CN102716489A - Modified starch composition plant capsule and preparation method thereof - Google Patents
Modified starch composition plant capsule and preparation method thereof Download PDFInfo
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- CN102716489A CN102716489A CN2012101747658A CN201210174765A CN102716489A CN 102716489 A CN102716489 A CN 102716489A CN 2012101747658 A CN2012101747658 A CN 2012101747658A CN 201210174765 A CN201210174765 A CN 201210174765A CN 102716489 A CN102716489 A CN 102716489A
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Abstract
The invention mainly discloses a modified starch composition plant capsule and a preparation method of the capsule. According to the preparation method, alkenyl succinic acid starch ester or other compositions is/are uniformly mixed, dispersed in distilled water, and then heated at the temperature of 60-90 DEG C for 15-30 minutes to enable the modified starch to be fully pasted, then a plasticizer, gels and other additives (like surfactant, opacifier, food colourant, preservative, antioxidant and intensifer) are added into the mixture according to the ratios, decompressing and deforming are carried out after the mixture is fully mixed, so as to obtain the hollow starch composition plant capsule made by means of glue solution viscose process, wherein the capsule temperature is 30-50 DEG C and the drying operation lasts for 24-48 hours to obtain a finished product of the capsule. The modified starch composition plant capsule has the advantages that the modified starch composition is taken as a main raw material, the starch is purely natural and is free from pollution, in addition the sources of the raw material are wide, and the production cost is low.
Description
Technical field
The present invention relates to medical and health, health product, cosmetics and functional food technical field, special relevant with a kind of modified starch compositions plant capsule and preparation method thereof.
Background technology
The capsule major part is that gelatin is processed at present, and gelatin is derived from skin or the skeleton of animal, and gelatin has following shortcoming:
1, the gelatin quality is influenced by animal health condition, and the edible animal sources gelatin of suffering from disease is prone to source of disease is propagated, and causes cross infection, causes food safety hidden danger;
2, gelatin source restriction, present domestic gelatin market receives the influence of poultry breeding stock, and be becoming tight in the source;
3, Islamic world, India, Jewry need carry out authentication to its source to special type source gelatin sensitivity, even so also can't guarantee its source absoluteness;
In addition, Buddhist, vegetarian avoid for gelatine capsule.
Therefore, plant capsule arises at the historic moment, and becomes the new lover in medical and health, health product, cosmetics and functional food market.At present, cellulose capsule has been applied to some medicine, health product, but because its cost of material is higher, can't contend with traditional gelatine capsule in price.
Summary of the invention
The purpose of this invention is to provide a kind of low cost, modified starch compositions plant capsule of natural reproducible and preparation method thereof.
In order to achieve the above object, the present invention realizes through following technical scheme:
A kind of modified starch compositions plant capsule, its component and content are following:
| Form | Percentage by weight |
| Starch octenyl succinate anhydride | 5～15% |
| Plasticizer | 1.25～4% |
| Gel | 0.25～1% |
| Other additives | 0～3% |
| Distilled water | 77～93.5% |
A kind of method for preparing of modified starch compositions plant capsule is following:
Starch octenyl succinate anhydride is dispersed in the distilled water, is warmed up to 60-90 ℃, heated 15-30 minute; Make the abundant gelatinizing of starch, add plasticizer and gel in proportion, and other additives; Vacuum defoaming behind the abundant mix homogeneously, the glue viscose process that obtains makes modified starch compositions plant hollow capsule, 30-50 ℃ of encystation temperature; Dry 24-48 hour, make capsule finished product.
Described starch octenyl succinate anhydride substitution value is 0.001-0.02.
The raw starch of said starch octenyl succinate anhydride can be one or more mixture in corn starch, potato starch, tapioca, rice starch, wheaten starch, sweet potato starch, green starch, pea starch, the Semen Viciae fabae starch; Also can be above cross-linking of starch or catabolite, the perhaps any mixture of ative starch, crosslinked starch and degradable starch.
Described plasticizer is polysaccharide or polyalcohols.
