CN102766915A - Pearl bamboo fiber and its preparation method - Google Patents
Pearl bamboo fiber and its preparation method Download PDFInfo
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Abstract
The present invention aims to provide a pearl bamboo fiber and its preparation method. The pearl bamboo fiber comprises the following ingredients of: by weight, 99-99.98% of bamboo fiber and 0.02-1% of a nanometer pearl powder compound, which is in the form of powder or dispersion. In comparison with the prior art, the pearl bamboo fiber has skin-friendly characteristics of pearl fiber as well as antibacterial, soft, smooth, cool and comfortable characteristics of bamboo fiber, contains no chemical products or harmful substances, has natural compatibility with skin, has smooth and cool surface and has pearl-like luster. If contacted with skin for a long time, the pearl bamboo fiber has pearl effects of skin care, inflammation and poison relief, skin whitening, ultraviolet resistance and far infrared emission so as to realize the purpose of the invention.
Description
Technical field
The present invention relates to a kind of fiber and preparation method thereof, particularly a kind of pearl bamboo fibre and preparation method thereof.
Background technology
The bamboo fibre product is with the characteristics of its high-tech content and soft and smooth soft warm, cool and comfortable, bacteriostasis antibiosis, environmental protection and natural health; The natural antibacterial of bamboo fiber, antibacterial, uvioresistant act on after repeatedly cyclic washing, Exposure to Sunlight, still can guarantee its original characteristics.
Pearl fiber has the pearl face skin-care effect, and the pearl fiber surface is uniform-distribution with pearl micro-particle, for a long time in contact skin, have the pearl face skin care, relieve inflammation or internal heat relieve internal heat, tender white muscle skin, anti-ultraviolet effect; Pearl fiber contains several amino acids and trace element, and fiber surface is smooth nice and cool, and gloss as the pearl is arranged.
Existing pearl fiber is to be carrier with viscose glue or terylene; Pearl is the precious Chinese herbal medicine that elite, the Bi Qiyi nacre of secreting estranged of pearl shell absorption water is polymerized.
The composition of pearl is very complicated; The modern science analysis shows, pearl contains various trace elements such as abundant calcium and magnesium, phosphorus, zinc, also has 18 seed amino acids; Wherein 7 kinds is that essential amino acid (promptly must be taken in from the external world; The amino acid that human body can not synthesize voluntarily), multiple proteins and small peptide, positive growth factor and the active factors that still can't study with some existing science and technology.
The invention provides a kind of pearl bamboo fibre and preparation method thereof, this fiber has combined the advantage of pearl fiber and bamboo fibre, not only has maintenance skin, and uvioresistant effect also has the performance of natural antibacterial.The pearl bamboo fibre is a kind of brand-new fiber, is in to spin the field and have broad application prospects.
Summary of the invention
The purpose of this invention is to provide a kind of pearl bamboo fibre and preparation method thereof; To overcome the above-mentioned defective that prior art exists; The characteristics of existing pearl fiber parent skin; The characteristics of antibiotic, soft and smooth soft warm, the cool and comfortable of bamboo fibre are arranged again, do not contain any chemical product harmful substance, natural compatibility is arranged with skin.
The technical problem that the present invention solved can adopt following technical scheme to realize:
First aspect of the present invention provides a kind of pearl bamboo fibre, it is characterized in that, it comprises the following component of percentage by weight: bamboo fibre 99%-99.98% and nano-pearl flour complexes 0.02-1%, nano-pearl flour complexes are powder or dispersion form.
