CN102697129B - Semen hoveniae plant beverage and preparation method thereof - Google Patents
Semen hoveniae plant beverage and preparation method thereof Download PDFInfo
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- CN102697129B CN102697129B CN201210159806.6A CN201210159806A CN102697129B CN 102697129 B CN102697129 B CN 102697129B CN 201210159806 A CN201210159806 A CN 201210159806A CN 102697129 B CN102697129 B CN 102697129B
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Abstract
The invention discloses a semen hoveniae plant beverage and a preparation method thereof. The preparation method comprises the following steps: mixing 15g of semen hoveniae and 15g of pueraria lobata, and adding water as heavy as five times of the obtained mixture for soaking for 30 minutes; boiling by intense fire, and then keeping faint boiling by soft fire for decocting for 1 hour; filtering and collecting a first-time extracting solution; adding water as heavy as three times to obtain residues, and boiling by the intense fire; then keeping faint boiling by the soft fire for 1 hour, filtering and collecting a second-time extracting solution; merging the two extracting solutions, and concentrating to obtain a concentrated solution with a relative density of 1.05-1.1 at a temperature of 60 DEG C; adding the obtained concentrated solution and 0.002-0.006g of sucralose to a proper quantity of pure water, dissolving, and then puttingthe obtained mixture into a constant volume pot for obtaining a constant volume of 180ml by using pure water; uniformly stirring, and then heating for boiling; and filtering, hot encapsulating, sterilizing and packaging to obtain the semen hoveniae plant beverage. The semen hoveniae plant beverage has the effects of preventing the human bodies from being damaged after drinking and avoiding chemical liver injury caused by drinking too much; and the semen hoveniae plant beverage has the advantages of simple preparation process, no introduction of organic solvents, no organic solvent residue and easiness of production.
Description
Technical field
The present invention relates to a kind of hoveniae semoveniae semen plant beverage and preparation method thereof.
Background technology
Spirits culture is the pith in Chinese food culture, and people participate in the activities such as social activity is entertained, commercial affairs are entertained, friend gets together in daily life, usually need to drink, and actively or passively, the situation of drinking beyond one's capacity.Often unconsciousness, vexed gas are hot-tempered in drunk for people, follow the situations such as appearance action is out of control, thirsty, n and V.Alcohol enters after human body, is mainly to carry out catabolism at liver, and the cocktail party of excess intake causes damage to liver, and long-term excessive consumption of alcohol also can cause fatty liver diseases, and health is caused to great harm.
FI puerariae is the flower of elegant jessamine, and nature and flavor are sweet cool, for relieving the effect of alcohol, sober up, apocleisis, vomiting etc.The FI puerariae soup of neutralizing the effect of alcoholic drinks is the prescription that represents of sobering up in Chinese prescription, for diseases such as alcoholism, poor appetites.Hoveniae semoveniae semen is the seed of Rhamnaceae plant trifoliate orange Dulcis, and the sweet acid of nature and flavor, flat is nontoxic, has the effect of reducing fever and causing diuresis, relieving alcoholism, cures mainly the diseases such as wine disease, dysphoria with smothery sensation, thirsty, vomiting, difficulty in urination and defecation.
Sober-up function based on FI puerariae and hoveniae semoveniae semen itself, existing researcher provides report to the independent extract of FI puerariae or hoveniae semoveniae semen or by the sobering up and liver protecting functions that FI puerariae and hoveniae semoveniae semen form relieving alcoholism and protecting liver composition at present.
But existing achievement in research is generally that FI puerariae is combined with hoveniae semoveniae semen and other Chinese herbal medicine, what bring into play is the common effect of multiple Chinese herbal medicine, a kind of alcohol-neutralize healthy product as disclosed in Chinese patent application CN200410090260.9, take the root of kudzu vine, FI puerariae, hoveniae semoveniae semen and Radix Glycyrrhizae as base-material; Or add other active Chinese drug component component to improve in the existing Chinese medicine recipes such as soup of neutralizing the effect of alcoholic drinks FI puerariae, a kind of sober-up oral liquid as disclosed in Chinese patent application CN200910017610.1, has comprised the various ingredients such as FI puerariae, hoveniae semoveniae semen, olive, dark plum, Poria cocos, coix seed, fructus amomi, dried orange peel, rde bean, ginger; The disclosed a kind of alcohol-dissolving liver-protecting drink of Chinese patent application CN200510035837.0, comprises shitosan, glycyrrhizin, FI puerariae water extract and hoveniae semoveniae semen water extraction liquid, and wherein glycyrrhizin has played important function of detoxification.Existing about FI puerariae and hoveniae semoveniae semen relieve the effect of alcohol formula in, be mostly take that FI puerariae is as monarch drug in a prescription, other important traditional Chinese medicine ingredients are ministerial drug simultaneously.Because adopt multiple Chinese herbal medicine and other raw materials, the more complicated of raw material composition own, the extraction preparation process of various Chinese herbal medicines is used multi-solvents, especially organic solvent, and security and effect are difficult to assurance, and cost is very high.
