CN102793169A - Macadamia nut oil dropping pill and preparation method thereof - Google Patents
Macadamia nut oil dropping pill and preparation method thereof Download PDFInfo
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- CN102793169A CN102793169A CN2012103088848A CN201210308884A CN102793169A CN 102793169 A CN102793169 A CN 102793169A CN 2012103088848 A CN2012103088848 A CN 2012103088848A CN 201210308884 A CN201210308884 A CN 201210308884A CN 102793169 A CN102793169 A CN 102793169A
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- nut oil
- queensland nut
- macrogol
- oil droplet
- matrix
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- 235000018330 Macadamia integrifolia Nutrition 0.000 title claims abstract description 72
- 235000003800 Macadamia tetraphylla Nutrition 0.000 title claims abstract description 71
- 239000010466 nut oil Substances 0.000 title claims abstract description 61
- 239000006187 pill Substances 0.000 title claims abstract description 32
- 238000002360 preparation method Methods 0.000 title abstract description 7
- 240000000912 Macadamia tetraphylla Species 0.000 title abstract 7
- 239000011159 matrix material Substances 0.000 claims abstract description 28
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000001828 Gelatine Substances 0.000 claims abstract description 9
- 229920002472 Starch Polymers 0.000 claims abstract description 9
- 229920000159 gelatin Polymers 0.000 claims abstract description 9
- 235000019322 gelatine Nutrition 0.000 claims abstract description 9
- 235000011187 glycerol Nutrition 0.000 claims abstract description 9
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims abstract description 9
- 229920000053 polysorbate 80 Polymers 0.000 claims abstract description 9
- 235000015424 sodium Nutrition 0.000 claims abstract description 9
- 239000011734 sodium Substances 0.000 claims abstract description 9
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 9
- 235000019698 starch Nutrition 0.000 claims abstract description 9
- 239000008107 starch Substances 0.000 claims abstract description 9
- 240000007575 Macadamia integrifolia Species 0.000 claims description 66
- TZBAVQKIEKDGFH-UHFFFAOYSA-N n-[2-(diethylamino)ethyl]-1-benzothiophene-2-carboxamide;hydrochloride Chemical compound [Cl-].C1=CC=C2SC(C(=O)NCC[NH+](CC)CC)=CC2=C1 TZBAVQKIEKDGFH-UHFFFAOYSA-N 0.000 claims description 19
- 239000002826 coolant Substances 0.000 claims description 18
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 15
- 229960003511 macrogol Drugs 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 15
- 230000004927 fusion Effects 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 8
- 238000009833 condensation Methods 0.000 claims description 7
- 230000005494 condensation Effects 0.000 claims description 7
- 239000012809 cooling fluid Substances 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 7
- 238000009413 insulation Methods 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 7
- 238000002844 melting Methods 0.000 claims description 7
- 230000008018 melting Effects 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- 238000005303 weighing Methods 0.000 claims description 7
- 239000011710 vitamin D Substances 0.000 claims description 5
- 229940046008 vitamin d Drugs 0.000 claims description 5
- 229930003427 Vitamin E Natural products 0.000 claims description 4
- 230000003078 antioxidant effect Effects 0.000 claims description 4
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims description 4
- 235000019165 vitamin E Nutrition 0.000 claims description 4
- 239000011709 vitamin E Substances 0.000 claims description 4
- 229940046009 vitamin E Drugs 0.000 claims description 4
- 229930003316 Vitamin D Natural products 0.000 claims description 3
- QYSXJUFSXHHAJI-XFEUOLMDSA-N Vitamin D3 Natural products C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CCCC(C)C)=C/C=C1\C[C@@H](O)CCC1=C QYSXJUFSXHHAJI-XFEUOLMDSA-N 0.000 claims description 3
- 239000003963 antioxidant agent Substances 0.000 claims description 3
- 235000006708 antioxidants Nutrition 0.000 claims description 3
- 235000019166 vitamin D Nutrition 0.000 claims description 3
- 150000003710 vitamin D derivatives Chemical class 0.000 claims description 3
