CN1026650C - Bactericidal composition for preventing and treating apple tree canker and preparation method thereof - Google Patents
Bactericidal composition for preventing and treating apple tree canker and preparation method thereof Download PDFInfo
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- CN1026650C CN1026650C CN 92106741 CN92106741A CN1026650C CN 1026650 C CN1026650 C CN 1026650C CN 92106741 CN92106741 CN 92106741 CN 92106741 A CN92106741 A CN 92106741A CN 1026650 C CN1026650 C CN 1026650C
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- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 39
- 239000000203 mixture Substances 0.000 title claims abstract description 38
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 244000141359 Malus pumila Species 0.000 title abstract description 18
- 235000011430 Malus pumila Nutrition 0.000 title abstract description 18
- 235000015103 Malus silvestris Nutrition 0.000 title abstract description 18
- 239000007788 liquid Substances 0.000 claims abstract description 35
- 239000004115 Sodium Silicate Substances 0.000 claims abstract description 15
- 235000006886 Zingiber officinale Nutrition 0.000 claims abstract description 15
- 239000003899 bactericide agent Substances 0.000 claims abstract description 15
- 235000008397 ginger Nutrition 0.000 claims abstract description 15
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229910052911 sodium silicate Inorganic materials 0.000 claims abstract description 12
- 241001645362 Valsa Species 0.000 claims description 15
- 241000234282 Allium Species 0.000 claims description 14
- 235000002732 Allium cepa var. cepa Nutrition 0.000 claims description 14
- 241000234314 Zingiber Species 0.000 claims description 12
- 239000012530 fluid Substances 0.000 claims description 5
- 230000000694 effects Effects 0.000 abstract description 11
- 230000001954 sterilising effect Effects 0.000 abstract description 7
- 238000004659 sterilization and disinfection Methods 0.000 abstract description 5
- 241000196324 Embryophyta Species 0.000 abstract description 4
- 244000273928 Zingiber officinale Species 0.000 abstract description 3
- 235000013399 edible fruits Nutrition 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 244000291564 Allium cepa Species 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 231100000957 no side effect Toxicity 0.000 abstract 1
- 231100000956 nontoxicity Toxicity 0.000 abstract 1
- 239000003814 drug Substances 0.000 description 13
- JYMHODZXTIGVPA-UHFFFAOYSA-N Cycloalliin Chemical compound CC1CS(=O)CC(C(O)=O)N1 JYMHODZXTIGVPA-UHFFFAOYSA-N 0.000 description 10
- 231100000241 scar Toxicity 0.000 description 10
- 240000002234 Allium sativum Species 0.000 description 6
- GAMFEMAXLMWCRG-UHFFFAOYSA-N bis(dimethylcarbamothioylsulfanyl)arsanyl n,n-dimethylcarbamodithioate Chemical compound CN(C)C(=S)S[As](SC(=S)N(C)C)SC(=S)N(C)C GAMFEMAXLMWCRG-UHFFFAOYSA-N 0.000 description 6
- 235000004611 garlic Nutrition 0.000 description 6
- 201000010099 disease Diseases 0.000 description 5
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 5
- 230000035876 healing Effects 0.000 description 5
- 208000015181 infectious disease Diseases 0.000 description 5
- 239000002420 orchard Substances 0.000 description 5
- 239000003905 agrochemical Substances 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 230000003449 preventive effect Effects 0.000 description 4
- 230000002265 prevention Effects 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 238000007363 ring formation reaction Methods 0.000 description 3
- 235000019351 sodium silicates Nutrition 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 241000894006 Bacteria Species 0.000 description 2
- 208000032420 Latent Infection Diseases 0.000 description 2
- 240000008790 Musa x paradisiaca Species 0.000 description 2
- 235000018290 Musa x paradisiaca Nutrition 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000000853 adhesive Substances 0.000 description 2
- 230000001070 adhesive effect Effects 0.000 description 2
- 238000010009 beating Methods 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 208000037771 disease arising from reactivation of latent virus Diseases 0.000 description 2
- 230000000857 drug effect Effects 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 241000233866 Fungi Species 0.000 description 1
- 240000005373 Panax quinquefolius Species 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 229910052785 arsenic Inorganic materials 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003640 drug residue Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 238000003898 horticulture Methods 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 238000011081 inoculation Methods 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- JKQOBWVOAYFWKG-UHFFFAOYSA-N molybdenum trioxide Chemical compound O=[Mo](=O)=O JKQOBWVOAYFWKG-UHFFFAOYSA-N 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 238000006303 photolysis reaction Methods 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000007790 scraping Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 1
- 229910001948 sodium oxide Inorganic materials 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- XTQHKBHJIVJGKJ-UHFFFAOYSA-N sulfur monoxide Chemical compound S=O XTQHKBHJIVJGKJ-UHFFFAOYSA-N 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention relates to a sterilization combination for preventing and treating apple tree canker and a preparation method thereof, which is characterized in that the sterilization combination contains 40-70 percent (weight) of plant bactericide and 30-60 percent (weight) of liquid sodium silicate (concentration is 60 percent). The plant bactericide consists of ginger liquid in 20-40 wt% and scallion liquid in 60-80 wt%. Mixing the above components at normal temperature and pressure. The sterilization composition has the advantages of obvious effect of preventing and treating apple tree canker, no toxicity, no harm, no side effect, convenient use, simple preparation method, easy acquisition of materials, low cost and easy popularization in fruit industry production areas.
