CN102795627A - Multi-parameter online monitoring and optimizing control device and method of polycrystalline silicon reduction furnace - Google Patents
Multi-parameter online monitoring and optimizing control device and method of polycrystalline silicon reduction furnace Download PDFInfo
- Publication number
- CN102795627A CN102795627A CN2012102038201A CN201210203820A CN102795627A CN 102795627 A CN102795627 A CN 102795627A CN 2012102038201 A CN2012102038201 A CN 2012102038201A CN 201210203820 A CN201210203820 A CN 201210203820A CN 102795627 A CN102795627 A CN 102795627A
- Authority
- CN
- China
- Prior art keywords
- infrared
- module
- image
- measurement module
- silicon rod
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000012544 monitoring process Methods 0.000 title claims abstract description 37
- 229910021420 polycrystalline silicon Inorganic materials 0.000 title claims abstract description 27
- 238000000034 method Methods 0.000 title claims abstract description 24
- 230000009467 reduction Effects 0.000 title abstract description 9
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims abstract description 51
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 50
- 239000010703 silicon Substances 0.000 claims abstract description 50
- 238000012545 processing Methods 0.000 claims abstract description 31
- 238000009529 body temperature measurement Methods 0.000 claims abstract description 19
- 239000000523 sample Substances 0.000 claims abstract description 18
- 230000008569 process Effects 0.000 claims abstract description 11
- 238000009826 distribution Methods 0.000 claims abstract description 9
- 238000005259 measurement Methods 0.000 claims description 35
- 238000005457 optimization Methods 0.000 claims description 23
- 239000011159 matrix material Substances 0.000 claims description 7
- 229920005591 polysilicon Polymers 0.000 claims description 7
- 238000001514 detection method Methods 0.000 claims description 6
- 230000003287 optical effect Effects 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 230000008859 change Effects 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 238000012937 correction Methods 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- 238000003384 imaging method Methods 0.000 claims description 3
- 238000002203 pretreatment Methods 0.000 claims description 3
- 238000007789 sealing Methods 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 9
- 238000005516 engineering process Methods 0.000 abstract description 3
- 238000010586 diagram Methods 0.000 description 4
- 230000005855 radiation Effects 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- 239000004744 fabric Substances 0.000 description 2
- 238000004062 sedimentation Methods 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 208000013132 neonatal intrahepatic cholestasis due to citrin deficiency Diseases 0.000 description 1
- 239000013307 optical fiber Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000004861 thermometry Methods 0.000 description 1
- 238000013519 translation Methods 0.000 description 1
Images
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Landscapes
- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
The invention discloses a multi-parameter online monitoring and optimizing control device and method of a polycrystalline silicon reduction furnace. The device comprises a multi-parameter infrared monitoring probe, an infrared image processing and vision measuring module and a process optimizing control module, wherein the multi-parameter infrared monitoring probe obtains an infrared image of a silicon rod in the furnace; the infrared image is collected by a data collecting module and is converted into a digital image; the digital image is analyzed and processed by an image processing module, and the diameter and the growing rate of the silicon rod are obtained through a vision measuring technology; a colorimetric temperature measurement method is used for measuring temperature distribution on the surface of the silicon rod and obtained data is accessed to a display through a user interface; and an optimizing control module is established through measured data obtained by analyzing, and different polycrystalline silicon reduction furnace types are combined to carry out closed ring optimizing control. According to the multi-parameter online monitoring and optimizing control device and method, a silicon rod growing process can be optimally controlled; and the device and the method are of great importance of saving energy and reducing consumption, improving the production efficiency, guaranteeing the production safety and reducing the labor intensity.
Description
Technical field
The present invention relates to Si reduction stove production field, be specifically related to a kind of polycrystalline silicon reducing furnace many reference amounts on-line monitoring and optimal control device and method.
