CN102757864A - Method for preparing essence fragrance used in rue cigarette - Google Patents
Method for preparing essence fragrance used in rue cigarette Download PDFInfo
- Publication number
- CN102757864A CN102757864A CN2011101048254A CN201110104825A CN102757864A CN 102757864 A CN102757864 A CN 102757864A CN 2011101048254 A CN2011101048254 A CN 2011101048254A CN 201110104825 A CN201110104825 A CN 201110104825A CN 102757864 A CN102757864 A CN 102757864A
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- CN
- China
- Prior art keywords
- grams
- cigarette
- fragrance
- gram
- rue
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 30
- 238000000034 method Methods 0.000 title claims abstract description 13
- 239000003205 fragrance Substances 0.000 title abstract description 11
- 239000000203 mixture Substances 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 238000000605 extraction Methods 0.000 claims abstract description 9
- 238000010992 reflux Methods 0.000 claims abstract description 9
- 238000007789 sealing Methods 0.000 claims abstract description 9
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 7
- 239000000654 additive Substances 0.000 claims abstract description 7
- 230000000996 additive effect Effects 0.000 claims abstract description 7
- 239000008103 glucose Substances 0.000 claims abstract description 7
- 150000003839 salts Chemical class 0.000 claims abstract description 7
- 240000004784 Cymbopogon citratus Species 0.000 claims description 15
- 235000017897 Cymbopogon citratus Nutrition 0.000 claims description 15
- 235000013599 spices Nutrition 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 8
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
- DPDMMXDBJGCCQC-UHFFFAOYSA-N [Na].[Cl] Chemical group [Na].[Cl] DPDMMXDBJGCCQC-UHFFFAOYSA-N 0.000 claims description 5
- 239000000052 vinegar Substances 0.000 claims description 5
- 235000021419 vinegar Nutrition 0.000 claims description 5
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Natural products CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 4
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 4
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 4
- 235000021110 pickles Nutrition 0.000 claims description 4
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 4
- 235000011152 sodium sulphate Nutrition 0.000 claims description 4
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 3
- 125000000218 acetic acid group Chemical group C(C)(=O)* 0.000 claims description 2
- 241000208125 Nicotiana Species 0.000 abstract description 7
- 235000002637 Nicotiana tabacum Nutrition 0.000 abstract description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 238000002360 preparation method Methods 0.000 abstract description 2
- 235000001347 Ruta graveolens Nutrition 0.000 abstract 3
- 240000005746 Ruta graveolens Species 0.000 abstract 3
- 239000001229 ruta graveolens Substances 0.000 abstract 3
- 239000000706 filtrate Substances 0.000 abstract 1
- 238000004321 preservation Methods 0.000 abstract 1
- 239000007789 gas Substances 0.000 description 4
- 239000002304 perfume Substances 0.000 description 4
- 239000000779 smoke Substances 0.000 description 4
- 239000000341 volatile oil Substances 0.000 description 3
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 description 2
- 229930006000 Sucrose Natural products 0.000 description 2
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000003546 flue gas Substances 0.000 description 2
- WTEVQBCEXWBHNA-JXMROGBWSA-N geranial Chemical compound CC(C)=CCC\C(C)=C\C=O WTEVQBCEXWBHNA-JXMROGBWSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000005720 sucrose Substances 0.000 description 2
- YSTPAHQEHQSRJD-UHFFFAOYSA-N 3-Carvomenthenone Chemical compound CC(C)C1CCC(C)=CC1=O YSTPAHQEHQSRJD-UHFFFAOYSA-N 0.000 description 1
- 241001113925 Buddleja Species 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- WTEVQBCEXWBHNA-UHFFFAOYSA-N Citral Natural products CC(C)=CCCC(C)=CC=O WTEVQBCEXWBHNA-UHFFFAOYSA-N 0.000 description 1
- IBVJWOMJGCHRRW-UHFFFAOYSA-N Delta22-Carene Natural products C1CC(C)=CC2C(C)(C)C12 IBVJWOMJGCHRRW-UHFFFAOYSA-N 0.000 description 1
- ZPKNTCZTABQJPS-UHFFFAOYSA-N Ethyl geranate Natural products CCOC(=O)C=C(C)CCC=C(C)C ZPKNTCZTABQJPS-UHFFFAOYSA-N 0.000 description 1
- 241000134874 Geraniales Species 0.000 description 1
- 239000005792 Geraniol Substances 0.000 description 1
- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 description 1
- 244000290333 Vanilla fragrans Species 0.000 description 1
- 235000009499 Vanilla fragrans Nutrition 0.000 description 1
