CN102861203B - Method for preparing medicines for treating cervical vertebra pain - Google Patents
Method for preparing medicines for treating cervical vertebra pain Download PDFInfo
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- CN102861203B CN102861203B CN201210281985.0A CN201210281985A CN102861203B CN 102861203 B CN102861203 B CN 102861203B CN 201210281985 A CN201210281985 A CN 201210281985A CN 102861203 B CN102861203 B CN 102861203B
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Abstract
The invention discloses a method for preparing medicines for treating cervical vertebra pain. The method comprises the following steps of: injecting water into the last batch of medicinal dregs which are left during the preparation of jingtongling medicinal liquor, and soaking fully to obtain a soak solution; and adding the soak solution into the next batch of medicinal materials for preparing the jingtongling medicinal liquor to be used circularly. By the method, the concentration and alcohol content of the current batch of medicinal liquor which is extracted by a new preparation process are increased substantially, the alcohol precipitation effect is improved, and the quality of the products is improved; when supernate is extracted to be centrifuged, the loss of liquid medicine is reduced greatly; and the problem of poor precipitation effect during the stilling of the liquid medicine is solved basically by innovating an extraction process, and the quality and yield of the products are improved under the condition of no increase of cost.
Description
Technical field
The present invention relates to field of medicaments, relate in particular to a kind of method of preparing treatment cervical vertebra ache medicine.
Background technology
Cervical spondylosis is very common in life, and former cervical spondylosis is old people's multiple disease, has brought very large harm to old people's health, and the trend linearly rising.But now cervical spondylosis is in rejuvenation progressively, along with social development, the change of life style, more many youngsters have been suffered from cervical spondylosis.Wherein in the majority with the word worker of office, such as editor, teacher, civilian etc.Simultaneously increasing driver has also suffered from cervical spondylosis, has even reached the more than 1/5th of Patients with Cervical Spondylopathy.
Treat now 6 therapies such as the common water skill of handling needles of cervical spondylosis, acupuncture with heated needle, Qiang Tongfa, wine therapy, dissolution, reflection point method, the medicated wine therapy of wherein treating cervical spondylosis is the most common, and it not only can treat cervical spondylosis, also has the effect of health care, building body.
The extraction of medicated wine, adds medical material a certain proportion of wine and water through high-temperature boiling conventionally, the immersion of certain hour, then be filtered extraction.After the medicated wine of this explained hereafter exists extracting solution precipitate with ethanol, separating liquid medicine effect is bad, contains alcohol amount problem on the low side in extracting solution.Because medicinal liquid does not have separator well, bottom residue is larger, when extraction supernatant is centrifugal, can cause the problem of very large loss, and effective ingredient all leaching can cause making soak time to extend, post processing expense is high, increase its manufacturing cost, increase the precipitate with ethanol time, also affected the drug effect for the treatment of cervical spondylosis medicated wine.
Therefore, prior art needs further improve and develop.
Summary of the invention
In view of above-mentioned the deficiencies in the prior art, the object of the present invention is to provide a kind of method of preparing treatment cervical vertebra ache medicine, to improve the alcohol amount that contains of medicated wine, shorten the precipitate with ethanol time.
Technical scheme of the present invention is as follows:
A method of preparing treatment cervical vertebra ache medicine, it comprises the following steps:
A, to last consignment of, prepare in the remaining medicinal residues of JINGTONGLING medicated wine injected water and fully soak and obtain soak, described soak is joined to next group and prepare the medical material internal recycle of JINGTONGLING medicated wine and use.
Described method, wherein, what described steps A was concrete comprises:
A1, Radix Rehmanniae Preparata, Rhizoma Gastrodiae, Myrrha, Rhizoma Homalomenae, Olibanum, Radix Polygoni Multiflori Preparata, Pachyrhizua angulatus, Ramulus Cinnamomi, Cortex Illicii, Rhizoma Dioscoreae, Semen Sesami Nigrum, Periostracum Serpentis, the Radix Astragali, Herba Visci, Radix Angelicae Sinensis, Rhizoma Cibotii, Radix Achyranthis Bidentatae, Fructus Lycii, Radix Ginseng, Radix Salviae Miltiorrhizae, Fructus Chaenomelis, Radix Glycyrrhizae, Radix Clematidis, Cornu Cervi Pantotrichum, the Radix Paeoniae Alba and Rhizoma Drynariae are put in alcohol extraction tank, then in alcohol extraction tank, inject yellow wine and water, boil a period of time, then remain under the condition of 35-60 ℃ fully warm macerating, after wine extracts, filter;
A2, to adding in filtrate crystal sugar to melt, be blended into Chinese liquor, then fully stir, filter, airtight, static 5-30 days, is then blended into Moschus, filters and obtains described medicinal residues, to injected water in described medicinal residues, fully soaks and obtains described soak.
