CN102726463B - The artificial repellant of a kind of Monochamus alternatus - Google Patents
The artificial repellant of a kind of Monochamus alternatus Download PDFInfo
- Publication number
- CN102726463B CN102726463B CN201210220602.9A CN201210220602A CN102726463B CN 102726463 B CN102726463 B CN 102726463B CN 201210220602 A CN201210220602 A CN 201210220602A CN 102726463 B CN102726463 B CN 102726463B
- Authority
- CN
- China
- Prior art keywords
- monochamus alternatus
- repellant
- artificial
- alternatus
- pine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The artificial repellant of a kind of Monochamus alternatus, belongs to insect control technical field.It is characterized in that containing: active component 8-19%, synergistic component 5-12%, stabilizing agent 2-11%, solvent 63-81%.The artificial repellant of above-mentioned a kind of Monochamus alternatus, mutually acted synergistically by the multiple active component with good avoidance effect, significantly can walk quickly and keep away and bore the alternatus Larva of moth in pine tree and the adult of tree body surface, thus reduce it and carry and propagate pine wood nematode, improve the survival rate of pine tree, can effectively prevent and treat spreading unchecked of pine wood nematode, cut off and propagate source.Its production process is easy, and Long-Time Service also can not make Monochamus alternatus produce resistance.It walks quickly and keeps away effective, low production cost, is suitable for large area in pine forest and sprays use.
Description
Technical field
The invention belongs to insect control technical field, be specially the artificial repellant of a kind of Monochamus alternatus.
Background technology
Monochamus alternatus is a kind of important injurious forest-insect, is mainly distributed in the ground such as Jiangsu, Anhui, Zhejiang, Guangdong, Shandong, Taiwan, Hong Kong at present in China.The main media insect of Monochamus alternatus or pine wood nematode, pine nematode is then the destructive disease of pine tree.At present, Monochamus alternatus and jointly causing harm of pine wood nematode, cause a large amount of pine death.
Someone passes through Monochamus alternatus repellency compounds Quality Research.Find in the hexane extract of the female worm hindgut of Monochamus alternatus containing the chemical substance to laying eggs with repellent action.In the extract of female male imago hindgut, australene, nopinene, laurene, 3-carene, citrene, terpinolene and 4-methyl-2 are identified, 6-DI-tert-butylphenol compounds, has also identified vinyl guaiacol in Monochamus alternatus female insect hindgut extract.The biological activity test of synthetic compound shows, lay eggs to the mixture repellent Monochamus alternatus of vinyl guaiacol and 4-methyl-2,6-DI-tert-butylphenol compounds, the two has the effect of mutual synergy.Cutting number on the juggle of the hexane extract process of alternatus Larva worm excrement and egg laying amount are all less than contrast.Australene, nopinene, 3-carene, citrene, longifolene and 4-methyl-2,6-DI-tert-butylphenol compounds 6 compounds have been identified from the hexane extract of larva worm excrement.Biological activity test result shows, the hexane extract of alternatus Larva worm excrement has oviposition-repelling activity.Compound 4-methyl-2, the 6-DI-tert-butylphenol compounds identified in larva worm excrement and the mixture of 5 terpene compounds have repellent action to the female worm of Monochamus alternatus.And the chemical substance that Monochamus alternatus female worm hindgut produces then can the female worm of repellent Monochamus alternatus to the acting in conjunction of vinyl guaiacol and 4-methyl-2,6-DI-tert-butylphenol compounds, male worm is not had a significant effect.
