CN102641231B - Traditional Chinese medicine body lotion with twelve whitening ingredients and preparation method thereof - Google Patents
Traditional Chinese medicine body lotion with twelve whitening ingredients and preparation method thereof Download PDFInfo
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Abstract
The utility model discloses a traditional Chinese medicine body lotion with twelve whitening ingredients and a preparation method thereof. The traditional Chinese medicine body lotion contains the following traditional Chinese medicine components and matrices (in parts by weight): 6-15 parts of rhizoma bletillae, 6-15 parts of sinapsis alba, 10-22 parts of radix angelicae, 5-10 parts of dictamnus dasycarpus, 5-10 parts of ampelopsis japonica, 1.5-3 parts of Chinese loive, 3-9 parts of ginkgo, 5-10 parts of artemisia stelleriana, 7-15 part of white paeony, 1-8 parts of Chinese pulsatilla root, 0-6 parts of rhizoma typhonii and 1-3 parts of white sandalwood. The body lotion can quickly infiltrate the inner layer of the skin, promote the absorption of nutritional ingredients, strongly exclude metabolism waste and free oxygen radicals, restrain activity of tyrosinase, promote skin metabolism, and enable the skin to regain elasticity and vitality and become ruddy, smooth and glossy, thereby realizing the effects of moistening and whitening the skin. According to the preparation method, the combination of supercritical extraction and water extraction is adopted, the active ingredients of the traditional Chinese medicine can be effectively extracted, the functions of traditional Chinese medicines are improved, the limited and expensive traditional Chinese medicine source is saved; and the body lotion has good economical and social benefits.
Description
Technical field
The invention belongs to the daily-use chemical industry technical field, relate to a kind of Chinese medicine 12 white emollient cream and preparation method thereof.
Background technology
Various types of pigments of application on human skin mainly are because the human endocrine imbalance causes free oxygen free radical activation in the body, and tyrosinase activity is increased, the pigment anomaly deposition, thus cause chloasma, tinea versicolor, freckle, senile plaque etc.Will stop these skin splashs to form artificially, have only free oxygen free radical in the cortex of removing and the body, the restraint of tyrosinase activity just can achieve the goal.Chinese medicine thinks that melanic formation is owing to due to the reasons such as QI and blood retardance, depression of liver-QI, deficiency of kidney yin, impairment caused by overstrain spleen soil unusually, can adopt to have and enrich blood, invigorate blood circulation, regulate the flow of vital energy and the Chinese medicine of promoting muscle growth functions, by nourish blood, invigorate blood circulation, soothing liver-QI for relieving depression reduces melanic formation and nurses one's health.Invigorate blood circulation with Chinese medicine, make mechanism of qi be able to smoothness, promote local blood circulation, improve the local skin metabolism, pigment is dribbled.
Along with technological level improves, raw material becomes increasingly abundant, present cosmetics have more and more adopted external raw material and technology, make that the function of cosmetics is more and more stronger, prepare more and more superior.But this cosmetics adopt chemicals as raw material mostly, and its toxic and side effects is more and more worried by people.The cosmetics of white-skinned face function are a lot of in the market, traditional skin-whitening agents, using hydrogen peroxide, hydrogen chloride base hydrargyrum and various phenol derivatives, these chemical compounds that existing or surperficial melanin is organized rapidly toward coming and going disintegrates, reaches the effect of whitening fast.But can not effectively suppress melanin regrows because its composition of whitening does not infiltrate through the skin internal layer, mottle can occur again after a period of time, can not be from basic solution because the human endocrine imbalance causes free oxygen free radical activation in the body, make tyrosinase activity increase the abnormal deposition of pigment; Because its corrosivity to skin, cytotoxicity and anaphylaxis make it have great danger, in the hygienic practice of many countries, forbid in addition.Still there is certain hidden danger in safety evaluatio to the whitening function cosmetics at present, a large amount of survey results show, there are serious problems in the whitening product of beauty parlor, and the hydrargyrum disqualification rate is up to 43.8%, and skin care item cause mercury accumulation or chronic mercury poisoning also more and more to use that clean skin is whitened etc.As seen, there is certain defective in traditional skin-lightening cosmetic.
Along with the raising of people's living standard, the modern is also more and more higher for the pursuit of U.S., and the effect that the body whitening cr Pear Power is preserved moisture is requisite a kind of skin care item during people live.Modern medicine study shows that Chinese medicine can be by improving unusual hemorheology, suppressing cheese hydracid enzymatic activity and melanocytic propagation is synthetic, it is active and remove the effect that unnecessary superoxide radical reaches whitening and speckle dispelling to improve body superoxide dismutase (SOD).Therefore, has theoretical foundation with the Chinese medicine whitening and moistening skin.The psychology of pursuing green cosmetics, back to nature people strengthens day by day, and the natural activity cosmetics are complied with the trend that goes back to nature and people's consumer psychology.Be that the cosmetic product of active additive and cosmetic material becomes fine chemicals industry one big focus with the natural product of no side effects, the whitening product that has no side effect safely, arises at the historic moment, some Chinese herbal medicine with good whitening effect more and more are subjected to the green grass or young crops of consumer at present and hide, and are cosmetics " green " themes of 21 century.
China application number CN200510015158.7, green tea skin cream and preparation method thereof.This green tea skin cream is with green tea 10-12%, Mel 10-12%, Lac regis apis 5-7%, Wei jasmine quintessence oil 5-7%, solvent 62-70%.Green tea contains concentrated polyphenol, and can suppress radical pair skin Muller's fibers and damage, be the effective free radical resisting factor.With emollient cream that green tea is made, composition is natural, and skin whitening reduces the free radical in the skin simultaneously in a large number, makes skin level and smooth, can protect the elasticity of skin effectively.