Description
The present invention relates to a kind of bactericidal composition of preventing and treating apple valsa canker.
Apple valsa canker is the important disease in China apple producing region, and control medicine commonly used in the production mainly is arsenical agricultural chemicals such as asomate and non-arsenic preparation agricultural chemicals such as Fubiqing, Fu Lan wait two big classes.To the control efficiency of apple valsa canker only about 70%, its complicated process of preparation, medicine cost height, and arsenical agricultural chemicals medicament residue is higher, environmental pollution is serious.
China's " plant protection " 1991 the 5th phases are utilized garlic treatment apple valsa canker, and treatment and healing effect are better, but undesirable to the latent infection point eradicant action of apple valsa canker, and the drug effect phase is shorter, need often scrape and control.
The present invention be directed to above-mentioned germ killing drugs cost height, control efficiency is undesirable, shortcomings such as complex manufacturing, and apple valsa canker mechanism studies for a long period of time, test obtains in that garlic is prevented and treated.The purpose of this invention is to provide a kind of novel bactericidal composition of preventing and treating apple valsa canker and the simple method for preparing said composition.
Bactericidal composition raw material of the present invention mainly comprises ginger, green onion and sodium silicate etc., utilize ginger anti-oxidant, [it is a precursor of preventing and treating the important composition cycloalliin of rot (cycloalliin) in the garlic to a large amount of S-acrylic-2-cysteine oxysulfide that contains in the characteristic of postponement compound oxidation and the green onion, and cyclization immediately generates cycloalliin (this point has obtained proof in department of horticulture of Zhejiang Agricultural Univ 11 China's Vegetable-1984CD-36) when the pH value is alkalescence greater than 7.] the cycloalliin sterilization of cyclization Cheng Sheng and the division that stimulates sick scar border cell.And be equipped with antibacterial adhesive sodium silicate (XNa
2O.YSIO
2), wherein sodium oxide molybdena has bacteriostasis, and the alkaline environment of cyclization cycloalliin is provided; Silica increases medicine adhesive force, forms diaphragm around infection court or sick scar, causes the bacterium anaerobic environment, stops the young cystospore infection way of rot fungi, and overcomes the medicine photodissociation, the phenomenon of deliquescence and rain drop erosion.
Main points of the present invention are:
1. this invention bactericidal composition contains 40-70%(weight) bactericide, 30-60%(weight) liquid sodium silicate (concentration is 60%).Bactericide comprises ginger liquid and green onion liquid.
＜2〉configuration proportion of bactericide (percentage by weight):
Ginger liquid: 20-40%
Green onion liquid: 60-80%
＜3〉the present invention prevents and treats the apple valsa canker bactericidal composition, preferably can select following prescription (percentage by weight) for use:
Bactericide 44-55%,
Liquid sodium silicate (concentration 60%) 45-56%.
Ginger liquid 25-35% in the bactericide, green onion liquid 65-75%.
＜4〉preparation method of bactericidal composition is:
With 40-70%(weight) bactericide, 30-60%(weight) liquid sodium silicate (concentration 60%), at normal temperatures and pressures, mixed preparing forms in proportion.
＜5〉preparation method of bactericide is:
Under the normal temperature and pressure, contained raw material is pulverized making beating respectively filter, get filtrate and mix in proportion.
