CN102784081B - Anti-dandruff combination containing traditional Chinese medicine herbal plants, shampoo and preparation method thereof - Google Patents
Anti-dandruff combination containing traditional Chinese medicine herbal plants, shampoo and preparation method thereof Download PDFInfo
- Publication number
- CN102784081B CN102784081B CN201210264457.4A CN201210264457A CN102784081B CN 102784081 B CN102784081 B CN 102784081B CN 201210264457 A CN201210264457 A CN 201210264457A CN 102784081 B CN102784081 B CN 102784081B
- Authority
- CN
- China
- Prior art keywords
- shampoo
- dandruff
- phase
- hair
- chinese medicine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Landscapes
- Cosmetics (AREA)
Abstract
The invention belongs to the field of articles for daily use and particularly discloses an anti-dandruff hair-nourishing combination containing traditional Chinese medicine herbal plants. The combination is prepared from the following raw materials in parts by weight: 10-30 parts of angelica, 10-30 parts of rhubarb, 10-20 parts of kuh-seng, 5-15 parts of curcuma, 5-15 parts of white caltrop and 10-20 parts of sealwort. The invention further discloses a shampoo containing the combination and a preparation method thereof. On the basis of the characteristics of hair and scalp and the dandruff forming mechanism, the traditional Chinese medicine combination and the shampoo can be used for intensively nursing the hair and the scalp, so as to recover the health of the scalp and achieve long-acting restoration and dandruff removal effects.
Description
Technical field
The present invention relates to a kind of Chinese medicine hair-washing composition, specifically a kind of have Chinese medicine (herbal plant) hair-washing composition of anti-dandruff hair care effect, the shampoo that contains said composition and a preparation method.
Background technology
Hair care hair care is more and more valued by the people, and some hairs or the scalp problems that in hair care hair care, often there will be are perplexing people always, as fat secretion too much, the dandruff or the withered bifurcated of hair etc.The adult of China nearly 60% is subject to the puzzlement of the too much dandruff problem of oils and fats to some extent, and wherein people's symptom of 15% is very serious.Although the at present commercially available anti-dandruff product that presses down fat emerges in an endless stream, varied, in use crowd, 70% people thinks that effect is unsatisfactory.It is anti-dandruff dose that shampoo in the market adopts antifungal (as pyrithione zinc ZPT) more, and on market, conventional anti-dandruff dose is salicylic acid, Zinc Pyrithione (being called for short ZPT), piroctone olamine salt (trade name Octopirox), climbazole (trade name climbazole) etc.These anti-dandruff dose all belongs to anti-dandruff dose of chemical classes, the approach of not only treating is single, and there is the problems such as sensitization, zest and unstability, and the hair scale sheet of hair is had to damage significantly, cause the dry withered bifurcated in long-time use back, especially on scalding, the impaired hair quality impact such as to dye even more serious.
Summary of the invention
The object of the invention is to propose a kind of external medicine composition with anti-dandruff hair care effect.
Another object of the present invention is to the Chinese medicine shampoo that proposition utilizes said extracted thing to prepare.
The 3rd object of the present invention is to propose the preparation method of above-mentioned shampoo.
In order to realize object of the present invention, the present invention adopts following concrete technical scheme:
The anti-dandruff hair nourishing composition of Chinese medicine, is comprised of following bulk drugs, and the proportioning of each raw material is weight portion:
Radix Angelicae Sinensis 10～30 Radix Et Rhizoma Rhei 10～30 Radix Sophorae Flavescentiss 10～20
Rhizoma Curcumae Longae 5～15 Fructus Atriplicis Sibiricae 5～15 Rhizoma Polygonatis 10～20
Compositions is prepared according to the following steps: each raw material, by aforementioned ratio feeding, is put in crude drug in water and decocts water extraction twice, and the mass ratio of crude drug and water is 1:10～1:30 for the first time, and decocting time is 30～120min; The mass ratio of crude drug and water is 1:5～1:20 for the second time, and decocting time is 60-120min, merges extracted twice liquid; Extracting solution is cooling, filter, get filtrate, obtain anti-dandruff hair nourishing composition.
The anti-dandruff hair nourishing composition of Chinese medicine of the present invention, the proportion optimization of each raw material is (weight portion):
Radix Angelicae Sinensis 20, Radix Et Rhizoma Rhei 15, Radix Sophorae Flavescentis 10, Rhizoma Curcumae Longae 10, Fructus Atriplicis Sibiricae 10, Rhizoma Polygonati 10.