- 229960005150 glycerol Drugs 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- 229940057838 polyethylene glycol 4000 Drugs 0.000 abstract 1
- 229940093429 polyethylene glycol 6000 Drugs 0.000 abstract 1
- 239000000244 polyoxyethylene sorbitan monooleate Substances 0.000 abstract 1
- 229940068968 polysorbate 80 Drugs 0.000 abstract 1
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 17
- 229920001030 Polyethylene Glycol 4000 Polymers 0.000 description 11
- 239000003921 oil Substances 0.000 description 9
- 235000019198 oils Nutrition 0.000 description 9
- 239000008118 PEG 6000 Substances 0.000 description 6
- 229920002584 Polyethylene Glycol 6000 Polymers 0.000 description 6
- 235000013399 edible fruits Nutrition 0.000 description 6
- 238000000227 grinding Methods 0.000 description 5
- 239000002932 luster Substances 0.000 description 5
- 238000000465 moulding Methods 0.000 description 5
- 239000008188 pellet Substances 0.000 description 5
- 239000002253 acid Substances 0.000 description 4
- 229940008099 dimethicone Drugs 0.000 description 4
- 239000004205 dimethyl polysiloxane Substances 0.000 description 4
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 4
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 4
- 235000013361 beverage Nutrition 0.000 description 3
- JZZIHCLFHIXETF-UHFFFAOYSA-N dimethylsilicon Chemical compound C[Si]C JZZIHCLFHIXETF-UHFFFAOYSA-N 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000004519 grease Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- 150000002978 peroxides Chemical class 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 239000010779 crude oil Substances 0.000 description 2
- UKMSUNONTOPOIO-UHFFFAOYSA-N docosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCC(O)=O UKMSUNONTOPOIO-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000284 extract Substances 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 230000036449 good health Effects 0.000 description 2
- 235000021281 monounsaturated fatty acids Nutrition 0.000 description 2
- 235000014571 nuts Nutrition 0.000 description 2
- SECPZKHBENQXJG-FPLPWBNLSA-N palmitoleic acid Chemical compound CCCCCC\C=C/CCCCCCCC(O)=O SECPZKHBENQXJG-FPLPWBNLSA-N 0.000 description 2
- 229960001295 tocopherol Drugs 0.000 description 2
- 239000011732 tocopherol Substances 0.000 description 2
- YZAZXIUFBCPZGB-QZOPMXJLSA-N (z)-octadec-9-enoic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O.CCCCCCCC\C=C/CCCCCCCC(O)=O YZAZXIUFBCPZGB-QZOPMXJLSA-N 0.000 description 1
- 235000021357 Behenic acid Nutrition 0.000 description 1
- 241001070941 Castanea Species 0.000 description 1
- 235000014036 Castanea Nutrition 0.000 description 1
- 240000007049 Juglans regia Species 0.000 description 1
- 235000009496 Juglans regia Nutrition 0.000 description 1
- 235000021319 Palmitoleic acid Nutrition 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 229940116226 behenic acid Drugs 0.000 description 1
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- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 235000019219 chocolate Nutrition 0.000 description 1
- SECPZKHBENQXJG-UHFFFAOYSA-N cis-palmitoleic acid Natural products CCCCCCC=CCCCCCCCC(O)=O SECPZKHBENQXJG-UHFFFAOYSA-N 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 239000008157 edible vegetable oil Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000007962 solid dispersion Substances 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 235000019871 vegetable fat Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
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- Cosmetics (AREA)
Abstract
The invention provides a macadamia nut oil dropping pill which comprises macadamia nut oil and a matrix, wherein the matrix is one or combination of multiple components in polyethylene glycol 4000, polyethylene glycol 6000, glycerin gelatine, polysorbate-80 and sodium carboxymethyl starch; and the mass ratio of the macadamia nut oil to the matrix is (1: 2)-(1: 6). The invention also provides a preparation method of the macadamia nut oil dropping pill. The macadamia nut oil dropping pill is small in size, light in weight, good in stability and hard in oxidation-hydrolysis, and has the advantages that the macadamia nut oil dropping pill is convenient to carry on and take, is environment-friendly, safe, etc.