- 235000012036 Vanilla tahitensis Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000000954 anitussive effect Effects 0.000 description 1
- 230000001088 anti-asthma Effects 0.000 description 1
- 230000000845 anti-microbial effect Effects 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- KMPWYEUPVWOPIM-UHFFFAOYSA-N cinchonidine Natural products C1=CC=C2C(C(C3N4CCC(C(C4)C=C)C3)O)=CC=NC2=C1 KMPWYEUPVWOPIM-UHFFFAOYSA-N 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- ZPKNTCZTABQJPS-PKNBQFBNSA-N ethyl (2e)-3,7-dimethylocta-2,6-dienoate Chemical compound CCOC(=O)\C=C(/C)CCC=C(C)C ZPKNTCZTABQJPS-PKNBQFBNSA-N 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 229940113087 geraniol Drugs 0.000 description 1
- 229930182478 glucoside Natural products 0.000 description 1
- 150000008131 glucosides Chemical class 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 238000005554 pickling Methods 0.000 description 1
- 229930006968 piperitone Natural products 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Abstract
The invention belongs to a preparation method of an essence fragrance used in cigarettes. Specifically, according to the method provided by the invention, common rue herb is preserved, and an effective component of the common rue herb is extracted and used for preparing fragrance used in cigarettes. According to the invention, 80-200g of common rue herb, 40-60g of water, 10-30g of glucose, 3-8g of an additive, and 3-8g of salt are stirred, such that the components are dissolved and well mixed; the mixture is compacted in a sealed vessel; the vessel is sealed by using a sealing film, and preservation is carried out; the mixture is stood under normal temperature for 15-30 days; 1000g of an alcohol solution with a mass percentage content of 70-90% is added to the mixture; reflux extraction is carried out for 2h; the obtained material is filtered; and a filtrate is concentrated until a relative density is 1.02-1, such that the essence fragrance used in cigarettes is obtained. The invention is advantaged in simple process and low production cost. The prepared fragrance is advantaged in high fragrance intensity and rich fragrance quality. The fragrance provides good improvements to tobacco quality.
Description
Technical field
The invention belongs to a kind of preparation method of essence spice for cigarette, a kind ofly specifically Remote Lemongrass Herb are pickled the back extract the method that its effective constituent is used to prepare tobacco aromatics using.
Background technology
Vegetable-pickling is a kind of ancient vegetables processing and storage method, no matter in China or long history is abroad all arranged.Because its process and apparatus is simple, raw materials used gathering materials on the spot is so formed the famous special local product of many unique styles in different areas.
Rue is a kind of vanilla, is exactly the present said Root of Lindley Butterflybush of people.Its leaf is similar to the pea leaf, the length of growing thickly for a short time.Leaf is fragrance very, and to turn white slightly between leaf the same as smearing with flour after autumn, with its favorable moth-proof special efficacy arranged.Herb contains acid soap glucoside material, tannin, protein, phlegmatic temperament, amaroid, and the bright grass of carbohydrate and phenolic substance contains volatile oil 0.7～1.0%, and it is about 1.8% that leaf contains volatile oil, and floral axis is about 0.5%, and stem is less than 0.05%.Contain piperitone 40～50%, carene-4 in the volatile oil: 20%, Mang geraniol 10%, Mang Ethylgeranate 10%, Mang geranial, PC 560 etc. are still arranged, have antiasthmatic effect, antitussive action, anti-microbial effect etc.Do not find as yet rue as the report of tobacco at present with essence and flavoring agent.
Summary of the invention
The object of the invention just provides a kind of method for preparing the rue essence spice for cigarette, the spices that it is processed, and aroma strength is high, and fragrance matter is abundanter, and cigarette quality is had good improvement.
The present invention is achieved in that it is that weight is Remote Lemongrass Herb 80-200 gram; Water 40-60 gram, glucose 10-30 gram, additive 3-8 gram, salt 3-8 gram stirring and dissolving mix, and put into the encloses container compacting and pickle with sealing film phonograph seal; Normal temperature was placed 15-30 days; And then to add the quality percentage composition be that spirituous solution 1000 grams of 70%-90% carried out refluxing extraction 2 hours, filters, and it is that 1.02-1.2 promptly gets essence spice for cigarette that filtrating is concentrated into specific density.