The anti-dandruff hair nourishing composition of Chinese medicine of the present invention, the ratio of quality and the number of copies of described extraction step Raw medicine to boil water and water is 1:20, the response time is 60min; The chilling temperature of cooling step is 20～50 ℃, is filtered into 100～200 orders.
The anti-dandruff hair care shampoo of Chinese medicine of the present invention is made by following raw material, and each component ratio is weight percentage:
Surplus is water.
The anti-dandruff hair care shampoo of Chinese medicine of the present invention, described method comprises the steps:
(1) make material dissolution complete 30～80 ℃ of stirrings of A heat phase;
(2) by mixing homogeneously mutually with A after B phase raw material mix homogeneously, be heated to 80～85 ℃, homogenizing 3～15min, is incubated cooling after 15～40 minutes, adds C to stir mutually, then adds D to stir evenly mutually, then add E phase after cooling, mixes.
The anti-dandruff hair care shampoo of Chinese medicine of the present invention adds C phase raw material stirring even, then adds D to stir evenly mutually when temperature drops to 40～50 ℃ in described step (2), continue cooling, when temperature drops to below 40 ℃, then adds E phase, mixes.
The compositions that above-mentioned raw materials and method prepare, different according to use approach, the present composition also can be made into other hair care category products after extracting, as hair care formulations, shampoo etc.
Shampoo of the present invention, its recommendation method is: within every 1～2 day, wash down once, after first getting foam in hands, evenly spread upon on hair more at every turn, after 1～2 month, the hair scale sheet that can effectively repair hair makes hair more smooth, and effectively maintenance scalp and hair-care, improves scalp pomade, head pruritus, dandruff problem.Consumption: freely determine according to individual use habit and hair length, use in right amount the present composition.
Beneficial effect of the present invention: raw material of the present invention is all selected natural Chinese medicine plant (herbal plant) composition, safe and non-stimulating to hair and scalp.Herbal mixture reasonable compatibility, has the multi-efficiencies such as anti-dandruff, oily, antipruritic, the reparation of control, can thoroughly repair scalp, and recovery scalp health, reaches long-acting anti-dandruff effect, and exploitation and application that this research is the anti-dandruff product of herbal mixture plant provide certain foundation.And the present invention also has the effect that promotes scalp blood microcirculation, improves scalp self metabolism, therefore activity extract of the present invention can be used as functional additive, be added on and wash in hair products.Raw material of the present invention obtains easily, preparation method is convenient feasible, is easy to be accepted by consumers in general, has a good application prospect and market prospect.
Accompanying drawing explanation
The experiment of Fig. 1 Chinese medicinal plant desquamation compositions In Vitro Bacteriostasis;
The assessment of Fig. 2 Chinese medicinal plant dandruff control shampoo containing clinical efficacy;
Fig. 3 Chinese medicinal plant desquamation compositions human body presses down fat experiment;
The external antiallergic experiment of Fig. 4 Chinese medicinal plant desquamation compositions;
Fig. 5 Chinese medicinal plant dandruff control shampoo containing is to hair repairing effect figure;
In figure, (a) is the hair before having one's hair wash, and (b) is the hair with after shampoo of the present invention, is (c) with the hair after product hair washing on market.
The specific embodiment
Invention thinking of the present invention is: in conjunction with China's Traditional Chinese Medicine theory, Chinese herbal medicine Radix Angelicae Sinensis, Radix Et Rhizoma Rhei, Radix Sophorae Flavescentis, Rhizoma Curcumae Longae, Fructus Atriplicis Sibiricae, Rhizoma Polygonati effectively combined, formed compound, and using it as active component.The hair-washing composition that contains this active component is hair conditioning and scalp better, thereby recovers scalp health, especially more obvious to impaired hair quality effect.