Description
Technical field
The invention belongs to the vegetable fat field, be specifically related to a kind of Queensland nut oil droplet ball and preparation method thereof.
Background technology
Queensland nut (Macadamia integrifolia) belongs to the Proteaceae Queensland nut and belongs to, and has another name called Hawaii fruit, Australia English walnut, Queensland's chestnut.Originate in the coastal hylaeion hypotropicum between 25～31 ° in the northern south latitude in the Queensland, Australia southeast and Xin Nan Weir state.Existing main product is in states such as Australia, the U.S., Brazil.China introduced a fine variety about 1910 greatly, 7 provinces and cities (autonomous region) popularizing planting in China south China so far, and the existing Yunnan that mainly is distributed in is regional with Guangdong and Guangxi Provinces.The edible part of Queensland nut is a kernel, and the kernel crisp-fried is sliding tender good to eat, and unique cream fragrance is arranged, and is the edible with fruit of performance optimal in the world, " dry fruit queen " is arranged, the laudatory title of " king of world's nut ".Its kernel oil content is up to (containing monounsaturated fatty acids more than 80% in the clean fruit oil) more than 70%, and wherein the main component of unrighted acid is palmitoleic acid, oleic acid ((Z)-9-octadecenoic acid), mountain Yu acid (behenic acid).Owing to be rich in monounsaturated fatty acids, modern medicine study shows that Queensland nut oil helps to reduce the cholesterol level in the blood of human body, and then helps to prevent and reduce the generation of angiocardiopathy, and human body is had the good health care function.
Present existing process technology is normally added finished kernel in the foods such as chocolate, cake directly edible, perhaps kernel is processed into beverage and drinks.But the Queensland nut oil content is high, and grease directly gets into beverage and causes beverage mouthfeel not good, does not meet the requirement of modern society to health food; Secondly extracts to take after refining and can reach health-care effect better, yet contained grease is a unrighted acid that the easy oxidation of grease produces peroxide, has unsafe factor.Therefore, develop a kind of healthy and safe, the Queensland nut of good health care effect oil health product and processing method and necessity thereof.
Summary of the invention
The objective of the invention is provides a kind of healthy and safe to the above technical problem that will solve, and fruit oiliness matter stability is high and use Queensland nut oil droplet ball easy to carry.
Another object of the present invention provides a kind of method for preparing said Queensland nut oil droplet ball.
The object of the invention is achieved through following technical scheme:
Queensland nut oil droplet ball of the present invention; Comprise Queensland nut oil and matrix; Wherein, Said matrix is one or more the mixture in Macrogol 4000, Macrogol 6000, glycerin gelatine, Tween-80, the sodium carboxymethyl starch, and said Queensland nut oil is 1:2～1:6 with the mass ratio of said matrix.
Preferably, said Queensland nut oil is 1:4～1:6 with the mass ratio of said matrix.
The preferred supercritical CO that adopts of said Queensland nut oil
2Fluid extraction technology extracts from the Queensland nut kernel and makes.
Preferably, said matrix is the mixture of Tween-80 and Macrogol 4000, and said Tween-80 is 1:5 with the ratio of the quality of said Macrogol 4000.
Preferably, said matrix is the mixture of sodium carboxymethyl starch, Macrogol 4000 and Macrogol 6000, and said sodium carboxymethyl starch, said Macrogol 4000 are 1:2:1 with the ratio of the quality of said Macrogol 6000.
Preferably, said matrix is the mixture of Macrogol 4000 and Macrogol 6000, and said Macrogol 4000 is 3:1 with the ratio of the quality of said Macrogol 6000.