Bactericidal composition of the present invention has desirable control efficiency to apple valsa canker.Adopt sessile drop method through Pesticides Testing chemical examination center, Weifang City, isolated shoot inoculation and bacterium medicine face-off cultivation respectively to the sterilizing power of the made medicine of the present invention, garlic juice, asomate, Fubiqing, performance is rooted out in infiltration and the term of validity compares measurement, the result shows: this invention bactericidal composition, to rotten pathogenic bacteria latent infection point, have strong eradicant action, its relative control efficiency reaches more than 95%, and sterilizing power is the highest, EDD is the longest, reaches 120 days.By the Weifang City institute of agricultural sciences, Anqiu county State Scientific and Technological Commission, Anqiu county plant protection unit unite carry out utilize this invention composition for preventing and controlling apple valsa canker field trial (40% asomate contrast medicament).The result: (1) curative effect is greater than 99%, and recurrence rate is less than 0.1%; (2) prevention morbidity effect is more than 94%; (3) large-area applications effect: 200,000 mu of orchard average effect are 96.5%, the one-sided average healing width 21mm of sick scar.
Bactericidal composition preparation method of the present invention is simple, and equipment investment is few, and raw material are easy to get, and medicine is with low cost, and easy to use, and sick scar is five lis of only, once cures and does not recur.Every mu can be reduced agricultural chemicals expense 16-20 unit.(according to 40/mu)
Bactericidal composition of the present invention is nuisanceless technology, and the medicine high effect nontoxic is without any side effects, and drug residue free to the person poultry harmless, is easy to preserve and use.Be suitable for the apple producing region and carry out the large tracts of land popularization.
Example 1:
(1) ginger, living green onion are cleaned, dried (removing ginger, the outside moisture of green onion);
(2) ginger, bright green onion being pulverized making beating respectively filters.
(3) under the normal temperature and pressure, get 135 kilograms of ginger liquids, 315 kilograms of living green onion liquid mix with 550 kilograms of liquid sodium silicates, make brown thick 1000 kilograms of bactericidal compositions.Prevent and treat the apple valsa canker effect for verifying this invention bactericidal composition, with 40% asomate is the contrast medicament, the inventor is on the heavier orchard state light of morbidity, red banana kind tree, the sick scar of 30-60 was selected in each processing after rot was scraped and controlled spring, in 4-6 month coating once, recurrence rate and the one-sided average healing width of sick scar that the Sheng phase investigation of falling ill 1 year spring is respectively handled, statistics control efficiency (table 1).Simultaneously, adopting 6 strains tree is an experimental plot, establishes six processing, three repetitions.State of an illness basically identical is respectively handled in the even assembly in each sub-district before the medicine.Before April, fruit tree germinateed, will set the drip washing formula entirely with 1000 times of liquid of this invention composition and spray, every mu with 100 kilograms of composition liquid, carries out composition prevention morbidity and test.Statistics preventive effect (table 2).
Example 2:
The preparation method is the same.
Under the normal temperature and pressure, get 280 kilograms of ginger liquid, 420 kilograms of green onion liquid mix with 300 kilograms of liquid sodium silicates, make 1000 kilograms of bactericidal compositions.
Example 3:
The preparation method is with example 1.
Get 80 kilograms of ginger liquids, 320 kilograms of living green onion liquid, 600 kilograms of liquid sodium silicates (concentration 60%), mixed 1000 kilograms of bactericidal compositions on the normal temperature and pressure.
The bactericidal composition using method:
1. in time scrape the piece of curing the disease (cut the good skin of the disease scar 0.5cm of edge, the corner is about 60 degree), do not limit a season newly scraping disease scar trowelling.
2. scrape spring and control on rot basis, 50-100 times of liquid of full tree drip washing formula sprinkling bactericidal composition before fruit tree germinates.Every mu with composition liquid 80-120 kilogram.