Described method, wherein, concrete the comprising of described steps A 2:
A21, replace water to put into next group described soak preparing in the medical material of JINGTONGLING medicated wine, soak the medical material of preparation JINGTONGLING medicated wine.
Described method, wherein, the weight ratio of described medicinal residues and water is 1:2-1:6, under 20-40 ℃ of conditions, described medicinal residues is soaked 20 minutes-300 minutes.
Described method, wherein, described steps A 2 also comprises: in filtrate, add crystal sugar to melt, be blended into Chinese liquor, fully stir 20 minutes-90 minutes.
Described method, wherein, described steps A 1 also comprises: in described alcohol extraction tank, the weight ratio of medical material and described yellow wine is 1:100-1:300; Described steps A 2 also comprises: the weight ratio of described Chinese liquor and described yellow wine is 1:0.5-1:5.
Described method, wherein, also comprises in described steps A: get Myrrha and Olibanum is removed impurity, broken section becomes the fritter of 0.8-1.2cm to put in pot, with slow fire, fries and slightly melts to surface, and taking out dries in the air after cool is joined in steps A 1.
The invention provides a kind of method of preparing treatment cervical vertebra ache medicine, because added the medicinal liquid of active substance in batch medicinal residues in the preparation technology for the treatment of cervical spondylosis, so that the concentration of this batch of medicinal liquid that new preparation process extracts and significantly increasing containing alcohol amount, not only improve the effect of precipitate with ethanol, also improved product quality; Extracting supernatant when centrifugal, greatly reduced medicinal liquid loss, the bad problem of sedimentation effect when the innovation reform of extraction process has been solved to medicinal liquid is static has substantially improved quality and the yield rate of product in the situation that not increasing cost.
Accompanying drawing explanation
Fig. 1 prepares the schematic flow sheet of JINGTONGLING medicated wine in the present invention.
The specific embodiment
The invention provides a kind of method of preparing treatment cervical vertebra ache medicine, for making object of the present invention, technical scheme and effect clearer, clear and definite, below the present invention is described in more detail.Should be appreciated that specific embodiment described herein, only in order to explain the present invention, is not intended to limit the present invention.
The invention provides a kind of method of preparing treatment cervical vertebra ache medicine, in the technique of existing preparation JINGTONGLING medicated wine, increase by one and again beat liquid step, what it was concrete comprises: to last consignment of, prepare in the remaining medicinal residues of JINGTONGLING medicated wine injected water and fully soak and obtain soak, described soak is joined to the medical material internal recycle use that next group is prepared JINGTONGLING medicated wine, improved the utilization rate of medical material.In the process of preparation JINGTONGLING medicated wine, prior art all adopts clear water to soak corresponding medical material, and its efficiency is lower, need to soak for a long time, just can make medical material effective ingredient infiltrate in clear water.And the present invention is by after the medicinal residues immersion of last consignment of, effective ingredient in medicinal residues can be re-used, and the soak of medicinal residues can infiltrate in medical material very soon, the active ingredient that makes medical material of prestissimo penetrates in soak, increased substantially dissolubility, the effect that has improved precipitate with ethanol, has improved product quality; And the present invention, extracting supernatant when centrifugal, has greatly reduced medicinal liquid loss, the bad problem of sedimentation effect when the innovation reform of extraction process has been solved to medicinal liquid is static has substantially improved quality and the yield rate of product in the situation that not increasing cost.