Described plasticizer is maltodextrin, maltose, Oligomeric maltose, one or several mixture in trehalose, sucrose, fructose, glycerol, Polyethylene Glycol, xylitol, mannitol, maltose alcohol, the Sorbitol.
Described gellant is one or more of arabic gum, carrageenan, Resina persicae, agar, locust bean gum, guar gum, tamarind gum, POLY-karaya, Tragacanth, pectin, pulullan polysaccharide, xanthan gum, kanjak mannan glue, gellan gum curdlan, sodium carboxymethyl cellulose or chitosan.
Described other additives are one or several mixture in surfactant, opacifier, food coloring, antiseptic, antioxidant or the reinforcing agent.
In described other additives, surfactant is a dodecyl sodium sulfate; Opacifier such as titanium dioxide; Food coloring is carmine; Antiseptic is a sodium benzoate; Antioxidant is ascorbic acid; Reinforcing agent is a polyvinylpyrrolidone.
After adopting such scheme, the present invention has many beneficial effects:
1, be that the capsule of primary raw material is the pure natural plant capsule with the modified starch, high safety can not spread disease, and is difficult for by infected by microbes yet.
2, be that the capsule of primary raw material is that the pure natural plant capsule does not contain gelatin with the modified starch, can satisfy the demand of special populations such as Islamic person, vegetarian.
3, the starch material source is wide, renewable, cost is low, and product has price advantage.
The specific embodiment
Embodiment 1
A kind of modified starch compositions plant capsule, its component and content are following:
| Form | Percentage by weight |
| Starch octenyl succinate anhydride | 15% |
| Mannitol | 4% |
| Carrageenan | 1% |
| Dodecylbenzene sodium sulfonate | 0.2% |
| Distilled water | 79.8% |
It is dispersed in the distilled water for the starch octenyl succinate anhydride (substitution value is 0.02) with the preparation of degrading maize starch, is warmed up to 60 ℃, heats 15 minutes; Make the abundant gelatinizing of starch octenyl succinate anhydride, add 4% mannitol, 1% carrageenan; Add 0.2% dodecylbenzene sodium sulfonate, vacuum defoaming behind the abundant mix homogeneously, the glue viscose process that obtains makes modified starch compositions plant hollow capsule; 30 ℃ of encystation temperature dry 48 hours, make capsule finished product.
Embodiment 2
A kind of modified starch compositions plant capsule, its component and content are following:
| Form | Percentage by weight |
| Starch octenyl succinate anhydride | 5% |
| Polyethylene Glycol | 3% |
| Arabic gum | 0.5% |
| Sodium benzoate | 0.1% |
| Distilled water | 91.4% |
Method for preparing is warmed up to 90 ℃ for the starch octenyl succinate anhydride (substitution value is 0.01) with the cross-linked potato starch preparation is dispersed in the distilled water, heats 30 minutes; Make the abundant gelatinizing of modified starch, add 3% Polyethylene Glycol, 0.5% arabic gum; Add 0.1% sodium benzoate, vacuum defoaming behind the abundant mix homogeneously, the glue viscose process that obtains makes modified starch compositions plant hollow capsule; 50 ℃ of encystation temperature dry 48 hours, make capsule finished product.
Embodiment 3
A kind of modified starch compositions plant capsule, its component and content are following:
| Form | Percentage by weight |
| Starch octenyl succinate anhydride | 10% |
| Fructose | 4% |
| Agar | 1% |
| Distilled water | 85% |
Method for preparing is warmed up to 70 ℃ for the starch octenyl succinate anhydride (substitution value is 0.015) with the rice starch preparation is dispersed in the distilled water, heats 20 minutes; Make the abundant gelatinizing of modified starch, add 4% fructose, 1% agar; Vacuum defoaming behind the abundant mix homogeneously, the glue viscose process that obtains makes modified starch compositions plant hollow capsule, 40 ℃ of encystation temperature; Dry 24 hours, make capsule finished product.