Technical background
Polysilicon is the basic material of electronic industry and solar energy industry, is widely used in semi-conductor chip, high-performance sensors, optical fiber, solar panel etc.To 2010, global polysilicon output reached 120,000 tons, and China has accounted for 50% of ultimate production, nearly 40,000,000,000 Renminbi of the output value.Estimate 2011, global polysilicon output will reach 160,000 tons, and Chinese proportion then will be brought up to more than 60% of ultimate production.
Parameters such as the temperature distribution on silicon rod surface, rod footpath, growth rate are the key links that improves the silicon rod growth quality in the reduction furnace.In the polycrystalline silicon rod process of growth, increase in temperature, the sedimentation rate of silicon on the silicon core increases, and the silicon rod growth is accelerated, but power consumption is too much, and temperature is high more, and gas phase condition is harsher, and the homogeneity of silicon rod is poor more; Temperature reduces, and the sedimentation rate of silicon is slack-off, and when temperature was lower than certain value, silicon rod ruptured easily, and what influence was grown proceeds.In addition, the diameter of silicon rod is the important evidence of temperature regulation and feed gas set of dispense ratio over time, and irrational proportioning can make the silicon rod growth velocity descend the mass consumption energy.Therefore, just press for a kind of can be in reduction furnace these parameters of on-line monitoring and the equipment that carries out closed-loop optimization control.
But the test of the on-line measurement of silicon rod many reference amounts and theoretical investigation that optimal control is all carried out and exploration does not have sophisticated plant and instrument and gets into production application at present both at home and abroad to reduction furnace.In the world, even all there is not the equipment of sophisticated on-line monitoring and control in the Siemens that is in the technological precedence status aspect the production of polysilicon technology controlling and process, Mitsubishi Electric Co. etc. yet; Blank especially at home, at present, the on-line monitoring and the optimal control of the many reference amounts (like silicon rod diameter, temperature etc.) in the reduction furnace rest on theoretical research stage basically.
So far; In the actual production of the whole nation over thousands of seat polycrystalline silicon reducing furnace; What adopt all is the open loop type master modes that are the basis with preset empirical curve, and temperature is by the some thermometric through observation window, fans out from point to area; And the measurement of diameter leans on the experience range estimation of workman's work to estimate that roughly obvious this method has certain subjectivity and randomness fully.
Given this, developed a kind of equipment that can in reduction furnace, carry out on-line measurement and carry out closed-loop optimization control to parameters such as the temperature distribution on silicon rod surface, excellent footpath, growth rates.
Summary of the invention
The invention solves the many reference amounts monitoring in real time of polycrystalline silicon growth process and the technical barrier of optimal control, the equipment of having developed the online accurate measurement of parameters such as a kind of silicon rod surface temperature distribution, silicon rod diameter, growth rate and having carried out closed-loop optimization control.To save energy and reduce the cost, enhance productivity, ensure production safety, reducing labor intensity all has very important meaning.
The technical scheme that the present invention adopts is:
Polycrystalline silicon reducing furnace many reference amounts on-line monitoring and optimal control device; It is characterized in that; Include many reference amounts infrared monitoring probe, infrared image processing and vision measurement module, process optimization control module; Described many reference amounts infrared monitoring probe includes near-infrared optical system, image capture module; The water-cooled shield cap is equipped with in many reference amounts infrared monitoring probe outside, and the front end of water-cooled shield cap is provided with water-cooling type and seals withstand voltage observation window, and many reference amounts infrared monitoring probe is deep in the polycrystalline silicon reducing furnace; Described infrared image processing and vision measurement module include infrared image processing module and vision measurement module; Data acquisition module, image processing module that the infrared image processing module links to each other successively; The vision measurement module includes color comparison temperature measurement module, diameter measurement module; The output terminal of image processing module is connected with color comparison temperature measurement module, diameter measurement module respectively, and the output terminal of color comparison temperature measurement module, diameter measurement module all inserts data output interface, user interface, and data output interface is circumscribed with the process optimization control module; The external indicating meter of user interface, the process optimization control module is connected with former system through a data interface.
Described process optimization control module is a closed-loop optimization control model.
