency distillation, high yield and high quality are energy-conservation, the pure combustion value height of ethanol, green safety environmental protection, overall economic efficiency and social benefit be the new technology of the efficient brew ethanol of the wild plant stalk folic acid fining-off liquid state fermentation energy particularly significantly.
The technical scheme that the present invention adopts for achieving the above object is: the liquid efficient system alcohol of a kind of wild stalk leaf, it is characterized in that, this ethanol brew method mainly is natural disposition or dryness wild plant stalk leaf to be carried out separately first or co-grinding is refined into pulpous state or powdery raw material, again according to pulpous state raw material and powdery raw material moisture content with when conditions such as ground temperatures, add in proportion the bent and water purification of plant raw material liquid fermentation alcohol and rapidly and efficiently ferment, drop into again behind the wine with dregs material fermenting-ripening and distill also appropriateness in the block high-efficiency energy-saving wine steaming equipment and blend production ethanol.
Described wild plant stalk leaf comprises natural disposition and dryness Chinese silvergrass, weeds, cauline leaf.
Blending process: 1, equipment configuration: the large-scale wild plant stalk leaf of having purchased stacks place or warehouse and ventilating and thermal insulating fermenting house and fermentor tank or pond, weighing apparatus, pulping engine, stirrer, take out pump machine, strainer, filling machine, ethanol gyrograph and special use accumulates the settings such as tank.2, the smart ferment of allotting: first by collected natural disposition and dryness Chinese silvergrass, weeds, the moisture content of cauline leaf wild plant, take 10 as basic rate, respectively by the natural disposition Chinese silvergrass, weeds, the cauline leaf ratio is 4-3: 2-3: the 2-1 weighing, and by natural disposition raw material and lime, the water purification ratio is 6-5: 2-1: the 5-4 weighing, and it is softening to place the pond to soak 13-15 angel dryness raw material robust fibre, by the dryness Chinese silvergrass, weeds, the cauline leaf ratio is 3-2: 2-1: the 2-3 weighing, and by dryness raw material and lime, the water purification ratio is 5-4: 3-2: the 6-5 weighing, and it is softening to place the pond to soak 16-18 angel dryness raw material robust fibre.Use subsequently strainer and water purification respectively that natural disposition and dryness raw material filtration and washing is clean, drop into again and carry out dispersion and fining in the pulping engine and become the pulpous state raw material, and, water purification ratio bent with alcohol in diploma raw material is 7-6: 4-3: the 8-7 weighing dropped in fermentor tank or the pond fermentation 15-17 days, per 3 days during this time with stirrer or hand mixing 1 time, fermenting-ripening when treating that the wine with dregs material all precipitates mash and becomes not good merchantable.Experiment showed, that slurry raw material sugar content is higher and fermentation is faster, and ethanol production is higher.3, efficiently distill: the wine with dregs material of fermenting-ripening is used to take out the pump machine or manually drop into seal, heat and distill in the high energy-efficient distillation plant of monomer of performance, and by high heating value distillation in early stage, in the distillation of interim calorific value homogeneous heating, the later stage basic heating principle of high heating value distillation is distilled ethanol, stops distillation when ethanol tail degree is lower than 10 °.Front middle and later periods distillation gained ethanol is mixed and measure the ethanol number of degrees with the ethanol gyrograph, be lower than 90 ° of the required number of degrees such as the gained ethanol number of degrees and can carry out again 1-2 time and distill, can obtain required ethanol.Last wort sludge is discharged from distillation plant with mash and separate with filters, the gained wort sludge can be made making sheet raw material and feed ingredient or make biogas etc., the mash that contains low ethanol can be used as again to ferment (fermentation rate and output can be higher).4, add encapsulation: take 10 as basic rate, with gained more than 90 ° ethanol use it for anything else and be 8-6: 2-3: 2-1 in ethanol and fuel oil and ignition dope, rare gas element ratio: 1-0.8 weighing and adding mixes, can obtain high value efficiently and the alcohol fuel of safety energy-conserving environment protection, the alcohol fuel that will add again pours into to seal up for safekeeping in the jar special with filling machine and can carry and utilize.
Press the 1-4 repeatable operation, can realize the purpose of high-efficiency high-quality production wild plant ethanol.