Embodiment 4
A kind of modified starch compositions plant capsule, its component and content are following:
| Form | Percentage by weight |
| Starch octenyl succinate anhydride | 8% |
| Maltose alcohol | 3% |
| Xanthan gum | 0.25% |
| Titanium dioxide | 0.2% |
| Distilled water | 88.55% |
Method for preparing is warmed up to 80 ℃ for the starch octenyl succinate anhydride (substitution value is 0.005) with the pea starch preparation is dispersed in the distilled water, heats 15 minutes; Make the abundant gelatinizing of modified starch, add 3% maltose alcohol, 0.25% xanthan gum; Add 0.2% titanium dioxide, vacuum defoaming behind the abundant mix homogeneously, the glue viscose process that obtains makes modified starch compositions plant hollow capsule; 30 ℃ of encystation temperature dry 36 hours, make capsule finished product.
Embodiment 5
A kind of modified starch compositions plant capsule, its component and content are following:
| Form | Percentage by weight |
| Starch octenyl succinate anhydride | 15% |
| Maltodextrin | 2% |
| Glycerol | 2% |
| Tragacanth | 1% |
| Distilled water | 80% |
Method for preparing is warmed up to 90 ℃ for the starch octenyl succinate anhydride (substitution value is 0.001) with crosslinked sweet potato starch preparation is dispersed in the distilled water, heats 30 minutes; Make the abundant gelatinizing of modified starch, add 2% maltodextrin, add 2% glycerol; Add 1% Tragacanth, vacuum defoaming behind the abundant mix homogeneously, the glue viscose process that obtains makes modified starch compositions plant hollow capsule; 50 ℃ of encystation temperature dry 48 hours, make capsule finished product.
Embodiment 6
A kind of modified starch compositions plant capsule, its component and content are following:
| Form | Percentage by weight |
| Starch octenyl succinate anhydride | 12% |
| Fructose | 1% |
| Xylitol | 3% |
| Tamarind gum | 0.5% |
| POLY-karaya | 0.5% |
| Distilled water | 83% |
Method for preparing is warmed up to 85 ℃ for the starch octenyl succinate anhydride (substitution value is 0.018) with the corn starch preparation is dispersed in the distilled water, heats 25 minutes, makes the abundant gelatinizing of modified starch; Add 1% fructose, 3% xylitol, 0.5% tamarind gum; 0.5% POLY-karaya, vacuum defoaming behind the abundant mix homogeneously, the glue viscose process that obtains makes modified starch compositions plant hollow capsule; 40 ℃ of encystation temperature dry 24 hours, make capsule finished product.
Embodiment 7
A kind of modified starch compositions plant capsule, its component and content are following:
| Form | Percentage by weight |
| Starch octenyl succinate anhydride | 12% |
| Fructose | 1.25% |
| Tamarind gum | 0.5% |
| POLY-karaya | 0.5% |
| Dodecyl sodium sulfate | 0.4% |
| Carmine | 0.1% |
| Sodium benzoate | 0.1% |
| Ascorbic acid | 0.2% |
| Polyvinylpyrrolidone | 2.2% |
| Distilled water | 82.75% |
Method for preparing is warmed up to 85 ℃ for the starch octenyl succinate anhydride (substitution value is 0.018) with the corn starch preparation is dispersed in the distilled water, heats 25 minutes, makes the abundant gelatinizing of modified starch; Add 1.25% fructose, 3% xylitol, 0.5% tamarind gum, 0.5% POLY-karaya; 3% other additives (0.4% dodecyl sodium sulfate, 0.1% carmine, 0.1% sodium benzoate; 0.2% ascorbic acid, 2.2% polyvinylpyrrolidone) abundant vacuum defoaming behind the mix homogeneously, the glue viscose process that obtains makes modified starch compositions plant hollow capsule; 40 ℃ of encystation temperature dry 24 hours, make capsule finished product.
The foregoing description only is used to the inventive concept of the present invention of explaining, but not to the qualification of rights protection of the present invention, allly utilizes this design that the present invention is carried out the change of unsubstantiality, all should fall into protection scope of the present invention.
Claims (10)
1. modified starch compositions plant capsule, its component and content are following:
。
2. a kind of modified starch compositions plant capsule as claimed in claim 1, it is characterized in that: described plasticizer is polysaccharide or polyalcohols; Described gellant is one or more of arabic gum, carrageenan, Resina persicae, agar, locust bean gum, guar gum, tamarind gum, POLY-karaya, Tragacanth, pectin, pulullan polysaccharide, xanthan gum, kanjak mannan glue, gellan gum curdlan, sodium carboxymethyl cellulose or chitosan.
