CN102767075A - Oiling agent for producing high-F terylene DTY and production method thereof - Google Patents
Oiling agent for producing high-F terylene DTY and production method thereof Download PDFInfo
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- CN102767075A CN102767075A CN2012102096052A CN201210209605A CN102767075A CN 102767075 A CN102767075 A CN 102767075A CN 2012102096052 A CN2012102096052 A CN 2012102096052A CN 201210209605 A CN201210209605 A CN 201210209605A CN 102767075 A CN102767075 A CN 102767075A
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- finish
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- lubricating oil
- polyester dty
- emulsifying agent
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Abstract
The invention discloses an oiling agent for producing a high-F terylene DTY and a production method thereof. The oiling agent is mainly composed of 90%-95% of a lightweight lubricating oil, 4%-10% of an emulsifier, 1%-3% of an antistatic agent and 1%-3% of an additive. The production method comprises the step of: weighing each component according to the proportion; adding the accurately weighed lubricating oil, emulsifier and antistatic agent into a reaction vessel; starting to mix; heating to 30-40 DEG C; pumping the additive into the reaction vessel after even mixing; maintaining the temperature and stirring for 20-30 min; and filtrating and packaging to obtain a finished product. The oiling agent has stable performance, strong yellowing resistance and good spinnability, and can meet requirements of non-yellowing protection on bleached flannel and texturizing process.
Description
Technical field
The present invention relates to a kind of finish and the manufacturing approach thereof that chemical fibre is produced, especially a kind of finish and production method thereof that is used to produce high F polyester DTY of being used for.
Background technology
Constantly weeding out the old and bring forth the new of reply market, the terylene thread product is constantly brought forth new ideas, and some top grades, high F terylene thread require finish to have stronger anti-yellowing property and lower viscosity and surface tension index, and existing finish product still can not satisfy these requirements fully.For the innovation of the terylene thread that follows up, finish will be accomplished with chemical fiber factory synchronous on stream, in time adjusts product performance.The special-purpose DTY finish of terylene 150D/288F white flannelette is exactly the new product of developing to the requirement of these dacron products.
Summary of the invention
The objective of the invention is that a kind of stable performance that designs for the deficiency that solves above-mentioned technology, anti-xanthochromia ability are strong, good spinnability, can satisfy and do the terylene thread not finish and the production method thereof that are used to produce high F polyester DTY of xanthochromia and texturing craft requirement.
The finish and the production method thereof that are used to produce high F polyester DTY that the present invention designed; Mainly be made up of light lubricating oil, emulsifying agent, antistatic additive, additive, the percentage by weight of each component is: light lubricating oil 90% ~ 95%, emulsifying agent 4% ~ 10%; Antistatic additive 1% ~ 3%, additive 1% ~ 3%.
As preferably:
Said light lubricating oil is 3
#White oil or 5
#White oil or aforementioned both mixture;
Said emulsifying agent is a kind of in AEO, sorbitan fatty acid ester, the cithrol or more than one mixture;
Said antistatic additive is fatty alcohol phosphate APEO sylvite or aliphatic alcohol polyoxyvinethene phosphate sylvite or aforementioned both mixture;
Said additive is made up of following component by weight percentage: the anti-agent 1% of splashing, modified silicon oil 0.1%, ultra-violet absorber 0.5% ~ 1%;
The present invention designed is used to produce the production method of the finish of high F polyester DTY; By the percentage by weight of each component claim each component, earlier light lubricating oil, emulsifying agent, the antistatic additive of accurate measurement dropped into agitated reactor then, open and stir; Be heated to 30 ℃ ~ 40 ℃; Again with in the additive suction agitated reactor, the maintenance temperature also stirred 20 minutes ~ 30 minutes after stirring, and after filtering, packing, made again.
Wherein, light lubricating oil act as and reduces between fiber and the fiber, the coefficient of friction between fiber and other contact components, and the characteristic of anti-xanthochromia is arranged; The effect of emulsifying agent is the various components in the finish are reached balance through physical and chemical process, makes finish become even, transparent, stable oily liquids in use, when pre-treatments such as follow-up water spray, plays the effect of emulsification, washing; The effect of antistatic additive is in spinning process, can be adsorbed on fiber surface, and the hygroscopicity that increases fiber improves electric conductivity, reduces the accumulation of static.
The finish and the production method thereof that are used to produce high F polyester DTY that the present invention designed, the present invention compared with prior art has following good effect:
1, the finish emulsion-stabilizing, do not have obvious corruption;
2, add the bullet good spinnability, viscosity is suitable, reduces frictional force and resistance that silk is crossed oil tanker, and texturing process is difficult for beating, no abnormal broken end;
3, anti-xanthochromia ability is strong, and the no obvious xanthochromia phenomenon under the higher temperature or ultraviolet ray irradiation back can satisfy the non-discoloring requirement of white flannelette, and the back road that does not influence terylene thread uses.