Beneficial effect: the present invention takes the complex art theory, for existing wild plant ethanol brew shortage and energy demand and development problem, and through many experiments, to have various regeneration wild plants now and make the Energy production raw material, and namely utilize the processing of the stalk folic acids such as Chinese silvergrass, weeds, cauline leaf to carry out the ferment new technology of the efficient brew ethanol energy of raw material liquid.Therefore, complex art of the present invention is leading, the batching fermentation is simplified, practical strong easily popularizations, wild stalk leaf raw material processed, refinement liquid state fermentation, quickness and high efficiency are distilled, high yield and high quality is energy-conservation, the pure combustion value height of ethanol, green safety environmental protection, and it promotes the use of great economic benefit and energy development strategic importance.
Embodiment 1: first by collected natural disposition and dryness Chinese silvergrass, weeds, the moisture content of cauline leaf wild plant, take 10 as basic rate, respectively by the natural disposition Chinese silvergrass, weeds, the cauline leaf ratio is 4: 2: 2 weighing Chinese silvergrass 40kg, weeds 20kg, cauline leaf 20kg, and by natural disposition raw material and lime, the water purification ratio is 6: 2: 5 weighing raw material 60kg, lime 20kg, water purification 50kg, and it is softening to place the pond to soak 13 angel's dryness raw material robust fibre, by the dryness Chinese silvergrass, weeds, the cauline leaf ratio is 3: 2: 2 weighing Chinese silvergrass 30kg, weeds 20kg, cauline leaf 20kg, and by dryness raw material and lime, the water purification ratio is 5: 3: 6 weighing raw material 50kg, lime 30kg, water purification 60kg, and it is softening to place the pond to soak 16 angel's dryness raw material robust fibre.Use subsequently strainer and water purification respectively that natural disposition and dryness raw material filtration and washing is clean, drop into again and carry out dispersion and fining in the pulping engine and become the pulpous state raw material, and, water purification ratio bent with alcohol in diploma raw material is about 30 ° of 100: 1: 280 weighing raw material 100kg, pure bent 1kg(temperature), water purification 280kg dropped in fermentor tank or the pond fermentation 15 days, per 3 days during this time with stirrer or hand mixing 1 time, fermenting-ripening when treating that the wine with dregs material all precipitates mash and becomes not good merchantable.With the wine with dregs material of fermenting-ripening with taking out pump machine or artificial the input in the high energy-efficient distillation plant of monomer of sealing, heating and distillation performance, and by high heating value distillation in early stage, in the distillation of interim calorific value homogeneous heating, the later stage basic heating principle of high heating value distillation is distilled ethanol, stops distillation when ethanol tail degree is lower than 10 °.Front middle and later periods distillation gained ethanol is mixed and measure the ethanol number of degrees with the ethanol gyrograph, be lower than 90 ° of the required number of degrees such as the gained ethanol number of degrees and can carry out again 1-2 time and distill, can obtain required ethanol.Last wort sludge is discharged from distillation plant with mash and separate with filters, the gained wort sludge can be made making sheet raw material and feed ingredient or make biogas etc., the mash that contains low ethanol can be used as again to ferment (fermentation rate and output can be higher).Take 10 as basic rate, with gained more than 90 ° ethanol: 1 weighing ethanol 80kg, fuel oil 20kg, ignition dope 20kg, the rare gas element 10kg and adding that use it for anything else and be 8: 2: 2 in ethanol and fuel oil and ignition dope, rare gas element ratio mix, can obtain high value efficiently and the alcohol fuel of safety energy-conserving environment protection, the alcohol fuel that will add again pours into to seal up for safekeeping in the jar special with filling machine and can carry and utilize.