The more important thing is, existing research is the drug research based on prevention or treatment use substantially, about the pure herbaceous plant beverage obtaining with FI puerariae and two kinds of active fraction preparations of hoveniae semoveniae semen, has no any technology report.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, a kind of hoveniae semoveniae semen plant beverage is provided, this hoveniae semoveniae semen plant beverage raw material is simple, has the effect of relieving the effect of alcohol significantly and protecting liver.
Another object of the present invention is to provide the preparation method of described hoveniae semoveniae semen plant beverage, the preparation method of described hoveniae semoveniae semen plant beverage, does not have the pollution of organic solvent in technique, there is not the problem of organic solvent residual, technique is simple, is easy to produce, more healthy and safe.
Above-mentioned purpose of the present invention is achieved by following technical solution:
A kind of hoveniae semoveniae semen plant beverage is provided, and described hoveniae semoveniae semen plant beverage prepares by the following method:
(1) by after 15g hoveniae semoveniae semen and the mixing of 15g FI puerariae, under normal temperature, add the light water that is equivalent to 5 times of weight of mixture to soak 30 minutes, after then big fire is boiled, with little fire, keep micro-boiling to decoct 1 hour, extract is for the first time collected in filtration; Toward filtering in the residue obtaining, add again the light water with respect to 3 times of weight of residue, with big fire, boiling the little fire of rear use again keeps micro-boiling to decoct 1 hour, extract is for the second time collected in filtration, extracted twice liquid is merged, then the extract of merging is concentrated and obtains the concentrate that at 60 ℃, relative density is 1.05 ~ 1.1;
(2) step (1) gained concentrate and Sucralose 0.002 ~ 0.006g are added in appropriate purified water, dissolve, be then placed in constant volume tank and be settled to 180ml by purified water, after stirring, heating is boiled, and filters hot embedding, sterilizing, packs and obtains described hoveniae semoveniae semen plant beverage.
As a kind of more preferably scheme, in step (2), described filtration was preferably 400 object silks.
As a kind of more preferably scheme, in step (2), described sterilizing is steam sterilizing 30 minutes at 121 ℃.
As a kind of most preferably scheme, in step (2), the addition of described Sucralose is 0.004g.Under this addition, plant beverage obtains best mouthfeel.
Compared with prior art, the present invention has following beneficial effect:
The present invention prepares hoveniae semoveniae semen plant beverage, has given full play to the sober-up function of FI puerariae and hoveniae semoveniae semen, before and after drinking, drinks beverage of the present invention, can effectively relieve the effect of alcohol, and liver protecting; Healthy and safe because of it, local flavor is excellent, fresh and sweet good to eat, in the situation that not drinking, also can be used as a kind of health drink, daily drinking.Hoveniae semoveniae semen plant beverage of the present invention is not containing any chemical composition, and or not containing anticorrisive agent and additive, useful and harmless to human body, men and women, old and young all can relievedly not drink.
By analysis, mainly contain saponin(e, alkaloid, Flavonoid substances, aliphatic acid isoreactivity composition in hoveniae semoveniae semen, described saponin(e comprises trifoliate orange Dulcis saponin A 1, A2, B1, B2 and hovenia dulcis saponin(e; Described alkaloid is loline and the frangulanine of β-carboine system; Described Flavonoid substances comprises Kaempferol, Quercetin, isoquercitin, Kaempferol-O-α-pyrans rhamnose (1-6)-β-D-galactopyranoside, Quercetin-3-O-α-L-pyrans rhamnose, the fragrant sugar of Kaempferol-O-cloud and rutin, two hydrogen Kaempferols, (+)-3,3 ', 5,5 ', 7-penta hydroxy group flavanone and (+)-Ampeloptin etc.; Flavonoid substances is the main active in trifoliate orange Dulcis platymiscium hepatoprotective effect.Hoveniae semoveniae semen aqueous extract can obviously shorten alcohol induced mouse sleep time, reduce the concentration of ethanol in blood, reduce mda content and can improve glutathione peroxidase activity, can stop the mouse liver MDA due to ethanol to raise and GSH decline, to the protective effect of ethanol induced mice hepatic lipid peroxidation tool, cholesterol due to reduction ethanol, triglyceride increases, point out it likely to delay and prevent the formation of the fatty liver due to ethanol, can obviously reduce the Serum ALT that ethanol causes, AST raises, in histology, can obviously improve hepatocellular steatosis and inflammation downright bad.In FI puerariae, mainly contain flavonoids, Coumarins, saponin class, steroid, terpene, sugar, glycoside, organic acid, volatilization wet goods material, not containing Anthraquinones or alkaloids substance.In FI puerariae, contained flavonoids is mainly isoflavone glycoside material.In Flos puerariae lobatae extract, contained isoflavones can reduce Ethanol concentration in rat blood after drinking, the rising of ADH activity and reduction BUN in enhancing liver, thus play antialcoholism action.FI puerariae water extraction liquid can promote the internal metabolism of ethanol, reduces the generation of MDA, improves the antioxidation that GST is active, strengthen the antioxidant system of glutathione (GSH).