The finish that the present invention designed is used to produce high F polyester DTY is used to produce high F (like 150D/288F) white flannelette terylene thread; Characteristics such as the terylene white flannelette of producing gained has not xanthochromia, good spinnability, oil evenly; Use through the Duo Jia chemical fibre factory; Produce normally, target level of product quality reaches customer requirements.
The specific embodiment
Through embodiment the present invention is done further description below.
Embodiment 1:
The described finish that is used to produce high F polyester DTY of present embodiment mainly is made up of light lubricating oil, emulsifying agent, antistatic additive, additive, and the percentage by weight of each component does
Light lubricating oil 92%, light lubricating oil are 5
#White oil;
Emulsifying agent 4%, wherein AEO 1.5%, sorbitan fatty acid ester 2.0%, cithrol 0.5%;
Antistatic additive 2%, wherein fatty alcohol phosphate APEO sylvite 1.6%, aliphatic alcohol polyoxyvinethene phosphate sylvite 0.4%;
Additive 2%, the wherein anti-agent 1% of splashing, modified silicon oil 0.1%, ultraviolet absorber 0.9%.
This production method that is used to produce the finish of high F polyester DTY; By the percentage by weight of each component claim each component, earlier light lubricating oil, emulsifying agent, the antistatic additive of accurate measurement dropped into agitated reactor then, open and stir; Be heated to 30 ℃; Again with in the additive suction agitated reactor, the maintenance temperature also stirred 20 minutes after stirring, and after filtering, packing, made again.
The finish that present embodiment is described to be used to produce high F polyester DTY is the special-purpose DTY finish of a kind of terylene 150D/288F white flannelette.Can reach following index according to the special-purpose DTY finish of the terylene 150D/288F white flannelette that proportioning and manufacturing approach of the present invention produced:
1, outward appearance (25 ℃) colourless transparent liquid
2, pH value (10% aqueous solution, 20 ℃) 5-6
3, active ingredient (%) >=99
4, kinematic viscosity (40 ℃, crude oil mm/s) 4.5-5.5
5, surface tension (mN/m) 23.5-24.5
Characteristics such as the terylene white flannelette of producing gained has not xanthochromia, good spinnability, oil are evenly used through the Duo Jia chemical fibre factory, produce normally, and target level of product quality reaches customer requirements.
Embodiment 2
The described finish that is used to produce high F polyester DTY of present embodiment mainly is made up of light lubricating oil, emulsifying agent, antistatic additive, additive, and the percentage by weight of each component does
Light lubricating oil 90%, wherein 3
#White oil 16%, 5
#White oil 74%;
Emulsifying agent 8%, wherein AEO 2.5%, sorbitan fatty acid ester 3.8%, cithrol 1.7%;
Antistatic additive 1%, wherein fatty alcohol phosphate APEO sylvite 0.7%, aliphatic alcohol polyoxyvinethene phosphate sylvite 0.3%;
Additive 2%, the wherein anti-agent 1% of splashing, modified silicon oil 0.1%, ultraviolet absorber 0.9%.
This production method that is used to produce the finish of high F polyester DTY; By the percentage by weight of each component claim each component, earlier light lubricating oil, emulsifying agent, the antistatic additive of accurate measurement dropped into agitated reactor then, open and stir; Be heated to 40 ℃; Again with in the additive suction agitated reactor, the maintenance temperature also stirred 30 minutes after stirring, and after filtering, packing, made again.
The finish that present embodiment is described to be used to produce high F polyester DTY is the special-purpose DTY finish of a kind of terylene 150D/288F white flannelette.Can reach following index according to the special-purpose DTY finish of the terylene 150D/288F white flannelette that proportioning and manufacturing approach of the present invention produced:
1, outward appearance (25 ℃) colourless transparent liquid
2, pH value (10% aqueous solution, 20 ℃) 5-6
3, active ingredient (%) >=99
4, kinematic viscosity (40 ℃, crude oil mm/s) 4.5-5.4
5, surface tension (mN/m) 23.5-24.4
Characteristics such as the terylene white flannelette of producing gained has not xanthochromia, good spinnability, oil are evenly used through the Duo Jia chemical fibre factory, produce normally, and target level of product quality reaches customer requirements.
Embodiment 2
The described finish that is used to produce high F polyester DTY of present embodiment mainly is made up of light lubricating oil, emulsifying agent, antistatic additive, additive, and the percentage by weight of each component does
Light lubricating oil 91%, wherein 3
#White oil 25%, 5
#White oil 67%;
Emulsifying agent 5%, wherein AEO 1.3%, sorbitan fatty acid ester 2.7%, cithrol 1%;
Antistatic additive 1%, wherein fatty alcohol phosphate APEO sylvite 1%
Additive 1.7%, the wherein anti-agent 1% of splashing, modified silicon oil 0.1%, ultraviolet absorber 0.6%.
