CN102838898A - Acidic dye ink for cold transfer printing and application method thereof - Google Patents
Acidic dye ink for cold transfer printing and application method thereof Download PDFInfo
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- CN102838898A CN102838898A CN2012103655805A CN201210365580A CN102838898A CN 102838898 A CN102838898 A CN 102838898A CN 2012103655805 A CN2012103655805 A CN 2012103655805A CN 201210365580 A CN201210365580 A CN 201210365580A CN 102838898 A CN102838898 A CN 102838898A
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Abstract
The invention discloses an acidic dye ink, a preparation method and an application method of the acidic dye ink in cold transfer printing. The acidic dye ink is composed of acidic dye, urea, a cosolvent, a chelating agent, ammonium sulfate, a surface tension regulator and water. The disperse dye ink is printed on transfer carriers such as cold transfer printing paper and so on, and the printed patterns are transferred to nylon fabrics from the transfer carriers during a transfer printing process, thereby cold transfer printing of the nylon fabrics is achieved.
Description
Technical field
The thickening agent ink that the present invention relates to use in the textile industry, specifically be meant a kind of with acid dye ink compound method and be applied to the method for cold-transfer printing.The present invention uses this acid dye ink and is printed on the transfer printing carriers such as cold transfer printing paper, and in the transfer printing process, decalcomania is transferred on the RIPSTOP from the transfer printing carrier, thereby has realized the cold-transfer printing of RIPSTOP.
Background technology
According to Japan's " processing technology " " transfer printing " special edition in 1972 introduction, transfer printing be French Prouvost Masurel company the investigator last century the fifties invented before year, this technology was actually the heat sublimation transfer printing at that time.Transfer printing is earlier suitable dye ink to be passed through method of printing with print process, is imprinted on the pattern of want stamp or literal on the extraordinary carrier, prints into a kind of transfer printing carrier; Again with one side that is printed on dyestuff on this transfer printing carrier and the fabric driving fit of being printed; Pass through tranfer printing machine; Under the effect of transfer device heating and pressure (subliming method) or solvent and pressure (wet method) and certain hour; Make dye sublimation or make dye ink break away from and peel off, the pattern of transfer printing carrier or words transfer printing to fabric, are accomplished the stamp task from carrier dissolving.Matching stain is in acid (or neutral) medium, to carry out painted dyestuff, contains water soluble groups such as sulfonic acid, carboxylic acid in its molecule.The chemical structure of nylon fiber is a polymeric amide, mainly is made up of three parts in the molecule, promptly constitutes the methene key of hydrophobic part in the molecule, the carboxamido-group of possess hydrophilic property and terminated amino and carboxyl.Therefore can dye with hydrophilic matching stain.Except direct printing, in recent years, in order to promote print quality, the transfering printing technology of matching stain has appearred also.For example number of patent application is that CN200710025330.6 " acid dye intaglio printing ink and preparation method thereof " discloses the acid dye intaglio printing ink on a kind of PET of being printed on and the BOPP plastics film, is applicable to wet transfer printing.But organic solvent accounts for more than 50% in its prescription, is solvent type ink, and Along with people's is to the enhancing of product and production process environmental consciousness thereof, and the use of solvent type ink will be restricted.Along with in recent years, the development in sportswear market, the demand of nylon printing lining rises year by year, so the water-soluble acid dyestuff of the using environment-friendly market vacancy of printing high-quality nylon facing material has caused the concern of printing technique research and development.
Summary of the invention
In order to realize adopting matching stain printing and dyeing RIPSTOP in the cold-transfer printing technology, overcome the pollution problem of solvent type ink, the invention provides a kind of cold-transfer printing dispersed dye ink and application method thereof.This acid dye ink is printed on the transfer printing carrier such as cold transfer printing paper, on cold-transfer printing equipment, decalcomania is transferred on the RIPSTOP from the transfer printing carrier, after vapour steaming colour fixing, washing typing back and process the PRINTED FABRIC finished product.
First aspect the invention provides a kind of cold-transfer printing acid dye ink, and its prescription according to weight percent is:
Wherein said solubility promoter adopts glycol ether ether, or polyoxyethylene glycol or thiocarbamide, or the alkyl substituted ureas, or a kind of or its compsn among the hot since time immemorial A; Said sequestrant is selected Sodium hexametaphosphate 99 SHMP for use, or edta edta, or HEDP HEDP, or 2-hydroxyethylidene diphosphonic acid guanidine-acetic acid HPAA, or hexanediamine tetramethyl fork phosphonic acids HDTMPA, or hydroxyethyl is for ethylenediamine triacetic acid HEEDTA; Said surface tension modifier is the spent glycol butyl ether, or propylene glycol n-butyl ether.