This research herbal mixture plant additive adopts Radix Angelicae Sinensis, Radix Et Rhizoma Rhei, Radix Sophorae Flavescentis, Rhizoma Curcumae Longae, Fructus Atriplicis Sibiricae, Rhizoma Polygonati, and reasonable compatibility is coordinated mutually, plays altogether the effect of removing scurf and relieving itching reparation.Radix Angelicae Sinensis, blood-nourishing skin-moisturizing, blood circulation promoting and blood stasis dispelling, dispelling wind for relieving itching; Radix Et Rhizoma Rhei, clearing up internal heat by using drugs of bitter in taste and cold in nature, blood stasis removing blood, cleanses excess-heat stagnant; Radix Sophorae Flavescentis, heat-clearing and toxic substances removing, dampness diuresis, wind dispelling insecticide.Rhizoma Curcumae Longae, blood-activating and qi-promoting, inducing menstruation to relieve menalgia, anti-inflammation.Fructus Atriplicis Sibiricae, dispelling wind for relieving itching, promoting flow of QI and blood.SHENGHUANG essence, the kidney invigorating and essence nourishing, nourshing Yin and drynsessmoistening prescription, be the important component of multiple compound nourishing medicament.Herbal mixture reasonable compatibility, plays good effect altogether.
The present embodiment medical material used all can be bought and obtain from China Medicament Group Corp., meets 2005 editions standards of Pharmacopoeia of People's Republic of China.
Shampoo raw material sources of the present invention are in Table 1
Table 1
The preparation of embodiment 1 extract of the present invention
1) weighting raw materials, Radix Angelicae Sinensis 20g, Radix Et Rhizoma Rhei 15g, Radix Sophorae Flavescentis 10g, Rhizoma Curcumae Longae 10g, Fructus Atriplicis Sibiricae 10g, Rhizoma Polygonati 10g, be put in crude drug in water and decoct and extract twice; The mass ratio of crude drug and water is 1:20 for the first time; Decoction extraction time is 60min; The mass ratio of crude drug and water is 1:10 for the second time, and decocting time is 90min, merges extracted twice liquid;
2) be cooled to 30 ℃, 200 orders filter, and get filtrate, then obtain activity extract through filter plate sucking filtration.
Measure pH value, solid content, electrical conductivity, measurement result is: pH value 4.6, solid content 2.5, electrical conductivity 1800us/cm
The preparation of embodiment 2 extracts of the present invention
1) weighting raw materials, Radix Angelicae Sinensis 10g, Radix Et Rhizoma Rhei 30g, Radix Sophorae Flavescentis 10g, Rhizoma Curcumae Longae 15g, Fructus Atriplicis Sibiricae 5g, Rhizoma Polygonati 20g, be put in crude drug in water and decoct and extract twice; The mass ratio of crude drug and water is 1:10 for the first time; Decocting extraction time is that 30min obtains extracting solution; The mass ratio of crude drug and water is 1:5 for the second time, and decocting time is 60min, merges extracted twice liquid;
2) be cooled to 50 ℃, 100 orders filter, and get filtrate, then obtain activity extract through filter plate sucking filtration.
Measure pH value, solid content, electrical conductivity, measurement result is: pH value 4.8, solid content 2.0, electrical conductivity 1600us/cm.
The preparation of embodiment 3 extracts of the present invention
1) weighting raw materials, Radix Angelicae Sinensis 30g, Radix Et Rhizoma Rhei 10g, Radix Sophorae Flavescentis 20g, Rhizoma Curcumae Longae 5g, Fructus Atriplicis Sibiricae 15g, Rhizoma Polygonati 10g, be put in crude drug in water and decoct and extract twice; The mass ratio of crude drug and water is 1:30 for the first time; Decocting extraction time is that 120min obtains extracting solution; The mass ratio of crude drug and water is 1:20 for the second time, and decocting time is 120min, merges extracted twice liquid;
2) be cooled to 20 ℃, 200 orders filter, and get filtrate, then obtain activity extract through filter plate sucking filtration.
Measure pH value, solid content, electrical conductivity, measurement result is: pH value 5.2, solid content 1.8, electrical conductivity 2100us/cm.
The preparation of embodiment 4 shampoo of the present invention
Raw material and proportioning are in Table 2
Table 2
Preparation method:
(1) A being heated respectively to 60 ℃ of stirrings mutually makes material dissolution complete;
(2) by adding A middle mix homogeneously mutually after B phase raw material mixing and stirring, be heated to 80 ℃, homogenizing 3min, is incubated after 15 minutes and stirs and lower the temperature, while being cooled to 50 ℃, add C phase, stir, then add D to stir evenly mutually, continue to be cooled to 40 ℃, then add E phase, mix rear discharging.