Preferably, said matrix is the mixture of Macrogol 4000, Macrogol 6000 and glycerin gelatine, and said Macrogol 4000, said Macrogol 6000 are 2:1:1 with the ratio of the quality of said glycerin gelatine.
For further strengthening the antioxidant effect of said Queensland nut oil droplet ball, preferably, also contain anti-oxidant in the said Queensland nut oil droplet ball.Said anti-oxidant is preferably vitamin E.
Preferably, also contain vitamin D in the said Queensland nut oil droplet ball.
Preferably, also contain vitamin E in the said Queensland nut oil droplet ball.
The present invention also provides a kind of method for preparing said Queensland nut oil droplet ball, and it may further comprise the steps:
(1) takes by weighing each component according to quantity;
(2) said matrix is heated to fusion in 60～90 ℃, said Queensland nut oil is added wherein mix again, heating and melting stirs to complete fusion, pours in the dripping pill device in 80～90 ℃ of insulations 10 minutes;
(3) above-mentioned fused materials is evenly splashed in the cooling agent through water dropper, drip and process ball, remove the cooling agent on surface, dry naturally; Wherein, The temperature of said water dropper is 50～80 ℃, and dripping speed when dripping the system dripping pill is 20～40 droplets/minute, and dripping distance is 4～6 centimetres; Cooling fluid upper temp (being mouth of pipe temperature) in the said dripping pill device condensation column is that 60～90 ℃, bottom temp are 0～15 ℃, and the temperature of cooling agent is 10～15 ℃.
Said cooling agent is preferably dimethicone, atoleine or vegetable oil.The chilling temperature of said cooling agent is preferably 10～15 ℃.
The preparation method of Queensland nut oil droplet ball involved in the present invention compares with existing process technology has following characteristics:
1, Queensland nut oil droplet ball involved in the present invention; Utilize various surfactants such as polyethylene glycol etc. to be matrix; Process solid dispersion with Queensland nut oil, not only make fruit oil in matrix, be the high degree of dispersion state, also owing to after fused with matrix; Reduce and the air contact area, can keep its active component to greatest extent.Simultaneously, this Queensland nut oil droplet ball volume is little, in light weight, have be convenient to carry, taking convenience, good stability, be difficult for the characteristics of oxydrolysis;
2, the Queensland nut oil droplet ball that the present invention relates to need not to add colouring agent, plasticizer, anticorrisive agent, practices thrift cost of supplementary product, reduces the safety problem of using additive to bring simultaneously.
The mode of production of the Queensland nut oil droplet ball that 3, the present invention adopted has characteristics with short production cycle, that process equipment is simple, automaticity is high, production cost is low, labour intensity is low.Simultaneously, operate under the liquid state and carry out, the process no dust pollution helps labour protection and environmental protection.
The specific embodiment
Below in conjunction with specific embodiment technical scheme of the present invention is done further to detail.But the present invention is not limited to following examples.
Embodiment 1
Taking by weighing mass ratio according to quantity is Queensland nut oil and the Macrogol 4000 (PEG4000) of 1:2.
PEG4000 is heated to fusion in 60 ℃, Queensland nut oil is mixed grinding well again with PEG4000, heating and melting stirs; To fusion fully, pour in the dripping pill device 80 ℃ of insulations into; Behind the 10min, fused materials evenly splashes in the dimethyl-silicon oil coolant through water dropper, and the water dropper temperature is 50 ℃; Dripping speed is 20 droplets/minute, drips apart from be 6cm, and the interior cooling fluid upper temp of said dripping pill device condensation column is that 90 ℃, bottom temp are 15 ℃.Coolant temperature is 15 ℃, leaches piller after the moulding, inhales the dimethicone that goes to the dripping pill surface with filter paper, dries naturally under the room temperature, promptly makes Queensland nut oil droplet ball.
More than made dripping pill profile rounding, the color and luster homogeneous, hardness is moderate, its dissolve scattered time limit is less than 30min, pellet sizes is even, the ball method of double differences is different from 8%.