In another preferred embodiment of the present invention, as shown in Figure 1, it specifically comprises the following steps:
Step 101: Radix Rehmanniae Preparata, Olibanum, Myrrha, Radix Polygoni Multiflori Preparata, Pachyrhizua angulatus, Ramulus Cinnamomi, Cortex Illicii, Rhizoma Dioscoreae, Semen Sesami Nigrum, Periostracum Serpentis, Herba Visci, Radix Angelicae Sinensis, Rhizoma Cibotii, Radix Achyranthis Bidentatae, Fructus Lycii, Radix Ginseng, Radix Salviae Miltiorrhizae, Fructus Chaenomelis, Radix Glycyrrhizae, Cornu Cervi Pantotrichum, the Radix Paeoniae Alba and Rhizoma Drynariae are put in extraction pot, then in extraction pot, inject yellow wine and water, boil a period of time, then remain under the condition of 35-60 ℃ fully warm macerating, after wine extracts, filter;
Step 102: add crystal sugar to melt in filtrate, be blended into Chinese liquor, then fully stir, filter, airtight, static 5-30 days, then be blended into Moschus, filtration obtains described medicinal residues, to injected water in described medicinal residues, fully soak and obtain described soak, then by described soak for soaking the medical material that next group is prepared JINGTONGLING medicated wine.
In step 101 and step 102 each medicine according to weight portion concrete be: Radix Rehmanniae Preparata 2-4, Rhizoma Gastrodiae 1-6, Myrrha 4-8, Rhizoma Homalomenae 5-7, Olibanum 3-8, Radix Polygoni Multiflori Preparata 3-9, Pachyrhizua angulatus 2-6, Ramulus Cinnamomi 3-6, Cortex Illicii 1-4, Rhizoma Dioscoreae 3-5, Semen Sesami Nigrum 2-5, Periostracum Serpentis 3-4, Radix Astragali 6-15, Herba Visci 3-9, Radix Angelicae Sinensis 3-10, Rhizoma Cibotii 3-8, Radix Achyranthis Bidentatae 4-6, Fructus Lycii 3-12, Radix Ginseng 1-3, Radix Salviae Miltiorrhizae 2-9, Fructus Chaenomelis 3-6, Radix Glycyrrhizae 2-6, Radix Clematidis 3-6, Cornu Cervi Pantotrichum 1-3, Radix Paeoniae Alba 3-8, Rhizoma Drynariae 1-4, Moschus 0.3.Can adopt following weight portion in the present embodiment: Radix Rehmanniae Preparata 3kg, Rhizoma Gastrodiae 1kg, Myrrha 4kg, Rhizoma Homalomenae 6kg, Olibanum 4kg, Radix Polygoni Multiflori Preparata 5kg, Pachyrhizua angulatus 4kg, Ramulus Cinnamomi 3kg, Cortex Illicii 5kg, Rhizoma Dioscoreae 3kg, Semen Sesami Nigrum 6kg, Periostracum Serpentis 3kg, Radix Astragali 8kg, Herba Visci 3kg, Radix Angelicae Sinensis 4kg, Rhizoma Cibotii 6kg, Radix Achyranthis Bidentatae 4kg, Fructus Lycii 10kg, Radix Ginseng 1kg, Radix Salviae Miltiorrhizae 2kg, Fructus Chaenomelis 4kg, Radix Glycyrrhizae 2kg, Radix Clematidis 6kg, Cornu Cervi Pantotrichum 1kg, Radix Paeoniae Alba 6kg, Rhizoma Drynariae 1kg, Moschus 0.1kg.Can certainly in upper scope, to each medicine, reasonably arrange in pairs or groups as required, at this, not enumerate.
Further, what described step 102 was concrete comprises: replace water to put into next group described soak and prepare in the medical material of JINGTONGLING medicated wine, soak the medical material of preparation JINGTONGLING medicated wine.
In another preferred embodiment of the present invention, the weight ratio of described medicinal residues and water is 1:2-1:6, under 20-40 ℃ of conditions, described medicinal residues is soaked 20 minutes-300 minutes, certainly can will adapt to adjustment to its ratio and soak time as required.
Further, described step 102 also comprises: in filtrate, add crystal sugar to melt, be blended into Chinese liquor, fully stir 20 minutes-90 minutes.