The preparation of embodiment 5 shampoo of the present invention
Raw material and proportioning are in Table 3
Table 3
Preparation method:
(1) A being heated respectively to 30 ℃ of stirrings mutually makes material dissolution complete;
(2) by adding A middle mix homogeneously mutually after B phase raw material mixing and stirring, be heated to 85 ℃, homogenizing 15min, is incubated after 40 minutes and stirs and lower the temperature, while being cooled to 40 ℃, add C phase, stir, then add D to stir evenly mutually, while continuing to be cooled to 30 ℃, then add E phase, mix rear discharging.
The preparation of embodiment 6 shampoo of the present invention
Raw material and proportioning are in Table 4
Table 4
Preparation method:
(1) A being heated respectively to 80 ℃ of stirrings mutually makes material dissolution complete;
(2) by adding A middle mix homogeneously mutually after B phase raw material mixing and stirring, be heated to 85 ℃, homogenizing 10min, is incubated after 40 minutes and stirs and lower the temperature, while being cooled to 50 ℃, add C phase, stir, then add D to stir evenly mutually, in the time of below continuing to be cooled to 40 ℃, then add E phase, mix rear discharging.
Chinese medicinal plant compositions effect evaluation experimental of the present invention
1. Chinese medicine extract In Vitro Bacteriostasis experiment
1.1 experimental principle
The amount reproduction of chlosma on scalp causes the cuticular hyperplasia of scalp, thereby impels corneocyte extremely to come off with the form of white or Lycoperdon polymorphum Vitt squama.Therefore, the horse traction color Salmonella of take is indicator bacteria, and Chinese medicine plant extract fungistatic effect is carried out to external effect evaluation.
1.2 materials, reagent and equipment
The Chinese medicine extract of testing sample: embodiment 1 preparation.
The main experimental apparatus summary sheet of table 5
1.3 experimental procedure departments
1) bacterial strain: chlosma ATCC44344.
2) culture medium preparation: culture medium weighs after good and has appropriate amount of deionized water to dissolve by formula, puts into autoclave sterilizing 20 minutes at 121 ℃, to be cooledly takes out during to 60 ℃, as does not have microbiological contamination available.
3) culture medium: olive oil culture medium
4) mensuration of inhibitory effect
The judgement of bacteriostasis: antibacterial circle diameter >=20mm has been judged to bacteriostasis for extremely responsive " +++ ", and the larger fungistatic effect of inhibition zone is better; 15mm >=bacteriostatic diameter <20mm is Gao Min " ++ "; 10mm >=bacteriostatic diameter <15mm be in quick "+"; Bacteriostatic diameter <10mm is invalid, is judged to without bacteriostasis.3 times repeated trials all has bacteriostasis result person, and it is qualified to be judged to.Negative control group produces without antibacterial ring, otherwise invalidate the test.
1.4 experimental results: as shown in Figure 1, the In Vitro Bacteriostasis design sketch of Chinese medicine extract.Wherein, the antibacterial circle diameter of the Chinese medicine extract of embodiment 1 preparation is 22.16 ± 0.25mm, is extremely responsive " +++ ", has strong fungistatic effect.Inventor utilizes the extract of embodiment 2,3 preparations to repeat above-mentioned experiment, and result, with embodiment 1, is not repeated herein.
2. Chinese medicinal plant extract histamine phosphate itch-threshold experiment
When body generation anaphylactic disease or generation inflammation, the histamine as chemical transmitter substance in mastocyte plays an important role.Histamine phosphate itch-threshold experiment is mainly the pruritus causing due to the release of histamine in the allergy of I type.The method can detect the inhibitory action of the pruritus that sample causes histamine fast and effectively.
2.1 materials, reagent and equipment
The Chinese medicine extract of testing sample: embodiment 1 preparation.
Histamine phosphate, Shanghai San Jie Bioisystech Co., Ltd; Cavia porcellus, male and female half and half.
2.2 experimental technique
Get 40 of Cavia porcelluss, male and female half and half, shave hair in first 1 day right back instep of experiment, are divided at random 5 groups.Within continuous 2 days, respectively at shaving hair place, evenly smear corresponding dosage sample, positive reference substance and distilled water.Test the 3rd day, it is appropriate that precision takes histamine phosphate reference substance.Calculate and respectively organize itch-threshold and compare group difference.
2.3 experimental results: table 6 is Chinese medicinal plant compositions histamine phosphate itch-threshold experiment effect table.
