CN102813956B - The warm warm skin agent composition and method of making the same of disposable sanitary articles - Google Patents

Abstract

The present invention relates to a kind of warm warm skin agent compositions of disposable sanitary articles, described compositions comprises warm agent and emollient, the composition of each component is warm agent 0.001 ~ 2%, plants essential oil 1 ~ 5%, plant extract 2 ~ 10%, antibacterial 0.5 ~ 5%, slow releasing agent 5 ~ 20%, skin protectant 5 ~ 15%, solvent 45 ~ 75%.Described compositions is applied to disposable sanitary articles can transmit sensation to wearer, and wearer can not be caused to aware the change of external condition, thus improve comfort.The invention also discloses the preparation method of this compositions, preparation technology is simple, easy to operate.

Description

The warm warm skin agent composition and method of making the same of disposable sanitary articles

Technical field

The present invention relates to a kind of warm warm skin agent, especially a kind of warm warm skin agent being suitable for disposable sanitary articles.

Background technology

Although disposable sanitary product is as the various characteristics of baby diaper or female sanitary towel etc., as the protection in use and comfort aspect, be greatly improved in some years recently.But consumer still needs further improvement, namely make the experience wearing this goods happier, especially after wearing these goods for a long time.

People are in use disposable sanitary product process, and because disposable toilet paper product absorb through liquid or urine, people wear for a long time and have feeling of oppression and heat, damp, very uncomfortable.Existing patent application at present relates to heat sensitizer, as the Chinese patent application of application number 201010271753.8, relates to a kind of heat sensitizer, mainly makes dysmenorrhea person reduce the misery of dysmenorrhea, spend menstrual period more giocoso.The Chinese patent application of application number CN201010523910.X also relates to a kind of Fa Nuan sanitary towel, makes women reduce painful in process in menstrual period.

But the user of most of disposable sanitary product, in use has sultry, moist offending sensation, also do not have this kind of product at present, reduce this sensation of user.

Summary of the invention

The object of this invention is to provide a kind of warm warm skin agent, be applied to disposable sanitary articles by this warm warm skin agent, by providing warming sense, wearer can be made to experience happy sense, and for realizing above object, the technical scheme of employing is:

For a warm warm skin agent for disposable sanitary articles, said composition is composed of the following components by weight percentage:

Preferably, described plants essential oil is selected from least one in Folium Artemisiae Argyi quintessence oil, Flos Rosae Rugosae quintessence oil, Folium Artemisiae Argyi quintessence oil, Rhizoma Chuanxiong quintessence oil, angelica essential oil, Rhizoma Cyperi quintessence oil, tea tree ethereal oil, Flos Lonicerae quintessence oil, Cananga odorata quintessence oil.(above quintessence oil is all bought from Shanghai Hua Ya cosmetics company limited)

Preferably, described plant extract is selected from one or more in Aloe extraction solution, Folium Artemisiae Argyi extracting solution, ginsenoside, Rhizoma Zingiberis Recens extract, Herba Leonuri extract.(above extract is all bought from Huzhou Zhenlu Biological Products Co., Ltd.)

Preferably, described sustained-release synergistic agent is selected from one or more in poly-ethyl cellulose, hydroxypropyl cellulose starch, polyvinylpyrrolidone, Span60, sodium cocoglyceryl ester, propylene glycol, castor oil hydrogenated polyoxyethylene ether.

Preferably, described skin protectant is selected from one or more in Jojoba oil, olive oil, sodium cocoglyceryl ester, glycerol;

Preferably, described solvent is the one in food grade full gear ethanol, sorbitol or deionized water.

Preferably, described antibacterial is one or more in triclosan, polyhexamethylene guanidine, chitosan or nanometer silver.

Stabilizing agent conventional in cosmetics and auxiliary agent can also be added in addition, guarantee that formula obtains stability, thermostability and clear permeability, be at least two kinds in water-soluble silicon oil, water solublity lanoline PEG-40, pure water, propylene glycol, sorbitol, glycerol, HP-β-CD, essence.

