CN102858749B - 吡唑羧酸酰胺的制备方法 - Google Patents

吡唑羧酸酰胺的制备方法 Download PDF

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Publication number
CN102858749B
CN102858749B CN201180019764.XA CN201180019764A CN102858749B CN 102858749 B CN102858749 B CN 102858749B CN 201180019764 A CN201180019764 A CN 201180019764A CN 102858749 B CN102858749 B CN 102858749B
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formula
compound
palladium
bromine
chlorine
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Chinese (zh)
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CN102858749A (zh
Inventor
F·施莱特
T·维蒂格
M·洛米尔
H·托布勒
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Syngenta Participations AG
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Syngenta Participations AG
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/263—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions
    • C07C17/2635—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions involving a phosphorus compound, e.g. Wittig synthesis
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/30—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by a Diels-Alder synthesis
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/35—Preparation of halogenated hydrocarbons by reactions not affecting the number of carbon or of halogen atoms in the reaction
    • C07C17/354—Preparation of halogenated hydrocarbons by reactions not affecting the number of carbon or of halogen atoms in the reaction by hydrogenation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C25/00—Compounds containing at least one halogen atom bound to a six-membered aromatic ring
    • C07C25/24—Halogenated aromatic hydrocarbons with unsaturated side chains

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Catalysts (AREA)
CN201180019764.XA 2010-04-20 2011-04-14 吡唑羧酸酰胺的制备方法 Active CN102858749B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP10160439 2010-04-20
EP10160439.5 2010-04-20
PCT/EP2011/055870 WO2011131544A1 (en) 2010-04-20 2011-04-14 Process for the preparation of pyrazole carboxylic acid amides

Publications (2)

Publication Number Publication Date
CN102858749A CN102858749A (zh) 2013-01-02
CN102858749B true CN102858749B (zh) 2014-07-02

Family

ID=43984050

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201180019764.XA Active CN102858749B (zh) 2010-04-20 2011-04-14 吡唑羧酸酰胺的制备方法

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US (1) US8524915B2 (enExample)
EP (1) EP2560960B1 (enExample)
JP (1) JP6153864B2 (enExample)
CN (1) CN102858749B (enExample)
AR (1) AR080923A1 (enExample)
BR (1) BR112012026456B1 (enExample)
ES (1) ES2458935T3 (enExample)
IL (1) IL222400A (enExample)
MX (1) MX2012012009A (enExample)
TW (1) TWI480041B (enExample)
UY (1) UY33341A (enExample)
WO (1) WO2011131544A1 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI534126B (zh) 2011-01-25 2016-05-21 先正達合夥公司 用於製備吡唑羧酸醯胺之方法
CN103483407B (zh) * 2013-10-10 2015-11-18 宁夏启元药业有限公司 一种硫氰酸红霉素萃取结晶用复合溶媒及萃取结晶方法
GB201403438D0 (en) * 2014-02-27 2014-04-16 Syngenta Participations Ag Polymorphs
CN105985254B (zh) * 2015-02-17 2018-03-16 上海中科绿碳化工科技有限公司 一种制备甲酰胺类化合物的方法
CN106588745B (zh) * 2016-12-02 2019-06-14 杭州百昂锐地科技有限公司 一种苯并烯氟菌唑的中间体及其制备方法和应用
CA3261352A1 (en) 2022-07-22 2024-01-25 Syngenta Crop Protection Ag SOLID FORM OF A HETEROCYCLIC AMIDE DERIVATIVE
WO2025157998A1 (en) 2024-01-26 2025-07-31 Syngenta Crop Protection Ag Chemical process

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH075487B2 (ja) 1985-11-14 1995-01-25 住友化学工業株式会社 １―ブロモ―２―クロロ―４―フルオロベンゼンの製造法
US5093347A (en) 1991-01-28 1992-03-03 Monsanto Company 3-difluoromethylpyrazolecarboxamide fungicides, compositions and use
US7223879B2 (en) 1998-07-10 2007-05-29 Massachusetts Institute Of Technology Ligands for metals and improved metal-catalyzed processes based thereon
TWI374126B (en) 2005-10-25 2012-10-11 Syngenta Participations Ag Novel microbiocides
PL1963251T3 (pl) 2005-12-12 2013-01-31 Syngenta Participations Ag Proces wytwarzania amin
US8088960B2 (en) 2006-10-25 2012-01-03 Syngenta Crop Protection Llc Process for the production of substituted bromobenzenes
US8227619B2 (en) 2008-05-14 2012-07-24 Syngenta Limited Process for the preparation of amides
MX2011006425A (es) * 2008-12-24 2011-07-20 Syngenta Ltd Metodos para la preparacion de fungicidas.
MX2012010666A (es) * 2010-03-31 2012-10-05 Actelion Pharmaceuticals Ltd Derivados de isoquinolin-3-ilurea antibacterianos.
EP2560957B1 (en) * 2010-04-20 2014-05-07 Syngenta Participations AG Process for the preparation of pyrazole carboxylic acid amides
ES2453919T3 (es) * 2010-04-20 2014-04-08 Syngenta Participations Ag Proceso para preparar amidas de ácidos carboxílicos pirazólicos
WO2011131545A1 (en) * 2010-04-20 2011-10-27 Syngenta Participations Ag Process for the preparation of pyrazole carboxylic acid amides

Also Published As

Publication number Publication date
BR112012026456A2 (pt) 2015-09-08
CN102858749A (zh) 2013-01-02
EP2560960A1 (en) 2013-02-27
US20130041160A1 (en) 2013-02-14
TW201210590A (en) 2012-03-16
UY33341A (es) 2011-12-01
JP6153864B2 (ja) 2017-06-28
US8524915B2 (en) 2013-09-03
AR080923A1 (es) 2012-05-16
WO2011131544A1 (en) 2011-10-27
BR112012026456B1 (pt) 2017-06-27
IL222400A (en) 2015-04-30
JP2013527840A (ja) 2013-07-04
ES2458935T3 (es) 2014-05-07
MX2012012009A (es) 2012-12-17
EP2560960B1 (en) 2014-02-26
TWI480041B (zh) 2015-04-11

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