Described image capture module is the infrared CCD camera.
The method of polycrystalline silicon reducing furnace many reference amounts on-line monitoring and optimal control is characterized in that, comprises following concrete steps:
1) many reference amounts infrared monitoring probe is through choosing optimum infrared band and highly sensitive infrared CCD camera; Obtain the picture signal of silicon rod growth in the stove through near-infrared optical system, infrared CCD camera; And carry out A/D through data acquisition module and change, obtain the infrared digital image of polysilicon rod;
2) infrared digital image of above-mentioned acquisition is sent into image processing module; And through image processing module carry out the image pre-treatment with cut apart; In conjunction with concrete image,, protected imaging surface temperature distribution characteristic to greatest extent through image denoising algorithm and level and smooth filtering algorithm; Find out the edge of sealing through carrying out the profile tracking, and carry out sub-pixel rim detection and fitting of a straight line, obtain the image border of degree of precision;
3) above-mentioned processed images is transported in the diameter measurement module of vision measurement module; The demarcation of at first carrying out the infrared CCD camera obtains the inside and outside parameter of camera; Carry out choosing of primary objective image border according to Hough fitting of a straight line algorithm, then image is carried out the tracking at edge, zonule; , the fundamental matrix that robustness is estimated carries out corresponding point matching under instructing; At last, pixel value and the effective unit system yardstick measured are converted, obtain the real-time diameter data of silicon rod according to above algorithm;
4) image of handling in the step 2 is transported in the color comparison temperature measurement module; Utilize the image processing system in the color comparison temperature measurement module that image is gone bad correction a little; To image cut apart, smoothly, layering, gradation conversion, call DB then, grey scale curve is carried out match; Temperature is demarcated, accomplish thermometric;
5) with the silicon rod diameter and the surface temperature data that obtain in the step 3,4, be transported in the process optimization control module, set up optimizing control models, instruct silicon rod under reasonable process conditions, to grow with feedback in conjunction with work information through data output interface;
6) silicon rod diameter and the surface temperature data with above-mentioned acquisition output to the terminal, obtain the real-time diameter and the growth rate of silicon rod, and the real time temperature of silicon rod surface any point, and in indicating meter, show.
Principle of work of the present invention is:
The present invention obtains silicon rod infrared image in the stove through many reference amounts infrared monitoring probe (NICCD); Analyze, handle by image processing module again through data collecting module collected, after converting digital picture into; Obtain silicon rod diameter and growth rate through the vision measurement technology; Adopt color comparison temperature measurement method to measure the temperature distribution on silicon rod surface; The gained data insert the take off data that indicating meter obtains through analysis through user interface, set up optimizing control models, carry out closed-loop optimization control in conjunction with different polycrystalline silicon reducing furnace types.
Beneficial effect of the present invention is:
1) the present invention compares with existing temperature measuring equipment and has that temperature-measuring range is big, precision is high, advantages such as long-term continuously measured;
2) the present invention compares with present artificial experience estimation silicon rod diameter and growth rate, and having can be continuously, the accurate advantage of measurement;
3) the present invention compares with the existing fixed master mode, has to be directed against the different type of furnaces and operating mode, and the advantage of corresponding closed-loop optimizing control models is provided.
Description of drawings
Fig. 1 is a system architecture functional block diagram of the present invention.
Fig. 2 optimizing control models synoptic diagram of the present invention,
Fig. 3 is a surface temperature monitoring result synoptic diagram in the silicon rod process of growth.
Fig. 4 is a silicon rod diameter monitoring result synoptic diagram in the silicon rod process of growth.
Embodiment
When doing furtherly to the present invention, but should not limit protection scope of the present invention with this below in conjunction with instance and accompanying drawing.
Structure of the present invention is formed as shown in Figure 1.