Embodiment 2
Taking by weighing mass ratio according to quantity is Queensland nut oil, Tween-80 and the PEG4000 of 1:1:5.
Tween-80 and PEG4000 are heated to fusion in 90 ℃, Queensland nut oil are mixed grinding well again with matrix, heating and melting stirs; To fusion fully, pour in the dripping pill device 80 ℃ of insulations into; Behind the 10min, fused materials evenly splashes in the atoleine cooling agent through water dropper, and the water dropper temperature is 75 ℃; Dripping speed is 30 droplets/minute, drips apart from be 6cm, and the interior cooling fluid upper temp of said dripping pill device condensation column is that 65 ℃, bottom temp are 12 ℃.Coolant temperature is 15 ℃, leaches piller after the moulding, inhales the atoleine that goes to the dripping pill surface with filter paper, dries naturally under the room temperature, promptly makes Queensland nut oil droplet ball.
More than made dripping pill profile rounding, the color and luster homogeneous, hardness is moderate, its dissolve scattered time limit is less than 30min, pellet sizes is even, the ball method of double differences is different from 8%.
Embodiment 3
Taking by weighing mass ratio according to quantity is Queensland nut oil, sodium carboxymethyl starch, PEG4000 and the PEG6000 (Macrogol 6000) of 1:1:2:1.
Sodium carboxymethyl starch, PEG4000 and PEG6000 are heated to fusion in 80 ℃, Queensland nut oil are mixed grinding well again with matrix, heating and melting stirs; To fusion fully, pour in the dripping pill device 85 ℃ of insulations into; Behind the 10min, fused materials evenly splashes in the dimethyl-silicon oil coolant through water dropper, and the water dropper temperature is 50 ℃; Dripping speed is 40 droplets/minute, drips apart from be 5cm, and the interior cooling fluid upper temp of said dripping pill device condensation column is that 60 ℃, bottom temp are 0 ℃.Coolant temperature is 10 ℃, leaches piller after the moulding, inhales the dimethicone that goes to the dripping pill surface with filter paper, dries naturally under the room temperature, promptly makes Queensland nut oil droplet ball.
More than made dripping pill profile rounding, the color and luster homogeneous, hardness is moderate, its dissolve scattered time limit is less than 30min, pellet sizes is even, the ball method of double differences is different from 8%.
Embodiment 4
Preparation B B-complex E Queensland nut oil droplet ball.
Taking by weighing mass ratio according to quantity is Queensland nut oil-tocopherol admixture, PEG4000 and the PEG6000 of 1:3:1.Wherein, the weight of vitamin E is 2/1000ths of Queensland nut weight of oil.
PEG4000 and PEG6000 are heated to fusion in 90 ℃, Queensland nut oil-tocopherol admixture are mixed grinding well again with matrix, heating and melting stirs; To fusion fully, pour in the dripping pill device 85 ℃ of insulations into; Behind the 10min, fused materials evenly splashes in the atoleine cooling agent through water dropper, and the water dropper temperature is 80 ℃; Dripping speed is 30 droplets/minute, drips apart from be 5cm, and the interior cooling fluid upper temp of said dripping pill device condensation column is that 70 ℃, bottom temp are 10 ℃.Coolant temperature is 10 ℃, leaches piller after the moulding, inhales the atoleine that goes to the dripping pill surface with filter paper, dries naturally under the room temperature, promptly makes Queensland nut oil droplet ball.
More than made dripping pill profile rounding, the color and luster homogeneous, hardness is moderate, its dissolve scattered time limit is less than 30min, pellet sizes is even, the ball method of double differences is different from 8%.
Embodiment 5
Preparation B B-complex D Queensland nut oil droplet ball.
Taking by weighing mass ratio according to quantity is Queensland nut oil-vitamin D mixture, PEG4000, PEG6000 and the glycerin gelatine of 1:2:1:1.Wherein, the weight of vitamin D is 2/1000ths of Queensland nut weight of oil.