In another preferred embodiment of the present invention, described step 101 also comprises: in described alcohol extraction tank, the weight ratio of medical material and described yellow wine is 1:100-1:300; Described step 102 also comprises: the weight ratio of described Chinese liquor and described yellow wine is 1:0.5-1:5.
And further, can also get Myrrha and Olibanum is removed impurity, broken section becomes the fritter of 0.8-1.2cm to put in pot, fries and slightly melts to surface with slow fire, taking out dries in the air after cool is joined in described step 101.
In order further to describe method of the present invention, its concrete method is:
(its medical material is above mentioned from clean material storehouse, to take out clean medical material in batches, do not repeat them here) drop in extraction pot, to injecting yellow wine and water in it, shut tank mouth, boil a period of time, pass through again warm macerating 2-8 hour, under 35-60 ℃ of condition, add yellow wine, yellow wine extraction liquid is filtered by finned filter, gained filtrate is injected wine liquid blending tank, add crystal sugar to stir and within 10-45 minute, make to melt, and obtain medicinal residues.
After this batch of extraction finishes, the water suitable with extracted amount is joined in described medicinal residues, soak after a period of time, then medicinal liquid is got, while replacing lower batch of product to throw, add the water of equivalent.The clean medical material of reclaiming from clean material storehouse in batches drops into alcohol extraction tank, inject the medicinal liquid of getting of yellow wine and upper batch described medicinal residues, shut tank mouth, boil a period of time, then pass through warm macerating 2-8 hour, under 35 ℃ of-60 ℃ of conditions, add yellow wine, yellow wine extraction liquid is filtered by finned filter, gained filtrate is injected wine liquid blending tank, adds crystal sugar to stir and within 10-45 minute, makes to melt, thereby obtain JINGTONGLING medicated wine.
Adopt method of the present invention, make in medicinal liquid containing the alcohol amount 20%-60% that is improved, while having shortened precipitate with ethanol, chien shih medicated wine outward appearance and inherent quality are all improved.This has not only guaranteed clarity and the drug effect of medicinal liquid, simultaneously when extraction supernatant is centrifugal, greatly reduced medicinal liquid loss, improved yield rate, significantly reduced production cost, and the bad problem of sedimentation effect when the present invention has solved to the innovation reform of extraction process that medicinal liquid is static has improved quality and the yield rate of product in the situation that not increasing cost.
Should be understood that, application of the present invention is not limited to above-mentioned giving an example, and for those of ordinary skills, can be improved according to the above description or convert, and all these improvement and conversion all should belong to the protection domain of claims of the present invention.
Claims (6)
1. a method of preparing treatment cervical vertebra ache medicine, it comprises the following steps:
A, to last consignment of, prepare in the remaining medicinal residues of JINGTONGLING medicated wine injected water and fully soak and obtain soak, described soak is joined to next group and prepare the medical material internal recycle of JINGTONGLING medicated wine and use;
What described steps A was concrete comprises:
A1, Radix Rehmanniae Preparata, Rhizoma Gastrodiae, Olibanum, Myrrha, Rhizoma Homalomenae, Radix Polygoni Multiflori Preparata, Pachyrhizua angulatus, Ramulus Cinnamomi, Cortex Illicii, Rhizoma Dioscoreae, Semen Sesami Nigrum, Periostracum Serpentis, the Radix Astragali, Herba Visci, Radix Angelicae Sinensis, Rhizoma Cibotii, Radix Achyranthis Bidentatae, Fructus Lycii, Radix Ginseng, Radix Salviae Miltiorrhizae, Fructus Chaenomelis, Radix Glycyrrhizae, Radix Clematidis, Cornu Cervi Pantotrichum, the Radix Paeoniae Alba and Rhizoma Drynariae are put in extraction pot, then in extraction pot, inject yellow wine and water, boil a period of time, then remain under the condition of 35-60 ℃ fully warm macerating, after wine extracts, filter;
A2, to adding in filtrate crystal sugar to melt, be blended into Chinese liquor, then fully stir, filter, airtight, static 5-30 days, is then blended into Moschus, filters and obtains described medicinal residues, to injected water in described medicinal residues, fully soaks and obtains described soak;
In steps A 1 and steps A 2 each medicine according to weight portion concrete be: Radix Rehmanniae Preparata 2-4, Rhizoma Gastrodiae 1-6, Myrrha 4-8, Rhizoma Homalomenae 5-7, Olibanum 3-8, Radix Polygoni Multiflori Preparata 3-9, Pachyrhizua angulatus 2-6, Ramulus Cinnamomi 3-6, Cortex Illicii 1-4, Rhizoma Dioscoreae 3-5, Semen Sesami Nigrum 2-5, Periostracum Serpentis 3-4, Radix Astragali 6-15, Herba Visci 3-9, Radix Angelicae Sinensis 3-10, Rhizoma Cibotii 3-8, Radix Achyranthis Bidentatae 4-6, Fructus Lycii 3-12, Radix Ginseng 1-3, Radix Salviae Miltiorrhizae 2-9, Fructus Chaenomelis 3-6, Radix Glycyrrhizae 2-6, Radix Clematidis 3-6, Cornu Cervi Pantotrichum 1-3, Radix Paeoniae Alba 3-8, Rhizoma Drynariae 1-4, Moschus 0.3.