In addition, the leaf volatiles of Monochamus alternatus non-host plant cdear, Chinese scholartree, Chinese parasol tree, Chinese holly tree, Chinese fir, willow, willow and cypress and some plants essential oils and chemical substance are as nicotine, eucalyptus oil, nerolidol, spearmint essential oil, benzaldehyde, also have impact to its oviposition behavior.Wherein, the repellent action of nicotine is the strongest.In addition, rotenone has the interference effect of significant repellent rate effect and imago feeding to Monochamus alternatus.Repellent rate effect and Antifeedant Effects strengthen with the increase of concentration, when concentration for the treatment of is 1000mg/L, the repellent rate rate of rotenone to adult is 75.63%, and selectivity and the non-selective anti-food rate of the rear 12h Monochamus alternatus of process are respectively 72.91% and 69.50%.The action of contace poison of rotenone to Monochamus alternatus 5 instar larvae is not obvious.Therefore, utilize rotenone to prevent and treat Monochamus alternatus, on the one hand can by suppressing to take food the propagation reducing pine wood nematode; By avoiding, keeping away lays eggs can reduce insect population of lower generation on the other hand.
Alternatus Larva bores moth causes harm, have stronger disguise, low instar larvae gnaws a large amount of phloem tissue and sapwood under bark, and trees conducting system is obstructed, 3,4 instar larvaes are eaten into and are destroyed xylem structure into heartwood, so the difficulty that Monochamus alternatus is is seriously prevented and treated pine tree harm is very large simultaneously.Although chemical control can obtain temporary transient better effects, but its negative effect also becomes increasingly conspicuous, be in particular in following two aspects: (1) chemical pesticide easily makes insect produce anti-drug resistance, and that causes dosage increases progressively the vicious circle of spreading unchecked with insect, causes cost accounting day by day to increase.(2) using in a large number of chemical pesticide causes residue of pesticide, and the natural enemy that kills off the insect pests causes pest resurgence, worsens natural environment and environment for human survival, serious harm human health.Simultaneously because longicorn is uneven from generation to generation, chemical control is made to have very large limitation, and more and more obvious, and the cry of society to this protest also improves day by day, is badly in need of seeking a kind of effective repellant.
Summary of the invention
For the above-mentioned problems in the prior art, the object of the invention is to design the technical scheme that the artificial repellant of a kind of Monochamus alternatus is provided, there is feeding cost low, easy and simple to handle, applied range, output is high, can not change the original biological property of longicorn simultaneously.
The described artificial repellant of a kind of Monochamus alternatus, is characterized in that the following component containing weight percentage: active component 8-19%, synergistic component 5-12%, stabilizing agent 2-11%, solvent 63-81%; Described active component is the mixture of the oxalic acid of equivalent, citric acid, ball spore element, oosporein, beauvericin, salicylic acid, phenyl-propane, iridoid glycoside composition; Described synergistic component is one or more mixtures in vitamin B1, laurene, paclobutrazol, citrene, guaiacol, oil of Cymbopogon winterianus; Described stabilizing agent is one or both mixtures in 1,2-butanediol, isopropyl phosphoric acid ester; Described solvent is one or more mixtures in ethanol, formic acid, water, glacial acetic acid.
The described artificial repellant of a kind of Monochamus alternatus, is characterized in that the content of active component is 9-17%, is preferably 10-15%.
The described artificial repellant of a kind of Monochamus alternatus, is characterized in that the content of synergistic component is 6-11%, is preferably 8-10%.
The described artificial repellant of a kind of Monochamus alternatus, is characterized in that the content of stabilizing agent is 3-10%, is preferably 4-9%.
The described artificial repellant of a kind of Monochamus alternatus, is characterized in that the content of solvent is 65-80%, is preferably 66-78%.
The artificial repellant of above-mentioned a kind of Monochamus alternatus, mutually acted synergistically by the multiple active component with good avoidance effect, significantly can walk quickly and keep away and bore the alternatus Larva of moth in pine tree and the adult of tree body surface, thus reduce it and carry and propagate pine wood nematode, improve the survival rate of pine tree, can effectively prevent and treat spreading unchecked of pine wood nematode, cut off and propagate source.Its production process is easy, and Long-Time Service also can not make Monochamus alternatus produce resistance.It walks quickly and keeps away effective, low production cost, is suitable for large area in pine forest and sprays use.
The percentage composition related in present specification unless otherwise indicated, other the weight percentage being pure material.
Embodiment
Below by way of specific embodiment, the invention will be further described, and binding tests further illustrates beneficial effect of the present invention.