PEG4000, PEG6000 and glycerin gelatine are heated to fusion in 70 ℃, Queensland nut oil-vitamin D mixture are mixed grinding well again with matrix, heating and melting stirs; To fusion fully, pour in the dripping pill device 90 ℃ of insulations into; Behind the 10min, fused materials evenly splashes in the dimethyl-silicon oil coolant through water dropper, and the water dropper temperature is 60 ℃; Dripping speed is 30 droplets/minute, drips apart from be 4cm, and the interior cooling fluid upper temp of said dripping pill device condensation column is that 80 ℃, bottom temp are 8 ℃.Coolant temperature is 10 ℃, leaches piller after the moulding, inhales the dimethicone that goes to the dripping pill surface with filter paper, dries naturally under the room temperature, promptly makes Queensland nut oil droplet ball.
More than made dripping pill profile rounding, the color and luster homogeneous, hardness is moderate, its dissolve scattered time limit is less than 30min, pellet sizes is even, the ball method of double differences is different from 8%.
Control Example: product stability is investigated experiment
For comparing embodiment 1～5 gained dripping pill and the stability that is not prepared into drops crude oil, analyze comparison according to " analytical method of GB/T5009.37-2003 edible vegetable oil sanitary standard " respectively, the result sees table 1.This oxidation experiment quickens to carry out under the experiment condition at 40 ℃.
The stability of table 1 crude oil and each embodiment relatively
Can know by the result, strengthen greatly, avoid generating the peroxide that has potential safety hazard after the oxidation of a large amount of unrighted acids by the stability of Queensland nut oil droplet ball provided by the invention.(peroxide value≤6.304meq/kg, GB 16326-2005 nut food hygienic standard)
Below only be concrete exemplary applications of the present invention, protection scope of the present invention is not constituted any limitation.Except that the foregoing description, the present invention can also have other embodiments.All employings are equal to the technical scheme of replacement or equivalent transformation formation, all drop within the present invention's scope required for protection.
Claims (10)
1. Queensland nut oil droplet ball; It is characterized in that comprising Queensland nut oil and matrix; Wherein, Said matrix is one or more the mixture in Macrogol 4000, Macrogol 6000, glycerin gelatine, Tween-80, the sodium carboxymethyl starch, and said Queensland nut oil is 1:2～1:6 with the mass ratio of said matrix.
2. Queensland nut oil droplet ball according to claim 1 is characterized in that: said Queensland nut oil is 1:4～1:6 with the mass ratio of said matrix.
3. Queensland nut oil droplet ball according to claim 1 and 2 is characterized in that: said matrix is the mixture of Tween-80 and Macrogol 4000, and said Tween-80 is 1:5 with the ratio of the quality of said Macrogol 4000.
4. Queensland nut oil droplet ball according to claim 1 and 2; It is characterized in that: said matrix is the mixture of sodium carboxymethyl starch, Macrogol 4000 and Macrogol 6000, and said sodium carboxymethyl starch, said Macrogol 4000 are 1:2:1 with the ratio of the quality of said Macrogol 6000.
5. Queensland nut oil droplet ball according to claim 1 and 2 is characterized in that: said matrix is the mixture of Macrogol 4000 and Macrogol 6000, and said Macrogol 4000 is 3:1 with the ratio of the quality of said Macrogol 6000.
6. Queensland nut oil droplet ball according to claim 1 and 2; It is characterized in that: said matrix is the mixture of Macrogol 4000, Macrogol 6000 and glycerin gelatine, and said Macrogol 4000, said Macrogol 6000 are 2:1:1 with the ratio of the quality of said glycerin gelatine.
7. Queensland nut oil droplet ball according to claim 1 and 2 is characterized in that: also contain anti-oxidant in the said Queensland nut oil droplet ball.
8. Queensland nut oil droplet ball according to claim 1 and 2 is characterized in that: also contain vitamin D in the said Queensland nut oil droplet ball.