Table 6 Chinese medicinal plant compositions causes the impact (x ± s, n=6) of the reaction of itching on Cavia porcellus histamine phosphate
T check; Compare * P<0.05, * * P<0.01 with model group
Conclusion: as seen from the above table, compare with model group, fluocinolone acetonide ointment and embodiment 1 extract cause to Cavia porcellus histamine phosphate the reaction of itching significant inhibitory action, and extract senior middle school low dose group has certain inhibitory action, particularly outstanding with middle dosage group.Inventor utilizes again the extract of embodiment 2,3 to repeat above-mentioned experiment, and result is with embodiment 1.
3. Chinese medicinal plant shampoo dandruff severity clinical assessment
3.1 experimental principle
Dandruff severity is standard by professional test personnel scoring, and this is earliest period, the most direct and effectively evaluating method.
3.2 experimental technique
Require experimenter need use non-anti-dandruff shampoo after 2 weeks, the shampoo that re-uses inventive embodiments 4 preparations is evaluated, and tests the anti-dandruff effect of its 1 week, 2 weeks, 3 weeks, 4 weeks, then uses non-anti-dandruff shampoo 2 weeks, observes and evaluates dandruff and improve effect.By technical staff, indices is evaluated during this time, tested weekly 1 time.
3.3 evaluation methodology
Use dandruff severity methods of marking-" ten grades of point systems of tackness dandruff "
0 grade indicates without dandruff; L～2 grade are the greyish white coarse squama of little flakes; 3～4 grades is little of median size bits sheet; 5～6 grades of large and thin bits sheets for loosening and be connected with scalp; 7～8 grades is large tackness bits sheet; 9～10 grades be with scalp close attachment from the thicker squama to yellow.
Functional observation index: wherein how many dandruff methods of marking marks to select the scurf number adhering on hair in scalp and the above 4cm of root of hair in viewing area.
3.4 experimental results: as shown in Figure 2, A
0use non-anti-dandruff shampoo after 2 weeks; A
1use anti-dandruff shampoo after 1 week; A
2use anti-dandruff shampoo after 2 weeks; A
3use anti-dandruff shampoo after 3 weeks; A
4use anti-dandruff shampoo after 4 weeks; A
5after inactive anti-dandruff shampoo, re-use non-anti-dandruff shampoo after 2 weeks.Conclusion: embodiment 4 shampoo are compared and are had good anti-dandruff effect with the anti-dandruff product in market.Inventor repeats above-mentioned experiment with the shampoo of embodiment 5,6 preparations equally, and result is with embodiment 4.
4. Chinese medicinal plant extract human body presses down fat experiment
Human body presses down fat experiment, and by particular experiment, crowd forms test population, and test subject makes the variation of (and cosmetic industry composition) front and back skin oil and fat content that applies some make up, thereby determines the effect of the oil-control secretion of cosmetics (or functional component).
4.1 experimental apparatus
Testing sample: embodiment 1 extract.
Experimental apparatus: skin oil and fat tester
4.2 experimental technique
Tested crowd 22-26 year, totally 20 people, men and women half and half.Select experimenter's forehead (minute left and right two parts) cycle labeling successively: tested region samples group and blank region; Technical staff uses skin oil and fat tester
test forehead specific part; Calculate and press down fat rate.
4.4 experimental results: as shown in Figure 3, Chinese medicine extract is compared the effect with good inhibition sebum secretion with blank.Inventor utilizes again the extract of embodiment 2,3 preparations to repeat above-mentioned experiment, and result is with embodiment 1.
5. external antiallergic experiment
Hyaluronidase is anaphylactoid participant, and research shows that hyaluronidase and inflammation, allergy have strong correlation, and many Claritins have the effect of strong hyaluronidase inhibitor.
5.1 materials, reagent and equipment
The activity extract of testing sample: embodiment 1 preparation.
The main experimental apparatus summary sheet of table 7 hyaluronidase vitro inhibition method
5.2 experimental technique
Get CaCl
237 ℃ of heat insulating culture 20min of solution and hyaluronidase liquid; Add sample liquid 0.5mL, heat insulating culture 20min; Add 37 ℃ of insulation 30min of 0.5mL hyaluronate sodium liquid, room temperature is placed 5min; Add NaOH solution and 0.5mL acetylacetone,2,4-pentanedione solution, be placed in after boiling water bath heats 15min and with frozen water, carry out cooling 5min immediately; Add Ehrlich's reagent 1.0mL and dilute with 3.0mL dehydrated alcohol, placing 20min colour developing, with its absorbance of spectrophotometric determination.Calculate hyaluronic acid enzyme inhibition rate.