200610129751.9 1 kinds of a kind of body whitening cr that are used for facial of China application number CN, it mainly is made up of liquid paraffin, vaseline, hexadecanol, linoleic acid first, propylene glycol, essence, distilled water.Body whitening cr is put on the skin drawing facial temperature rising on the face, and facial blood circulation is improved; The skin surface moisture evaporated is longer in the following time of staying of film, is conducive to skin moisture-keeping, makes the keratodermatitis softness; Putting back skin on the skin has tightly slightly, can make the skin smooth warship beautiful, prevents wrinkle, also can clean skin of face.
200710177764.8 1 kinds of incense cure emollient creams of China application number CN and preparation method thereof, it cooperates excipient paraffin 30-60 part, glycerol 30-60 part mix homogeneously to form mainly by Olibanum quintessence oil 1-5 part, Benzoinum quintessence oil 1-5 part, orange blossom quintessence oil 2-10 part, tea tree oil 5-20 part, the essential oil 1-5 part of returning from the grave.This emollient cream energy rapid permeability promotes the absorption of nutritional labeling to the skin internal layer, promotes skin metabolism, makes skin recover elasticity and vigor; Tighten skin pore simultaneously, make skin careful, smooth; Can effectively prevent the generation of mottle and wrinkle, have moistening effect and strengthen the preserve moisture water holding capacity of layer of skin, make skin lubricated and be rich in gloss.
China application number CN 200910101139.4 is manufacture methods of a kind of anti-aging moisturizer.Manufacture method is to take by weighing Rhizoma Atractylodis Macrocephalae 5-part by weight, Poria 5-10 part, and Pseudobulbus Bletillae (Rhizoma Bletillae) 5-10 part, Radix Angelicae Dahuricae 5-10 part, Radix Ampelopsis 5-10 part is pulverized, and mix homogeneously gets mixture A; Ratio in mixture A and water weight ratio 1: 3-5 will decoct 1-3 hour in the mixture A input water, filtration, and filtering residue repeats to decoct once again, filters, and the filtrate that merges 2 times gets liquor B; With the liquor B reverse osmosis concentration, get concentrated solution C again; Take by weighing distilled water 10-20 part then by weight, add glycerol 3-8 part, tea polyphenols 1-3 part, vitamin A 1-2 part, SOD 0.3-0.7 part, the kojic acid palm fibre is put acid esters 0.5-2 part, and heating for dissolving gets mixture D; The last vaseline that takes by weighing 20-50 part by weight after heating is dissolved, adds concentrated solution C and mixture D, stirs, and cooling namely gets product.This invention contains SOD, tea polyphenols, the stronger composition of this class removing free radical of the Rhizoma Atractylodis Macrocephalae, by removing the free radical in the tissue, keeps the integrity of cell function, thereby reaches the purpose of opposing senility of humanbody, not only can take stopgap measures but also can effect a permanent cure.The kojic acid palm fibre put acid esters, Poria, poliosis, in vain just, the Radix Ampelopsis composition, have good white-skinned face function, vitamin A can also well smooth away wrinkles, mottle, glycerol and vaseline can also stop the loss of moisture, keep skin wet.Therefore be a Pear Power, speckle dispelling, reduce wrinkle, preserve moisture, emollient cream of anti-senescence function.
China application number CN 201010522529.1 is a kind of medicine skin skin whiteners and preparation method thereof.This frost with dog oil, Adeps Caprae seu ovis, in vain just, Radix Glycyrrhizae, the Rhizoma Pinelliae, Fructus Mume, Herba Spirodelae, Fructus Gleditsiae Abnormalis be raw material, dog oil in the component, Adeps Caprae seu ovis are heated to 40 ℃ in pot, again will be in vain just, Radix Glycyrrhizae, the Rhizoma Pinelliae, Fructus Mume, Herba Spirodelae, Fructus Gleditsiae Abnormalis add in the pot, continue to be heated to boiling, slow fire boiled 40-50 minute again, carried out packing namely after removing slag after filtration, cooling off.
At present; cosmetics on the market are of a great variety; as cosmetic cream, beauty cream, fair complexion cream, cleansing milk etc.; its prescription contains all generally that octadecanol, glycerol, nipalgin second are cured, silicone oil, monoglyceride, water etc.; production technology and prescription that this class beauty treatmentization is herded product all are similar basically; also in various degree human body skin is had the effect of protection beauty treatment, but effect is not fine, the thin skin ulcer of face, comedo is not had yet the effect of nursing for treating.Emollient cream is a kind of of emulsion, can deeply moisten dry skin, replenishes the moisture content of skin loss every day.Traditional emollient cream, freckle effect is relatively poor, and contains synthetics, and zest is bigger, and abnormal smells from the patient is relatively poor.Existing medicine emollient cream is because its extracts active ingredients steam distillation, there are a lot of drawbacks in this preparation technology, its extraction ratio is low, can not be with some high boiling point, the composition of low volatility all extracts, and is under the condition of high temperature for a long time, the easy loss of the volatile ingredient of medicine, the material of some easy pyrolysis or chemical instability composition are also easily destroyed, and the loss of effective components of medicine is huge, have had a strong impact on the curative effect of medicine.Traditional water boiling and extraction also is at high temperature to carry out, and make the part effective ingredient of medical material destroyed because being heated for a long time, and extraction ratio is low, and the curative effect of medicine is also had very big influence.