Embodiment 2: first by collected natural disposition and dryness Chinese silvergrass, weeds, the moisture content of cauline leaf wild plant, take 10 as basic rate, respectively by the natural disposition Chinese silvergrass, weeds, the cauline leaf ratio is 3.5: 2.5: 1.5 weighing Chinese silvergrass 35kg, weeds 25kg, cauline leaf 15kg, and by natural disposition raw material and lime, the water purification ratio is 5.5: 1.5: 4.5 weighing raw material 55kg, lime 15kg, water purification 45kg, and it is softening to place the pond to soak 14 angel's dryness raw material robust fibre, by the dryness Chinese silvergrass, weeds, the cauline leaf ratio is 2.5: 1.5: 2.5 weighing Chinese silvergrass 25kg, weeds 15kg, cauline leaf 25kg, and by dryness raw material and lime, the water purification ratio is 4.5: 2.5: 5.5 weighing raw material 45kg, lime 25kg, water purification 55kg, and it is softening to place the pond to soak 17 angel's dryness raw material robust fibre.Use subsequently strainer and water purification respectively that natural disposition and dryness raw material filtration and washing is clean, drop into again and carry out dispersion and fining in the pulping engine and become the pulpous state raw material, and, water purification ratio bent with alcohol in diploma raw material is about 20 ° of 100: 1.5: 270 weighing raw material 100kg, pure bent 1.5kg(temperature), water purification 270kg dropped in fermentor tank or the pond fermentation 16 days, per 3 days during this time with stirrer or hand mixing 1 time, fermenting-ripening when treating that the wine with dregs material all precipitates mash and becomes not good merchantable.With the wine with dregs material of fermenting-ripening with taking out pump machine or artificial the input in the high energy-efficient distillation plant of monomer of sealing, heating and distillation performance, and by high heating value distillation in early stage, in the distillation of interim calorific value homogeneous heating, the later stage basic heating principle of high heating value distillation is distilled ethanol, stops distillation when ethanol tail degree is lower than 10 °.Front middle and later periods distillation gained ethanol is mixed and measure the ethanol number of degrees with the ethanol gyrograph, be lower than 90 ° of the required number of degrees such as the gained ethanol number of degrees and can carry out again 1-2 time and distill, can obtain required ethanol.Last wort sludge is discharged from distillation plant with mash and separate with filters, the gained wort sludge can be made making sheet raw material and feed ingredient or make biogas etc., the mash that contains low ethanol can be used as again to ferment (fermentation rate and output can be higher).Take 10 as basic rate, with gained more than 90 ° ethanol: 0.9 weighing ethanol 70kg, fuel oil 25kg, ignition dope 15kg, the rare gas element 9kg and adding that use it for anything else and be 7: 2.5: 1.5 in ethanol and fuel oil and ignition dope, rare gas element ratio mix, can obtain high value efficiently and the alcohol fuel of safety energy-conserving environment protection, the alcohol fuel that will add again pours into to seal up for safekeeping in the jar special with filling machine and can carry and utilize.
Embodiment 3: first by collected natural disposition and dryness Chinese silvergrass, weeds, the moisture content of cauline leaf wild plant, take 10 as basic rate, respectively by the natural disposition Chinese silvergrass, weeds, the cauline leaf ratio is 3: 3: 1 weighing Chinese silvergrass 30kg, weeds 30kg, cauline leaf 10kg, and by natural disposition raw material and lime, the water purification ratio is 5: 1: 4 weighing raw material 50kg, lime 10kg, water purification 40kg, and it is softening to place the pond to soak 15 angel's dryness raw material robust fibre, by the dryness Chinese silvergrass, weeds, the cauline leaf ratio is 2: 1: 3 weighing Chinese silvergrass 20kg, weeds 10kg, cauline leaf 30kg, and by dryness raw material and lime, the water purification ratio is 4: 2: 5 weighing raw material 40kg, lime 20kg, water purification 50kg, and it is softening to place the pond to soak 18 angel's dryness raw material robust fibre.Use subsequently strainer and water purification respectively that natural disposition and dryness raw material filtration and washing is clean, drop into again and carry out dispersion and fining in the pulping engine and become the pulpous state raw material, and, water purification ratio bent with alcohol in diploma raw material is about 10 ° of 100: 2: 260 weighing raw material 100kg, pure bent 2kg(temperature), water purification 260kg dropped in fermentor tank or the pond fermentation 17 days, per 3 days during this time with stirrer or hand mixing 1 time, fermenting-ripening when treating that the wine with dregs material all precipitates mash and becomes not good merchantable.With the wine with dregs material of fermenting-ripening with taking out pump machine or artificial the input in the high energy-efficient distillation plant of monomer of sealing, heating and distillation performance, and by high heating value distillation in early stage, in the distillation of interim calorific value homogeneous heating, the later stage basic heating principle of high heating value distillation is distilled ethanol, stops distillation when ethanol tail degree is lower than 10 °.Front middle and later periods distillation gained ethanol is mixed and measure the ethanol number of degrees with the ethanol gyrograph, be lower than 90 ° of the required number of degrees such as the gained ethanol number of degrees and can carry out again 1-2 time and distill, can obtain required ethanol.Last wort sludge is discharged from distillation plant with mash and separate with filters, the gained wort sludge can be made making sheet raw material and feed ingredient or make biogas etc., the mash that contains low ethanol can be used as again to ferment (fermentation rate and output can be higher).Take 10 as basic rate, with gained more than 90 ° ethanol: 0.8 weighing ethanol 60kg, fuel oil 30kg, ignition dope 10kg, the rare gas element 8kg and adding that use it for anything else and be 6: 3: 1 in ethanol and fuel oil and ignition dope, rare gas element ratio mix, can obtain high value efficiently and the alcohol fuel of safety energy-conserving environment protection, the alcohol fuel that will add again pours into to seal up for safekeeping in the jar special with filling machine and can carry and utilize.