Embodiment 1
780kg ethanol is dropped in 1000L reactor, drop into 12.5kg oxalic acid, 12.5kg citric acid, 12.5kg ball spore element, 12.5kg oosporein, 12.5kg beauvericin, 12.5kg salicylic acid, 12.5kg phenyl-propane and 12.5kg iridoid glycoside again, slowly 20kg vitamin B1,20kg paclobutrazol, 20kg citrene and 20kg oil of Cymbopogon winterianus is dropped into again after stirring and dissolving, stir half an hour, mix, then 20kg1 is added, 2-butanediol and 20kg isopropyl phosphoric acid ester, be finally uniformly mixed final products.
Embodiment 2
660kg formic acid is dropped in 1000L reactor, drop into 18.75kg oxalic acid, 18.75kg citric acid, 18.75kg ball spore element, 18.75kg oosporein, 18.75kg beauvericin, 18.75kg salicylic acid, 18.75kg phenyl-propane and 18.75kg iridoid glycoside again, slowly 10kg vitamin B1,10kg laurene, 20kg paclobutrazol, 20kg guaiacol and 40kg oil of Cymbopogon winterianus is dropped into again after stirring and dissolving, stir half an hour, mix, then 90kg1 is added, 2-butanediol, be finally uniformly mixed final products.
Embodiment 3
755kg water is dropped in 1000L reactor, drop into 13.75kg oxalic acid, 13.75kg citric acid, 13.75kg ball spore element, 13.75kg oosporein, 13.75kg beauvericin, 13.75kg salicylic acid, 13.75kg phenyl-propane and 13.75kg iridoid glycoside again, slowly 15kg vitamin B1,10kg laurene, 10kg paclobutrazol, 10kg citrene, 20kg guaiacol and 20kg oil of Cymbopogon winterianus is dropped into again after stirring and dissolving, stir half an hour, mix, then add 50kg isopropyl phosphoric acid ester, be finally uniformly mixed final products.
Embodiment 4
730kg glacial acetic acid is dropped in 1000L reactor, drop into 15kg oxalic acid, 15kg citric acid, 15kg ball spore element, 15kg oosporein, 15kg beauvericin, 15kg salicylic acid, 15kg phenyl-propane and 15kg iridoid glycoside again, slowly 10kg vitamin B1,20kg laurene, 20kg paclobutrazol, 20kg citrene and 20kg guaiacol is dropped into again after stirring and dissolving, stir half an hour, mix, then 30kg1 is added, 2-butanediol and 30kg isopropyl phosphoric acid ester, be finally uniformly mixed final products.
Embodiment 5
105kg ethanol, 200kg formic acid, 200kg water and 200kg glacial acetic acid is dropped in 1000L reactor, drop into 16.25kg oxalic acid, 16.25kg citric acid, 16.25kg ball spore element, 16.25kg oosporein, 16.25kg beauvericin, 16.25kg salicylic acid, 16.25kg phenyl-propane and 16.25kg iridoid glycoside again, slowly 25kg laurene, 25kg citrene, 15kg guaiacol and 30kg oil of Cymbopogon winterianus is dropped into again after stirring and dissolving, stir half an hour, mix, then add 70kg isopropyl phosphoric acid ester, be finally uniformly mixed final products.
Embodiment 6
382kg ethanol and 300kg glacial acetic acid is dropped in 1000L reactor, drop into 17.5kg oxalic acid, 17.5kg citric acid, 17.5kg ball spore element, 17.5kg oosporein, 17.5kg beauvericin, 17.5kg salicylic acid, 17.5kg phenyl-propane and 17.5kg iridoid glycoside again, slowly 48kg vitamin B1 and 50kg oil of Cymbopogon winterianus is dropped into again after stirring and dissolving, stir half an hour, mix, then add 80kg1,2-butanediol, be finally uniformly mixed final products.
The good result of above-mentioned Monochamus alternatus repellant is described below by way of test.