Summary of the invention
The objective of the invention is: the one, adopt the pure natural material to make, abnormal smells from the patient delicate fragrance, and it is non-stimulated, do not have irritated reaction, make medicine energy rapid permeability to the skin internal layer, promote the absorption of nutritional labeling, promote skin metabolism, remove free oxygen free radical in cortex and the body, the restraint of tyrosinase activity makes skin recover elasticity and vigor; The 2nd, its extraction ratio that overcomes the prior preparation method existence is low, the composition of some high boiling point medicine all can not be put forward, the easy loss of volatile ingredient of low volatility medicine, the deficiency that the loss of effective components of medical material is big and a kind of Chinese medicine 12 white emollient cream and preparation method thereof are provided.
Technical scheme of the present invention is:
The present invention thinks that according to first inventor's secret recipe handed down in the family and Chinese medicine melanic formation is owing to due to the reasons such as QI and blood retardance, depression of liver-QI, deficiency of kidney yin, impairment caused by overstrain spleen soil unusually, can adopt to have and enrich blood, invigorate blood circulation, regulate the flow of vital energy and the Chinese medicine of promoting muscle growth functions, by nourish blood, invigorate blood circulation, soothing liver-QI for relieving depression reduces melanic formation and nurses one's health.Invigorate blood circulation with Chinese medicine, make mechanism of qi be able to smoothness, promote local blood circulation, improve the local skin metabolism, pigment is dribbled.Selecting for use can heat-clearing and toxic substances removing, the eliminating carbuncle eliminating stagnation, removing heat from blood nourishes blood, astringing to arrest bleeding, detumescence and promoting granulation, granulation promoting pain relieving, antibiotic radioprotective, remove free radical, can improve microcirculation in human body, promote skin metabolism, eliminate the Chinese medicine 12 BAIYAO materials that pigment is excessively piled up in tissue, adopt supercritical extraction and water extracting method, extract the effective ingredient in Chinese composition, preparation can be goed deep into the skin internal layer through Transdermal absorption, promote the absorption of nutritional labeling, endocrine regulation balance for oral administration is got rid of metabolic waste and free oxygen free radical, suppress tyrosine bacterium activity, promote skin metabolism, effectively prevent the generation of mottle and wrinkle, make skin recover elasticity and vigor, have moistening effect and strengthen the preserve moisture water holding capacity of layer of skin, make skin lubricated and be rich in Chinese medicine 12 white emollient cream of gloss.
The Chinese medicine pharmacology that the present invention adopts:
1, Pseudobulbus Bletillae (Rhizoma Bletillae): Pseudobulbus Bletillae (Rhizoma Bletillae) (Bletilla striata (Thunb.) Reichb.f., another name: sweet, give free of charge, indocalamus orchid, Zhu Lan, Rhizoma Bletillae, purple a species of orchid, hundred large bamboo hats with a conical crown and broad brim, Bletilla striata (Thunb.ex A.Murray)Rchb.f., Pseudobulbus Bletillae (Rhizoma Bletillae), Cold boiled chicken, Cold boiled chicken baby, Lian Jicao, YANGJIAOQI, sweet, pleionebulbocodioides rolfe, white black youngster's head, monarch's ball.Bitter in the mouth, sweet, puckery, cold nature is returned lung, liver, stomach warp.Has astringing to arrest bleeding, the detumescence and promoting granulation effect.Be used for spitting of blood and spit blood traumatic hemorrhage, sore swollen toxin, chapped skin; The pulmonary tuberculosis hemoptysis, ulcer haemorrhage.
2, Caulis et Folium Sinapis albee: Caulis et Folium Sinapis albee (Sinapis alba L.), another name: Hu mustard, another name for Sichuan Province mustard, hot food, white hot food.Acrid in the mouth, warm in nature, return lung meridian.Has warming the lung eliminating phlegm promoting the circulation of QI, resolving mass and removing the obstruction of the collateral pain relieving, antibiotic effect.Be used for cold-phlegm and breath with cough, distending pain in the chest and hypochondrium, the expectorant meridians that stagnate, joint numbness, pain, phlegm-damp oozing in the body, carbuncle of yin nature toxic swelling.
3, the Radix Angelicae Dahuricae: the Radix Angelicae Dahuricae (A.dahurica (Fisch.) Benth.et Hook), another name: the root of Dahurian angelica, fragrance, membrane inside the rush stalk Li, Ze Fen, Bai Chen, kind Radix Angelicae Dahuricae, Xingan's Radix Angelicae Dahuricae, the storehouse page or leaf Radix Angelicae Dahuricae, Radix angelicae dahuricae, the post Radix Angelicae Dahuricae, angelica anomala, fragrant rod, Chai.Warm in nature, acrid in the mouth are returned lung, spleen, stomach warp.Has wind-damp dispelling, the evacuation of pus of invigorating blood circulation, granulation promoting pain relieving, antibiotic radioprotective effect.Be used for headache, toothache, hemorrhoidal hamorrhage anal fistula, leucorrhea with red and white discharge, ulcer sores, skin pruritus, can improve microcirculation in human body, promote skin metabolism, eliminate pigment and in tissue, excessively pile up, remove facial colour spot cicatrix etc.
4, shaggy-fruited dittany: shaggy-fruited dittany (Dictamnus dasycarpus Turcz.), another name: Cortex Dictamni, stereotyped writing cattle, Cortex Argyreiae Seguinii Radicis, the bright grass of sheep, northern Cortex Dictamni, moss skin, pericarpium Zanthoxyli root bark, smelly root bark.Bitter in the mouth, cold in nature is returned spleen, stomach, urinary bladder channel.Has heat clearing and damp drying, the detoxifcation of dispeling the wind, antibiotic effect.Be used for damp and hot sore, yellow fluid is dripping, eczema, rubella, scabies skin ulcer leprosy, rheumatism pyretic arthralgia, jaundice dark coloured urine.