Table 2: invention bactericidal composition prevention morbidity experimental control table
In March, 1989 year March in March, 1988-1989-year March March nineteen ninety-1991 March nineteen ninety
Handle preventive effect initial stage at administration time initial stage preventive effect initial stage preventive effect
Infection court (%) infection court (%) infection court (%)
Invention composition (1) (100) times liquid spring 100 96 123 95 213 97.5
Sodium silicate (100) times liquid spring 123 40 135 42 220 43.5
Garlic (100) times liquid spring 112 62.5 168 66.4 176 60
Fubiqing (100) times liquid spring and summer 139 46.9 137 41.7 234 49.5
Asomate (100) times liquid spring and summer 99 6.2 79 66.4 183 60.8
Blank 262 235 467
Table 1: the invention bactericidal composition is prevented and treated apple valsa canker, recurrence, drug effect, sick scar
Healing is contrast table (1) (2) as a result
Year March in March, 1989 year March in March, 1988-1989-March nineteen ninety-1991 March nineteen ninety the sick one-sided average healing width of scar (mm)
Cure effectively to cure effectively and cure effectively
Handle recurrence processing recurrence and handle recurrence 1,988 1,989 1990
Effect phase effect phase effect phase
Piece digit rate (%) piece digit rate (%) piece digit rate (%)-1989-1990-1991
(%) (my god) (%) (my god) (%) (my god)
The invention sterilization
Composition paint (3) 42 0 100 120 51 0.1 99.5 119 55 0 100 121 21 23 22.5
Sodium silicate 30 15 60 160 40 17 57 160 45 17.5 55 160 6.4 7 7.2
Garlic 40 1 95 7 50 0.8 96 8 50 1.2 94.5 788 8.8
Fubiqing paint 38 2.6 92.6 26 36 2.8 95.8 27 33 3 94.8 27 8.6 8.4 9.2
Asomate (50 times) 40 7.5 78.8 49 50 12.0 81.4 50 55 14.6 74.8 48 6.5 6.4 7.3
Blank 34 35.3-50 6.6-55 58-8.4 6.7 8.4
Remarks: kind such as (1) 10 year state's light, red banana;
(2) the sub-orchard of place: Zhou Jialou, big nearly dagger-axe orchard, waterlogging depression orchard;
(3) invention bactericidal composition coating weight percentage: ginger liquid 13.5%, green onion liquid 31.5%, sodium silicate (strength of fluid 60%) 55%.
Claims (3)
1, a kind of bactericidal composition of preventing and treating apple valsa canker, it is characterized in that the bactericide of said composition by 40-70% (weight), the liquid sodium silicate of 30-60% (weight) (concentration 60%) is formed, and bactericide is made up of the ginger homogenate filtered fluid of 20-40% (weight), the green onion homogenate filtered fluid of 60-80% (weight).
2, the bactericidal composition of preventing and treating apple valsa canker according to claim 1, the compositing formula (percentage by weight) that it is characterized in that it is preferably selected for use: bactericide 44-55%, liquid sodium silicate (concentration 60%) 45-56%, ginger homogenate filtered fluid 25-35%, green onion homogenate filtered fluid 65-75% in the bactericide.
3, a kind of preparation method who prevents and treats the bactericidal composition of apple valsa canker is characterized in that the weight with 40-70%() bactericide, 30-60%(weight) liquid sodium silicate (concentration 60%), mixed preparing forms in proportion at normal temperatures.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 92106741 CN1026650C (en) | 1992-10-05 | 1992-10-05 | Bactericidal composition for preventing and treating apple tree canker and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 92106741 CN1026650C (en) | 1992-10-05 | 1992-10-05 | Bactericidal composition for preventing and treating apple tree canker and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1072065A CN1072065A (en) | 1993-05-19 |
| CN1026650C true CN1026650C (en) | 1994-11-23 |
Family
ID=4942381
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 92106741 Expired - Fee Related CN1026650C (en) | 1992-10-05 | 1992-10-05 | Bactericidal composition for preventing and treating apple tree canker and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1026650C (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102180748A (en) * | 2011-03-03 | 2011-09-14 | 广西田园生化股份有限公司 | Foliar medicinal fertilizer containing water-soluble silicon |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE29722774U1 (en) * | 1997-12-23 | 1998-02-19 | EVO-K. Appel GmbH, 89075 Ulm | Spelled-based plant treatment products |
| CN101623013B (en) * | 2009-08-03 | 2013-12-04 | 青岛星牌作物科学有限公司 | Botanical fungicide, extracting method and usage thereof |
| CN104381348A (en) * | 2014-11-28 | 2015-03-04 | 李晓枫 | Botanical fungicide for preventing and controlling peach tree bleeding disease and preparation method of botanical fungicide for preventing and controlling peach tree bleeding disease |
-
1992
- 1992-10-05 CN CN 92106741 patent/CN1026650C/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102180748A (en) * | 2011-03-03 | 2011-09-14 | 广西田园生化股份有限公司 | Foliar medicinal fertilizer containing water-soluble silicon |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1072065A (en) | 1993-05-19 |
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