Said cold-transfer printing acid dye ink compound method is: solubility promoter, sequestrant add in the warm water; After fully stirring; Matching stain, urea and ammonium sulfate are added, fully after the stirring and dissolving, water is adjusted to 95-98% again; Parameter with surface tension modifier reconciliation statement surface tension sets to printing equipment promptly makes the cold-transfer printing acid dye ink.
Second aspect the invention provides a kind of cold-transfer printing with acid dye ink application method:
Said cold-transfer printing is specially with the acid dye ink application method: earlier with transfer printing carrier matrix with separant through the coating machine primary coat; And be printed as the cold-transfer printing carrier with acid dye ink according to the invention by printing press, again cold-transfer printing carrier and RIPSTOP are sent into cold-transfer printing machine together.RIPSTOP is handled through the fabric pretreatment liquid of cold-transfer printing machine pretreating device, again with the driving fit of cold-transfer printing carrier jointly through cold transfer device transfer printing, process PRINTED FABRIC.PRINTED FABRIC is after oven dry under 95 ℃ of conditions, and in 100-102 ℃ of steam, decatize 20-30min fixation is after the washing typing is the PRINTED FABRIC finished product again.Wherein said transfer printing carrier matrix can be selected plastics films such as paper, or PET, PP for use, or mf such as aluminium foil.
The 3rd aspect the invention provides the fabric pretreatment liquid described in a kind of above-mentioned cold-transfer printing acid dye ink application method, and its prescription according to weight percent is:
Wherein said pH regulator agent is ammonium sulfate or trolamine; Said sequestrant is selected Sodium hexametaphosphate 99 SHMP for use, or edta edta, or HEDP HEDP, or 2-hydroxyethylidene diphosphonic acid guanidine-acetic acid HPAA, or hexanediamine tetramethyl fork phosphonic acids HDTMPA, or hydroxyethyl is for ethylenediamine triacetic acid HEEDTA; Said moisture adsorbent is urea or hot since time immemorial A; Said laking agent can be selected tartrate for use, or vapour crust CibatexEB, or CibatexFB; Or Clariant Nylofixan MF2N; Or Bayer Mesitol MB or Mesitol S or Mesitol PS, or the big auspicious Chromaset R-Z in Taiwan, or ICI Matexil FA-SNX-Cerico; Said thickener is a modified polysaccharide dry powder, can select CMS for use, or cross-linking starch, or CMC 99.5 or etherification starch, or the etherificate sodium-alginate, or ether of cellulose, or water-soluble thickener such as hydroxypropyl etherificate guar gum.
Beneficial effect of the present invention is, one of which, and cold-transfer printing acid dye ink of the present invention is water-soluble system, has avoided the pollution that solvent evaporates is brought in the production process; Its two, cold-transfer printing acid dye ink of the present invention can carry solubility up to the acid dyestuff of 40% high density, makes product the black inadequately problem of color when transfer printing, can not occur; Its three, the application method of matching stain cold-transfer printing of the present invention improves the soaping fastness and the wet colour fastness of matching stain stamp RIPSTOP, seal back fabric has kept the consistence with original design style.
Embodiment
Followingly further specify the present invention, it should be noted that it is limitation of the present invention that these embodiment should not be regarded as with non-limiting example.
Embodiment 1
Fabric: fabric: Ta Silong; Raw material: 100% nylon, specification: 70D * 160D.
The cold-transfer printing acid dye ink, its prescription according to weight percent is:
Wherein said matching stain can be selected weak acid yellow 6G for use, weak acid red E-BL, the gorgeous blue FFR of slightly acidic, Weakly Acid Black BR; Said solubility promoter adopts glycol ether ether; Said sequestrant HEDP HEDP; Said surface tension modifier is selected propylene glycol n-butyl ether for use.
Said cold-transfer printing acid dye ink compound method is: solubility promoter, sequestrant add in the warm water; After fully stirring; Matching stain, urea and ammonium sulfate are added, fully after the stirring and dissolving, water is adjusted to 95% again; Parameter with 5% surface tension modifier reconciliation statement surface tension sets to printing equipment promptly makes the cold-transfer printing acid dye ink.