Second aspect of the present invention provides a kind of preparation method of pearl bamboo fibre, it is characterized in that, it comprises the steps:
(1) pearl is ground the back and obtain thick pearl powder; Thick pearl powder and water are pressed 1: 5 mixed; And grinding obtains the dispersion liquid of oyster pearl powder; Add the anti-oxidant of the heat stabilizer of thick pearl powder weight 0.005%-1%, thick pearl powder weight 0.005%-1% and the emulsifying agent of thick pearl powder weight 1-10% then, drying obtains nano-pearl powder compound;
(2) nano-pearl flour complexes that step (1) is obtained and mutual-phenenyl two acid bromide two alcohol ester are by weight 1: after 0.1-0.5 mixed at normal temperatures, mixed liquor was 1%-10% in the ratio of viscose;
(3) spinning gets into the acid bath coagulation forming with the bamboo fibre viscose glue that is mixed with Margarita nano-particle, through drawing-off, cut-out, washing, desulfurization, bleach, oil, dewater, dry and process the pearl bamboo fibre.
In one embodiment of the invention, experienced, yellow, the dissolving of nano-pearl flour complexes in the fiber production flow process, mixed processes is sneaked into or adopt spin before the mode of injection sneak into.
In one embodiment of the invention, the viscose glue index of sneaking into behind the nano-pearl flour complexes is: the fine content of first is 6-12%, and sodium hydrate content is 3-9%, and viscosity is 30-65 second, and the degree of ripeness of 10% ammonium chloride value is 7-18ml.
In one embodiment of the invention, said heat stabilizer comprises one or more the combination in tribasic lead sulfate, dibasic Lead Phosphite, barium stearate, lead stearate or the cadmium stearate.
In one embodiment of the invention, said anti-oxidant is four (3,5-di-t-butyl-4-hydroxyl) benzenpropanoic acid pentaerythritol ester, β-(3; The 5-di-tert-butyl-4-hydroxyl benzyl) propionic acid octadecanol ester or 1; 3,4-trimethyl-2,4; The combination of one or more in 6-three (3, the 5-di-tert-butyl-4-hydroxyl benzyl) benzene.
In one embodiment of the invention, said emulsifying agent is one or more the combination in polyglyceryl fatty acid ester, soybean lecithin, sorbierite or the glyceryl monostearate.
In one embodiment of the invention, process that bone dry fiber content is 80-95% in the pearl bamboo fibre, surplus is water and trace impurity.
Pearl bamboo fibre of the present invention and preparation method thereof, compared with prior art, the characteristics of the existing pearl fiber parent of its pearl bamboo fibre skin; The characteristics of antibiotic, soft and smooth soft warm, the cool and comfortable of bamboo fibre are arranged again, do not contain any chemical product harmful substance, natural compatibility is arranged with skin; Smooth surface is nice and cool, gloss as the pearl is arranged, long-term and contact skin; Have the pearl face skin care, relieve inflammation or internal heat relieve internal heat, tender white muscle skin, uvioresistant and emitting far-infrared effect, realize the object of the invention.
Characteristics of the present invention can be consulted the detailed description of following better embodiment and obtained to be well understood to.
The specific embodiment
In order to make technological means of the present invention, creation characteristic, to reach purpose and effect and be easy to understand and understand,, further set forth the present invention below in conjunction with specific embodiment.
A kind of pearl bamboo fibre of the present invention, it comprises the following component of percentage by weight: bamboo fibre 99%-99.98% and nano-pearl flour complexes 0.02-1%, nano-pearl flour complexes are powder or dispersion form.
The preparation method of pearl bamboo fibre of the present invention, it comprises the steps:
(1) pearl is ground the back and obtain thick pearl powder; Thick pearl powder and water are pressed 1: 5 mixed; And grinding obtains the dispersion liquid of oyster pearl powder; Add the anti-oxidant of the heat stabilizer of thick pearl powder weight 0.005%-1%, thick pearl powder weight 0.005%-1% and the emulsifying agent of thick pearl powder weight 1-10% then, drying obtains nano-pearl powder compound;
(2) nano-pearl flour complexes that step (1) is obtained and mutual-phenenyl two acid bromide two alcohol ester are by weight 1: after 0.1-0.5 mixed at normal temperatures, mixed liquor was 1%-10% in the ratio of viscose;
(3) spinning gets into the acid bath coagulation forming with the bamboo fibre viscose glue that is mixed with Margarita nano-particle, through drawing-off, cut-out, washing, desulfurization, bleach, oil, dewater, dry and process the pearl bamboo fibre.