5, hold back in vain: hold back (Ampelopsis japondca (Thunb.) Makino.) in vain, another name: rabbit nuclear, Bletilla striata (Thunb.ex A.Murray)Rchb.f., the Kunlun, cat ovum, goose hatch, JIANZHONGXIAO, wear that mountain mouse, white water tank, mountain region melon, ferrum mouse, hen band son, Cortex Capparis Spinosae Radicis potato, mountain Semen Castaneae, people's divinatory symbol cattle, white slurry jar, wild Radix Ipomoeae, DILAOSHU, the outstanding potato in open country, hen hatch, nine Niu Li.Bitter in the mouth, cold nature, GUIXIN, stomach warp.Have heat-clearing and toxic substances removing, the eliminating carbuncle eliminating stagnation suppresses fungal efficacy.Be used for the carbuncle carbuncle on the back, furuncle, scrofula, burn due to hot liquid or fire.
6, BAIYAO: BAIYAO (Radix Aconiti Ecalcarati), another name: BAIYAO Radix Aconiti Kusnezoffii, BAIYAO root, Stephania cepharatha Hayata.Bitter in the mouth, cold in nature is returned spleen, lung, kidney channel.Has dissipating blood stasis for subsidence of swelling, detoxifcation, pain relieving effect.Be used for swollen ulcer drug, parotitis, venom, treating swelling and pain by traumatic injury.
7, Semen Ginkgo: Semen Ginkgo (Ginkgo biloba L.), another name: duck bottom sediment, mental eye, Herba Sedi Multicaulis, Ginkgo biloba Linn.cv.Fozhi Citrus chachiensis Hort., Semen Ginkgo, Gong Sunshuzi.Sweet in the mouth, hardship, puckery, property is flat, and mild toxicity is returned lung meridian.Have astringing lung QI for relieving asthma, leukorrhagia stopping is turbid, and is antibiotic, removes free radical, the convergence effect.Be used for abundant expectoration and breath with cough leukorrhagia nebulousurine, the enuresis, frequent micturition, innominate toxic swelling, Zha nose, tinea skin ulcer.
8, Herba Artemisiae Sieversianae: Herba Artemisiae Sieversianae (Herba Artimisiae Sieversianae), another name: cyclophanes, white Artemisia, by Hu, certain kind of berries mother, other vigorous, white Radix Artemisia ordosicae, Herba Artemisiae Sieversianae, Herba Artemisiae Sieversianae, Artemisia sieversiana, smelly Herba Artemisiae, sierra salvia, major part Artemisia, Herba Acroptili repentis greatly.Bitter in the mouth, little sweet, cool in nature.Has clearing away heat-damp and promoting diuresis, the cooling blood for hemostasis effect.Be used for swollen heat cough, laryngopharynx swelling and pain, jaundice due to damp-heat, hematodiarrhoea, gonorrhea, rheumatic arthralgia is spitted blood, spitting of blood, traumatic hemorrhage, scabies La malignant boil.
9, the Radix Paeoniae Alba: the Radix Paeoniae Alba (Paeonia lactiflora Pall.), another name: Radix Paeoniae, golden Radix Paeoniae, Radix Paeoniae Alba.Bitter in the mouth, acid, cold nature is returned liver, spleen channel.Have antibiotic, suppressing the hyperactive liver pain relieving, nourishing blood for regulating menstruation, astringing YIN to stop sweating effect.It is dizzy to be used for headache, hypochondriac pain, stomachache, limb pain twin, blood deficiency and yellow complexion, menoxenia, spontaneous perspiration, night sweat.
10, the Radix Pulsatillae: the Radix Pulsatillae (RADIX PULSATILLAE), another name: how grass, powder silkweed, hoary hair's grass, Lao Gucao, chrysanthemum chrysanthemum Seedling, old man spend, always hat flower, the sub-flower of ram's horn, husband spend, Mao aunt's flower.Bitter in the mouth, cold in nature.Return stomach, large intestine channel.Have heat-clearing and toxic substances removing, eliminating pathogenic heat from blood to cure dysentery, antibiotic, analgesia, disinsection efficiency.Be used for toxic-heat and blood stasis, pudendal pruritus leukorrhagia, carbuncle skin ulcer, scrofula.
11, Rhizoma Typhonii: Rhizoma Typhonii (Typhonium giganteum Engl.), another name: the ginseng of dripping, Rhizoma Arisaematis, Rhizoma Colocasiae antiquori, Rhizoma Typhonii, Rhizoma Typhonium Gigantei (Rhizoma Typhonii), furunculosis bean, the Folium Colocasiae Esculentae Rhizoma Pinelliae, the wild Rhizoma Pinelliae, Rhizoma typhonii divaricati, Herba clinopodii confinis (Herba Clinopodii Gracilis), beautifully comply with one's wishes, wild arrowhead, one in copy be red.Acrid in the mouth, warm in nature, mild toxicity.Return stomach, Liver Channel.Have antiinflammatory, the expectorant that dispels the wind, arresting convulsion is jerked, detoxicating and resolving stagnation of pathogens pain relieving effect.Be used for wind-phlegm and stop up, facial hemiparalysis, language is puckery stuttering, syncope due to accumulation of phlegm headache, migraine and general headache, sore throat pharyngalgia, tetanus; External treatment scrofula sucutaneous nodule, venom.