Cold-transfer printing is specially with the acid dye ink application method: earlier with transfer printing carrier matrix with separant through the coating machine primary coat; And be printed as the cold-transfer printing carrier with acid dye ink according to the invention by printing press, again cold-transfer printing carrier and RIPSTOP are sent into cold-transfer printing machine together.RIPSTOP is handled through the fabric pretreatment liquid of cold-transfer printing machine pretreating device, again with the driving fit of cold-transfer printing carrier jointly through cold transfer device transfer printing, process PRINTED FABRIC.PRINTED FABRIC is after oven dry under 95 ℃ of conditions, and in 102 ℃ of steam, decatize 20min fixation is after the washing typing is the PRINTED FABRIC finished product again.Wherein said transfer printing carrier matrix is selected the PET plastics film for use.
Fabric pretreatment liquid described in the cold-transfer printing acid dye ink application method, its prescription according to weight percent is:
Trolamine is selected in wherein said pH regulator agent for use; Said sequestrant is selected HEDP HEDP for use; Said laking agent is selected ICI Matexil FA-SNX-Cerico for use; Said thickener is selected cross-linking starch for use.
Embodiment 2
Fabric: Nylon Taffeta, raw material: 100% nylon, specification: 70D * 70D.
The cold-transfer printing acid dye ink, its prescription according to weight percent is:
Wherein said matching stain is selected acid scarlet FGRS for use, turmeric yellow RXL, turmeric yellow RXL, acid blue 2R, Acid Black 10B; Said solubility promoter adopts hot since time immemorial A; Said sequestrant is selected edta edta for use; Said surface tension modifier is selected butyl glycol ether for use.
Said cold-transfer printing acid dye ink compound method is: solubility promoter, sequestrant add in the warm water; After fully stirring; Matching stain, urea and ammonium sulfate are added, fully after the stirring and dissolving, water is adjusted to 98% again; Parameter with 2% surface tension modifier reconciliation statement surface tension sets to printing equipment promptly makes the cold-transfer printing acid dye ink.
Cold-transfer printing is specially with the acid dye ink application method: earlier with transfer printing carrier matrix with separant through the coating machine primary coat; And be printed as the cold-transfer printing carrier with acid dye ink according to the invention by printing press, again cold-transfer printing carrier and RIPSTOP are sent into cold-transfer printing machine together.RIPSTOP is handled through the fabric pretreatment liquid of cold-transfer printing machine pretreating device, again with the driving fit of cold-transfer printing carrier jointly through cold transfer device transfer printing, process PRINTED FABRIC.PRINTED FABRIC is after oven dry under 95 ℃ of conditions, and in 100 ℃ of steam, decatize 30min fixation is after the washing typing is the PRINTED FABRIC finished product again.Wherein said transfer printing carrier matrix is selected paper for use.
Fabric pretreatment liquid described in the cold-transfer printing acid dye ink application method, its prescription according to weight percent is:
Ammonium sulfate is selected in wherein said pH regulator agent for use; Said sequestrant is selected edta edta for use; Said laking agent is selected tartrate for use; Said thickener is selected etherification starch for use.
Embodiment 3
Fabric: Nylon Taffeta, raw material: 100% nylon, specification: 40D * 40D.
The invention provides a kind of cold-transfer printing acid dye ink, its prescription according to weight percent is:
Wherein said matching stain is selected neutral dark yellow GRL for use, toluylene red 2GL, neutral blue BNL, neutral black M-SRL; Said solubility promoter adopts thiocarbamide; Said sequestrant is selected Sodium hexametaphosphate 99 SHMP for use, and said surface tension modifier is selected butyl glycol ether for use.
Said cold-transfer printing acid dye ink compound method is: solubility promoter, sequestrant add in the warm water; After fully stirring; Matching stain and urea are added, fully after the stirring and dissolving, water is adjusted to 97% again; The parameter that sets to printing equipment with 3% surface tension modifier reconciliation statement surface tension at last promptly makes the cold-transfer printing acid dye ink.