The present invention is analyzing on the contained active component and special efficacy basis of FI puerariae and hoveniae semoveniae semen, adopt water to extract FI puerariae and hoveniae semoveniae semen simultaneously, and determined the extraction process condition that is simultaneously applicable to FI puerariae and hoveniae semoveniae semen, under short, few prerequisite that consumes energy consuming time, effectively guarantee the activity of extract, the effect that relieves the effect of alcohol provided by the invention has proved that the inventive method extracts the active ingredient in hoveniae semoveniae semen and FI puerariae effectively.
The present invention is further condensed into extract the concentrate of certain density, on the basis of the specific concentrate of the present invention, by rational compatibility and proportioning, only add the sweetener of denier, just can make all good hoveniae semoveniae semen plant beverages of local flavor, mouthfeel, sugariness, and there is the remarkable efficacy that prevents from being harmful to the health after drinking, avoids because taking in chemical damage that capacity for liquor too much causes, alleviates uncomfortable sensation after drinking, shortens the time of sobering up.
Hoveniae semoveniae semen plant beverage raw material of the present invention is easy to get, and preparation technology is simple, does not introduce any organic solvent and to the disadvantageous composition of health, healthy and safe, meets very much the demand of the modern life.
The specific embodiment
Below in conjunction with specific embodiment, the invention will be further described, but embodiments of the present invention is not limited in any way.
embodiment 1
The preparation method of hoveniae semoveniae semen plant beverage of the present invention:
(1) get 15 grams of hoveniae semoveniae semens, 15 grams of FI puerariaes, add in 150 grams of light waters under normal temperature, soak 30 minutes, after then big fire is boiled, little fire keeps micro-boiling to decoct 1 hour, filters, and collects respectively extract and residue for the first time;
(2) in residue, add 90 grams of light waters, then after boiling with big fire, with little fire, keep micro-boiling to decoct 1 hour, collect extract for the second time;
(3) merge extract and for the second time extract for the first time, at 60 ~ 85 ℃, adopt Vacuum Concentration method that extract is concentrated into the concentrate that at 60 ℃, relative density is 1.05;
(4) above-mentioned concentrate, Sucralose 0.002g are added in appropriate purified water, dissolve, then be placed in constant volume tank and be settled to 180ml by purified water, after stirring, heating is boiled, cross 400 order silks, carry out hot embedding, every bottle of 180ml, 121 ℃ of steam sterilizings 30 minutes, are packaged to be described hoveniae semoveniae semen plant beverage.Described hoveniae semoveniae semen plant beverage product characteristics are shown in Table 1.
embodiment 2
(1) get 15 grams of hoveniae semoveniae semens, 15 grams of FI puerariaes, under normal temperature, add in 150 grams of light waters, soak 30 minutes, after then big fire is boiled, little fire keeps micro-boiling to decoct 1 hour, filters, and collects respectively extract and residue for the first time;
(2) in residue, add 90 grams of light waters, then after boiling with big fire, with little fire, keep micro-boiling to decoct 1 hour, collect extract for the second time;
(3) merge extract and for the second time extract for the first time, at 60 ~ 85 ℃, adopt Vacuum Concentration method that extract is concentrated into the concentrate that at 60 ℃, relative density is 1.06;
(4) by above-mentioned concentrate, Sucralose 0.004g, add in appropriate purified water, dissolve, then be placed in constant volume tank and be settled to 180ml by purified water, after stirring, heating is boiled, and crosses 400 order silks, carry out hot embedding, every bottle of 180ml, 121 ℃ of steam sterilizings 30 minutes, are packaged to be described hoveniae semoveniae semen plant beverage.Described hoveniae semoveniae semen plant beverage product characteristics are shown in Table 1.