12, Santalum album: Santalum album (Santalum album L.), another name: ZHA GANZAN DAN, Symplocoris Paniculatae, Lignum Santali Albi.Warm in nature, acrid in the mouth, nontoxic, return spleen, stomach, lung meridian.Have interior-heat clearly, vicious swelling due to wind is separated in nourishing, and is antibiotic, disinsection efficiency.Be used for the cough due to lung-heat, chest pain asthma, cardiopalmus, precordial pain.
13, Margarita: Margarita (Pernulo), the Margarita salty in the mouth is sweet cold nontoxic.The Main Ingredients and Appearance of Margarita is calcium carbonate, prove through modern medicine study, Margarita is rich in needed by human body several amino acids such as leucine, glycine methionine, alanine, glutamic acid, aspartic acid and 20 various trace elements such as ferrum, copper, magnesium, zinc, manganese, sodium, selenium etc., can effectively participate in and promote the human life activity, endocrine regulation, the conditioning homoiostasis is taken good care of QI and blood, skin care.Three kinds of trace element such as the manganese of Margarita powder, copper, zinc are the compositions of forming SOD, are coated with face with Margarita powder, can promote the activity of human skin superoxide dismutase (SOD), Pear Power, control oil, anti-acne, pore cleanser, light speckle, granulation promoting effect.
The present invention is achieved in that
A kind of Chinese medicine 12 white emollient cream, Chinese medicinal components and emollient cream substrate are formed (weight portion): Pseudobulbus Bletillae (Rhizoma Bletillae) 6-15 part, Caulis et Folium Sinapis albee 6-15 part, Radix Angelicae Dahuricae 10-22 part, shaggy-fruited dittany 5-10 part, hold back 5-10 part, BAIYAO 1.5-3 part, Semen Ginkgo 3-9 part, Herba Artemisiae Sieversianae 5-10 part, Radix Paeoniae Alba 10-15 part, Radix Pulsatillae 1-8 part, Rhizoma Typhonii 0-6 part, Santalum album 1-3 part and emollient cream substrate in vain; Described emollient cream substrate is sodium carboxymethyl cellulose 1-6 part, TC 1-5 part, triethanolamine 0.5-1 part, Tween 80 1-5 part, deionized water 15-35 part; Described Rhizoma Typhonii or replace with commercially available ultra-fine Margarita powder 0.1-3.5 part.
Above-described emollient cream, Chinese medicinal components and emollient cream substrate are formed (weight portion): Chinese medicine Pseudobulbus Bletillae (Rhizoma Bletillae) 10-12 part, Caulis et Folium Sinapis albee 10-12 part, Radix Angelicae Dahuricae 16-20 part, shaggy-fruited dittany 6-8 part, hold back 6-8 part, BAIYAO 1.5-2 part, Semen Ginkgo 5-6 part, Herba Artemisiae Sieversianae 6-8 part, Radix Paeoniae Alba 11-13 part, Radix Pulsatillae 5-6 part, Margarita powder 0.1-3.5 part, Santalum album 2-2.5 part and emollient cream substrate in vain; Described emollient cream substrate is sodium carboxymethyl cellulose 3-4 part, TC 2-3 part, triethanolamine 0.5-0.7 part, Tween 80 3-4 part, deionized water 20-30 part.
Above-described emollient cream replaces Rhizoma Typhonii with Margarita powder, and Chinese medicinal components and emollient cream substrate are formed (weight portion): 11 parts of Chinese medicine Pseudobulbus Bletillae (Rhizoma Bletillae), 11 parts of Caulis et Folium Sinapis albees, 18 parts of the Radixs Angelicae Dahuricae, 7 parts of shaggy-fruited dittanies, hold back 7 parts, 2 parts of BAIYAO, 5 parts of Semen Ginkgoes, 7 parts of Herba Artemisiae Sieversianaes, 12 parts of the Radix Paeoniae Albas, 5 parts of the Radix Pulsatillaes, 2 parts of Margarita powder, 2.5 parts of Santalum albums and emollient cream substrate in vain; Described emollient cream substrate is 3.5 parts of sodium carboxymethyl cellulose, 3 parts of TC, 0.6 part of triethanolamine, 4 parts of Tween 80s, 26 parts of deionized waters.