Polycrystalline silicon reducing furnace many reference amounts on-line monitoring and optimal control device; It is characterized in that; Include many reference amounts infrared monitoring probe 1, infrared image processing and vision measurement module 2, process optimization control module 3; Many reference amounts infrared monitoring probe 1 includes near-infrared optical system 4, image capture module 5; The water-cooled shield cap is equipped with in many reference amounts infrared monitoring probe outside, and the front end of water-cooled shield cap is provided with water-cooling type and seals withstand voltage observation window, and many reference amounts infrared monitoring probe is deep in the polycrystalline silicon reducing furnace; Infrared image processing and vision measurement module 2 include infrared image processing module and vision measurement module; Data acquisition module 6, image processing module 7 that the infrared image processing module links to each other successively; The vision measurement module includes color comparison temperature measurement module 8, diameter measurement module 9; The output terminal of image processing module 7 is connected with color comparison temperature measurement module 8, diameter measurement module 9 respectively; The output terminal of color comparison temperature measurement module 8, diameter measurement module 9 all inserts data output interface 12, user interface 10; Data output interface is circumscribed with process optimization control module 3, the external indicating meter 11 of user interface, and process optimization control module 3 is connected with former system through a data interface.
Process optimization control module 3 is closed-loop optimization control model.
The method of polycrystalline silicon reducing furnace many reference amounts on-line monitoring and optimal control comprises following concrete steps:
1) many reference amounts infrared monitoring probe 1 is through choosing optimum infrared band and highly sensitive infrared CCD camera; Obtain the picture signal of silicon rod growth in the stove through near-infrared optical system 4, infrared CCD camera; And carry out A/D through data acquisition module 6 and change, obtain the infrared digital image of polysilicon rod;
2) infrared digital image of above-mentioned acquisition is sent into image processing module 7; And through image processing module 7 carry out the image pre-treatment with cut apart; In conjunction with concrete image,, protected imaging surface temperature distribution characteristic to greatest extent through image denoising algorithm and level and smooth filtering algorithm; Find out the edge of sealing through carrying out the profile tracking, and carry out sub-pixel rim detection and fitting of a straight line, obtain the image border of degree of precision;
3) above-mentioned processed images is transported in the diameter measurement module 9 of vision measurement module; The demarcation of at first carrying out the infrared CCD camera obtains the inside and outside parameter of camera; Carry out choosing of primary objective image border according to Hough fitting of a straight line algorithm, then image is carried out the tracking at edge, zonule; , the fundamental matrix that robustness is estimated carries out corresponding point matching under instructing; At last, pixel value and the effective unit system yardstick measured are converted, obtain the real-time diameter data of silicon rod according to above algorithm;
4) image of handling in the step 2 is transported in the color comparison temperature measurement module 8; Utilize the image processing system in the color comparison temperature measurement module that image is gone bad correction a little; To image cut apart, smoothly, layering, gradation conversion, call DB then, grey scale curve is carried out match; Temperature is demarcated, accomplish thermometric;
5) with the silicon rod diameter and the surface temperature data that obtain in the step 3,4, be transported in the process optimization control module 3, set up optimizing control models, instruct silicon rod under reasonable process conditions, to grow with feedback in conjunction with work information through data output interface;
6) silicon rod diameter and the surface temperature data with above-mentioned acquisition output to the terminal, obtain the real-time diameter and the growth rate of silicon rod, and the real time temperature of silicon rod surface any point, and in indicating meter 11, show.
Inventive principle of the present invention is following:
In the vision measurement module, according to the real-time growth diameter of the captured silicon rod growth image amount of measuring silicon rod.
(1) demarcation of camera system
The pixel value that will in picture processing, obtain is converted into effective unit system scale-value, needs calibration system, promptly confirms how much shooting models of camera.Known spatial target three-dimensional point homogeneous coordinates are
; Its corresponding two-dimentional picture point homogeneous coordinates are
, and the projective rejection between spatial point
and the picture point
does
Utilize least square solution overdetermination system of linear equations, provide external parameter; Find the solution inner parameter,, can solve,, then find the solution through the optimization searching of a ternary if there is radial distortion by an overdetermination linear equation if pick up camera does not have lens distortion.Finally solve inside and outside parameter, focal distance f, coefficient of radial distortion k, rotation matrix R and translation vector T.
