CN102787462A - New rapid proofing method for cold pad batch dyeing - Google Patents

New rapid proofing method for cold pad batch dyeing Download PDF

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CN102787462A
CN102787462A CN2012102616714A CN201210261671A CN102787462A CN 102787462 A CN102787462 A CN 102787462A CN 2012102616714 A CN2012102616714 A CN 2012102616714A CN 201210261671 A CN201210261671 A CN 201210261671A CN 102787462 A CN102787462 A CN 102787462A
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gently
sample
reactive dyes
sealing bag
dyeing
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CN102787462B (en
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蒋志平
栾金鑫
孟胜锋
傅卫红
张志伟
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Zhejiang Yide New Material Co., Ltd
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ZHEJIANG YIDE CHEMICAL CO Ltd
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Abstract

The invention relates to a new rapid proofing method for cold pad batch dyeing. The method comprises the following steps of: (1) preparing the reactive dye pad dyeing solution which is consistent with the production formulation of a large sample, and using up reactive dye, penetrant solution and reactive dye cold pad batch alkaline agent which are mixed together in 40-90 minutes; (2) according to the soaking time and mangle expression which are consistent with the large sample production, alternately soaking and rolling a small cotton sample; (3) rolling the pad dyed small cotton sample along a glass rod which has the same breadth as the small cotton sample, putting the rolled small cotton sample into a plastic hermetic bag which is matched with the small cotton sample, extracting the gas in the plastic bag, and keeping tight; (4) slightly putting the plastic hermetic bag which contains the small cotton sample into a water bath of 20-40 DEG C to be banked up for 20-60 minutes in a thermal insulation manner, pulling the hermetic bag out, and putting the hermetic bag into a water bath of 40-70 DEG C to be banked up for 5-30 minutes in a thermal insulation manner, pulling the hermetic bag out, and taking the dyed cotton fabric out; and (5) according to the dyeing which is consistent with the technology of the large sample production, matching the colors of the small dyed cotton sample. The method has the following beneficial effects that the method is simple to operate, the requirements on the technological equipment are low, the proofing colors can be accurately produced by corresponding to the colors of the large sample, and delta E (DE) is not more than 1 according to color measurement committee (CMC).