A kind of preparation method of Chinese medicine 12 white emollient cream, comprise the Chinese medicine extracts active ingredients, decolouring and preparation cream, described Chinese medicine extracts active ingredients is to adopt carbon dioxide supercritical fluid extraction and recirculation water to put forward two-step method to extract, earlier with raw material Chinese medicine Pseudobulbus Bletillae (Rhizoma Bletillae) 6-15 part, Caulis et Folium Sinapis albee 6-15 part, Radix Angelicae Dahuricae 10-22 part, shaggy-fruited dittany 5-10 part, hold back 5-10 part in vain, BAIYAO 1.5-3 part, Semen Ginkgo 3-9 part, Herba Artemisiae Sieversianae 5-10 part, Radix Paeoniae Alba 10-15 part, Radix Pulsatillae 1-8 part, Rhizoma Typhonii 0-6 part, Santalum album 1-3 part is ground into coarse powder, obtain supercritical extract through carbon dioxide supercritical fluid extraction, the medicinal residues water refluxes and decocts the back filtration, the filtrate vacuum concentration obtains water extract, merges carbon dioxide supercritical fluid extraction thing and water extract and obtains Chinese medicine extract; Described decolouring is that Chinese medicine extract is dissolved in the ethanol water, adds activated carbon decolorizing, filters, and vacuum concentration obtains the Chinese medicine clear paste; Described preparation cream is that the Chinese medicine clear paste is added emollient cream substrate and/or Chinese medicine Margarita powder 0.1-3.5 part, uses conventional method emulsifying, and homogenizing obtains Chinese medicine 12 white emollient cream, and its step is as follows:
1, pulverize: it is standby that medicinal pulverizer in the clean raw material is ground into 30-60 order Chinese medicine coarse powder;
2, supercritical extraction: obtain supercritical extract with carrying out carbon dioxide supercritical fluid extraction in the input of the Chinese medicine coarse powder except the venezuelan powder supercritical extraction device;
3, water is carried: drop in the backflow digester through the medicinal residues of supercritical extraction, after adding the water recirculation water and carrying, filter, 55-80 ℃ of vacuum concentration of control temperature obtains the decocting in water extract;
4, decolouring: Chinese medicine supercritical extract and decocting in water extract are dissolved in the ethanol water, add activated carbon decolorizing, filter, 55-80 ℃ of vacuum concentration of control temperature obtains the Chinese medicine clear paste, recovered carbon and alcoholic solution;
5, mix: Chinese medicine clear paste and emollient cream base starting material sodium carboxymethyl cellulose 1-6 part, TC 1-5 part, triethanolamine 0.5-1 part, Tween 80 1-5 part, deionized water 15-35 part and/or Chinese medicine Margarita powder 0.1-3.5 part are used conventional method emulsifying, and homogenizing obtains Chinese medicine 12 white emollient cream.
The extracting pressure of above-described carbon dioxide supercritical fluid extraction is 12-35Mpa, and extraction temperature is 30-50 ℃, and the extraction time is 0.5-2 hour, and carbon dioxide flow is 16-40kg/ hour;
Above-described recirculation water is put forward 85-100 ℃ of control temperature, and the decocting in water time is 1-2.5 hour;
The determining alcohol of above-described ethanol water is 45-80%.
Advantage of the present invention and good effect:
1, this product employing Chinese medicine is raw material, has treating both the principal and secondary aspects of a disease, have no side effect, and to the skin nonirritant, the emulsion particle exquisiteness, coating is even, and feel is cunning, and spreadability is good.Have powerful eliminating metabolic waste and free oxygen free radical, suppress cheese ammonia enzymatic activity, the energy rapid permeability is to the skin internal layer, promote the absorption of nutritional labeling, promote skin metabolism, make skin recover elasticity and vigor, skin is ruddy, lubricated and be rich in gloss, reach the effect of skin care and skin whitening.
2, this preparation method adopts supercritical extraction and the combination of water extracting method, has overcome traditional emollient cream, and freckle effect is relatively poor, and contains synthetics, and zest is bigger, the shortcoming that abnormal smells from the patient is relatively poor.Overcome existing Chinese medicine emollient cream because there are a lot of drawbacks in its extracts active ingredients with steam distillation preparation technology; extraction ratio is higher; the composition of some high boiling point and low volatility all can be extracted; and the volatile ingredient of medicine is not easy loss; easily material or the chemical instability composition of pyrolysis are protected; the loss of effective components of medicine is less; can effectively extract the effective ingredient in Chinese composition; improve the function of Chinese medicine; and save limited and the high Chinese medicine of valency money is former, have favorable economic benefit and social benefit.
The specific embodiment
Describe in further detail below in conjunction with the present invention of embodiment, listed embodiment only is the present invention is described and never is limited to the present invention.
Embodiment 1
(1) Chinese medicinal components and emollient cream substrate are formed:
Chinese medicine: 1 kilogram of Pseudobulbus Bletillae (Rhizoma Bletillae), 1 kilogram of Caulis et Folium Sinapis albee, 1.6 kilograms of the Radixs Angelicae Dahuricae, 0.8 kilogram of shaggy-fruited dittany, hold back 0.8 kilogram, 0.25 kilogram of BAIYAO, 0.6 kilogram of Semen Ginkgo, 0.8 kilogram of Herba Artemisiae Sieversianae, 1.1 kilograms of the Radix Paeoniae Albas, 0.6 kilogram of the Radix Pulsatillae, 0.5 kilogram of Rhizoma Typhonii, 0.3 kilogram of Santalum album in vain.
Emollient cream substrate: 0.3 kilogram of sodium carboxymethyl cellulose, 0.2 kilogram of TC, 0.1 kilogram of triethanolamine, 0.35 kilogram of Tween 80,2.2 kilograms of deionized waters.
(2) preparation method:
Medicinal pulverizer in the clean raw material is ground into 40 order Chinese medicine coarse powder, to carry out carbon dioxide supercritical fluid extraction in the Chinese medicine coarse powder input supercritical extraction device, extracting pressure is 12.5Mpa, extraction temperature is 50 ℃, the extraction time is 1 hour, and carbon dioxide flow is to obtain supercritical extract in 40kg/ hour; Drop in the backflow digester through the medicinal residues of supercritical extraction, add water again recirculation water carry, recirculation water is put forward 100 ℃ of control temperature, the time is 1 hour, filters according to a conventional method then, 55 ℃ of vacuum concentration of control temperature obtain the decocting in water extract, reclaim alcoholic solution; It is in 50% the ethanol water that Chinese medicine supercritical extract and decocting in water extract are dissolved in concentration, adds activated carbon decolorizing, filters, and adopts conventional vacuum concentration to obtain the Chinese medicine clear paste, recovered carbon and ethanol; At last Chinese medicine clear paste and emollient cream base starting material are obtained Chinese medicine 12 white emollient cream with conventional method emulsifying homogenizing.