Claims (8)
1. the liquid efficient system of wild stalk leaf is pure, it is characterized in that, liquid efficient alcohol processed of described wild stalk leaf mainly be purchased first the large-scale stacking of wild plant stalk leaf place or warehouse and ventilating and thermal insulating fermenting house and fermentor tank or pond, weighing apparatus, pulping engine, stirrer, take out pump machine, strainer, filling machine, ethanol gyrograph and special use and accumulate the settings such as tank.
2. again by collected natural disposition and dryness Chinese silvergrass, weeds, the moisture content of cauline leaf wild plant, take 10 as basic rate, respectively by the natural disposition Chinese silvergrass, weeds, the cauline leaf ratio is 4-3: 2-3: the 2-1 weighing, and by natural disposition raw material and lime, the water purification ratio is 6-5: 2-1: the 5-4 weighing also places pond immersion 13-15 angel dryness raw material robust fibre softening, by the dryness Chinese silvergrass, weeds, the cauline leaf ratio is 3-2: 2-1: the 2-3 weighing, and by dryness raw material and lime, the water purification ratio is 5-4: 3-2: the 6-5 weighing, and it is softening to place the pond to soak 16-18 angel dryness raw material robust fibre.
3. use subsequently strainer and water purification respectively that natural disposition and dryness raw material filtration and washing is clean, drop into again and carry out dispersion and fining in the pulping engine and become the pulpous state raw material, and, water purification ratio bent with alcohol in diploma raw material is 7-6: 4-3: the 8-7 weighing dropped in fermentor tank or the pond fermentation 15-17 days, per 3 days during this time with stirrer or hand mixing 1 time, fermenting-ripening when treating that the wine with dregs material all precipitates mash and becomes not good merchantable.
4. the wine with dregs material of fermenting-ripening is used and taken out pump machine or artificial input sealing, heat and distill in the high energy-efficient distillation plant of monomer of performance, and by high heating value distillation in early stage, in the distillation of interim calorific value homogeneous heating, the later stage basic heating principle of high heating value distillation is distilled ethanol, stops distillation when ethanol tail degree is lower than 10 °.
5. front middle and later periods distillation gained ethanol is mixed and measure the ethanol number of degrees with the ethanol gyrograph, be lower than 90 ° of the required number of degrees such as the gained ethanol number of degrees and can carry out again 1-2 time and distill, can obtain required ethanol.
6. last wort sludge is discharged from distillation plant with mash and separate with filters, the gained wort sludge can be made making sheet raw material and feed ingredient or make biogas etc., the mash that contains low ethanol can be used as again to ferment (fermentation rate and output can be higher).
7. take 10 as basic rate, with gained more than 90 ° ethanol use it for anything else and be 8-6: 2-3: 2-1 in ethanol and fuel oil and ignition dope, rare gas element ratio: 1-0.8 weighing and adding mixes, can obtain high value efficiently and the alcohol fuel of safety energy-conserving environment protection, the alcohol fuel that will add again pours into to seal up for safekeeping in the jar special with filling machine and can carry and utilize.
8. the liquid efficient system alcohol of wild stalk leaf as claimed in claim 1 is characterized in that, described wild plant stalk leaf comprises natural disposition and dryness Chinese silvergrass, weeds, cauline leaf.
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CN104531776A (en) * | 2014-12-12 | 2015-04-22 | 柳州市京阳节能科技研发有限公司 | Efficient optimized alcohol-preparing technology by wild grass raw material |
CN104593111A (en) * | 2014-12-12 | 2015-05-06 | 柳州市京阳节能科技研发有限公司 | Technology for optimization of efficient fuel energy preparation by bamboo wood sawdust |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN104531776A (en) * | 2014-12-12 | 2015-04-22 | 柳州市京阳节能科技研发有限公司 | Efficient optimized alcohol-preparing technology by wild grass raw material |
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Application publication date: 20130109 |