2. method according to claim 1, is characterized in that, concrete the comprising of described steps A 2:
A21, replace water to put into next group described soak preparing in the medical material of JINGTONGLING medicated wine, soak the medical material of preparation JINGTONGLING medicated wine.
3. method according to claim 1, is characterized in that, the weight ratio of described medicinal residues and water is 1:2-1:6, under 20-40 ℃ of condition, described medicinal residues is soaked 20 minutes-300 minutes.
4. method according to claim 1, is characterized in that, described steps A 2 also comprises: in filtrate, add crystal sugar to melt, be blended into Chinese liquor, fully stir 20 minutes-90 minutes.
5. method according to claim 1, is characterized in that, described steps A 1 also comprises: in alcohol extraction tank, the weight ratio of medical material and described yellow wine is 1:100-1:300; Described steps A 2 also comprises: the weight ratio of described Chinese liquor and described yellow wine is 1:0.5-1:5.
6. method according to claim 2, is characterized in that, in described steps A, also comprises: get Myrrha and Olibanum is removed impurity, broken section becomes the fritter of 0.8-1.2cm to put in pot, with slow fire, fries and slightly melts to surface, and taking out dries in the air after cool is joined in steps A 1.
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| CN201210281985.0A CN102861203B (en) | 2012-08-09 | 2012-08-09 | Method for preparing medicines for treating cervical vertebra pain |
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| CN201210281985.0A CN102861203B (en) | 2012-08-09 | 2012-08-09 | Method for preparing medicines for treating cervical vertebra pain |
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Citations (4)
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|---|---|---|---|---|
| CN1040320A (en) * | 1988-08-20 | 1990-03-14 | 周欣初 | slimming cream and preparation method thereof |
| CN300847603S (en) * | 2007-11-14 | 2008-11-12 | 潘首德 | Medicine packaging box (Jingtongling medicinal wine) |
| CN102021101A (en) * | 2009-09-11 | 2011-04-20 | 董必进 | Healthy wine for preventing and treating cardiovascular and cerebrovascular diseases |
| CN102580024A (en) * | 2012-02-22 | 2012-07-18 | 王景胜 | Composition for treating cardiovascular diseases |
-
2012
- 2012-08-09 CN CN201210281985.0A patent/CN102861203B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1040320A (en) * | 1988-08-20 | 1990-03-14 | 周欣初 | slimming cream and preparation method thereof |
| CN300847603S (en) * | 2007-11-14 | 2008-11-12 | 潘首德 | Medicine packaging box (Jingtongling medicinal wine) |
| CN102021101A (en) * | 2009-09-11 | 2011-04-20 | 董必进 | Healthy wine for preventing and treating cardiovascular and cerebrovascular diseases |
| CN102580024A (en) * | 2012-02-22 | 2012-07-18 | 王景胜 | Composition for treating cardiovascular diseases |
Non-Patent Citations (2)
| Title |
|---|
| 美容养颜佳品灵芝枣的研制;雷萍;《食用菌》;20031231(第4期);第47页 * |
| 雷萍.美容养颜佳品灵芝枣的研制.《食用菌》.2003,(第4期),第47页. |
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