3. the method for preparing of a modified starch compositions plant capsule is characterized in that:
Starch octenyl succinate anhydride is dispersed in the distilled water, is warmed up to 60-90 ℃, heated 15-30 minute; Make the abundant gelatinizing of starch, add plasticizer and gel in proportion, and other additives; Vacuum defoaming behind the abundant mix homogeneously, the glue viscose process that obtains makes modified starch compositions plant hollow capsule, 30-50 ℃ of encystation temperature; Dry 24-48 hour, make capsule finished product.
4. the method for preparing of a kind of modified starch compositions plant capsule as claimed in claim 3 is characterized in that: described starch octenyl succinate anhydride substitution value is 0.001-0.02.
5. the method for preparing of a kind of modified starch compositions plant capsule as claimed in claim 3; It is characterized in that: the raw starch of starch octenyl succinate anhydride can be one or more mixture in corn starch, potato starch, tapioca, rice starch, wheaten starch, sweet potato starch, green starch, pea starch, the Semen Viciae fabae starch; Also can be above cross-linking of starch or catabolite, the perhaps any mixture of ative starch, crosslinked starch and degradable starch.
6. the method for preparing of a kind of modified starch compositions plant capsule as claimed in claim 3 is characterized in that: described plasticizer is polysaccharide or polyalcohols.
7. the method for preparing of a kind of modified starch compositions plant capsule as claimed in claim 3; It is characterized in that: described plasticizer is maltodextrin, maltose, Oligomeric maltose, one or several mixture in trehalose, sucrose, fructose, glycerol, Polyethylene Glycol, xylitol, mannitol, maltose alcohol, the Sorbitol.
8. the method for preparing of a kind of modified starch compositions plant capsule as claimed in claim 3 is characterized in that: described gellant is one or more of arabic gum, carrageenan, Resina persicae, agar, locust bean gum, guar gum, tamarind gum, POLY-karaya, Tragacanth, pectin, pulullan polysaccharide, xanthan gum, kanjak mannan glue, gellan gum curdlan, sodium carboxymethyl cellulose or chitosan.
9. the method for preparing of a kind of modified starch compositions plant capsule as claimed in claim 3 is characterized in that: described other additives are one or several mixture in surfactant, opacifier, food coloring, antiseptic, antioxidant or the reinforcing agent.
10. the method for preparing of a kind of modified starch compositions plant capsule as claimed in claim 3 is characterized in that: in described other additives, surfactant is a dodecyl sodium sulfate; Opacifier such as titanium dioxide; Food coloring is carmine; Antiseptic is a sodium benzoate; Antioxidant is ascorbic acid; Reinforcing agent is a polyvinylpyrrolidone.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012101747658A CN102716489A (en) | 2012-05-31 | 2012-05-31 | Modified starch composition plant capsule and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012101747658A CN102716489A (en) | 2012-05-31 | 2012-05-31 | Modified starch composition plant capsule and preparation method thereof |
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| CN2012101747658A Pending CN102716489A (en) | 2012-05-31 | 2012-05-31 | Modified starch composition plant capsule and preparation method thereof |
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| CN103933574A (en) * | 2014-04-01 | 2014-07-23 | 中国科学院化学研究所 | Vegetable jelly for preparing hollow capsules, and applications of vegetable jelly |