In the present invention, experienced, yellow, the dissolving of nano-pearl flour complexes in the fiber production flow process, mixed processes is sneaked into or adopt spin before the mode of injection sneak into.
In the present invention, the viscose glue index of sneaking into behind the nano-pearl flour complexes is: the fine content of first is 6-12%, and sodium hydrate content is 3-9%, and viscosity is 30-65 second, and the degree of ripeness of 10% ammonium chloride value is 7-18ml.
In the present invention, said heat stabilizer comprises one or more the combination in tribasic lead sulfate, dibasic Lead Phosphite, barium stearate, lead stearate or the cadmium stearate; Said anti-oxidant is four (3,5-di-t-butyl-4-hydroxyl) benzenpropanoic acid pentaerythritol ester, β-(3, the 5-di-tert-butyl-4-hydroxyl benzyl) propionic acid octadecanol ester or 1; 3,4-trimethyl-2,4; The combination of one or more in 6-three (3, the 5-di-tert-butyl-4-hydroxyl benzyl) benzene; Said emulsifying agent is one or more the combination in polyglyceryl fatty acid ester, soybean lecithin, sorbierite or the glyceryl monostearate.
In the present invention, process that bone dry fiber content is 80-95% in the pearl bamboo fibre, surplus is water and trace impurity.
Embodiment 1
Get after the 100g pearl cleans up with clear water, grind thick pearl powder, thick pearl powder and water are pressed 1: 5 mixed; Use ball mill grinding, obtain the dispersion liquid of oyster pearl powder, add 1 of the tribasic lead sulfate of thick pearl powder weight 0.1%, thick pearl powder weight 0.5% then; 3,4-trimethyl-2,4; The soybean lecithin of 6-three (3, the 5-di-tert-butyl-4-hydroxyl benzyl) benzene and thick pearl powder weight 2%, drying obtains nano-pearl powder compound.
With the nano-pearl flour complexes that obtains and mutual-phenenyl two acid bromide two alcohol ester by weight 1: after 0.1-0.5 mixed at normal temperatures, adopting concentration was that 20% pearl powder compound is sneaked into the bamboo viscose glue at dissolution process, and mixed liquor is 5% in the ratio of viscose;
The viscose glue index of sneaking into behind the nano-pearl flour complexes is: the fine content of first is 6%, and sodium hydrate content is 5%, and viscosity is 30 seconds, degree of ripeness 10ml (10% ammonium chloride value).
Spinning gets into the acid bath coagulation forming with the bamboo fibre viscose glue that is mixed with Margarita nano-particle, through drawing-off, cut-out, washing, desulfurization, bleach, oil, dewater, dry and process the pearl bamboo fibre.
Embodiment 2
Get after the 100g pearl cleans up with clear water; Grind thick pearl powder, thick pearl powder and water are pressed 1: 5 mixed, use ball mill grinding; Obtain the dispersion liquid of oyster pearl powder; Add (3,5-di-t-butyl-4-hydroxyl) the benzenpropanoic acid pentaerythritol ester of the tribasic lead sulfate of thick pearl powder weight 0.05%, thick pearl powder weight 1% and the glyceryl monostearate of thick pearl powder weight 5% then, drying obtains nano-pearl powder compound.
With the nano-pearl flour complexes that obtains and mutual-phenenyl two acid bromide two alcohol ester by weight 1: after 0.1-0.5 mixed at normal temperatures, adopting concentration was that 20% pearl powder compound is sneaked into the bamboo viscose glue at dissolution process, and mixed liquor is 8% in the ratio of viscose.