The present invention's technical scheme preferably is to be Remote Lemongrass Herb 100 grams with weight, water 50 grams, and glucose 20 grams, additive 5 grams, salt 5 gram stirring and dissolving mix; Putting into the encloses container compacting pickles with sealing film phonograph seal again; Normal temperature was placed 15-30 days, and then to add the quality percentage composition be that spirituous solution 1000 grams of 70%-90% carried out refluxing extraction 2 hours, filtered; It is 1.12 that filtrating is concentrated into specific density, promptly gets essence spice for cigarette.
Wherein said additive is acetic acid, vinegar, Hydrocerol A, ammoniacal liquor or sodium hydroxide, preferred vinegar or Hydrocerol A.Described salt is sodium-chlor or sodium sulfate, preferred sodium-chlor.Described spirituous solution quality percentage composition is 75%.
Technology of the present invention is simple, low cost of manufacture, and the spices that it is processed, aroma strength is high, and fragrance matter is abundanter, and cigarette quality is had good improvement.
Embodiment
Further illustrate content of the present invention below in conjunction with instance, but these implement not limit protection scope of the present invention.
Embodiment 1
Get Remote Lemongrass Herb 100 grams of having smashed, get 50 gram water, adding glucose 20 grams, vinegar 5 grams, sodium-chlor 5 gram stirring and dissolving mix in water; Put into the wide-necked bottle compacting again with sealing film phonograph seal; Normal temperature was placed 15 to 30 days, took out the Remote Lemongrass Herb of having pickled then and emitted in the extractor of 2000ml, added 70% spirituous solution 1000 grams again and carried out refluxing extraction 2 hours; Filter, filtrating concentrating promptly gets required tobacco aromatics using.Join in the cigarette and smoke panel test, have the flavouring essence quality that improves cigarette, increase perfume quantity, cover assorted gas, improved the mouthfeel characteristic of cigarette.
Embodiment 2
Get Remote Lemongrass Herb 100 grams of having smashed, get 50 gram water, adding sucrose 20 grams, ammoniacal liquor 3 grams, sodium sulfate 5 gram stirring and dissolving mix in water; Put into the wide-necked bottle compacting again with sealing film phonograph seal; Normal temperature was placed 15 to 30 days, took out the Remote Lemongrass Herb of having pickled then and emitted in the extractor of 2000ml, added 75% spirituous solution 1000 grams again and carried out refluxing extraction 2 hours; Filter, filtrating concentrating promptly gets required tobacco aromatics using.Join in the cigarette and smoke panel test, have the flavouring essence quality that improves cigarette, increase perfume quantity, increase flue gas concentration, cover assorted gas, improved the mouthfeel characteristic of cigarette.
Embodiment 3
Get Remote Lemongrass Herb 100 grams of having smashed, get 1000 gram water, adding glucose 20 grams, vinegar 5 grams, sodium-chlor 5 gram stirring and dissolving mix in water; Pour the solution that has prepared again into and seal sealing and preserve putting into the Remote Lemongrass Herb wide-necked bottle; Normal temperature was placed 5 to 10 days, took out Remote Lemongrass Herb and the liquid pickled then and all emitted in the extractor of 5000ml, and alcohol 1000 grams that add quality percentage composition 95% again carried out refluxing extraction 2 hours; Filter, filtrating concentrating promptly gets required tobacco aromatics using.Join in the cigarette and smoke panel test, have the flavouring essence quality that improves cigarette, increase perfume quantity, cover assorted gas, improved the mouthfeel characteristic of cigarette.
Embodiment 4
Get Remote Lemongrass Herb 100 grams of having smashed, get 60 gram water, adding sucrose 20 grams, ammoniacal liquor 3 grams, sodium sulfate 5 gram stirring and dissolving mix in water; Pour the solution that has prepared again into and seal sealing and preserve putting into the Remote Lemongrass Herb wide-necked bottle; Normal temperature was placed 5 to 10 days, took out Remote Lemongrass Herb and the liquid pickled then and all emitted in the extractor of 5000ml, and alcohol 1000 grams that add quality percentage composition 80% again carried out refluxing extraction 2 hours; Filter, filtrating concentrating promptly gets required tobacco aromatics using.Join in the cigarette and smoke panel test, have the flavouring essence quality that improves cigarette, increase perfume quantity, cover assorted gas, increase flue gas concentration, improved the mouthfeel characteristic of cigarette.