Description

A kind of fast proofing new method that is used for cold-rolling heap staining
Technical field
The present invention relates to the field that dyeing use REACTIVE DYES mixing alkaline agent carries out cold-rolling heap staining, especially a kind of fast proofing new method that is used for cold-rolling heap staining.
Background technology
Dyeing uses REACTIVE DYES mixing alkaline agent to carry out cold-rolling heap staining production, during need stacking at room temperature about 24 hours, could accomplish dyeing.And full-page proof often need be beaten sample before cold-rolling heap staining; So that confirm dyeing prescription, dyeing when the full-page proof cold-rolling heap staining is produced; If yet cold-rolling heap staining is beaten sample and is also adopted the stacking at room temperature 24 hour time the same with the production of full-page proof cold-rolling heap staining; Then tend to incur loss through delay the full-page proof cold-rolling heap staining production schedule, finally incured loss through delay the product time of delivery because of beating the sample overlong time.
For this reason; The sample time method is all beaten actively groping how to shorten cold-rolling heap staining by many printing and dyeing producer; The present more employing micro-wave oven of printing and dyeing producer method, the baking oven method etc. of drawing a design of drawing a design, but because there is aberration greatly in the cotton color that the cotton color of beating sample and full-page proof are produced, and dyeing prescription, dyeing equally; Repeat to beat between the cotton color batch of sample at every turn and also exist big aberration; Its reason is that above-mentioned these method of drawing a design all exists dyeing temperature and can't stably be controlled at identical conditions, and the dyeing temperature fluctuation is bigger, causes beating the cotton color of sample and the big aberration of cotton color existence of full-page proof production.Therefore, look often will be repaiied by printing and dyeing mill after the production of full-page proof cold-rolling heap staining, had a strong impact on the raising of product quality stability and production efficiency like this.
Domestic document or patent report have also been arranged the cotton color that adopts the water bath with thermostatic control method of drawing a design to solve to beat sample and the full-page proof cotton color of producing have the problem of aberration greatly; Although obtained significant progress, put into practice the cotton color of dozen sample and the cotton color of full-page proof production and still have certain aberration.This mainly is because of beating actual state and the condition that little sample testing situation and condition are also not too produced near full-page proof.In addition, also ignored the cold rolling heap alkaline agent of REACTIVE DYES hydrolysis of reactive dye has been influenced this key factor.
Summary of the invention
The present invention is directed to above-mentioned defective, a kind of fast proofing new method that is used for cold-rolling heap staining is provided, simple to operate, process equipment requires low, can effectively shorten the time of beating sample, reduces the aberration of the cotton color of sample and the cotton color existence that full-page proof is produced.
For this reason, the present invention takes following technical scheme, and a kind of fast proofing new method that is used for cold-rolling heap staining comprises the following steps:
(1) the preparation REACTIVE DYES pad dyeing solution consistent with the full-page proof factory formula made in 40-90 minute after REACTIVE DYES, osmotic agent solution are mixed with the cold rolling heap alkaline agent of REACTIVE DYES and uses up;
(2) according to producing consistent dip time, pick-up rate, sample cotton one is soaked one roll with full-page proof;
(3) the identical fabric width with it in the sample dyed cotton fabric edge after the pad dyeing is long glass bar is reeled, and puts into the plastic sealing bag that matches with it, and extracts the gas in the plastic bag out, keeps sealing;
(4) sample dyed cotton fabric plastic sealing bag will be housed earlier, and put into 20-40 ℃ of water-bath gently, the plastic bag sealing mouth will be higher than liquid level; After insulation was banked up 20-60 minute, propose plastic sealing bag more gently, put into 40-70 ℃ of water-bath gently; After insulation was banked up 20-60 minute, propose plastic sealing bag more gently, put into 20-40 ℃ of water-bath gently; After insulation was banked up 5-30 minute, propose plastic sealing bag gently, take out the dyeing cloth specimen;
(5) according to the washing consistent with full-page proof production, soap, washing process dyes post processing, again with checking colors after the oven dry of sample dyed cotton fabric, pressing, the balance.
The cold rolling heap alkaline agent of described REACTIVE DYES wherein supplies alkaline constituents to comprise NaOH, potassium hydroxide, sodium carbonate, potash, tertiary sodium phosphate by supplying alkaline constituents, buffer components and filling components to form; Buffer components comprises sodium metasilicate, sodium metasilicate, sodium acid carbonate, saleratus, sodium hydrogen phosphate, calgon, trisodium citrate, potassium sodium tartrate; Filling components comprises sodium chloride, potassium chloride, sodium sulphate, potassium sulfate.