Cold-transfer printing is specially with the acid dye ink application method: earlier with transfer printing carrier matrix with separant through the coating machine primary coat; And be printed as the cold-transfer printing carrier with acid dye ink according to the invention by printing press, again cold-transfer printing carrier and RIPSTOP are sent into cold-transfer printing machine together.RIPSTOP is handled through the fabric pretreatment liquid of cold-transfer printing machine pretreating device, again with the driving fit of cold-transfer printing carrier jointly through cold transfer device transfer printing, process PRINTED FABRIC.PRINTED FABRIC is after oven dry under 95 ℃ of conditions, and in 102 ℃ of steam, decatize 25min fixation is after the washing typing is the PRINTED FABRIC finished product again.Wherein said transfer printing carrier matrix is selected aluminium foil for use.
Fabric pretreatment liquid described in the cold-transfer printing acid dye ink application method, its prescription according to weight percent is:
Ammonium sulfate is selected in wherein said pH regulator agent for use; Said sequestrant is selected Sodium hexametaphosphate 99 SHMP for use; Said moisture adsorbent is selected hot since time immemorial A for use; Said laking agent is selected vapour crust CibatexEB for use; Said thickener is selected ether of cellulose for use.
Claims (8)
1. a cold-transfer printing is used acid dye ink, is made up of matching stain, urea, solubility promoter, sequestrant, ammonium sulfate, surface tension modifier and water;
It is characterized in that:
Said cold-transfer printing uses acid dye ink according to each component concentration of weight percent to be:
2. cold-transfer printing according to claim 1 is used acid dye ink, it is characterized in that:
Said solubility promoter adopts glycol ether ether, or polyoxyethylene glycol or thiocarbamide, or the alkyl substituted ureas, or a kind of or its compsn among the hot since time immemorial A; Said sequestrant is selected Sodium hexametaphosphate 99 SHMP for use, or edta edta, or HEDP HEDP, or 2-hydroxyethylidene diphosphonic acid guanidine-acetic acid HPAA, or hexanediamine tetramethyl fork phosphonic acids HDTMPA, or hydroxyethyl is for ethylenediamine triacetic acid HEEDTA; Said surface tension modifier is a butyl glycol ether, or propylene glycol n-butyl ether.
3. cold-transfer printing according to claim 1 is used acid dye ink, it is characterized in that:
Said its collocation method of cold-transfer printing acid dye ink is: solubility promoter, sequestrant add in the warm water; After fully stirring; Matching stain, urea and ammonium sulfate are added, fully after the stirring and dissolving, water is adjusted to 95-98% again; Parameter with surface tension modifier reconciliation statement surface tension sets to printing equipment promptly makes the cold-transfer printing acid dye ink.
4. a cold-transfer printing is characterized in that with the application method of acid dye ink:
Earlier with transfer printing carrier matrix with separant through the coating machine primary coat, and be printed as the cold-transfer printing carrier with acid dye ink according to the invention by printing press, again cold-transfer printing carrier and RIPSTOP are sent into cold-transfer printing machine together.RIPSTOP is handled through the fabric pretreatment liquid of cold-transfer printing machine pretreating device, again with the driving fit of cold-transfer printing carrier jointly through cold transfer device transfer printing, process PRINTED FABRIC.PRINTED FABRIC is after oven dry under 95 ℃ of conditions, and in 100-102 ℃ of steam, decatize 20-30min fixation is after the washing typing is the PRINTED FABRIC finished product again.
5. according to the application method of the said cold-transfer printing of claim 4, it is characterized in that with acid dye ink:
Said transfer printing carrier matrix can be selected plastics films such as paper, or PET, PP for use, or mf such as aluminium foil.
6. according to the application method of the said cold-transfer printing of claim 4, it is characterized in that with acid dye ink:
Fabric pretreatment liquid, its prescription according to weight percent is:
7. according to claim 4 and the application method of 6 said cold-transfer printings, it is characterized in that with acid dye ink:
Said pH regulator agent is an ammonium sulfate, or trolamine; Said sequestrant is selected Sodium hexametaphosphate 99 SHMP for use, or edta edta, or HEDP HEDP, or 2-hydroxyethylidene diphosphonic acid guanidine-acetic acid HPAA, or hexanediamine tetramethyl fork phosphonic acids HDTMPA, or hydroxyethyl is for ethylenediamine triacetic acid HEEDTA; Said moisture adsorbent is a urea, or hot since time immemorial A; Said laking agent can be selected tartrate for use, or vapour crust CibatexEB, or CibatexFB; Or Clariant Nylofixan MF2N; Or Bayer Mesitol MB or Mesitol S or Mesitol PS, or the big auspicious Chromaset R-Z in Taiwan, or ICI Matexil FA-SNX-Cerico; Said thickener is a modified polysaccharide.