(2) rim detection and Hough fitting of a straight line
Rim detection utilizes single order and second dervative to detect based on the discontinuity of sensed luminance value.(x, gradient y) is defined as vector to two-dimensional function f
This vectorial amplitude is
Generally be reduced to
Their values in constant brightness region are zero.
Use Hough conversion carrying out line to detect and link and at first will do the peak value detection; Find and include peaked Hough converter unit; Hough converter unit in the peak neighborhood of a point that finds is made as 0, repeats this step, till finding the peak value that needs.For each peak value, find the synthetic line segment of the relevant pixel groups in position.
(3) image corresponding point matching
Above-mentioned detected unique point is mated, promptly find out the picture point in the different images of corresponding the same space point.
Suppose to take two width of cloth pictures for the silicon rod of synchronization; The characteristic of correspondence point set is
in two width of cloth images; X (x, y, 1), x ' (x '; Y ', 1) representes the homogeneous coordinates of the corresponding points of left and right pick up camera respectively.Definition by fundamental matrix can know,
Wherein,
, satisfy constraint || f||=1;
After obtaining fundamental matrix and three-dimensional accurately matching point with the robustness algorithm for estimating,, fundamental matrix carries out more corresponding point matching under instructing.
(4) foundation of optimizing control models
Through the process variable that measurement is obtained, combine work information to set up optimizing control models again, instruct silicon rod growth rationally to carry out, reduce cost, improve the quality of products to reach and the purpose of energy-saving and emission-reduction
The color comparison temperature measurement method of color comparison temperature measurement system is following:
Thermodynamic temperature is the general object of T, and its radiation and distribution are described by the Planck radiation law:
In the formula, M
E λBe spectrum spoke out-degree, wherein λ is a wavelength, and T is a thermodynamic temperature, C
1=3.741832 * 10
-12Wcm
2Be first radiation constant, C
2=1.438786 * 10
4μ mK is a second radiation constant; Work as c
2/ λ T>>1 o'clock, planck formula can be replaced by Wien equation, can be reduced to:
< in the 2698 μ mK zones, the error of Wien equation and planck formula is less than 1% at λ T;
If two wavelength X
1And λ
2Measure the spectrum spoke out-degree M (T, the λ that send by the object same point simultaneously down,
1) and M (T, λ
2), then can this temperature according to both ratio, formula is:
Suppose
; Be proximately to be used as grey body to object and to handle, then formula (9) can be reduced to:
This is the calculation formula of two-color thermometry.
Claims (4)
1. polycrystalline silicon reducing furnace many reference amounts on-line monitoring and optimal control device; It is characterized in that; Include many reference amounts infrared monitoring probe, infrared image processing and vision measurement module, process optimization control module; Described many reference amounts infrared monitoring probe includes near-infrared optical system, image capture module; The water-cooled shield cap is equipped with in many reference amounts infrared monitoring probe outside, and the front end of water-cooled shield cap is provided with water-cooling type and seals withstand voltage observation window, and many reference amounts infrared monitoring probe is deep in the polycrystalline silicon reducing furnace; Described infrared image processing and vision measurement module include infrared image processing module and vision measurement module; Data acquisition module, image processing module that the infrared image processing module links to each other successively; The vision measurement module includes color comparison temperature measurement module, diameter measurement module; The output terminal of image processing module is connected with color comparison temperature measurement module, diameter measurement module respectively, and the output terminal of color comparison temperature measurement module, diameter measurement module all inserts data output interface, user interface, and data output interface is circumscribed with the process optimization control module; The external indicating meter of user interface, the process optimization control module is connected with former system through a data interface.
2. polycrystalline silicon reducing furnace many reference amounts on-line monitoring according to claim 1 and optimal control device is characterized in that, described process optimization control module is a closed-loop optimization control model.
3. polycrystalline silicon reducing furnace many reference amounts on-line monitoring according to claim 1 and optimal control device is characterized in that, described image capture module is the infrared CCD camera.