As preferably: REACTIVE DYES pad dyeing solution in the step (1), REACTIVE DYES, osmotic agent solution mix with the cold rolling heap alkaline agent of REACTIVE DYES then in 60 minutes, to make uses up, and sample dyed cotton fabric plastic sealing bag will be housed earlier in the step (4); Put into 30 ℃ of water-baths gently, after insulation was banked up 30 minutes, propose plastic sealing bag more gently; Put into 60 ℃ of water-baths gently, after insulation was banked up 30 minutes, propose plastic sealing bag more gently; Put into 30 ℃ of water-baths gently; After insulation was banked up 15 minutes, propose plastic sealing bag gently, take out the dyeing cloth specimen.
Quite slow in the step (1) owing to REACTIVE DYES hydrolysis in 40-90 minute; Make the pad dyeing solution of using up in the meantime; Can avoid REACTIVE DYES under alkali condition because of too fast hydrolysis, uncontrollable hydrolysis rate and causing is played the generation of this situation of color that the color of sample can't accurately corresponding full-page proof produces.According to producing consistent dip time, pick-up rate, sample cotton one is soaked one roll when doing little sample testing, actual state and the condition that can produce very much near full-page proof with full-page proof.
Glass bar in the step (2) that the identical fabric width with it in the sample dyed cotton fabric edge after the pad dyeing is long is reeled, and puts into the plastic sealing bag that matches with it, and drives the gas in the plastic bag away, sealing.Do actual state and condition that little sample testing can be produced near full-page proof very much like this, and can avoid the sample dyed cotton fabric pasting plastic bag because of monoblock, the dye liquor on the cotton is infected with plastic bag unevenly easily and is caused the final dyeing of cotton inhomogeneous.
It mainly is the stacking at room temperature environment that the simulation full-page proof is produced that the phase I of step of the present invention (4) and phase III bank up with 20-40 ℃ of water bath heat preservation; And second stage is banked up with 40-70 ℃ of water bath heat preservation; Can shorten the time of banking up greatly, through groping to test the color that the color of finding its dozen sample can very accurately corresponding full-page proof be produced, CMC DE≤1; And fix because of dyeing temperature, dyeing time; Adopt same dyeing prescription, dyeing, repeat to beat sample at every turn, the aberration between its batch does not have significant change basically.
The present invention has researched and solved the cold rolling heap alkaline agent of REACTIVE DYES influences this major issue to hydrolysis of reactive dye; Secondly will beat actual state and the condition that little sample testing situation and condition are produced near full-page proof as much as possible; Banking up through 40-70 ℃ of water bath heat preservation in the centre, banks up the time to shorten greatly.
Beneficial effect of the present invention is following:
(1) simple to operate, process equipment requires simple;
(2) adopt the fast proofing new method of this cold-rolling heap staining, can shorten greatly and beat the sample time, operated about about 2 hours front and back, just can accomplish dozen little sample testing.
(3) the sample dyed cotton fabric color even of being up to.
(4) beat the color of sample can be very accurately corresponding the full-page proof color of producing, CMC DE≤1.
(5) owing to prepared the cold rolling heap alkaline agent of new reactive dyes that hydrolysis of reactive dye is had good shock-absorbing capacity; All fix because of dyeing temperature, dyeing time simultaneously; Same dyeing prescription, dyeing repeat to beat sample at every turn, and the aberration between its batch does not have significant change basically.
Description of drawings
Fig. 1 is a process chart of the present invention.
The specific embodiment
Below in conjunction with specific embodiment, further set forth the present invention.
Embodiment 1
Experiment material: COTTON FABRIC mercerising bleaching semi-products (30cm * 10cm)
Dye the chemical drug article: the red 20g of REACTIVE DYES EDB, penetrating agent JFC, the cold rolling heap alkaline agent of REACTIVE DYES, the liquid of soaping (1-5g/L soap flakes, 1-5g/L soda ash).
Instrument and equipment: beaker, electronic balance, graduated pipette, volumetric flask, glass bar (long 11cm), salable plastic bag (20cm * 14cm), clip, padding machine, electric heating temperature controlled water bath pot, baking oven, electric iron, colour photometer.
The cold rolling heap dye solution prescription of table-1 REACTIVE DYES
Figure BDA0000193683251
The cold rolling heap alkaline agent of table-2 REACTIVE DYES solution prescription
Figure BDA0000193683252
The cold rolling heap alkaline agent prescription of table-3 REACTIVE DYES
1. technological process and condition
With dye liquor and the alkali lye mixed by 3-5:1-2, fabric soaks 2-5 second before padding, through the padding machine pressure rolling, and bundle roller pressure 2-5kg/cm 2, speed 5-25 rice/minute.(one soaks one rolls to pad dye liquor; Pick-up rate 70%) → and the glass bar coiling that the identical fabric width with it in the sample dyed cotton fabric edge after the pad dyeing is long, put into the plastic sealing bag that matches with it, and drive the gas in the plastic bag away; Sample dyed cotton fabric plastic sealing bag seal → will be housed earlier; Put into 20-40 ℃ of water-bath gently, the clip that the plastic bag sealing mouth will be higher than liquid level and be fixed in the top is clamped, insulation bank up 20-60 minute → plastic sealing bag proposed gently again; Put into 40-70 ℃ of water-bath gently; Insulation bank up 20-60 minute → plastic sealing bag is proposed gently again, put into 20-40 ℃ of water-bath gently, insulation bank up 5-30 minute → plastic sealing bag proposed gently; (1-5g/L soap flakes, 1-5g/L soda ash are checked colors after 95-100 ℃ * 10-15min) → hot water wash → cold wash → oven dry → pressing → balance to take out dyeing cloth specimen → washing → soap boiling.