8. according to claim 4 and the application method of 6 said cold-transfer printings, it is characterized in that with acid dye ink:
Said thickener is a modified polysaccharide, can select CMS for use, or cross-linking starch, or CMC 99.5 or etherification starch, or the etherificate sodium-alginate, or ether of cellulose, or water-soluble thickener such as hydroxypropyl etherificate guar gum.
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105648793A (en) * | 2016-04-01 | 2016-06-08 | 东莞市中纺化工有限公司 | Print paste with high chlorine resistance as well as preparation method and application of print paste |
| CN107083698A (en) * | 2017-04-07 | 2017-08-22 | 常州旭荣针织印染有限公司 | Nylon fabric wet transfer printing padding liquid and its compound method |
| CN108239887A (en) * | 2016-12-27 | 2018-07-03 | 长胜纺织科技发展(上海)有限公司 | One kind gives liquid pre-treating method to version |
| CN108239888A (en) * | 2016-12-27 | 2018-07-03 | 长胜纺织科技发展(上海)有限公司 | With no paper method for transfer printing |
| CN108342914A (en) * | 2017-01-23 | 2018-07-31 | 长胜纺织科技发展(上海)有限公司 | Transfer dyeing method |
| CN109577045A (en) * | 2018-12-28 | 2019-04-05 | 北京泛博科技有限责任公司 | A kind of fur color fixing agent and its preparation method and application |
| TWI659138B (en) * | 2017-10-25 | 2019-05-11 | Everlight Chemical Industrial Corporation | Acid dye composition and use thereof on dying nylon texture |
| CN110055775A (en) * | 2019-05-07 | 2019-07-26 | 东丽酒伊织染（南通）有限公司 | A kind of cold-transfer printing technique of the highly dense polyester fabric of fine-denier |
| CN113584752A (en) * | 2021-08-06 | 2021-11-02 | 长胜纺织科技发展(上海)有限公司 | Method and system for dyeing field jet fabric |
| CN115679720A (en) * | 2022-11-24 | 2023-02-03 | 浙江迎丰科技股份有限公司 | Cold transfer printing method for acid dye |
| CN115772812A (en) * | 2022-11-28 | 2023-03-10 | 东莞市伊时针织印花有限公司 | Environment-friendly mixed acid dye for mixed wool and production method thereof |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105648793A (en) * | 2016-04-01 | 2016-06-08 | 东莞市中纺化工有限公司 | Print paste with high chlorine resistance as well as preparation method and application of print paste |
| CN108239887B (en) * | 2016-12-27 | 2020-07-31 | 长胜纺织科技发展(上海)有限公司 | Pretreatment method for plate-alignment liquid feeding |
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| CN107083698A (en) * | 2017-04-07 | 2017-08-22 | 常州旭荣针织印染有限公司 | Nylon fabric wet transfer printing padding liquid and its compound method |
| CN107083698B (en) * | 2017-04-07 | 2021-05-25 | 常州旭荣针织印染有限公司 | Padding liquid for wet transfer printing of chinlon fabric and its compounding process |
| TWI659138B (en) * | 2017-10-25 | 2019-05-11 | Everlight Chemical Industrial Corporation | Acid dye composition and use thereof on dying nylon texture |
| CN109577045A (en) * | 2018-12-28 | 2019-04-05 | 北京泛博科技有限责任公司 | A kind of fur color fixing agent and its preparation method and application |
| CN110055775A (en) * | 2019-05-07 | 2019-07-26 | 东丽酒伊织染（南通）有限公司 | A kind of cold-transfer printing technique of the highly dense polyester fabric of fine-denier |
| CN113584752A (en) * | 2021-08-06 | 2021-11-02 | 长胜纺织科技发展(上海)有限公司 | Method and system for dyeing field jet fabric |
| CN115679720A (en) * | 2022-11-24 | 2023-02-03 | 浙江迎丰科技股份有限公司 | Cold transfer printing method for acid dye |
| CN115772812A (en) * | 2022-11-28 | 2023-03-10 | 东莞市伊时针织印花有限公司 | Environment-friendly mixed acid dye for mixed wool and production method thereof |
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