The absorbent sanitary product that warm warm skin agent of the present invention can be used for comprises sanitary towel, sanitary pad, baby or adult diaper, wet tissue or diaper.

The invention provides a kind of warm warm skin agent, by being applied to disposable sanitary articles, being sent the comfort of improvement by these articles for use, especially warming sense and dry feeling, but without feeling of oppression and heat.Particularly female menstrual product is as sanitary towel, sanitary pad etc., this article delivery warming sense, to alleviate the symptoms such as the dysmenorrhea of part user.Safety and environmental protection of the present invention, pain relieving of releiving, have the warm warm skin agent of targeting and controlled capability better.

The present invention also provides the described a kind of application of warm warm skin agent in sanitary towel, sanitary pad, baby or the disposable sanitary articles such as adult diaper and wet tissue for disposable sanitary articles: by warm warm skin agent compositions continuously or be interrupted and be sprayed on sanitary towel or protective pad, diaper surface layer, then be finished product through physics heat seal and sprinkling gum, or directly compositions can be made warm warm skin wet tissue according to soaking non-woven fabrics after certain dilution proportion.

The beneficial effect of the warm warm skin agent for disposable sanitary articles provided by the invention is:

(1) product adopts slow releasing agent, is wrapped up by functional component, avoids the hotness composition of excessive concentrations and contact skin and the stimulation that brings; Extend the warm time, ensure that the persistence of effect.

(2) product adopts food stage, cosmetics-stage raw material, safe and harmless, acts on skin surface and can not produce any negative effect.

(3) administered area is concentrated, and consumption is few, reduces the production cost of disposable sanitary articles, improves the quality of product.

(4) the present invention is applied in disposable sanitary articles and by stimulating the sensor at the focus place of human body, can makes local telangiectasis, can promote human body skin blood circulation, and then activating biological cell, brings a kind of warm sensation to people.The present invention is by adding some natural plants (Folium Artemisiae Argyi etc.) quintessence oil or extract, and it can help women to accelerate the growth of cell and hemoglobin, reaches the effect nourished blood.Can warming the meridian for stopping bleeding, dispersing cold for relieving pain, relieving dysmenorrhea.

Accompanying drawing explanation

Fig. 1 is that the chromatography of gases of warm warm skin functional component-VBE of the present invention detects collection of illustrative plates.

Detailed description of the invention

Provide concrete embodiment below and further illustrate the present invention, but scope of the present invention is not construed as limiting.

Embodiment one:

VBE: 1kg

Folium Artemisiae Argyi quintessence oil: 3kg

Rhizoma Chuanxiong extract: 6kg

Propylene glycol: 18kg

Ethanol: 16.4kg

Triclosan: 0.6kg

Deionized water: 39kg

Castor oil hydrogenated polyoxyethylene ether: 13kg

Essence: 3kg

1) by the dissolve with ethanol of the VBE 16.4kg of the triclosan of 0.6kg, the essence of 3kg and 1kg;

2) deionized water of the Rhizoma Chuanxiong extract of the Folium Artemisiae Argyi quintessence oil of 3kg, 6kg, 18kg propylene glycol, 13kg castor oil hydrogenated polyoxyethylene ether and 39kg is joined in reactor be uniformly mixed;

3) until 2) in component mix homogeneously after, by 1) join 2) in, with the speed of 1000r/min stir 45min make it dissolve completely, obtain the product of clear.

Following series of experiments checking is carried out to the product that example one obtains:

1 antiseptic effect checking:

The total plate count of microorganism detection antibacterial, fungus

Examination criteria: GB15979-2002 " Appendix B 2< total number of bacterial colonies and initial contaminating bacteria detection method > " and " Appendix B 7< fungus colony sum detection method > "

Sample treatment: evenly spray sample 0.10g on sanitary towel top layer, cuts off 2 × 3cm sanitary towel top layer, adds bacterium liquid, and cultivate 14 days under 54 DEG C of conditions, concrete outcome sees the following form:

Group	1#	2#	3#	4#	5#
						Antibacterial (cfu/g)	0	0	0	0	0
Fungus (cfu/g)	0	0	0	0	0

This result shows, this product has very strong antisepsis, within a certain period of time can the regrowing, for women provides safer physiological hygiene environment of anti-bacteria and fungus.