Table 1 shows: embodiment 1-6 all has good effect to the expulsion of Monochamus alternatus, and lasting effect is better, embodiment 1 is better than embodiment 2, embodiment 4 is better than embodiment 3, embodiment 5 is better than embodiment 6, advise by the extension rate of adjustment agricultural chemicals, the object of expelling Monochamus alternatus completely to be reached in the process used in reality.Working concentration is doubly advisable to dilute 250-350.
Claims (5)
1. the artificial repellant of Monochamus alternatus, is characterized in that the following component containing weight percentage: active component 8-19%, synergistic component 5-12%, stabilizing agent 2-11%, solvent 63-81%;
Described active component is the mixture of the oxalic acid of equivalent, citric acid, ball spore element, oosporein, beauvericin, salicylic acid, phenyl-propane and iridoid glycoside composition; Described synergistic component is one or more mixtures in vitamin B1, laurene, paclobutrazol, citrene, guaiacol, oil of Cymbopogon winterianus; Described stabilizing agent is one or both mixtures in 1,2-butanediol, isopropyl phosphoric acid ester; Described solvent is one or more mixtures in ethanol, formic acid, water, glacial acetic acid.
2. the artificial repellant of a kind of Monochamus alternatus as described in right 1, is characterized in that the content of active component is 9-17%.
3. the artificial repellant of a kind of Monochamus alternatus as described in right 1, is characterized in that the content of synergistic component is 6-11%.
4. the artificial repellant of a kind of Monochamus alternatus as described in right 1, is characterized in that the content of stabilizing agent is 3-10%.
5. the artificial repellant of a kind of Monochamus alternatus as described in right 1, is characterized in that the content of solvent is 65-80%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210220602.9A CN102726463B (en) | 2012-06-29 | 2012-06-29 | The artificial repellant of a kind of Monochamus alternatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210220602.9A CN102726463B (en) | 2012-06-29 | 2012-06-29 | The artificial repellant of a kind of Monochamus alternatus |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102726463A CN102726463A (en) | 2012-10-17 |
| CN102726463B true CN102726463B (en) | 2015-07-29 |
Family
ID=46983342
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210220602.9A Expired - Fee Related CN102726463B (en) | 2012-06-29 | 2012-06-29 | The artificial repellant of a kind of Monochamus alternatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102726463B (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP6130986B2 (en) * | 2014-06-05 | 2017-05-17 | 理研香料ホールディングス株式会社 | Insect repellent and insect repellent method |
| CN105409506B (en) * | 2015-11-09 | 2018-07-13 | 广西壮族自治区农业科学院植物保护研究所 | Prevent preparation and its control method of the sugarcane top compost of crop root knot nematode disease |
| CN106942224B (en) * | 2017-04-28 | 2019-12-13 | 广东省微生物研究所（广东省微生物分析检测中心） | Application of oosporin in preparation of biopesticide |
| CN108684720A (en) * | 2018-06-28 | 2018-10-23 | 南京林衡农业科技有限公司 | A kind of repellant for Bursaphelenchus xylophilus communication media insect |
| CN110140733A (en) * | 2019-05-16 | 2019-08-20 | 南京生兴有害生物防治技术股份有限公司 | A kind of Monochamus alternatus repellant and its preparation method |
| CN110506745A (en) * | 2019-09-18 | 2019-11-29 | 南京生兴有害生物防治技术股份有限公司 | A kind of preparation method of Monochamus alternatus Hope compounding repellant |
| CN113303152A (en) * | 2021-06-11 | 2021-08-27 | 巢湖市友林林业有害生物防治有限公司 | Comprehensive treatment method for controlling spreading of longicorn disease epidemic situation |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1075845A (en) * | 1992-02-07 | 1993-09-08 | 株式会社共立 | The pest control chemicals of antagonism pine wood nematodes |
| CN1631168A (en) * | 2004-11-10 | 2005-06-29 | 中国科学院武汉植物园 | Insectifuge and its preparation method |