4. the method for polycrystalline silicon reducing furnace many reference amounts on-line monitoring and optimal control is characterized in that, comprises following concrete steps:
Many reference amounts infrared monitoring probe is through choosing optimum infrared band and highly sensitive infrared CCD camera; Obtain the picture signal of silicon rod growth in the stove through near-infrared optical system, infrared CCD camera; And carry out A/D through data acquisition module and change, obtain the infrared digital image of polysilicon rod;
2) infrared digital image of above-mentioned acquisition is sent into image processing module; And through image processing module carry out the image pre-treatment with cut apart; In conjunction with concrete image,, protected imaging surface temperature distribution characteristic to greatest extent through image denoising algorithm and level and smooth filtering algorithm; Find out the edge of sealing through carrying out the profile tracking, and carry out sub-pixel rim detection and fitting of a straight line, obtain the image border of degree of precision;
3) above-mentioned processed images is transported in the diameter measurement module of vision measurement module; The demarcation of at first carrying out the infrared CCD camera obtains the inside and outside parameter of camera; Carry out choosing of primary objective image border according to Hough fitting of a straight line algorithm, then image is carried out the tracking at edge, zonule; , the fundamental matrix that robustness is estimated carries out corresponding point matching under instructing; At last, pixel value and the effective unit system yardstick measured are converted, obtain the real-time diameter data of silicon rod according to above algorithm;
4) image of handling in the step 2 is transported in the color comparison temperature measurement module; Utilize the image processing system in the color comparison temperature measurement module that image is gone bad correction a little; To image cut apart, smoothly, layering, gradation conversion, call DB then, grey scale curve is carried out match; Temperature is demarcated, accomplish thermometric;
5) with the silicon rod diameter and the surface temperature data that obtain in the step 3,4, be transported in the process optimization control module, set up optimizing control models, instruct silicon rod under reasonable process conditions, to grow with feedback in conjunction with work information through data output interface;
6) silicon rod diameter and the surface temperature data with above-mentioned acquisition output to the terminal, obtain the real-time diameter and the growth rate of silicon rod, and the real time temperature of silicon rod surface any point, and in indicating meter, show.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2012102038201A CN102795627B (en) | 2012-06-19 | 2012-06-19 | Multi-parameter online monitoring and optimizing control device and method of polycrystalline silicon reduction furnace |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2012102038201A CN102795627B (en) | 2012-06-19 | 2012-06-19 | Multi-parameter online monitoring and optimizing control device and method of polycrystalline silicon reduction furnace |
Publications (2)
Publication Number | Publication Date |
---|---|
CN102795627A true CN102795627A (en) | 2012-11-28 |
CN102795627B CN102795627B (en) | 2013-12-25 |
Family
ID=47194973
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2012102038201A Expired - Fee Related CN102795627B (en) | 2012-06-19 | 2012-06-19 | Multi-parameter online monitoring and optimizing control device and method of polycrystalline silicon reduction furnace |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN102795627B (en) |
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2014090994A2 (en) * | 2012-12-14 | 2014-06-19 | Sikora Ag | Method and device for contactlessly determining the temperature of a moving object having an unknown degree of emission |