Embodiment 2
Experiment material: COTTON FABRIC mercerising bleaching semi-products (30cm * 10cm)
Dye the chemical drug article: the yellow 20g of REACTIVE DYES EDB, penetrating agent JFC, the cold rolling heap alkaline agent of REACTIVE DYES, the liquid of soaping (1-5g/L soap flakes, 1-5g/L soda ash).
Instrument and equipment: beaker, electronic balance, graduated pipette, volumetric flask, glass bar (long 11cm), salable plastic bag (20cm * 14cm), clip, padding machine, electric heating temperature controlled water bath pot, baking oven, electric iron, colour photometer.
2. the dyeing leach mill solution is write out a prescription
The cold rolling heap dye solution prescription of table-1 REACTIVE DYES
Figure BDA0000193683254
The cold rolling heap alkaline agent of table-2 REACTIVE DYES solution prescription
Figure BDA0000193683255
The cold rolling heap alkaline agent prescription of table-3 REACTIVE DYES
Figure BDA0000193683256
3. technological process and condition
With dye liquor and the alkali lye mixed by 3-5:1-2, fabric soaks 2-5 second before padding, through the padding machine pressure rolling, and bundle roller pressure 2-5kg/cm 2, speed 5-25 rice/minute.(one soaks one rolls to pad dye liquor; Pick-up rate 70%) → and the glass bar coiling that the identical fabric width with it in the sample dyed cotton fabric edge after the pad dyeing is long, put into the plastic sealing bag that matches with it, and drive the gas in the plastic bag away; Sample dyed cotton fabric plastic sealing bag seal → will be housed earlier; Put into 20-40 ℃ of water-bath gently, the clip that the plastic bag sealing mouth will be higher than liquid level and be fixed in the top is clamped, insulation bank up 20-60 minute → plastic sealing bag proposed gently again; Put into 40-70 ℃ of water-bath gently; Insulation bank up 20-60 minute → plastic sealing bag is proposed gently again, put into 20-40 ℃ of water-bath gently, insulation bank up 5-30 minute → plastic sealing bag proposed gently; (1-5g/L soap flakes, 1-5g/L soda ash are checked colors after 95-100 ℃ * 10-15min) → hot water wash → cold wash → oven dry → pressing → balance to take out dyeing cloth specimen → washing → soap boiling.
Embodiment 3
Experiment material: COTTON FABRIC mercerising bleaching semi-products (30cm * 10cm)
Dye the chemical drug article: REACTIVE DYES EDB zhang blue or green 20g, penetrating agent JFC, the cold rolling heap alkaline agent of REACTIVE DYES, the liquid of soaping (1-5g/L soap flakes, 1-5g/L soda ash).
Instrument and equipment: beaker, electronic balance, graduated pipette, volumetric flask, glass bar (long 11cm), salable plastic bag (20cm * 14cm), clip, padding machine, electric heating temperature controlled water bath pot, baking oven, electric iron, colour photometer.
4. the dyeing leach mill solution is write out a prescription
The cold rolling heap dye solution prescription of table-1 REACTIVE DYES
Figure BDA0000193683257
The cold rolling heap alkaline agent of table-2 REACTIVE DYES solution prescription
The cold rolling heap alkaline agent prescription of table-3 REACTIVE DYES
5. technological process and condition
With dye liquor and the alkali lye mixed by 3-5:1-2, fabric soaks 2-5 second before padding, through the padding machine pressure rolling, and bundle roller pressure 2-5kg/cm 2, speed 5-25 rice/minute.(one soaks one rolls to pad dye liquor; Pick-up rate 70%) → and the glass bar coiling that the identical fabric width with it in the sample dyed cotton fabric edge after the pad dyeing is long, put into the plastic sealing bag that matches with it, and drive the gas in the plastic bag away; Sample dyed cotton fabric plastic sealing bag seal → will be housed earlier; Put into 20-40 ℃ of water-bath gently, the clip that the plastic bag sealing mouth will be higher than liquid level and be fixed in the top is clamped, insulation bank up 20-60 minute → plastic sealing bag proposed gently again; Put into 40-70 ℃ of water-bath gently; Insulation bank up 20-60 minute → plastic sealing bag is proposed gently again, put into 20-40 ℃ of water-bath gently, insulation bank up 5-30 minute → plastic sealing bag proposed gently; (1-5g/L soap flakes, 1-5g/L soda ash are checked colors after 95-100 ℃ * 10-15min) → hot water wash → cold wash → oven dry → pressing → balance to take out dyeing cloth specimen → washing → soap boiling.
Embodiment 4
Experiment material: COTTON FABRIC mercerising bleaching semi-products (30cm * 10cm)
Dye the chemical drug article: the red 2.8g of REACTIVE DYES EDP, the yellow 4.3g of REACTIVE DYES EDP, REACTIVE DYES zhang blue or green 12.9g, penetrating agent JFC, the cold rolling heap alkaline agent of REACTIVE DYES, the liquid of soaping (1-5g/L soap flakes, 1-5g/L soda ash).
Instrument and equipment: beaker, electronic balance, graduated pipette, volumetric flask, glass bar (long 11cm), salable plastic bag (20cm * 14cm), clip, padding machine, electric heating temperature controlled water bath pot, baking oven, electric iron, colour photometer.
7. the dyeing leach mill solution is write out a prescription
The cold rolling heap dye solution prescription of table-1 REACTIVE DYES
The cold rolling heap alkaline agent of table-2 REACTIVE DYES solution prescription
Figure BDA00001936832511
The cold rolling heap alkaline agent prescription of table-3 REACTIVE DYES
Figure BDA00001936832512
8. technological process and condition