5.3 experimental results: as shown in Figure 4, embodiment 1 extract antiallergic effect, more than 70%, almost approaches positive control, i.e. 1% glycyrrhizic acid dipotassium.Therefore, this extract has good antiallergic effect.Inventor utilizes again the extract of embodiment 2,3 preparations to repeat above-mentioned experiment, and result is with embodiment 1.
6. the shampoo repairing effect experiment of embodiment 4 preparations
Hair cuticle is the outermost structure of hair, and enemy is initiated to the effect of protective layer.General said hair damage, is the damage of hair cuticle.Hair hair scale sheet marshalling, hair is smooth, glossy, attractive in appearance.If hair is impaired, hair cuticle comes off completely, hair cortex is exposed, will give the coarse sensation of a kind of hair quality of people.Therefore we,, with the microstructure of sem observation hair top layer hair scale sheet, evaluate the repairing effect of shampoo to hair.
6.1 experimental apparatus
Testing sample: embodiment 4 shampoo.
Experimental apparatus: scanning electron microscope TESCAN VEGA II.
6.2 experimental technique
The shampoo of the embodiment that is 1% by Hair grooming concentration 4 preparations soaks 5min, then takes out and cleans, and dries electric Microscopic observation.With commercially available certain brand shampoo matched group the most, method is the same.
6.3 conclusion
As shown in Figure 5, use shampoo hair washing front and back (left figure, the middle figure) contrast of the embodiment of the present invention 4 preparations to find out, the present invention has good reparation effect to hair, and the docile and obedient hair of middle figure hair top layer hair scale sheet is smooth.Can find out with commercially available shampoo (right figure) contrast, middle figure is more smooth more smooth than right figure hair scale sheet, and repairing effect of the present invention is better than commercially available prod.
Claims (6)
1. the anti-dandruff hair nourishing composition of Chinese medicine, is comprised of following bulk drugs, and the proportioning of each raw material is weight portion:
Radix Angelicae Sinensis 10～30 Radix Et Rhizoma Rhei 10～30 Radix Sophorae Flavescentiss 10～20
Rhizoma Curcumae Longae 5～15 Fructus Atriplicis Sibiricae 5～15 Rhizoma Polygonatis 10～20
Compositions is prepared according to the following steps: each raw material, by aforementioned ratio feeding, is put in crude drug in water and decocts water extraction twice, and the mass ratio of crude drug and water is 1:10～1:30 for the first time, and decocting time is 30～120min; The mass ratio of crude drug and water is 1:5～1:20 for the second time, and decocting time is 60-120min, merges extracted twice liquid; Extracting solution is cooling, filter, get filtrate, obtain anti-dandruff hair nourishing composition.
2. the anti-dandruff hair nourishing composition of Chinese medicine according to claim 1, each crude drug proportion optimization is:
Radix Angelicae Sinensis 20 weight portions, Radix Et Rhizoma Rhei 15 weight portions, Radix Sophorae Flavescentis 10 weight portions, Rhizoma Curcumae Longae 10 weight portions, Fructus Atriplicis Sibiricae 10 weight portions, Rhizoma Polygonati 10 weight portions.
3. compositions according to claim 1, is characterized in that, the mass ratio that decocts water extraction step Raw medicine and water is 1:20, and decocting time is 60min; The chilling temperature of cooling step is 20～50 ℃, is filtered into 100～200 orders.
4. a shampoo with anti-dandruff hair care effect, is made by following raw material, and each component ratio is weight percentage:
A phase:
Laureth sulfuric ester ammonium 10～25
B phase:
C phase:
Cetearyl alcohol 0.1～1
The anti-dandruff hair nourishing composition 1～5 of Chinese medicine described in claim 1
D phase:
Dimethyl siloxane and cocamido propyl betaine 1～5
E phase:
5. a preparation method of preparing shampoo described in claim 4, is characterized in that, in order to lower order step, carries out:
(1) make material dissolution complete 30～80 ℃ of stirrings of A heat phase;
(2) by mixing homogeneously mutually with A after B phase raw material mix homogeneously, be heated to 80～85 ℃, homogenizing 3～15min, is incubated cooling after 15～40 minutes, adds C to stir mutually, then adds D to stir evenly mutually, then add E phase after cooling, mixes to obtain shampoo.