This production method that is used to produce the finish of high F polyester DTY; By the percentage by weight of each component claim each component, earlier light lubricating oil, emulsifying agent, the antistatic additive of accurate measurement dropped into agitated reactor then, open and stir; Be heated to 35 ℃; Again with in the additive suction agitated reactor, the maintenance temperature also stirred 25 minutes after stirring, and after filtering, packing, made again.
The finish that present embodiment is described to be used to produce high F polyester DTY is the special-purpose DTY finish of a kind of terylene 150D/288F white flannelette.Can reach following index according to the special-purpose DTY finish of the terylene 150D/288F white flannelette that proportioning and manufacturing approach of the present invention produced:
1, outward appearance (25 ℃) colourless transparent liquid
2, pH value (10% aqueous solution, 20 ℃) 5-6
3, active ingredient (%) >=99
4, kinematic viscosity (40 ℃, crude oil mm/s) 4.5-5.4
5, surface tension (mN/m) 23.5-24.4
Characteristics such as the terylene white flannelette of producing gained has not xanthochromia, good spinnability, oil are evenly used through the Duo Jia chemical fibre factory, produce normally, and target level of product quality reaches customer requirements.
Above-mentioned three described finishes of embodiment can also be used to produce other high F kinds, like terylene thread 533D/192F etc.
Specific embodiment described herein only is that design of the present invention is illustrated.Person of ordinary skill in the field of the present invention can make various modifications or replenishes or adopt similar mode to substitute described specific embodiment, but can't depart from spirit of the present invention or surmount the defined scope of appended claims.
Claims (6)
1. finish that is used to produce high F polyester DTY; It is characterized in that mainly being made up of light lubricating oil, emulsifying agent, antistatic additive, additive, the percentage by weight of each component is: light lubricating oil 90% ~ 95%, emulsifying agent 4%～10%; Antistatic additive 1% ~ 3%, additive 1% ~ 3%.
2. the finish that is used to produce high F polyester DTY according to claim 1 is characterized in that said light lubricating oil is 3# white oil or 5# white oil or aforementioned both mixture.
3. according to claim 1 or the described finish that is used to produce high F polyester DTY, it is characterized in that said emulsifying agent is a kind of in AEO, sorbitan fatty acid ester, the cithrol or more than one mixture.
4. the finish that is used to produce high F polyester DTY according to claim 1 is characterized in that said antistatic additive is fatty alcohol phosphate APEO sylvite or aliphatic alcohol polyoxyvinethene phosphate sylvite or aforementioned both mixture.
5. the finish that is used to produce high F polyester DTY according to claim 1 is characterized in that said additive is made up of following component by weight percentage: the anti-agent 1% of splashing, modified silicon oil 0.1%, ultra-violet absorber 0.5% ~ 1%.
6. one kind like the described production method that is used to produce the finish of high F polyester DTY of claim 1 to 5; It is characterized in that by the percentage by weight of each component claim each component, earlier light lubricating oil, emulsifying agent, the antistatic additive of accurate measurement dropped into agitated reactor then, open and stir; Be heated to 30 ℃ ~ 40 ℃; Again with in the additive suction agitated reactor, the maintenance temperature also stirred 20 minutes ~ 30 minutes after stirring, and after filtering, packing, made again.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2012102096052A CN102767075A (en) | 2012-06-25 | 2012-06-25 | Oiling agent for producing high-F terylene DTY and production method thereof |
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|---|---|---|---|
| CN2012102096052A CN102767075A (en) | 2012-06-25 | 2012-06-25 | Oiling agent for producing high-F terylene DTY and production method thereof |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103015183A (en) * | 2012-11-29 | 2013-04-03 | 桐乡市恒隆化工有限公司 | Compound type emulsifier for DTY (drawn twisted yarn) oil agent compounding |