With dye liquor and the alkali lye mixed by 3-5:1-2, fabric soaks 2-5 second before padding, through the padding machine pressure rolling, and bundle roller pressure 2-5kg/cm 2, speed 5-25 rice/minute.(one soaks one rolls to pad dye liquor; Pick-up rate 70%) → and the glass bar coiling that the identical fabric width with it in the sample dyed cotton fabric edge after the pad dyeing is long, put into the plastic sealing bag that matches with it, and drive the gas in the plastic bag away; Sample dyed cotton fabric plastic sealing bag seal → will be housed earlier; Put into 20-40 ℃ of water-bath gently, the clip that the plastic bag sealing mouth will be higher than liquid level and be fixed in the top is clamped, insulation bank up 20-60 minute → plastic sealing bag proposed gently again; Put into 40-70 ℃ of water-bath gently; Insulation bank up 20-60 minute → plastic sealing bag is proposed gently again, put into 20-40 ℃ of water-bath gently, insulation bank up 5-30 minute → plastic sealing bag proposed gently; (1-5g/L soap flakes, 1-5g/L soda ash are checked colors after 95-100 ℃ * 10-15min) → hot water wash → cold wash → oven dry → pressing → balance to take out dyeing cloth specimen → washing → soap boiling.
Embodiment 5
Experiment material: COTTON FABRIC mercerising bleaching semi-products (30cm * 10cm)
Dye the chemical drug article: REACTIVE DYES EDP deceives 20g, penetrating agent JFC, the cold rolling heap alkaline agent of REACTIVE DYES, the liquid of soaping (1-5g/L soap flakes, 1-5g/L soda ash).
Instrument and equipment: beaker, electronic balance, graduated pipette, volumetric flask, glass bar (long 11cm), salable plastic bag (20cm * 14cm), clip, padding machine, electric heating temperature controlled water bath pot, baking oven, electric iron, colour photometer.
9. the dyeing leach mill solution is write out a prescription
The cold rolling heap dye solution prescription of table-1 REACTIVE DYES
Figure BDA00001936832513
The cold rolling heap alkaline agent of table-2 REACTIVE DYES solution prescription
Figure BDA00001936832514
The cold rolling heap alkaline agent prescription of table-3 REACTIVE DYES
Figure BDA00001936832515
10. technological process and condition
With dye liquor and the alkali lye mixed by 3-5:1-2, fabric soaks 2-5 second before padding, through the padding machine pressure rolling, and bundle roller pressure 2-5kg/cm 2, speed 5-25 rice/minute.(one soaks one rolls to pad dye liquor; Pick-up rate 70%) → and the glass bar coiling that the identical fabric width with it in the sample dyed cotton fabric edge after the pad dyeing is long, put into the plastic sealing bag that matches with it, and drive the gas in the plastic bag away; Sample dyed cotton fabric plastic sealing bag seal → will be housed earlier; Put into 20-40 ℃ of water-bath gently, the clip that the plastic bag sealing mouth will be higher than liquid level and be fixed in the top is clamped, insulation bank up 20-60 minute → plastic sealing bag proposed gently again; Put into 40-70 ℃ of water-bath gently; Insulation bank up 20-60 minute → plastic sealing bag is proposed gently again, put into 20-40 ℃ of water-bath gently, insulation bank up 5-30 minute → plastic sealing bag proposed gently; (1-5g/L soap flakes, 1-5g/L soda ash are checked colors after 95 ℃ * 10min) → hot water wash → cold wash → oven dry → pressing → balance to take out dyeing cloth specimen → washing → soap boiling.
Embodiment 6
Experiment material: COTTON FABRIC mercerising bleaching semi-products (30cm * 10cm)
Dye the chemical drug article: REACTIVE DYES, penetrating agent JFC, the cold rolling heap alkaline agent of new reactive dyes (reference formulation is seen table 3), the liquid of soaping (2g/L soap flakes, 2g/L soda ash).
Instrument and equipment: beaker, electronic balance, graduated pipette, volumetric flask, glass bar (long 11cm), salable plastic bag (20cm * 14cm), clip, padding machine, electric heating temperature controlled water bath pot, baking oven, electric iron, colour photometer.
11. dyeing leach mill solution prescription
The cold rolling heap dye solution prescription of table-1 REACTIVE DYES
Figure BDA00001936832516
The cold rolling heap alkaline agent of table-2 REACTIVE DYES solution prescription
Figure BDA00001936832517
The cold rolling heap alkaline agent prescription of table-3 REACTIVE DYES
12. technological process and condition
Padding dye liquor (soaks rolls, dip time 2-6 second, pick-up rate 60-80%) → glass bar that the identical fabric width with it in the sample dyed cotton fabric edge after the pad dyeing is long reels; Put into the plastic sealing bag that matches with it; And drive the gas in the plastic bag away, 30 ℃ of water-baths are put in sealing → sample dyed cotton fabric plastic sealing bag will be housed earlier gently; The plastic bag sealing mouth to be higher than liquid level and be fixed in the top clip clamp; Insulation bank up 30 minutes → plastic sealing bag is proposed gently again, put into 60 ℃ of water-baths gently, insulation bank up 30 minutes → plastic sealing bag proposed gently again; Put into 30 ℃ of water-baths gently; Insulation bank up 15 minutes → plastic sealing bag proposed gently, (2g/L soap flakes, 2g/L soda ash are checked colors after 95 ℃ * 10min) → hot water wash → cold wash → oven dry → pressing → balance to take out dyeing cloth specimen → washing → soap boiling.
Should be understood that these embodiment only to be used to the present invention is described and be not used in the restriction scope of the present invention.Should be understood that in addition those skilled in the art can do various changes or modification to the present invention after the content of having read the present invention's instruction, these equivalent form of values fall within the application's appended claims institute restricted portion equally.