Embodiment 2
(1) Chinese medicinal components and emollient cream substrate are formed:
Chinese medicine: 1.1 kilograms of Pseudobulbus Bletillae (Rhizoma Bletillae), 1.1 kilograms of Caulis et Folium Sinapis albees, 1.8 kilograms of the Radixs Angelicae Dahuricae, 0.7 kilogram of shaggy-fruited dittany, hold back 0.7 kilogram, 0.2 kilogram of BAIYAO, 0.7 kilogram of 0.5 kilogram of Herba Artemisiae Sieversianae of Semen Ginkgo, 1.2 kilograms of the Radix Paeoniae Albas, 0.5 kilogram of the Radix Pulsatillae, 0.2 kilogram of Margarita powder, 0.25 kilogram of Santalum album in vain.
Emollient cream substrate: 0.35 kilogram of sodium carboxymethyl cellulose, 0.3 kilogram of TC, 0.06 kilogram of triethanolamine, 0.3 kilogram of Tween 80,2.6 kilograms of deionized waters.
(2) preparation method:
Medicinal pulverizer in the clean raw material is ground into 60 order Chinese medicine coarse powder, to carry out carbon dioxide supercritical fluid extraction in the Chinese medicine coarse powder input supercritical extraction device, extracting pressure is 35Mpa, extraction temperature is 30 ℃, the extraction time is 0.5 hour, and carbon dioxide flow is to obtain supercritical extract in 36kg/ hour; Drop in the backflow digester through the medicinal residues of supercritical extraction, add water again recirculation water carry, recirculation water is put forward 85 ℃ of control temperature, the time is 2.5 hours, filters according to a conventional method then, 70 ℃ of vacuum concentration of control temperature obtain the decocting in water extract, reclaim alcoholic solution; It is in 70% the ethanol water that Chinese medicine supercritical extract and decocting in water extract are dissolved in concentration, adds activated carbon decolorizing, filters, and adopts conventional vacuum concentration to obtain the Chinese medicine clear paste, recovered carbon and ethanol; At last Chinese medicine clear paste and emollient cream base starting material and Margarita powder are obtained Chinese medicine 12 white emollient cream with conventional method emulsifying homogenizing.
Embodiment 3
(1) Chinese medicinal components and emollient cream substrate are formed:
Chinese medicine: 0.6 kilogram of Pseudobulbus Bletillae (Rhizoma Bletillae), 1.5 kilograms of Caulis et Folium Sinapis albees, 1.2 kilograms of the Radixs Angelicae Dahuricae, 0.6 kilogram of shaggy-fruited dittany, hold back 0.6 kilogram, 0.2 kilogram of BAIYAO, 0.3 kilogram of Semen Ginkgo, 1 kilogram of Herba Artemisiae Sieversianae, 1.1 kilograms of the Radix Paeoniae Albas, 0.7 kilogram of the Radix Pulsatillae, 0.1 kilogram of Rhizoma Typhonii, 0.15 kilogram of Santalum album in vain.
Emollient cream substrate: 0.2 kilogram of sodium carboxymethyl cellulose, 0.15 kilogram of TC, 0.05 kilogram of triethanolamine, 0.15 kilogram of Tween 80,2.5 kilograms of deionized waters.
Medicinal pulverizer in the clean raw material is ground into 60 order Chinese medicine coarse powder, to carry out carbon dioxide supercritical fluid extraction in the Chinese medicine coarse powder input supercritical extraction device, extracting pressure is 25Mpa, extraction temperature is 35 ℃, the extraction time is 1 hour, and carbon dioxide flow is to obtain supercritical extract in 20kg/ hour; Drop in the backflow digester through the medicinal residues of supercritical extraction, add water again recirculation water carry, recirculation water is put forward 90 ℃ of control temperature, the time is 2 hours, filters according to a conventional method then, the control temperature is carried out vacuum concentration for 75 ℃, obtains the decocting in water extract, reclaims alcoholic solution; It is in 60% the ethanol water that Chinese medicine supercritical extract and decocting in water extract are dissolved in concentration, adds activated carbon decolorizing, filters, and adopts conventional vacuum concentration to obtain the Chinese medicine clear paste, recovered carbon and ethanol; At last Chinese medicine clear paste and emollient cream base starting material are obtained Chinese medicine 12 white emollient cream with conventional method emulsifying homogenizing.
Embodiment 4
(1) Chinese medicinal components and emollient cream substrate are formed:
Chinese medicine: 1.5 kilograms of Pseudobulbus Bletillae (Rhizoma Bletillae), 0.8 kilogram of Caulis et Folium Sinapis albee, 2 kilograms of the Radixs Angelicae Dahuricae, 1 kilogram of shaggy-fruited dittany, hold back 0.9 kilogram, 0.3 kilogram of BAIYAO, 0.8 kilogram of Semen Ginkgo, 0.6 kilogram of Herba Artemisiae Sieversianae, 1.5 kilograms of the Radix Paeoniae Albas, 0.1 kilogram of the Radix Pulsatillae, 0.4 kilogram of Rhizoma Typhonii, 0.25 kilogram of Santalum album in vain.
Emollient cream substrate: 0.35 kilogram of sodium carboxymethyl cellulose, 0.4 kilogram of TC, 0.1 kilogram of triethanolamine, 0.4 kilogram of Tween 80,3 kilograms of deionized waters.