The viscose glue index of sneaking into behind the nano-pearl flour complexes is: the fine content of first is 10%, and sodium hydrate content is 9%, and viscosity is 45 seconds, degree of ripeness 16ml (10% ammonium chloride value).
Spinning gets into the acid bath coagulation forming with the bamboo fibre viscose glue that is mixed with Margarita nano-particle, through drawing-off, cut-out, washing, desulfurization, bleach, oil, dewater, dry and process the pearl bamboo fibre.
Embodiment 3
Get after the 100g pearl cleans up with clear water; Grind thick pearl powder, thick pearl powder and water are pressed 1: 5 mixed, use ball mill grinding; Obtain the dispersion liquid of oyster pearl powder; Add (3,5-di-t-butyl-4-hydroxyl) the benzenpropanoic acid pentaerythritol ester of the tribasic lead sulfate of thick pearl powder weight 0.1%, thick pearl powder weight 1% and the sorbierite of thick pearl powder weight 2% then, drying obtains nano-pearl powder compound.
With the nano-pearl flour complexes that obtains and mutual-phenenyl two acid bromide two alcohol ester by weight 1: after 0.1-0.5 mixed at normal temperatures, adopting concentration was that 20% pearl powder compound is sneaked into the bamboo viscose glue at dissolution process, and mixed liquor is 7% in the ratio of viscose.
The viscose glue index of sneaking into behind the nano-pearl flour complexes is: the fine content of first is 7%, and sodium hydrate content is 6%, and viscosity is 50 seconds, degree of ripeness 12ml (10% ammonium chloride value).
Spinning gets into the acid bath coagulation forming with the bamboo fibre viscose glue that is mixed with Margarita nano-particle, through drawing-off, cut-out, washing, desulfurization, bleach, oil, dewater, dry and process the pearl bamboo fibre.
Embodiment 4
Get after the 100g pearl cleans up with clear water, grind thick pearl powder, thick pearl powder and water are pressed 1: 5 mixed; Use ball mill grinding, obtain the dispersion liquid of oyster pearl powder, add 1 of the barium stearate of thick pearl powder weight 0.1%, thick pearl powder weight 0.5% then; 3,4-trimethyl-2,4; The soybean lecithin of 6-three (3, the 5-di-tert-butyl-4-hydroxyl benzyl) benzene and thick pearl powder weight 5%, drying obtains nano-pearl powder compound.
With the nano-pearl flour complexes that obtains and mutual-phenenyl two acid bromide two alcohol ester by weight 1: after 0.1-0.5 mixed at normal temperatures, adopting concentration was that 20% pearl powder compound is sneaked into the bamboo viscose glue at dissolution process, and mixed liquor is 6% in the ratio of viscose.
The viscose glue index of sneaking into behind the nano-pearl flour complexes is: the fine content of first is 6%, and sodium hydrate content is 6%, and viscosity is 45 seconds, degree of ripeness 12ml (10% ammonium chloride value).
Spinning gets into the acid bath coagulation forming with the bamboo fibre viscose glue that is mixed with Margarita nano-particle, through drawing-off, cut-out, washing, desulfurization, bleach, oil, dewater, dry and process the pearl bamboo fibre.
Embodiment 5
Get after the 100g pearl cleans up with clear water; Grind thick pearl powder, thick pearl powder and water are pressed 1: 5 mixed, use ball mill grinding; Obtain the dispersion liquid of oyster pearl powder; Add β-(3, the 5-di-tert-butyl-4-hydroxyl benzyl) the propionic acid octadecanol ester of the barium stearate of thick pearl powder weight 0.05%, thick pearl powder weight 0.5% and the glyceryl monostearate of thick pearl powder weight 2% then, drying obtains nano-pearl powder compound.
With the nano-pearl flour complexes that obtains and mutual-phenenyl two acid bromide two alcohol ester by weight 1: after 0.1-0.5 mixed at normal temperatures, adopting concentration was that 20% pearl powder compound is sneaked into the bamboo viscose glue at dissolution process, and mixed liquor is 5% in the ratio of viscose.