CN104535003A (en) * | 2014-11-29 | 2015-04-22 | 内蒙古神舟硅业有限责任公司 | Detection device and detection method for detecting the growth rate and diameter of polycrystalline silicon rod |
CN104562194A (en) * | 2013-10-24 | 2015-04-29 | 上海西门子工业自动化有限公司 | Technical process control method |
CN105043552A (en) * | 2015-04-24 | 2015-11-11 | 中国科学院西安光学精密机械研究所 | Display and calibration method for chromometry-based temperature measurement system |
CN110182811A (en) * | 2019-06-12 | 2019-08-30 | 新疆协鑫新能源材料科技有限公司 | A kind of reduction furnace auxiliary imaging system and autocontrol method |
TWI690705B (en) * | 2017-12-05 | 2020-04-11 | 德商瓦克化學公司 | Method for determining a surface temperature |
CN111591997A (en) * | 2020-06-15 | 2020-08-28 | 亚洲硅业(青海)股份有限公司 | Automatic control method for polycrystalline silicon reduction furnace |
CN113483662A (en) * | 2021-04-29 | 2021-10-08 | 大连耐视科技有限公司 | Visual detection device for improving crystal pulling quality |
CN113544090A (en) * | 2019-07-16 | 2021-10-22 | 瓦克化学股份公司 | Method for preparing polycrystalline silicon |
CN113834585A (en) * | 2021-09-24 | 2021-12-24 | 中国恩菲工程技术有限公司 | Silicon rod detection method, system, device, medium and electronic equipment in reduction furnace |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1553157A (en) * | 2003-12-12 | 2004-12-08 | 安徽大学特种电视技术研究中心 | Image temperature measuring apparatus based on color and near infrared double CCD |
CN101008103A (en) * | 2006-12-28 | 2007-08-01 | 西安理工大学 | Hough transform based CZ monocrystal silicon bar diameter measuring method |
CN101566503A (en) * | 2009-04-30 | 2009-10-28 | 彭小奇 | High-temperature field measuring instrument of CCD image sensor |
-
2012
- 2012-06-19 CN CN2012102038201A patent/CN102795627B/en not_active Expired - Fee Related
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1553157A (en) * | 2003-12-12 | 2004-12-08 | 安徽大学特种电视技术研究中心 | Image temperature measuring apparatus based on color and near infrared double CCD |
CN101008103A (en) * | 2006-12-28 | 2007-08-01 | 西安理工大学 | Hough transform based CZ monocrystal silicon bar diameter measuring method |
CN101566503A (en) * | 2009-04-30 | 2009-10-28 | 彭小奇 | High-temperature field measuring instrument of CCD image sensor |
Cited By (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2014090994A2 (en) * | 2012-12-14 | 2014-06-19 | Sikora Ag | Method and device for contactlessly determining the temperature of a moving object having an unknown degree of emission |
WO2014090994A3 (en) * | 2012-12-14 | 2014-09-04 | Sikora Ag | Method and device for contactlessly determining the temperature of a moving object having an unknown degree of emission |
US9804030B2 (en) | 2012-12-14 | 2017-10-31 | Sikora Ag | Method and device for contactlessly determining the temperature of a moving object having an unknown degree of emission |
CN104562194A (en) * | 2013-10-24 | 2015-04-29 | 上海西门子工业自动化有限公司 | Technical process control method |
CN104562194B (en) * | 2013-10-24 | 2017-05-31 | 西门子工厂自动化工程有限公司 | The temprature control method of polysilicon production process |
CN104535003A (en) * | 2014-11-29 | 2015-04-22 | 内蒙古神舟硅业有限责任公司 | Detection device and detection method for detecting the growth rate and diameter of polycrystalline silicon rod |
CN104535003B (en) * | 2014-11-29 | 2017-06-30 | 内蒙古神舟硅业有限责任公司 | The detection means and detection method of a kind of polycrystalline silicon rod speed of growth and diameter |
CN105043552A (en) * | 2015-04-24 | 2015-11-11 | 中国科学院西安光学精密机械研究所 | Display and calibration method for chromometry-based temperature measurement system |
CN105043552B (en) * | 2015-04-24 | 2018-03-02 | 中国科学院西安光学精密机械研究所 | Colorimetric temperature measurement system is shown and scaling method |
TWI690705B (en) * | 2017-12-05 | 2020-04-11 | 德商瓦克化學公司 | Method for determining a surface temperature |
KR20200074183A (en) * | 2017-12-05 | 2020-06-24 | 와커 헤미 아게 | How to determine the surface temperature |
CN111527242A (en) * | 2017-12-05 | 2020-08-11 | 瓦克化学股份公司 | Method for determining surface temperature |
CN111527242B (en) * | 2017-12-05 | 2021-09-07 | 瓦克化学股份公司 | Method for determining surface temperature |