The method of testing of 2 warm degree and checking:

Method 1:

1) test of human temperature hot comfort:

The warm warm skin agent sample of accurate sprinkling 0.10g, in sanitary towel top layer, is chosen each 80 tests carrying out the warm comfort level of hot body of the women of Different age group, be the results are shown in following table:

Above-mentioned test result proves that the present invention can safeguard the warm comfortable dry and comfortable environment of women's privates, and is applicable to the women of all age group.

2) test of warm time and checking:

The warm warm skin agent of accurate sprinkling 0.10g, in sanitary towel top layer, is chosen all ages and classes degree women 80 respectively and is done warm time test, the results are shown in following table:

Above-mentioned test proves that the present invention just can provide the warm time substantially to maintain 1 hours to the women of Different age group.

Method 2:

After stability test is finished to the sanitary towel adding warm warm skin agent sample, choose different time sections, do the assay of the warm skin factor (VBE).

Chromatographic column: HP-1MS, 30m × 0.25mm;

Column temperature: initial column temperature 80 DEG C, keeps 4.5min, with the ramp to 220 DEG C of 40 DEG C/min, keeps 7min;

Injector temperature: 240 DEG C, detector temperature: 280 DEG C

The preparation of mark liquid in carrier gas: 0.12MPa, hydrogen: 0.1MPa, air: 0.2MPa, split ratio: 10:1:

Get Ketohexamethylene 1ml, be configured to the interior mark liquid of the normal hexane of 1mg/ml respectively.

The mensuration of correction factor:

Take the VBE titer of 0.03g, accurately weighed, add the interior mark liquid of 10ml, precision measures, and injects chromatography of gases chromatograph 1 μ l.Get three meansigma methodss, calculate the correction factor of VBE.

Accurately tearing a certain amount of sanitary towel top layer non-woven fabrics off is placed in 50ml color comparison tube, add mark liquid in 2.5ml, then add normal hexane and be diluted to 25ml, get filtrate 1ml sample introduction with pipet, calculate the content of warm warm skin composition in Mei Pian sanitary towel by internal standard method, measurement result sees the following form:

The growth of time proves the content of the warm skin factor in Mei Pian sanitary towel in 54 DEG C of stable experiments along with can decline to some extent, but finally tend towards stability, through experimental verification repeatedly, after stable experiment in 14 days terminates, in sanitary towel, the content of the warm skin factor still can bring obvious warm sensation to human body.

Embodiment two

VBE: 1.2kg

Angelica essential oil: 2kg

Herba Leonuri extract: 9kg

Propylene glycol: 14kg

Sorbitol: 14kg

Ethanol: 12.5kg

Polyhexamethylene guanidine: 5kg

Deionized water: 34.3kg

Castor oil hydrogenated polyoxyethylene ether: 8kg

1) by the dissolve with ethanol of the VBE of 1.2kg and 2kg angelica essential oil 12.5kg;

2) Herba Leonuri extract of 9kg, 12kg propylene glycol, 14kg sorbitol, 8kg castor oil hydrogenated, 34.3kg deionized water and 7kg polyhexamethylene guanidine are joined in reactor be uniformly mixed;

3) until 2) in component mix homogeneously after, by 1) join 2) in, with the speed of 1000r/min stir 45min make it dissolve completely, obtain the product of clear.