embodiment 3
(1) get 15 grams of hoveniae semoveniae semens, 15 grams of FI puerariaes, add in 150 grams of light waters, soak 30 minutes, after then big fire is boiled, little fire keeps micro-boiling to decoct 1 hour, filters, and collects respectively extract and residue for the first time;
(2) in residue, add 90 grams of light waters, then after big fire boils, little fire keeps micro-boiling to decoct 1 hour, collects extract for the second time;
(3) merge extract and for the second time extract for the first time, at 60 ~ 85 ℃, adopt Vacuum Concentration method that extract is concentrated into the concentrate that at 60 ℃, relative density is 1.7;
(4) by above-mentioned concentrate, Sucralose 0.006g, add in appropriate purified water, dissolve, then be placed in constant volume tank and be settled to 180ml by purified water, after stirring, heating is boiled, and crosses 400 order silks, carry out hot embedding, every bottle of 180ml, 121 ℃ of steam sterilizings 30 minutes, are packaged to be described hoveniae semoveniae semen plant beverage.Described hoveniae semoveniae semen plant beverage product characteristics are shown in Table 1.
embodiment 4
Described hoveniae semoveniae semen plant beverage preparation method is with embodiment 2, and different is that step (3) merges extract and for the second time extract for the first time, adopts the concentrate that at Vacuum Concentration method to 60 ℃, relative density is 1.08.Described hoveniae semoveniae semen plant beverage product characteristics are shown in Table 1.
embodiment 5
Described hoveniae semoveniae semen plant beverage preparation method is with embodiment 2, and different is that step (3) merges extract and for the second time extract for the first time, adopts the concentrate that at Vacuum Concentration method to 60 ℃, relative density is 1.09.Described hoveniae semoveniae semen plant beverage product characteristics are shown in Table 1.
Table 1 product characteristics
embodiment 7 Application Examples
The hoveniae semoveniae semen plant beverage that embodiment 1～3 is prepared carries out the protective effect test to rat chronic hepatic injury
Animal used as test: rat, male, body weight: 250 left and right, 100.
Experimental technique: be blank group, positive controls, administration group A and administration group B by body weight random packet by rat.Except blank group, other respectively organizes hypodermic injection 40%CCl
4olive oil solution 5ml/kg, later hypodermic injection 40% CCl weekly
4olive oil solution 3ml/kg twice, continues six weeks, blank group of olive oil that gives same volume.Meanwhile, administration group A and administration group B difference gastric infusion every day 1 time, successive administration six weeks, weighs weekly once, according to the variation of body weight, adjusts dosage.Administration group A is the hoveniae semoveniae semen plant beverage of the embodiment of the present invention 1～3 preparation, and administration group B is silymarin.The animal of drug withdrawal time daily femoral artery sacrificed by exsanguination, is cooked substantially and histopathologic examination.Measure weight and the coefficient of liver, spleen; Take out each treated animal liver, the conventional dehydration of left lobe of liver, embedding and section, histological examination is done in HE dyeing.
Experimental result: liver khaki is observed in positive controls gross anatomy, and surface and tangent plane are coarse, have atrophy phenomenon, quality toughness; Microscopy finds that institutional framework reduces, swelling of liver cell, the sex change of cavity sample and downright bad and early stage Fibrotic formation.Administration group A and administration group B gross anatomy are observed liver pathological changes degree and are obviously alleviated.
Shown in liver assessment of indices result table 2:
Table 2 liver assessment of indices result
As can be seen from Table 2, compare with positive controls, the liver exponential experiment p<0.01 of blank group, administration group A and administration group B, result has statistical significance, and embodiment 1,2,3 does not have marked difference, and product efficacy is more stable.
embodiment 7 Application Examples
Choose two groups of drunk persons that light and heavy degree is different, each organizes 20 people, takes hoveniae semoveniae semen plant beverage described in embodiment 1.
For occurring instability of gait, dizzy slight group, taking described in embodiment 1 after hoveniae semoveniae semen plant beverage, all in 10～15 minutes, recover normal.
For occurring vomiting, headache, the severe group that cannot stand, taking described in embodiment 1 after hoveniae semoveniae semen plant beverage, all in 25 minutes, malaise symptoms obviously disappears, and no longer occurs vomiting sensation, and headache phenomenon is alleviated to some extent, can stand firm and recover walking.
Claims (2)
1. a hoveniae semoveniae semen plant beverage, is characterized in that, described hoveniae semoveniae semen plant beverage prepares by the following method:
(1) get 15 grams of hoveniae semoveniae semens, 15 grams of FI puerariaes, under normal temperature, add in 150 grams of light waters, soak 30 minutes, after then big fire is boiled, little fire keeps micro-boiling to decoct 1 hour, filters, and collects respectively extract and residue for the first time;
(2) in residue, add 90 grams of light waters, then after boiling with big fire, with little fire, keep micro-boiling to decoct 1 hour, collect extract for the second time;
(3) merge extract and for the second time extract for the first time, at 60 ~ 85 ℃, adopt Vacuum Concentration method that extract is concentrated into the concentrate that at 60 ℃, relative density is 1.06;
(4) by above-mentioned concentrate, Sucralose 0.004g, add in appropriate purified water, dissolve, then be placed in constant volume tank and be settled to 180ml by purified water, after stirring, heating is boiled, and crosses 400 order silks, carry out hot embedding, every bottle of 180ml, 121 ℃ of steam sterilizings 30 minutes, are packaged to be described hoveniae semoveniae semen plant beverage.
2. the preparation method of hoveniae semoveniae semen plant beverage described in claim 1, is characterized in that, comprises the steps:
(1) get 15 grams of hoveniae semoveniae semens, 15 grams of FI puerariaes, under normal temperature, add in 150 grams of light waters, soak 30 minutes, after then big fire is boiled, little fire keeps micro-boiling to decoct 1 hour, filters, and collects respectively extract and residue for the first time;
(2) in residue, add 90 grams of light waters, then after boiling with big fire, with little fire, keep micro-boiling to decoct 1 hour, collect extract for the second time;
(3) merge extract and for the second time extract for the first time, at 60 ~ 85 ℃, adopt Vacuum Concentration method that extract is concentrated into the concentrate that at 60 ℃, relative density is 1.06;
(4) by above-mentioned concentrate, Sucralose 0.004g, add in appropriate purified water, dissolve, then be placed in constant volume tank and be settled to 180ml by purified water, after stirring, heating is boiled, and crosses 400 order silks, carry out hot embedding, every bottle of 180ml, 121 ℃ of steam sterilizings 30 minutes, are packaged to be described hoveniae semoveniae semen plant beverage.
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| CN103005556B (en) * | 2012-12-18 | 2015-04-22 | 段海庆 | Beverage |
| CN103478843B (en) * | 2013-10-16 | 2016-01-20 | 蔡强 | A kind of alcohol-decomposing beverage and preparation method thereof |
| CN106235235A (en) * | 2016-07-28 | 2016-12-21 | 武汉黄鹤楼香精香料有限公司 | A kind of essence of energy relieving alcoholism and protecting the liver and preparation method thereof |
| CN107969588A (en) * | 2017-10-30 | 2018-05-01 | 陈茂锐 | A kind of sugar-free sweet Antialcoholic liver-protecting coralhead plant stem with leaf plant beverage and preparation method thereof |
| CN108967796A (en) * | 2018-07-09 | 2018-12-11 | 宁波赛世健康科技有限公司 | A kind of lemon hoveniae semoveniae semen solid beverage ingredient |
| CN115777855A (en) * | 2022-12-28 | 2023-03-14 | 四川享寿生商贸有限公司 | A plant beverage for preventing hemorrhoid and halitosis, and its preparation method |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1238148A (en) * | 1999-05-27 | 1999-12-15 | 张荣生 | Sobering-up health-care beverage |
| CN1736270A (en) * | 2005-07-05 | 2006-02-22 | 黄恒燊 | Alcohol-dissolving liver-protecting drink and preparation method thereof |
| CN1927285A (en) * | 2006-09-06 | 2007-03-14 | 大连轻工业学院 | Medicament for neutralizing the effect of alcohol and protecting liver |
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| KR20050049681A (en) * | 2003-11-22 | 2005-05-27 | 주식회사 씨메드 | A manufacturing process of yeast, asparagine acid and a beverage for dissolving efficacy of toxic effect by drunken frenzy |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1238148A (en) * | 1999-05-27 | 1999-12-15 | 张荣生 | Sobering-up health-care beverage |
| CN1736270A (en) * | 2005-07-05 | 2006-02-22 | 黄恒燊 | Alcohol-dissolving liver-protecting drink and preparation method thereof |
| CN1927285A (en) * | 2006-09-06 | 2007-03-14 | 大连轻工业学院 | Medicament for neutralizing the effect of alcohol and protecting liver |
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