Claims (5)
1. method for preparing the rue essence spice for cigarette, it is to be Remote Lemongrass Herb 80-200 gram with weight, water 40-60 gram; Glucose 10-30 gram, additive 3-8 gram, salt 3-8 gram stirring and dissolving mix; Put into the encloses container compacting and pickle with sealing film phonograph seal, normal temperature was placed 15-30 days, and then to add the quality percentage composition be that spirituous solution 1000 grams of 70%-90% carried out refluxing extraction 2 hours; Filter, it is that 1.02-1.2 promptly gets essence spice for cigarette that filtrating is concentrated into specific density.
2. a kind of method for preparing the rue essence spice for cigarette according to claim 1, it is to be Remote Lemongrass Herb 100 grams with weight, water 50 grams; Glucose 20 grams, additive 5 grams, salt 5 gram stirring and dissolving mix, and put into the encloses container compacting and pickle with sealing film phonograph seal, and normal temperature was placed 15-30 days; And then to add the quality percentage composition be that spirituous solution 1000 grams of 70%-90% carried out refluxing extraction 2 hours; Filter, it is 1.12 that filtrating is concentrated into specific density, promptly gets essence spice for cigarette.
3. a kind of method for preparing the rue essence spice for cigarette according to claim 1 and 2, wherein said additive is acetic acid, vinegar, Hydrocerol A, ammoniacal liquor or sodium hydroxide.
4. a kind of method for preparing the rue essence spice for cigarette according to claim 1 and 2, wherein said salt is sodium-chlor or sodium sulfate.
5. a kind of method for preparing the rue essence spice for cigarette according to claim 1 and 2, wherein said spirituous solution quality percentage composition is 75%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110104825 CN102757864B (en) | 2011-04-25 | 2011-04-25 | Method for preparing essence fragrance used in rue cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110104825 CN102757864B (en) | 2011-04-25 | 2011-04-25 | Method for preparing essence fragrance used in rue cigarette |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102757864A true CN102757864A (en) | 2012-10-31 |
| CN102757864B CN102757864B (en) | 2013-06-05 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201110104825 Expired - Fee Related CN102757864B (en) | 2011-04-25 | 2011-04-25 | Method for preparing essence fragrance used in rue cigarette |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102757864B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102952637A (en) * | 2012-11-13 | 2013-03-06 | 湖北中烟工业有限责任公司 | Salty sweet tipping paper essence and preparation method as well as application thereof |
| CN103013669A (en) * | 2012-12-31 | 2013-04-03 | 浙江绿晶香精有限公司 | Preparation method of tobacco leaf moisturizing liquor for lowering tar content and benzopyrene content |
| CN103549651A (en) * | 2013-11-14 | 2014-02-05 | 赵秋芝 | Toxicity attenuation cigarette with anti-cough effect |
| CN113633730A (en) * | 2021-09-29 | 2021-11-12 | 浙江养和健康管理科技有限公司 | Traditional Chinese medicine composition for treating asthma and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101671696A (en) * | 2008-09-10 | 2010-03-17 | 江西中烟工业公司 | Pilocarpus plant extract for reducing smoke dry sensation of cigarettes and preparation method thereof |
-
2011
- 2011-04-25 CN CN 201110104825 patent/CN102757864B/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101671696A (en) * | 2008-09-10 | 2010-03-17 | 江西中烟工业公司 | Pilocarpus plant extract for reducing smoke dry sensation of cigarettes and preparation method thereof |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102952637A (en) * | 2012-11-13 | 2013-03-06 | 湖北中烟工业有限责任公司 | Salty sweet tipping paper essence and preparation method as well as application thereof |
| CN102952637B (en) * | 2012-11-13 | 2014-03-26 | 湖北中烟工业有限责任公司 | Salty sweet tipping paper essence and preparation method as well as application thereof |
| CN103013669A (en) * | 2012-12-31 | 2013-04-03 | 浙江绿晶香精有限公司 | Preparation method of tobacco leaf moisturizing liquor for lowering tar content and benzopyrene content |
| CN103013669B (en) * | 2012-12-31 | 2014-03-12 | 浙江绿晶香精有限公司 | Preparation method of tobacco leaf moisturizing liquor for lowering tar content and benzopyrene content |
| CN103549651A (en) * | 2013-11-14 | 2014-02-05 | 赵秋芝 | Toxicity attenuation cigarette with anti-cough effect |
| CN103549651B (en) * | 2013-11-14 | 2015-06-10 | 郄美莲 | Toxicity attenuation cigarette with anti-cough effect |
| CN113633730A (en) * | 2021-09-29 | 2021-11-12 | 浙江养和健康管理科技有限公司 | Traditional Chinese medicine composition for treating asthma and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102757864B (en) | 2013-06-05 |
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Granted publication date: 20130605 Termination date: 20140425 |