The checking of bacteriostasis rate test experience is carried out to the product that example two obtains:

Sample treatment: evenly spray the warm warm skin antibacterial of 0.10g example two on blank sanitary towel print, in 37 DEG C of baking oven, place dry 2h(simulate body temperature and service time) take out effective site in the middle of print clip and do bacteriostasis rate and detect (with reference to the operation of GB15979-2002 method), parallel testing three groups, result is as following table:

Illustrate that this product of this product has very strong antisepsis, within a certain period of time can the regrowing, for women provides safer physiological hygiene environment of anti-bacteria and fungus.

After 2 years stability tests, the bacteriostasis rate of sanitary towel detects:

With reference to GB15979-2002 sanitary towel stability experiment operational approach, warm for example two warm skin antibacterial sample is evenly sprayed at sanitary towel top layer (every sheet sprays 0.10g), be placed in 37 DEG C of baking ovens and do bacteriostasis rate detection after three months again, result is as following table:

This testing result meets in the People's Republic of China's Disposable Sanitary Accessory sanitary standard regulation killing rate of escherichia coli, staphylococcus aureus and Candida albicans being more than or equal to 50% completely, and result proves that this product has good stability and fungistatic effect.

Embodiment three

VBE: 1.5kg

Flos Rosae Rugosae quintessence oil: 2kg

Flos Lonicerae extract: 7kg

Jojoba oil: 4kg

Sorbitan ester: 8kg

Ethanol: 14.5kg

Chitosan: 0.6kg

Deionized water: 56.9kg

Castor oil hydrogenated polyoxyethylene ether: 5kg

Lactic acid: 0.5kg

1) by the dissolve with ethanol of the VBE of 1.5kg and 2kg Flos Rosae Rugosae quintessence oil 14.5kg;

2) Flos Lonicerae extract of 7kg, 4kg Jojoba oil, 8kg sorbitan ester, 5kg castor oil hydrogenated polyoxyethylene ether, 56.9kg deionized water, 0.5kg lactic acid and 0.6kg chitosan are joined in reactor be uniformly mixed;

3) until 2) in component mix homogeneously after, by 1) join 2) in, with the speed of 1000r/min stir 45min make it dissolve completely, obtain the product of clear.

The pH value change of simulation service condition detection example three sample in sanitary towel:

Sample treatment: evenly spray the warm warm skin agent of 0.10g example three on blank sanitary towel print, 2h is placed in 37 DEG C of baking ovens, in the middle of taking-up print clip, in effective site 1g input 99g deionized water, (pH value of water is in neutral, be about 7), use Accurate pH measurement to determine the pH value change of solution, result is as following table:

Time

5min

20min

30min

1h

2h

3h

4h

PH value

4.3-4.4

4.4-4.5

4.4-4.5

4.5-4.6

4.6-4.7

4.7-4.8

4.7-4.8

Simulate the pH value change in use procedure after testing, the present invention can provide weakly acidic condition to maintain 4 hours for women's privates, privates pH value through document document announcement display healthy women menstrual period is generally between 4-6, faintly acid of the present invention meets the pH value in menstrual period of healthy women completely, and can helping to be in subhealth state or unsound women's adjust ph to recovering normal, improving the autoimmunity of women.

Embodiment four stability test

Embodiment one, two, three sample liquid and sprinkling are had the print stability (1 year and 2 years) of sample liquid good, sample liquid variable color, the print whiteness and the structure that are added with sample liquid are unaffected, and functional component still can quantitatively detect after 2 years stability tests terminate.Result is as following table:

Claims (1)

1. the warm warm skin agent compositions of disposable sanitary articles, it is characterized in that, said composition is composed of the following components:

1) by the dissolve with ethanol of the VBE 16.4kg of the triclosan of 0.6kg, the essence of 3kg and 1kg;

2) deionized water of the Rhizoma Chuanxiong extract of the Folium Artemisiae Argyi quintessence oil of 3kg, 6kg, 18kg propylene glycol, 13kg castor oil hydrogenated polyoxyethylene ether and 39kg is joined in reactor be uniformly mixed;

3) until 2) in component mix homogeneously after, by 1) join 2) in, with the speed of 1000r/min stir 45min make it dissolve completely, obtain the product of clear.