The viscose glue index of sneaking into behind the nano-pearl flour complexes is: the fine content of first is 8%, and sodium hydrate content is 9%, and viscosity is 40 seconds, degree of ripeness 15ml (10% ammonium chloride value).
Spinning gets into the acid bath coagulation forming with the bamboo fibre viscose glue that is mixed with Margarita nano-particle, through drawing-off, cut-out, washing, desulfurization, bleach, oil, dewater, dry and process the pearl bamboo fibre.
Embodiment 6
Get after the 100g pearl cleans up with clear water; Grind thick pearl powder, thick pearl powder and water are pressed 1: 5 mixed, use ball mill grinding; Obtain the dispersion liquid of oyster pearl powder; Add β-(3, the 5-di-tert-butyl-4-hydroxyl benzyl) the propionic acid octadecanol ester of the cadmium stearate of thick pearl powder weight 0.1%, thick pearl powder weight 1% and the soybean lecithin of thick pearl powder weight 2% then, drying obtains nano-pearl powder compound.
With the nano-pearl flour complexes that obtains and mutual-phenenyl two acid bromide two alcohol ester by weight 1: after 0.1-0.5 mixed at normal temperatures, adopting concentration was that 20% pearl powder compound is sneaked into the bamboo viscose glue at dissolution process, and mixed liquor is 5% in the ratio of viscose.
The viscose glue index of sneaking into behind the nano-pearl flour complexes is: the fine content of first is 6%, and sodium hydrate content is 5%, and viscosity is 30 seconds, degree of ripeness 17ml (10% ammonium chloride value).
Spinning gets into the acid bath coagulation forming with the bamboo fibre viscose glue that is mixed with Margarita nano-particle, through drawing-off, cut-out, washing, desulfurization, bleach, oil, dewater, dry and process the pearl bamboo fibre.
Embodiment 7
Get after the 100g pearl cleans up with clear water, grind thick pearl powder, thick pearl powder and water are pressed 1: 5 mixed; Use ball mill grinding, obtain the dispersion liquid of oyster pearl powder, add 1 of the cadmium stearate of thick pearl powder weight 0.05%, thick pearl powder weight 1% then; 3,4-trimethyl-2,4; The soybean lecithin of 6-three (3, the 5-di-tert-butyl-4-hydroxyl benzyl) benzene and thick pearl powder weight 5%, drying obtains nano-pearl powder compound.
With the nano-pearl flour complexes that obtains and mutual-phenenyl two acid bromide two alcohol ester by weight 1: after 0.1-0.5 mixed at normal temperatures, adopting concentration was that 20% pearl powder compound is sneaked into the bamboo viscose glue at dissolution process, and mixed liquor is 10% in the ratio of viscose.
The viscose glue index of sneaking into behind the nano-pearl flour complexes is: the fine content of first is 9%, and sodium hydrate content is 8%, and viscosity is 35 seconds, degree of ripeness 14ml (10% ammonium chloride value).
Spinning gets into the acid bath coagulation forming with the bamboo fibre viscose glue that is mixed with Margarita nano-particle, through drawing-off, cut-out, washing, desulfurization, bleach, oil, dewater, dry and process the pearl bamboo fibre.
More than show and described basic principle of the present invention, principal character and advantage of the present invention.The technical staff of the industry should understand; The present invention is not restricted to the described embodiments; That describes in the foregoing description and the specification just explains principle of the present invention; The present invention also has various changes and modifications under the prerequisite that does not break away from spirit and scope of the invention, and these variations and improvement all fall in the scope of the invention that requires protection.The present invention requires protection domain to be defined by appending claims and equivalent thereof.