| CN104042589A (en) * | 2014-06-20 | 2014-09-17 | 刘杰 | Capsule without animal proteins and preparation method thereof |
| CN104055748A (en) * | 2013-03-21 | 2014-09-24 | 中国科学院化学研究所 | Composition for preparing modified starch matrix-containing hard capsule |
| CN104056274A (en) * | 2013-03-21 | 2014-09-24 | 中国科学院化学研究所 | Reinforcing and toughening agent for preparing starch hard capsule and application thereof |
| CN104146984A (en) * | 2014-08-07 | 2014-11-19 | 陕西科技大学 | Method for preparing hollow plant capsules from celery and starch |
| CN104738627A (en) * | 2015-03-31 | 2015-07-01 | 甘肃圣大方舟马铃薯变性淀粉有限公司 | Vitamin linseed oil compounded soft capsule and preparation method thereof |
| CN104800852A (en) * | 2015-05-04 | 2015-07-29 | 湖南尔康制药股份有限公司 | Method for melting gelatin for preparing starch hollow capsule |
| CN104873977A (en) * | 2015-05-08 | 2015-09-02 | 浙江万里学院 | Special glue for composite starch and preparation method of empty capsule of special glue |
| CN105395513A (en) * | 2015-12-02 | 2016-03-16 | 湖南尔康制药股份有限公司 | Method for preparing hard capsule from modified starch |
| CN105694118A (en) * | 2016-01-29 | 2016-06-22 | 上海盈美机电工程有限公司 | Novel lightly crosslinked-starch succinate-based empty capsule and preparation method thereof |
| CN105832698A (en) * | 2016-04-19 | 2016-08-10 | 常州市蓝勖化工有限公司 | Method for preparing hollow capsule shells by using ocentyl succinic anhydride taro starch ester |
| CN105997928A (en) * | 2016-05-20 | 2016-10-12 | 夏放军 | Sweet hollow capsule and preparation method thereof |
| CN105997930A (en) * | 2016-07-04 | 2016-10-12 | 安顺济世科技有限公司 | Empty capsule and soft capsule based on modified starch |
| CN106666822A (en) * | 2016-11-29 | 2017-05-17 | 将军烟草集团有限公司 | Cigarette blast bead and preparation method thereof |
| CN107188978A (en) * | 2017-07-04 | 2017-09-22 | 华南理工大学 | A kind of starch octenyl succinate anhydride and its preparation method and application |
| CN107496371A (en) * | 2016-06-14 | 2017-12-22 | 中国科学院化学研究所 | A kind of starch matrix Capsules with biology auxiliary sexual function pharmacological action |
| CN108851154A (en) * | 2017-05-11 | 2018-11-23 | 康师傅饮品控股有限公司 | Embedded particles and preparation method thereof |
| CN112552555A (en) * | 2020-12-31 | 2021-03-26 | 河南省化工研究所有限责任公司 | Preparation method of modified high amylose-based plant capsule |
| CN113041229A (en) * | 2021-02-09 | 2021-06-29 | 深圳市新指南医学科技发展有限公司 | Modified potato starch empty capsule shell and preparation method thereof |
| CN113365596A (en) * | 2019-02-04 | 2021-09-07 | 奇华顿股份有限公司 | Improvements in or relating to organic compounds |
| CN114788820A (en) * | 2022-04-18 | 2022-07-26 | 陕西省动物研究所 | Starch matrix empty capsule with biological auxiliary function pharmacological action |
| CN116196289A (en) * | 2023-03-09 | 2023-06-02 | 上海荃吉康医药科技有限公司 | Medical capsule composite adhesive and raw material proportion and preparation method thereof |
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| CN104055748A (en) * | 2013-03-21 | 2014-09-24 | 中国科学院化学研究所 | Composition for preparing modified starch matrix-containing hard capsule |
| CN104056274A (en) * | 2013-03-21 | 2014-09-24 | 中国科学院化学研究所 | Reinforcing and toughening agent for preparing starch hard capsule and application thereof |
| CN104056274B (en) * | 2013-03-21 | 2016-12-28 | 中国科学院化学研究所 | For preparing activeness and quietness agent and the purposes of starch hard capsule |
| CN104055748B (en) * | 2013-03-21 | 2018-12-25 | 中国科学院化学研究所 | It is used to prepare the composition of the hard capsule comprising converted starch matrix |