Claims (3)

1. a fast proofing new method that is used for cold-rolling heap staining comprises the following steps:
A. the preparation REACTIVE DYES pad dyeing solution consistent with the full-page proof factory formula made in 40-90 minute after REACTIVE DYES, osmotic agent solution are mixed with the cold rolling heap alkaline agent of REACTIVE DYES and uses up;
B. according to producing consistent dip time, pick-up rate, sample cotton one is soaked one roll with full-page proof;
C. the identical fabric width with it in the sample dyed cotton fabric edge after the pad dyeing is long glass bar is reeled, and puts into the plastic sealing bag that matches with it, and extracts the gas in the plastic bag out, keeps sealing;
D., sample dyed cotton fabric plastic sealing bag will be housed earlier, put into 20-40 ℃ of water-bath gently, the plastic bag sealing mouth will be higher than liquid level; After insulation was banked up 20-60 minute, propose plastic sealing bag more gently, put into 40-70 ℃ of water-bath gently; After insulation was banked up 20-60 minute, propose plastic sealing bag more gently, put into 20-40 ℃ of water-bath gently; After insulation was banked up 5-30 minute, propose plastic sealing bag gently, take out the dyeing cloth specimen;
E. according to the washing consistent with full-page proof production, soap, washing process dyes post processing, again with checking colors after the oven dry of sample dyed cotton fabric, pressing, the balance.
2. a kind of fast proofing new method that is used for cold-rolling heap staining according to claim 1; It is characterized in that the cold rolling heap alkaline agent of described REACTIVE DYES by supplying alkaline constituents, buffer components and filling components to form, wherein supplies alkaline constituents to comprise NaOH, potassium hydroxide, sodium carbonate, potash, tertiary sodium phosphate; Buffer components comprises sodium metasilicate, sodium metasilicate, sodium acid carbonate, saleratus, sodium hydrogen phosphate, calgon, trisodium citrate, potassium sodium tartrate; Filling components comprises sodium chloride, potassium chloride, sodium sulphate, potassium sulfate.
3. a kind of fast proofing new method that is used for cold-rolling heap staining according to claim 1 and 2 is characterized in that REACTIVE DYES pad dyeing solution in the step (1), in 60 minutes, makes after REACTIVE DYES, osmotic agent solution are mixed with the cold rolling heap alkaline agent of REACTIVE DYES and uses up; Sample dyed cotton fabric plastic sealing bag will be housed earlier in the step (4), put into 30 ℃ of water-baths gently, after insulation was banked up 30 minutes; Propose plastic sealing bag more gently, put into 60 ℃ of water-baths gently, after insulation was banked up 30 minutes; Propose plastic sealing bag more gently, put into 30 ℃ of water-baths gently, after insulation was banked up 15 minutes; Propose plastic sealing bag gently, take out the dyeing cloth specimen.
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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103924462A (en) * 2014-05-08 2014-07-16 际华三五四三针织服饰有限公司 Hand sample color imitation process for cotton knitted fabric
CN105239420A (en) * 2015-10-13 2016-01-13 青岛大学 Cold pad batch dyeing method of non-pretreated cotton knitted fabric
CN108774906A (en) * 2018-06-27 2018-11-09 彭伟民 A method of with bath agent and its applied to dyeing
CN109505159A (en) * 2018-12-05 2019-03-22 谢建林 A kind of cotton fabrics Cold Pad-Batch Dyeing with Reactive Dyes spline method
CN110067140A (en) * 2019-04-25 2019-07-30 江阴职业技术学院 A kind of sample colour combination method of terylene/cellulose fiber blended fabric