9. Queensland nut oil droplet ball according to claim 1 and 2 is characterized in that: also contain vitamin E in the said Queensland nut oil droplet ball.
10. prepare the method for each said Queensland nut oil droplet ball of claim 1 to 9, it is characterized in that may further comprise the steps:
(1) takes by weighing each component according to quantity;
(2) said matrix is heated to fusion in 60～90 ℃, said Queensland nut oil is added wherein mix again, heating and melting stirs to complete fusion, pours in the dripping pill device in 80～90 ℃ of insulations 10 minutes;
(3) above-mentioned fused materials is evenly splashed in the cooling agent through water dropper, drip and process ball, remove the cooling agent on surface, dry naturally; Wherein, The temperature of said water dropper is 50～80 ℃, and dripping speed when dripping the system dripping pill is 20～40 droplets/minute, and dripping distance is 4～6 centimetres; Cooling fluid upper temp in the said dripping pill device condensation column is that 60～90 ℃, bottom temp are 0～15 ℃, and the temperature of cooling agent is 10～15 ℃.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210308884.8A CN102793169B (en) | 2012-08-27 | 2012-08-27 | Macadamia nut oil dropping pill and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210308884.8A CN102793169B (en) | 2012-08-27 | 2012-08-27 | Macadamia nut oil dropping pill and preparation method thereof |
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| CN102793169A true CN102793169A (en) | 2012-11-28 |
| CN102793169B CN102793169B (en) | 2014-04-02 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103462026A (en) * | 2013-10-08 | 2013-12-25 | 云南迪思企业集团坚果有限公司 | Macadamia nut oil capsule with stable quality and manufacturing method thereof |
| CN107969702A (en) * | 2017-12-05 | 2018-05-01 | 董悫 | A kind of macadimia nut oil oral liquid |
| CN109527336A (en) * | 2018-11-27 | 2019-03-29 | 宁夏春升源生物科技有限公司 | A method of sauce class flavouring is produced using pellet technology |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101606528A (en) * | 2009-07-23 | 2009-12-23 | 中国热带农业科学院南亚热带作物研究所 | A kind of soup composition and method of making the same and application of cottage propagation macadamia nut |
| CN102551054A (en) * | 2011-12-29 | 2012-07-11 | 广西壮族自治区药用植物园 | Walnut oil dropping pills and preparation method thereof |
-
2012
- 2012-08-27 CN CN201210308884.8A patent/CN102793169B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101606528A (en) * | 2009-07-23 | 2009-12-23 | 中国热带农业科学院南亚热带作物研究所 | A kind of soup composition and method of making the same and application of cottage propagation macadamia nut |
| CN102551054A (en) * | 2011-12-29 | 2012-07-11 | 广西壮族自治区药用植物园 | Walnut oil dropping pills and preparation method thereof |
Non-Patent Citations (4)
| Title |
|---|
| 《药学中级》 20070130 全国卫生专业技术资格考试专家委员会 第一章药剂学 人民卫生出版社 , * |
| 全国卫生专业技术资格考试专家委员会: "《药学中级》", 30 January 2007, 人民卫生出版社 * |
| 曾德惠等: "《滴丸剂的生产与理论》", 30 June 1994 * |
| 杜丽清等: "澳洲坚果果仁中粗脂肪与脂肪酸含量的变异分析", 《经济林研究》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103462026A (en) * | 2013-10-08 | 2013-12-25 | 云南迪思企业集团坚果有限公司 | Macadamia nut oil capsule with stable quality and manufacturing method thereof |
| CN107969702A (en) * | 2017-12-05 | 2018-05-01 | 董悫 | A kind of macadimia nut oil oral liquid |
| CN109527336A (en) * | 2018-11-27 | 2019-03-29 | 宁夏春升源生物科技有限公司 | A method of sauce class flavouring is produced using pellet technology |
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| CN102793169B (en) | 2014-04-02 |
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