US11515184B2 (en) | 2017-12-05 | 2022-11-29 | Wacker Chemie Ag | Method for determining a surface temperature |
CN110182811A (en) * | 2019-06-12 | 2019-08-30 | 新疆协鑫新能源材料科技有限公司 | A kind of reduction furnace auxiliary imaging system and autocontrol method |
CN113544090A (en) * | 2019-07-16 | 2021-10-22 | 瓦克化学股份公司 | Method for preparing polycrystalline silicon |
CN113544090B (en) * | 2019-07-16 | 2024-06-04 | 瓦克化学股份公司 | Method for preparing polycrystalline silicon |
CN111591997A (en) * | 2020-06-15 | 2020-08-28 | 亚洲硅业(青海)股份有限公司 | Automatic control method for polycrystalline silicon reduction furnace |
CN113483662A (en) * | 2021-04-29 | 2021-10-08 | 大连耐视科技有限公司 | Visual detection device for improving crystal pulling quality |
CN113834585A (en) * | 2021-09-24 | 2021-12-24 | 中国恩菲工程技术有限公司 | Silicon rod detection method, system, device, medium and electronic equipment in reduction furnace |
CN113834585B (en) * | 2021-09-24 | 2024-04-05 | 中国恩菲工程技术有限公司 | Method, system, device, medium and electronic equipment for detecting silicon rod in reduction furnace |
Also Published As
Publication number | Publication date |
---|---|
CN102795627B (en) | 2013-12-25 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN102795627B (en) | Multi-parameter online monitoring and optimizing control device and method of polycrystalline silicon reduction furnace | |
CN102183237B (en) | Device and method for measuring two-waveband cloud height of foundation | |
CN103196564B (en) | Infrared thermal imaging temperature measuring method by correcting surface emissivity through image segmentation | |
CN103134599A (en) | Method and system for real-time monitoring of molten bath state in direct molding process of laser metal | |
CN202865254U (en) | Converter flame temperature detection system | |
CN116879308A (en) | Industrial machine vision system image processing method | |
CN101506634A (en) | Method and device for measuring surface temperature of continuous casting ingot | |
CN103383360A (en) | Thin strip continuous casting billet surface defect sinusoidal grating phase shifting detection device and method | |
CN104215334A (en) | Real-time online monitoring method of temperature of molten steel in RH refining furnace | |
CN102634632A (en) | System and method for detecting temperature of converter flame | |
CN102181598B (en) | Prejudgment and control method of tapping and slagging of converter based on thermal image | |
CN101905293A (en) | High-temperature slab imaging temperature detecting system in secondary cooling zone of continuous casting machine and temperature detecting method thereof | |
CN110182811A (en) | A kind of reduction furnace auxiliary imaging system and autocontrol method | |
CN108279071A (en) | Full filed temperature field of molten pool detecting system based on two-color thermometry | |
CN100353152C (en) | Method for monitoring temperature of rotary kiln barrel through infrared scanning | |
CN111337132B (en) | Temperature measuring method and device and digital image acquisition equipment | |
CN107248157A (en) | A kind of aluminium cell sees the method and its device of fire automatically | |
CN108871189B (en) | Slag position detection device and detection method for metal smelting slag discharge | |
CN108344742B (en) | Sapphire inoculation detection device and method based on multi-frame image motion information | |
CN109341542A (en) | Method and its monitoring device based on digital signal sequences length identification fracture width | |
Zhang et al. | Online surface temperature measurement of billets in secondary cooling zone end-piece based on data fusion | |
EP2732067B1 (en) | Methods and systems for monitoring and controlling silicon rod temperature | |
CN103344187A (en) | Metallurgical product width on-line measurement device and method | |
CN108645522A (en) | Temperature field of molten pool detecting system based on colored CCD under CMT welding procedures | |
CN106197683B (en) | A kind of portable intelligent infrared temperature measurement system |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20131225 |