Claims (8)
1. a pearl bamboo fibre is characterized in that, it comprises the following component of percentage by weight: bamboo fibre 99%-99.98% and nano-pearl flour complexes 0.02-1%, nano-pearl flour complexes are powder or dispersion form.
2. the preparation method of a pearl bamboo fibre is characterized in that, it comprises the steps:
(1) pearl is ground the back and obtain thick pearl powder; Thick pearl powder and water are pressed 1: 5 mixed; And grinding obtains the dispersion liquid of oyster pearl powder; Add the anti-oxidant of the heat stabilizer of thick pearl powder weight 0.005%-1%, thick pearl powder weight 0.005%-1% and the emulsifying agent of thick pearl powder weight 1-10% then, drying obtains nano-pearl powder compound;
(2) nano-pearl flour complexes that step (1) is obtained and mutual-phenenyl two acid bromide two alcohol ester are by weight 1: after 0.1-0.5 mixed at normal temperatures, mixed liquor was 1%-10% in the ratio of viscose;
(3) spinning gets into the acid bath coagulation forming with the bamboo fibre viscose glue that is mixed with Margarita nano-particle, through drawing-off, cut-out, washing, desulfurization, bleach, oil, dewater, dry and process the pearl bamboo fibre.
3. the preparation method of pearl bamboo fibre according to claim 2 is characterized in that, experienced, yellow, the dissolving of nano-pearl flour complexes in the fiber production flow process, mixed processes is sneaked into or adopt spin before the mode of injection sneak into.
4. the preparation method of pearl bamboo fibre according to claim 2; It is characterized in that the viscose glue index of sneaking into behind the nano-pearl flour complexes is: the fine content of first is 6-12%, and sodium hydrate content is 3-9%; Viscosity is 30-65 second, and the degree of ripeness of 10% ammonium chloride value is 7-18ml.
5. the preparation method of pearl bamboo fibre according to claim 2 is characterized in that, said heat stabilizer comprises one or more the combination in tribasic lead sulfate, dibasic Lead Phosphite, barium stearate, lead stearate or the cadmium stearate.
6. the preparation method of pearl bamboo fibre according to claim 2 is characterized in that, said anti-oxidant is four (3; 5-di-t-butyl-4-hydroxyl) benzenpropanoic acid pentaerythritol ester, β-(3, the 5-di-tert-butyl-4-hydroxyl benzyl) propionic acid octadecanol ester or 1,3; 4-trimethyl-2; 4, the combination of one or more in 6-three (3, the 5-di-tert-butyl-4-hydroxyl benzyl) benzene.
7. the preparation method of pearl bamboo fibre according to claim 2 is characterized in that, said emulsifying agent is one or more the combination in polyglyceryl fatty acid ester, soybean lecithin, sorbierite or the glyceryl monostearate.
8. the preparation method of pearl bamboo fibre according to claim 2 is characterized in that, processes that bone dry fiber content is 80-95% in the pearl bamboo fibre, and surplus is water and trace impurity.
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| CN103031614A (en) * | 2012-12-19 | 2013-04-10 | 罗莱家纺股份有限公司 | Pearl particle dispersion liquid, pearl fiber and preparation method thereof |
| CN104746161A (en) * | 2013-12-31 | 2015-07-01 | 上海水星家用纺织品股份有限公司 | Production process of medicine fibers and medicine home textile fibers |
| CN105239185A (en) * | 2014-07-09 | 2016-01-13 | 众地家纺有限公司 | Anti-bacterial, health-caring and skin-beautifying viscose fiber and preparation method thereof |
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| CN105239185A (en) * | 2014-07-09 | 2016-01-13 | 众地家纺有限公司 | Anti-bacterial, health-caring and skin-beautifying viscose fiber and preparation method thereof |
| CN105239185B (en) * | 2014-07-09 | 2018-06-26 | 众地家纺有限公司 | A kind of antibiotic health care skin makeup viscose rayon and preparation method thereof |
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Application publication date: 20121107 |