| CN103933574A (en) * | 2014-04-01 | 2014-07-23 | 中国科学院化学研究所 | Vegetable jelly for preparing hollow capsules, and applications of vegetable jelly |
| CN103933574B (en) * | 2014-04-01 | 2016-05-11 | 中国科学院化学研究所 | For the preparation of phyteral glue and the application thereof of Capsules |
| CN104042589B (en) * | 2014-06-20 | 2016-04-06 | 刘杰 | Capsule of a kind of animal protein-free and preparation method thereof |
| CN104042589A (en) * | 2014-06-20 | 2014-09-17 | 刘杰 | Capsule without animal proteins and preparation method thereof |
| CN104146984A (en) * | 2014-08-07 | 2014-11-19 | 陕西科技大学 | Method for preparing hollow plant capsules from celery and starch |
| CN104146984B (en) * | 2014-08-07 | 2017-06-16 | 陕西科技大学 | A kind of method for preparing plant hollow capsule with celery and starch |
| CN104738627A (en) * | 2015-03-31 | 2015-07-01 | 甘肃圣大方舟马铃薯变性淀粉有限公司 | Vitamin linseed oil compounded soft capsule and preparation method thereof |
| CN104800852A (en) * | 2015-05-04 | 2015-07-29 | 湖南尔康制药股份有限公司 | Method for melting gelatin for preparing starch hollow capsule |
| CN104800852B (en) * | 2015-05-04 | 2017-12-22 | 湖南尔康制药股份有限公司 | A kind of sol gel process for being used to prepare starch hollow capsule |
| CN104873977A (en) * | 2015-05-08 | 2015-09-02 | 浙江万里学院 | Special glue for composite starch and preparation method of empty capsule of special glue |
| CN104873977B (en) * | 2015-05-08 | 2018-01-30 | 浙江万里学院 | The preparation method of composite starch special glue and its Capsules |
| CN105395513A (en) * | 2015-12-02 | 2016-03-16 | 湖南尔康制药股份有限公司 | Method for preparing hard capsule from modified starch |
| CN105395513B (en) * | 2015-12-02 | 2017-09-22 | 湖南尔康制药股份有限公司 | A kind of method that modified starch prepares hard shell capsules |
| CN105694118A (en) * | 2016-01-29 | 2016-06-22 | 上海盈美机电工程有限公司 | Novel lightly crosslinked-starch succinate-based empty capsule and preparation method thereof |
| CN105832698A (en) * | 2016-04-19 | 2016-08-10 | 常州市蓝勖化工有限公司 | Method for preparing hollow capsule shells by using ocentyl succinic anhydride taro starch ester |
| CN105997928A (en) * | 2016-05-20 | 2016-10-12 | 夏放军 | Sweet hollow capsule and preparation method thereof |
| CN107496371A (en) * | 2016-06-14 | 2017-12-22 | 中国科学院化学研究所 | A kind of starch matrix Capsules with biology auxiliary sexual function pharmacological action |
| CN105997930A (en) * | 2016-07-04 | 2016-10-12 | 安顺济世科技有限公司 | Empty capsule and soft capsule based on modified starch |
| CN106666822A (en) * | 2016-11-29 | 2017-05-17 | 将军烟草集团有限公司 | Cigarette blast bead and preparation method thereof |
| CN108851154A (en) * | 2017-05-11 | 2018-11-23 | 康师傅饮品控股有限公司 | Embedded particles and preparation method thereof |
| CN107188978A (en) * | 2017-07-04 | 2017-09-22 | 华南理工大学 | A kind of starch octenyl succinate anhydride and its preparation method and application |
| CN113365596A (en) * | 2019-02-04 | 2021-09-07 | 奇华顿股份有限公司 | Improvements in or relating to organic compounds |
| CN112552555A (en) * | 2020-12-31 | 2021-03-26 | 河南省化工研究所有限责任公司 | Preparation method of modified high amylose-based plant capsule |
| CN113041229A (en) * | 2021-02-09 | 2021-06-29 | 深圳市新指南医学科技发展有限公司 | Modified potato starch empty capsule shell and preparation method thereof |
| CN114788820A (en) * | 2022-04-18 | 2022-07-26 | 陕西省动物研究所 | Starch matrix empty capsule with biological auxiliary function pharmacological action |
| CN116196289A (en) * | 2023-03-09 | 2023-06-02 | 上海荃吉康医药科技有限公司 | Medical capsule composite adhesive and raw material proportion and preparation method thereof |
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Application publication date: 20121010 |