| CN103469568A (en) * | 2013-09-26 | 2013-12-25 | 江苏立新化纤科技有限公司 | Oiling agent for fluorine-containing polyester FDY fiber and preparation method of oiling agent |
| CN103469587A (en) * | 2013-09-26 | 2013-12-25 | 江苏立新化纤科技有限公司 | Oil agent for fluorine-containing polyester POY fiber and method for preparing oil agent |
| CN103806268A (en) * | 2014-03-04 | 2014-05-21 | 天津工业大学 | Polyester DTY (draw texturing yarn) oil agent and preparation method thereof |
| CN103981712A (en) * | 2014-04-30 | 2014-08-13 | 杭州传化化学品有限公司 | Anti-splashing chinlon DTY oil agent and preparation method thereof |
| CN104358112A (en) * | 2014-10-10 | 2015-02-18 | 中国石油化工股份有限公司 | Polypropylene oil and preparation method thereof |
| CN105019246A (en) * | 2015-07-31 | 2015-11-04 | 江苏恒科新材料有限公司 | Oiling agent and preparation method thereof |
| CN105839393A (en) * | 2015-09-09 | 2016-08-10 | 杨恩弟 | Multifunctional multielement textile finishing agent |
| CN106120343A (en) * | 2016-07-08 | 2016-11-16 | 苏州夏尔植物油脂科技有限公司 | A kind of terylene, cotton synthetic fibre silk oil preparation, preparation method and applications |
| WO2017024423A1 (en) * | 2015-08-13 | 2017-02-16 | 太仓市隆纺油剂有限公司 | Environmentally-friendly anti-yellowing dacron dty oiling agent and preparation method therefor |
| CN109056326A (en) * | 2018-09-07 | 2018-12-21 | 浙江新胜油脂科技有限公司 | A kind of excellent anti-splashing agent of using effect |
| CN109267183A (en) * | 2018-09-07 | 2019-01-25 | 浙江新胜油脂科技有限公司 | A kind of polyamide fibre DTY oil formula and production method |
| CN109267338A (en) * | 2018-09-07 | 2019-01-25 | 浙江新胜油脂科技有限公司 | A kind of polyester oiling agent |
| CN111945426A (en) * | 2020-08-18 | 2020-11-17 | 江苏双江能源科技股份有限公司 | Terylene DTY oiling agent and preparation method thereof |
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| CN101463564A (en) * | 2008-12-31 | 2009-06-24 | 桐昆集团股份有限公司 | Terylene middle strength filament oil solution and production method thereof |
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Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103015183A (en) * | 2012-11-29 | 2013-04-03 | 桐乡市恒隆化工有限公司 | Compound type emulsifier for DTY (drawn twisted yarn) oil agent compounding |
| CN103469587B (en) * | 2013-09-26 | 2016-06-29 | 江苏立新化纤科技有限公司 | A kind of fluorine-containing polyester POY Finish for fiber |
| CN103469568A (en) * | 2013-09-26 | 2013-12-25 | 江苏立新化纤科技有限公司 | Oiling agent for fluorine-containing polyester FDY fiber and preparation method of oiling agent |
| CN103469587A (en) * | 2013-09-26 | 2013-12-25 | 江苏立新化纤科技有限公司 | Oil agent for fluorine-containing polyester POY fiber and method for preparing oil agent |
| CN103806268A (en) * | 2014-03-04 | 2014-05-21 | 天津工业大学 | Polyester DTY (draw texturing yarn) oil agent and preparation method thereof |
| CN103981712A (en) * | 2014-04-30 | 2014-08-13 | 杭州传化化学品有限公司 | Anti-splashing chinlon DTY oil agent and preparation method thereof |
| CN104358112B (en) * | 2014-10-10 | 2017-11-10 | 中国石油化工股份有限公司 | A kind of polypropylene fibre oil and preparation method thereof |
| CN104358112A (en) * | 2014-10-10 | 2015-02-18 | 中国石油化工股份有限公司 | Polypropylene oil and preparation method thereof |
| CN105019246A (en) * | 2015-07-31 | 2015-11-04 | 江苏恒科新材料有限公司 | Oiling agent and preparation method thereof |
| CN105019246B (en) * | 2015-07-31 | 2017-11-03 | 江苏恒科新材料有限公司 | A kind of finish and preparation method thereof |
| WO2017024423A1 (en) * | 2015-08-13 | 2017-02-16 | 太仓市隆纺油剂有限公司 | Environmentally-friendly anti-yellowing dacron dty oiling agent and preparation method therefor |
| CN105839393A (en) * | 2015-09-09 | 2016-08-10 | 杨恩弟 | Multifunctional multielement textile finishing agent |
| CN106120343A (en) * | 2016-07-08 | 2016-11-16 | 苏州夏尔植物油脂科技有限公司 | A kind of terylene, cotton synthetic fibre silk oil preparation, preparation method and applications |
| CN109056326A (en) * | 2018-09-07 | 2018-12-21 | 浙江新胜油脂科技有限公司 | A kind of excellent anti-splashing agent of using effect |
| CN109267183A (en) * | 2018-09-07 | 2019-01-25 | 浙江新胜油脂科技有限公司 | A kind of polyamide fibre DTY oil formula and production method |
| CN109267338A (en) * | 2018-09-07 | 2019-01-25 | 浙江新胜油脂科技有限公司 | A kind of polyester oiling agent |
| CN111945426A (en) * | 2020-08-18 | 2020-11-17 | 江苏双江能源科技股份有限公司 | Terylene DTY oiling agent and preparation method thereof |
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Application publication date: 20121107 |