6. preparation method according to claim 5, is characterized in that, adds C phase raw material stirring even in described step (2) when temperature drops to 40～50 ℃, add again D to stir evenly mutually, continue cooling, when temperature drops to below 40 ℃, add again E phase, mix to obtain shampoo.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210264457.4A CN102784081B (en) | 2012-07-27 | 2012-07-27 | Anti-dandruff combination containing traditional Chinese medicine herbal plants, shampoo and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210264457.4A CN102784081B (en) | 2012-07-27 | 2012-07-27 | Anti-dandruff combination containing traditional Chinese medicine herbal plants, shampoo and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102784081A CN102784081A (en) | 2012-11-21 |
| CN102784081B true CN102784081B (en) | 2014-03-26 |
Family
ID=47149804
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210264457.4A Active CN102784081B (en) | 2012-07-27 | 2012-07-27 | Anti-dandruff combination containing traditional Chinese medicine herbal plants, shampoo and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102784081B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111973530B (en) * | 2020-09-08 | 2023-04-07 | 广州智尚生物科技有限公司 | Dandruff-removing and itching-relieving composition and application thereof |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101249058B (en) * | 2008-02-26 | 2011-06-29 | 昆明理工大学 | Anti-dandruff relieve itching hair washing cream liquid containing inorganic salt and Chinese medicine, and preparation thereof |
| CN101288635A (en) * | 2008-05-04 | 2008-10-22 | 王跃进 | Natural back hair antidandruff shampoo |
-
2012
- 2012-07-27 CN CN201210264457.4A patent/CN102784081B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN102784081A (en) | 2012-11-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105769654B (en) | A kind of Shu Min skin care compositions and its application in cosmetics | |
| CN102028752B (en) | Chinese herbal medicine compound freckle-removing and skin-whitening composition and external preparation | |
| CN102614102B (en) | Dandruff-removing medicinal composition and preparation method thereof | |
| CN103520053B (en) | Hair and body bathing powder | |
| CN102038626B (en) | Traditional Chinese medicinal hair-restoring and anti-alopecia shampoo and preparation method thereof | |
| CN105902418A (en) | Imitated sebum matrix, external preparation including imitated sebum matrix and application thereof | |
| CN101890080B (en) | Hair-loss preventing and hair-restoring medicinal composition and preparation method thereof, shampoo containing medicinal composition and preparation method thereof | |
| CN107007518A (en) | Plant shampoo medicinal extract and preparation method thereof | |
| CN106726993B (en) | Chinese medicine hair cream and preparation method | |
| CN108553371A (en) | Have effects that skin care compositions that antiallergic is releived and preparation method and application | |
| CN104784466A (en) | External traditional Chinese medicine composition with effects of relieving allergy and resisting irritation and preparation method of composition | |
| CN102764226B (en) | Eyebrow nourishing liquid, and preparation method and application thereof | |
| CN102784081B (en) | Anti-dandruff combination containing traditional Chinese medicine herbal plants, shampoo and preparation method thereof | |
| CN102048815B (en) | Traditional Chinese medicine composition and preparation with whitening and anti-speck efficacies, as well as preparation method thereof | |
| Gholve et al. | Formulation and evaluation of polyherbal antidandruff powder shampoo | |
| CN105816718A (en) | External traditional Chinese medicine composition with hair care and hair blackening effects | |
| CN103142434B (en) | Traditional Chinese medical hair loss preventing and developing formula and product for females as well as preparation method of product | |
| CN104856900A (en) | Pore cleanser mask and preparation method thereof | |
| KR101575768B1 (en) | Humectant made by herbs composition | |
| CN110141542B (en) | Allergy-relieving agent containing radix pseudostellariae and preparation method thereof | |
| CN107375613A (en) | A kind of Chinese medical extract and its external preparation that red blood trace on face effect is removed with Eradicates | |
| CN106390061A (en) | Hair follicle stem cell awakening factor composition for external use, hair loss prevention, and hair regeneration, and preparation method thereof | |
| CN106539725A (en) | Dispel Chinese medicine extract, protective skin cream of red blood trace on face and preparation method thereof | |
| CN102961316B (en) | Bacteriostatic and skin moisturizing traditional Chinese medicine composition, and detergent and skin care product manufactured by same | |
| CN104188847A (en) | Non-silicone-oil plant anti-allergic shampoo |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |