CN102670457A - Tooth powder and fabrication process thereof - Google Patents
Tooth powder and fabrication process thereof Download PDFInfo
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- CN102670457A CN102670457A CN2012101838977A CN201210183897A CN102670457A CN 102670457 A CN102670457 A CN 102670457A CN 2012101838977 A CN2012101838977 A CN 2012101838977A CN 201210183897 A CN201210183897 A CN 201210183897A CN 102670457 A CN102670457 A CN 102670457A
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Abstract
The invention discloses a tooth powder which is characterized by comprising anti-staining active ingredient, acid-free desensitization ingredient, odour removal ingredient and base stock ingredient, wherein the anti-staining active ingredient comprises modified phytic acid sodium and urea hydrogen peroxide; the acid-free desensitization ingredient comprises sodium monofluorophosphate and Chinese medicine desensitization agent; the odour removal ingredient comprises angelica root extract and liex rotunda extract; and the base stock ingredient comprises dicalcium phosphate dehydrate, calcium carbonate, silica, soluble saccharin, glycerol, essence, sodium lauryl sulfate and the balance of preservative. When being in fabrication, the tooth powder not only has the functions of cleaning dental plaque, complexing and dissolving pigmentation of tooth surface but also can reduce the irritation to the oral cavity and the aching, limp and allergic feeding can not be caused during use process through a combination technology.
Description
Technical field
The invention belongs to the oral care product field, specifically, relate to a kind of dentifrice and processing technology thereof.
Background technology
People are owing to smoking, drink colored drink and with advancing age, and facing will calm mottle, causes xanthodont black tooth, and dental plaque is piled up also can cause decayed tooth.In order to keep the tooth health brilliant white, have xanthodont or the Pigmented people of facing, need to carry out regular toothwash to dental clinic.Therefore, the toothpaste for teeth fastness of whitening on the market arises at the historic moment.Toothpaste belongs to colloid substance, wherein contains moisture, and a lot of active substance can chemical reaction take place in water environment, influence its useful effect.Simultaneously, because solidifying content, also can reduce moisture its, to some jaundice or serious Pigmented tooth; In cleaning course; Need certain mechanism to add suitable chemical process, just can reach effective result, the mechanical cleaning power of dentifrice is higher than toothpaste.But because dentifrice is flour, wherein the zest to the oral cavity is better than toothpaste.
Summary of the invention
The technical problem that the present invention will solve is to overcome above-mentioned defective, provides a kind of and has cleaning bacterial plaque, complexation dissolving facing pigment and reduce the zest to the oral cavity, reduces the dentifrice that in use produces aching and limp SSP.
For addressing the above problem, the technical scheme that the present invention adopted is:
A kind of dentifrice is characterized in that: comprise and steep active component, acid-proof desensitization composition, elimination smell component and base material composition;
Saidly remove to steep active component and comprise following component by mass percent: modification sodium phytate 1~10%, percarbamide 1~10%;
Said acid-proof desensitization composition comprises following component by mass percent: sodium monofluorophosphate 0.76~0.9% and Chinese medicine desensitizer 0.2~2%;
Said elimination smell component comprises following component by mass percent: Radix Angelicae Dahuricae extract 0~3%, Fel Ursi wood extract 0~3%;
Said base material composition comprises following component by mass percent: dicalcium phosphate dehydrate 0~80%, calcium carbonate 0~80%, silica 1~10%, saccharin sodium 0.2%, glycerol 2~8%, essence 1~2%, sodium lauryl sulfate 1~4%;
Surplus is an antiseptic.
As a kind of improvement of the present invention:
Said Chinese medicine desensitizer is Pericarpium Zanthoxyli fiber crops element and eugenol, and Pericarpium Zanthoxyli fiber crops mass percent plain and eugenol is respectively 0.1~1%.
As further improvement of the present invention:
Saidly remove to steep active component and comprise following component by mass percent: modification sodium phytate 3%, percarbamide 10%;
Said acid-proof desensitization composition comprises following component by mass percent: sodium monofluorophosphate 0.76%, Pericarpium Zanthoxyli fiber crops element 0.1%, eugenol 0.7%;
Said elimination smell component comprises following component by mass percent: Radix Angelicae Dahuricae extract 1%, Fel Ursi wood extract 1%;
Said base material composition comprises following component by mass percent: dicalcium phosphate dehydrate 44.54%, calcium carbonate 26%, silicon dioxide 5%, saccharin sodium 0.2%, glycerol 4%, essence 1.2%, sodium lauryl sulfate 2%;
Surplus is an antiseptic 0.5%.
The processing technology of dentifrice of the present invention is characterized in that:
Comprise following steps:
1), dicalcium phosphate dehydrate, calcium carbonate, silicon dioxide are weighed up premixing respectively by prescription;
2), modification sodium phytate and percarbamide and sodium monofluorophosphate weigh up premixing by prescription;
3), with the saccharin sodium thermosol in glycerol, for use;
4), with the mixture in step 1 and the step 2; Be put in the static mixer, add sodium lauryl sulfate, Fel Ursi wood extract and Radix Angelicae Dahuricae extract, antiseptic according to prescription simultaneously; Start static mixer, the speed of static mixer is 10~30 rev/mins;
5), the material that step 3 obtained through aerosol apparatus, and essence mixes, while stir in the material that is sprayed onto step 4, spray velocity is 50~100ml/ minute;
6), treat the liquid material add finish after, the speed of static mixer is transferred to 50 rev/mins; Mix discharging half an hour;
7), with material as in the 100 order vibrosieves, sieve, afterwards the packing.
Since adopted technique scheme, compared with prior art, four sodium phosphates of the sodium phytate band after the modification among the present invention; PH value can be stabilized between 5 ~ 9; Mottle on the facing or the alkaline bacterial plaque that is deposited on the facing are played good chelating agent dissolution, simultaneously, because it has powerful complex performance; Can mix with percarbamide, percarbamide can be stabilized in the dentifrice system.
In addition, sodium monofluorophosphate, Pericarpium Zanthoxyli fiber crops element and eugenol have good acid-proof desensitization function.The Radix Angelicae Dahuricae and Fel Ursi wood extract are widely used in the various medicines for the good medicine of treatment halitosis.
The present invention through compounded technology, when making dentifrice have cleaning bacterial plaque, complexation dissolving facing pigment, reduces the zest of dentifrice to the oral cavity when making, reduce the sensation aching and limp hypersensitive that dentifrice does not in use produce.After the use, can keep the tooth brilliant white, breath freshening.
The specific embodiment
Embodiment:
A kind of dentifrice in the present invention, comprises and steeps active component, acid-proof desensitization composition, elimination smell component and base material composition.
Wherein, remove to steep active component and comprise following component by mass percent: modification sodium phytate 1~10%, percarbamide 1~10%.
Acid-proof desensitization composition comprises following component by mass percent: sodium monofluorophosphate 0.76~0.9% and Chinese medicine desensitizer 0.2~2%.
Eliminate smell component and comprise following component by mass percent: Radix Angelicae Dahuricae extract 0~3%, Fel Ursi wood extract 0~3%.
The base material composition comprises following component by mass percent: dicalcium phosphate dehydrate 0~80%, calcium carbonate 0~80%, silica 1~10%, saccharin sodium 0.2%, glycerol 2~8%, essence 1~2%, sodium lauryl sulfate 1~4%.
Surplus is an antiseptic.
In the present embodiment, according to repeatedly test and trial repeatedly, the Chinese medicine desensitizer is Pericarpium Zanthoxyli fiber crops element and eugenol, and Pericarpium Zanthoxyli fiber crops mass percent plain and eugenol is respectively 0.1~1%.
The present invention has also comprised the processing technology of dentifrice, comprises following steps:
1), dicalcium phosphate dehydrate, calcium carbonate, silicon dioxide are weighed up premixing respectively by prescription.
2), modification sodium phytate and percarbamide and sodium monofluorophosphate weigh up premixing by prescription.
3), with the saccharin sodium thermosol in glycerol, for use.
4), with the mixture in step 1 and the step 2; Be put in the static mixer, add sodium lauryl sulfate, Fel Ursi wood extract and Radix Angelicae Dahuricae extract, antiseptic according to prescription simultaneously; Start static mixer, the speed of static mixer is 10~30 rev/mins.
5), the material that step 3 obtained through aerosol apparatus, and essence mixes, while stir in the material that is sprayed onto step 4, spray velocity is 50~100ml/ minute.
6), treat the liquid material add finish after, the speed of static mixer is transferred to 50 rev/mins; Mix discharging half an hour.
7), with material as in the 100 order vibrosieves, sieve, afterwards the packing.
Adopt above formulation ratio and processing technique; Four sodium phosphates of modification sodium phytate band in the dentifrice after the modification, pH value can be stabilized between 5 ~ 9, and mottle on the facing or the alkaline bacterial plaque that is deposited on the facing are played good chelating agent dissolution; Simultaneously; Because it has powerful complex performance, can mix with percarbamide, and percarbamide can be stabilized in the dentifrice system.
In addition, sodium monofluorophosphate, Pericarpium Zanthoxyli fiber crops element and eugenol have good acid-proof desensitization function.The Radix Angelicae Dahuricae and Fel Ursi wood extract are the good medicine of treatment halitosis.
The present invention through compounded technology, when making dentifrice have cleaning bacterial plaque, complexation dissolving facing pigment, reduces the zest of dentifrice to the oral cavity when making, reduce the sensation aching and limp hypersensitive that dentifrice does not in use produce.After the use, can keep the tooth brilliant white, breath freshening.
As a kind of concrete prescription of the present invention, also be that best a kind of prescription is:
Improved plant sodium 3%, percarbamide 10%, sodium monofluorophosphate 0.76%, Pericarpium Zanthoxyli fiber crops plain 0.1%; Eugenol 0.7%, Radix Angelicae Dahuricae extract 1%, Fel Ursi wood extract 1%, dicalcium phosphate dehydrate 44.54%; Calcium carbonate 26%, silicon dioxide 5%, saccharin sodium 0.2%, glycerol 4%; Essence 1.2%, sodium lauryl sulfate 2%, surplus is an antiseptic 0.5%.
The dentifrice that above-mentioned prescription is processed, user tooth after using for two weeks obviously bleaches, and use does not have sense of discomfort and breath freshening.
The present invention is not limited to above-mentioned preferred forms; Anyone should learn dosage or the prescription of under enlightenment of the present invention, making; And be the conspicuous variations of those skilled in the art; Every have identical or akin technical scheme with the present invention, all belongs to protection scope of the present invention.
Claims (4)
1. a dentifrice is characterized in that: comprise and steep active component, acid-proof desensitization composition, elimination smell component and base material composition;
Saidly remove to steep active component and comprise following component by mass percent: modification sodium phytate 1~10%, percarbamide 1~10%;
Said acid-proof desensitization composition comprises following component by mass percent: sodium monofluorophosphate 0.76~0.9% and Chinese medicine desensitizer 0.2~2%;
Said elimination smell component comprises following component by mass percent: Radix Angelicae Dahuricae extract 0~3%, Fel Ursi wood extract 0~3%;
Said base material composition comprises following component by mass percent: dicalcium phosphate dehydrate 0~80%, calcium carbonate 0~80%, silica 1~10%, saccharin sodium 0.2%, glycerol 2~8%, essence 1~2%, sodium lauryl sulfate 1~4%;
Surplus is an antiseptic.
2. according to the dentifrice described in the claim 1, it is characterized in that: said Chinese medicine desensitizer is Pericarpium Zanthoxyli fiber crops element and eugenol, and Pericarpium Zanthoxyli fiber crops mass percent plain and eugenol is respectively 0.1~1%.
3. according to the dentifrice described in the claim 2, it is characterized in that:
Saidly remove to steep active component and comprise following component by mass percent: modification sodium phytate 3%, percarbamide 10%;
Said acid-proof desensitization composition comprises following component by mass percent: sodium monofluorophosphate 0.76%, Pericarpium Zanthoxyli fiber crops element 0.1%, eugenol 0.7%;
Said elimination smell component comprises following component by mass percent: Radix Angelicae Dahuricae extract 1%, Fel Ursi wood extract 1%;
Said base material composition comprises following component by mass percent: dicalcium phosphate dehydrate 44.54%, calcium carbonate 26%, silicon dioxide 5%, saccharin sodium 0.2%, glycerol 4%, essence 1.2%, sodium lauryl sulfate 2%;
Surplus is an antiseptic 0.5%.
4. the processing technology of a dentifrice is characterized in that:
Comprise following steps:
1), dicalcium phosphate dehydrate, calcium carbonate, silicon dioxide are weighed up premixing respectively by prescription;
2), modification sodium phytate and percarbamide and sodium monofluorophosphate weigh up premixing by prescription;
3), with the saccharin sodium thermosol in glycerol, for use;
4), with the mixture in step 1 and the step 2; Be put in the static mixer, add sodium lauryl sulfate, Fel Ursi wood extract and Radix Angelicae Dahuricae extract, antiseptic according to prescription simultaneously; Start static mixer, the speed of static mixer is 10~30 rev/mins;
5), the material that step 3 obtained through aerosol apparatus, and essence mixes, while stir in the material that is sprayed onto step 4, spray velocity is 50~100ml/ minute;
6), treat the liquid material add finish after, the speed of static mixer is transferred to 50 rev/mins; Mix discharging half an hour;
7), with material as in the 100 order vibrosieves, sieve, afterwards the packing.
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CN2012101838977A CN102670457A (en) | 2012-06-06 | 2012-06-06 | Tooth powder and fabrication process thereof |
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CN2012101838977A CN102670457A (en) | 2012-06-06 | 2012-06-06 | Tooth powder and fabrication process thereof |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104287992A (en) * | 2014-09-26 | 2015-01-21 | 福建爱洁丽日化有限公司 | Tooth powder for whitening, removing stains and preventing tooth decay |
CN106389235A (en) * | 2016-12-01 | 2017-02-15 | 广州中汉口腔用品有限公司 | Toothpaste with breath freshening and whitening functions and manufacturing technology thereof |
CN107157866A (en) * | 2017-07-25 | 2017-09-15 | 何家平 | A kind of dried peppermint leaf Chinese traditional medicine tooth powder technique |
CN107280981A (en) * | 2017-04-24 | 2017-10-24 | 南昌登特科技有限公司 | A kind of activated carbon tooth powder |
CN107519026A (en) * | 2017-10-10 | 2017-12-29 | 广州立白企业集团有限公司 | It is a kind of have remove tooth powder of stain and fresh breath and preparation method thereof |
EP3156038A4 (en) * | 2014-06-10 | 2018-01-03 | Kao Corporation | Composition for use in oral cavity |
Citations (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1103579A (en) * | 1993-12-09 | 1995-06-14 | 胡洪宇 | Tooth paste |
CN1105558A (en) * | 1994-03-09 | 1995-07-26 | 罗焕凡 | Health-care toothpaste removing dental calculus and its preparation technology |
CN1229641A (en) * | 1998-03-20 | 1999-09-29 | 湖北医科大学附属第二医院 | False tooth cleaning agent |
CN101330900A (en) * | 2005-12-20 | 2008-12-24 | 宝洁公司 | Oral care compositions comprising zinc and phytate |
CN101404976A (en) * | 2006-03-29 | 2009-04-08 | 宝洁公司 | Oral care compositions providing enhanced whitening and stain prevention |
CN101690699A (en) * | 2009-09-29 | 2010-04-07 | 广东名臣有限公司 | Teeth-cleaning whitening toothpaste composition |
CN101756801A (en) * | 2008-11-18 | 2010-06-30 | 陈恩平 | Phytate sodium dental plaque and calculus prevention mouthwash |
CN101829032A (en) * | 2010-05-11 | 2010-09-15 | 李少君 | Dual-purpose toothpaste composition and preparation method thereof |
CN101829329A (en) * | 2010-05-11 | 2010-09-15 | 李少君 | Tooth antiallergic composition |
CN101843562A (en) * | 2010-05-11 | 2010-09-29 | 李少君 | Solid composition for removing teeth stains |
CN101889960A (en) * | 2009-05-20 | 2010-11-24 | 广州薇美姿个人护理用品有限公司 | Teeth whitening dentifrice |
-
2012
- 2012-06-06 CN CN2012101838977A patent/CN102670457A/en active Pending
Patent Citations (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1103579A (en) * | 1993-12-09 | 1995-06-14 | 胡洪宇 | Tooth paste |
CN1105558A (en) * | 1994-03-09 | 1995-07-26 | 罗焕凡 | Health-care toothpaste removing dental calculus and its preparation technology |
CN1229641A (en) * | 1998-03-20 | 1999-09-29 | 湖北医科大学附属第二医院 | False tooth cleaning agent |
CN101330900A (en) * | 2005-12-20 | 2008-12-24 | 宝洁公司 | Oral care compositions comprising zinc and phytate |
CN101404976A (en) * | 2006-03-29 | 2009-04-08 | 宝洁公司 | Oral care compositions providing enhanced whitening and stain prevention |
CN101756801A (en) * | 2008-11-18 | 2010-06-30 | 陈恩平 | Phytate sodium dental plaque and calculus prevention mouthwash |
CN101889960A (en) * | 2009-05-20 | 2010-11-24 | 广州薇美姿个人护理用品有限公司 | Teeth whitening dentifrice |
CN101690699A (en) * | 2009-09-29 | 2010-04-07 | 广东名臣有限公司 | Teeth-cleaning whitening toothpaste composition |
CN101829032A (en) * | 2010-05-11 | 2010-09-15 | 李少君 | Dual-purpose toothpaste composition and preparation method thereof |
CN101829329A (en) * | 2010-05-11 | 2010-09-15 | 李少君 | Tooth antiallergic composition |
CN101843562A (en) * | 2010-05-11 | 2010-09-29 | 李少君 | Solid composition for removing teeth stains |
Non-Patent Citations (9)
Title |
---|
(美)艾伦(ALLEN,L.V.)等主编;王浩等主译: "《安塞尔药物剂型给药系统》", 29 February 2012, article ""安塞尔药物剂型给药系统"" * |
CASSIE_123: ""复方药物牙膏"", 《HTTP://BAIKE.BAIDU.COM/LINK?URL=0CRA3ZWR67N__U45UCRSBUI6NA8QNBWWB2MKKRV0XB_BUUBN8YH6Y4RYQKSKLF-F-CWFTOK5Z87O8YP4ZRRKWK》, 7 September 2010 (2010-09-07) * |
中华人民共和国卫生部: "《化妆品卫生规范》", 31 January 2007, article ""表2(2)化妆品禁用组分"", pages: 56-58 * |
刘玮等: "《皮肤科学与化妆品功效评价》", 31 January 2005, article ""皮肤科学与化妆品功效评价"" * |
奚念朱: "《药剂学》", 30 April 1996, article ""药剂学"" * |
戴卫波等: ""救必应化学成分研究及临床应用进展"", 《亚太传统医药》, vol. 4, no. 12, 31 December 2008 (2008-12-31) * |
戴国登等: "《实用化工产品开发及制造工艺》", 30 April 1995, article ""实用化工产品开发及制造工艺"" * |
王振忠 等: ""花椒麻味素的研究概况"", 《食品与药品》, vol. 8, no. 03, 31 December 2006 (2006-12-31) * |
高国强等: "《化妆品卫生与管理》", 30 April 1994, article ""化妆品卫生与管理"", pages: 121-122 - 193-194 * |
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP3156038A4 (en) * | 2014-06-10 | 2018-01-03 | Kao Corporation | Composition for use in oral cavity |
US9918920B2 (en) | 2014-06-10 | 2018-03-20 | Kao Corporation | Oral composition |
RU2686681C2 (en) * | 2014-06-10 | 2019-04-30 | Као Корпорейшн | Oral composition |
CN104287992A (en) * | 2014-09-26 | 2015-01-21 | 福建爱洁丽日化有限公司 | Tooth powder for whitening, removing stains and preventing tooth decay |
CN106389235A (en) * | 2016-12-01 | 2017-02-15 | 广州中汉口腔用品有限公司 | Toothpaste with breath freshening and whitening functions and manufacturing technology thereof |
CN107280981A (en) * | 2017-04-24 | 2017-10-24 | 南昌登特科技有限公司 | A kind of activated carbon tooth powder |
CN107280981B (en) * | 2017-04-24 | 2020-07-28 | 南昌登特科技有限公司 | Activated carbon tooth powder |
CN107157866A (en) * | 2017-07-25 | 2017-09-15 | 何家平 | A kind of dried peppermint leaf Chinese traditional medicine tooth powder technique |
CN107519026A (en) * | 2017-10-10 | 2017-12-29 | 广州立白企业集团有限公司 | It is a kind of have remove tooth powder of stain and fresh breath and preparation method thereof |
CN107519026B (en) * | 2017-10-10 | 2020-08-04 | 广州立白企业集团有限公司 | Dentifrice with stain removing and breath freshening functions and preparation method thereof |
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Application publication date: 20120919 |