Families Citing this family (1)

* Cited by examiner, † Cited by third party
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CN104264518B (en) * 2014-10-28 2016-05-04 中山宝德绿色农业有限公司 A kind of new cold rolling colouring method

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101275351A (en) * 2008-05-04 2008-10-01 浙江丝绸科技有限公司 Fast proofing method for cold pad batch dyeing
CN101328652A (en) * 2007-06-21 2008-12-24 郭利 Cold pad-batch dyeing method with active dyes capable of realizing color correction successfully at one time
CN101613956A (en) * 2009-07-22 2009-12-30 吴道平 Exhaust dyeing and cold batching process in low liquor ratio

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101328652A (en) * 2007-06-21 2008-12-24 郭利 Cold pad-batch dyeing method with active dyes capable of realizing color correction successfully at one time
CN101275351A (en) * 2008-05-04 2008-10-01 浙江丝绸科技有限公司 Fast proofing method for cold pad batch dyeing
CN101613956A (en) * 2009-07-22 2009-12-30 吴道平 Exhaust dyeing and cold batching process in low liquor ratio

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
于晓成: "棉织物活性染料冷轧堆染色打样方法改进", 《印染》 *

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103924462A (en) * 2014-05-08 2014-07-16 际华三五四三针织服饰有限公司 Hand sample color imitation process for cotton knitted fabric
CN103924462B (en) * 2014-05-08 2016-03-16 际华三五四三针织服饰有限公司 The sample colour combination technique of cotton fabrics
CN105239420A (en) * 2015-10-13 2016-01-13 青岛大学 Cold pad batch dyeing method of non-pretreated cotton knitted fabric
CN108774906A (en) * 2018-06-27 2018-11-09 彭伟民 A method of with bath agent and its applied to dyeing
CN109505159A (en) * 2018-12-05 2019-03-22 谢建林 A kind of cotton fabrics Cold Pad-Batch Dyeing with Reactive Dyes spline method
CN110067140A (en) * 2019-04-25 2019-07-30 江阴职业技术学院 A kind of sample colour combination method of terylene/cellulose fiber blended fabric
CN110067140B (en) * 2019-04-25 2021-06-08 江阴职业技术学院 Sample color-imitating method for polyester/cellulose fiber blended fabric

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