| CN102217592A (en) * | 2011-04-26 | 2011-10-19 | 福建省林业科学研究院 | Fungus sticking paste and making method and application of the fungus sticking paste |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2802773B1 (en) * | 1999-12-23 | 2003-01-03 | Centre Nat Rech Scient | USE OF WOOD WASTE OR EXTRACTS AS AN INSECTICIDE |
-
2012
- 2012-06-29 CN CN201210220602.9A patent/CN102726463B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1075845A (en) * | 1992-02-07 | 1993-09-08 | 株式会社共立 | The pest control chemicals of antagonism pine wood nematodes |
| CN1631168A (en) * | 2004-11-10 | 2005-06-29 | 中国科学院武汉植物园 | Insectifuge and its preparation method |
| CN102217592A (en) * | 2011-04-26 | 2011-10-19 | 福建省林业科学研究院 | Fungus sticking paste and making method and application of the fungus sticking paste |
Non-Patent Citations (1)
| Title |
|---|
| 松墨天牛成虫对幼虫虫粪挥发性物质的触角电位反应及林间驱避试验;李水清等;《昆虫学报》;20080430;第51卷(第3期);第284-289页 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102726463A (en) | 2012-10-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102726463B (en) | The artificial repellant of a kind of Monochamus alternatus | |
| Ma et al. | Insecticidal activity of essential oil from Cephalotaxus sinensis and its main components against various agricultural pests | |
| Monteiro et al. | Chemical composition and acaricide activity of an essential oil from a rare chemotype of Cinnamomum verum Presl on Rhipicephalus microplus (Acari: Ixodidae) | |
| PaVela | Effectiveness of some botanical insecticides against Spodoptera littoralis Boisduvala (Lepidoptera: Noctudiae), Myzus persicae Sulzer (Hemiptera: Aphididae) and Tetranychus urticae Koch (Acari: Tetranychidae) | |
| CN108633932A (en) | Injurious insect control formulation and manufacture and use its method | |
| CN107580927A (en) | A kind of pest control method of citrus | |
| CN101564051A (en) | Monochamus alternatus imago attractant | |
| Karemu et al. | Repellent effects of essential oils from selected eucalyptus species and their major constituents against Sitophilus zeamais (Coleoptera: Curculionidae) | |
| CN103329943A (en) | Insecticide composition containing natural celastrus angulatus and natural pyrethrin | |
| Ahmed et al. | Evaluation of plant extracts on mortality and tunneling activities of subterranean termites in Pakistan | |
| CN102499240A (en) | Monochamus alternatus adult attractant based on insect patient-oriented pheromone, preparation method and applications | |
| Radha et al. | Efficacy of plant extracts on the toxicity, ovipositional deterrence and damage assessment of the cowpea weevil, Callosobruchus maculatus (Coleoptera: Bruchidae) | |
| CN102487953A (en) | Buffalobur extract insecticide and preparation method thereof | |
| CN102860310B (en) | Synergistic insecticidal composition used for preventing and curing icerya purchasi maskell | |
| Chen et al. | Chemical composition and bioactivities of Alpinia Katsumadai Hayata seed essential oil against three stored product insects | |
| Reena et al. | Evaluation of Pongamia pinnata seed extracts as an insecticide against American bollworm Helicoverpa armigera (Hubner). | |
| CN101803605A (en) | Insecticidal composition of butene-fipronil and spinosad | |
| CN103355322A (en) | Compound biological insecticide and application thereof | |
| CN102487966B (en) | Botanical pesticide for effectively controlling Dioryctria splendidella Herrich-Schaeffer, preparation thereof and application thereof | |
| Rashid et al. | The effect of neem (Azadirachta indica) leaves extract on the ecdysis and mortality of immature stages of common house mosquito Culex pipiens fatigans | |
| CN104222117A (en) | Pesticide preparation containing spirotetramat for preventing and treating liriomyza sativae blanchard and bemisia tabaci | |
| CN103070186A (en) | Insecticidal composition containing thiamethoxam and application of insecticidal composition | |
| Nunes et al. | Control of the South American fruit fly in pear with natural-based products | |
| CN102246779A (en) | Pesticide composition containing spirotetramat and spinosad | |
| CN105052924A (en) | Apocheima cinerarius erschoff sex attractant |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150729 Termination date: 20160629 |