Medicinal pulverizer in the clean raw material is ground into 30 order Chinese medicine coarse powder, to carry out carbon dioxide supercritical fluid extraction in the Chinese medicine coarse powder input supercritical extraction device, extracting pressure is 12Mpa, extraction temperature is 45 ℃, the extraction time is 2.5 hours, and carbon dioxide flow is to obtain supercritical extract in 16kg/ hour; Drop in the backflow digester through the medicinal residues of supercritical extraction, add water again recirculation water carry, recirculation water is put forward 85 ℃ of control temperature, the time is 1.5 hours, filters according to a conventional method then, the control temperature is carried out vacuum concentration for 55 ℃, obtains the decocting in water extract, reclaims alcoholic solution; It is in 45% the ethanol water that Chinese medicine supercritical extract and decocting in water extract are dissolved in concentration, adds activated carbon decolorizing, filters, and adopts conventional vacuum concentration to obtain the Chinese medicine clear paste, recovered carbon and ethanol water; At last Chinese medicine clear paste and emollient cream base starting material are obtained Chinese medicine 12 white emollient cream with conventional method emulsifying homogenizing.
Application example
1, cover X X: the women, occupation: the workman of plant, 24 years old age, the skin of face dark, nonelastic, body limbs is because job specification forms pachylosis, and there is tinea versicolor not of uniform size at the neck of health, back, and palm, heel have thick cocoon partial fracture.Once used multiple skincare product not improve, trial edition embodiment 1 product is After Hours used the Water-heating shower whole body every afternoon, and present embodiment 1 product is smeared one time, allows it absorb naturally; Again the health epidermis is smeared once before the sleep at night, carried out skin massaging then and comfort stranding 5-10 minute.20 days extensive elasticity of rear section skin and vigor have improvement, and it is ruddy that the skin of face dark is transformed into skin, and be lubricated, and glossy; Body limbs skin lubrication after 40 days, the neck of health, the tinea versicolor at back disappear, but hands, foot have the thick cocoon part skin that breaks still to improve not obvious; Increase hands every morning afterwards, the foot skin skin is smeared once, adheres to 80 days, hands, foot had the part skin all rehabilitations of breaking of thick cocoon originally, the ill symptoms of all body skins disappears, face skin is ruddy and glossy.
2, poplar X: the women, occupation: construction supervision, at 35 years old age, skin of face obviously has freckle, and body skin is coarse, skin pore expansion, sweat gland prosperity, body odor are serious.Trial edition embodiment 2 products are smeared on the whole skin after morning every day, late twice shower, allow it absorb naturally.Facial skin at first improved in 21 days, and black partly disappears flexible; Facial skin freckle disappeared in 42 days, and the colour of skin is ruddy, and surface lubrication is glossy; The body skin pore shrinks, and body odor reduces; The ill symptoms of body skin disappears after 66 days, and whole skin is lubricated glossy, and face skin is ruddy.Pay a return visit poplar X after 1 year, she adheres to smearing present embodiment 2 products after the shower in evening every day, and skin is good always, and body skin is more and more delicate, face skin is ruddy, coloured and dazzling.
3, father-in-law X X: the women, at 30 years old age, skin of face is coarse, and black clouds shape dark is arranged.Trial edition embodiment 3 products, every day, early, middle and late each suds cleaned face, and present embodiment 3 products are smeared.Facial pachylosis sense in 10 days improves, and black clouds shape dark is thin out; 20 days dark eliminations of facial skin black clouds shape, the colour of skin begins to carry bright, the delicacy of having rosy cheeks.
4, Lee X X, the women, the age: 22, occupation: student, skin symptom: skin greasing, colour of skin inequality.Before the use: the skin of face HUANGBAI(sic) has concurrently, and skin oiliness is stronger, glossy having one's face covered with, use present embodiment 4 products, early, evening each water clean facially, present embodiment 4 products are smeared, yellow cutin came off gradually in 14 days, cutin skin was penetrating in 28 days, and oiliness weakens, and yellow colloid all came off in 42 days, glossy disappearance, facial skin was fair and clear ruddy in 60 days, and colour of skin water is tender evenly, and is glossy.
5, old X X: the male, at 26 years old age, occupation: the civil servant, skin symptom: facial skin is coarse, and red point is arranged.Before the use: skin is intensely dark, and is dry coarse, and red point is arranged, and trial edition embodiment 2 products after shower every night, are smeared present embodiment 2 products 30 minutes on the face, clean up then.The red point of facial skin was thin out in 7 days; Pachylosis sense in 14 days improves; Red point disappeared in 30 days, and skin begins smooth bright; Facial skin complexion was even in 60 days, and is smoothly glossy.
Claims (8)
1. Chinese medicine 12 white emollient cream, it is characterized in that: made by following Chinese medicinal components and emollient cream substrate, its parts by weight are: Pseudobulbus Bletillae (Rhizoma Bletillae) 6-15 part, Caulis et Folium Sinapis albee 6-15 part, Radix Angelicae Dahuricae 10-22 part, shaggy-fruited dittany 5-10 part, hold back 5-10 part, BAIYAO 1.5-3 part, Semen Ginkgo 3-9 part, Herba Artemisiae Sieversianae 5-10 part, Radix Paeoniae Alba 10-15 part, Radix Pulsatillae 1-8 part, Rhizoma Typhonii 0-6 part, Santalum album 1-3 part and emollient cream substrate in vain; Described emollient cream substrate is sodium carboxymethyl cellulose 1-6 part, TC 1-5 part, triethanolamine 0.5-1 part, Tween 80 1-5 part, deionized water 15-35 part.
2. Chinese medicine 12 white emollient cream, it is characterized in that: made by following Chinese medicinal components and emollient cream substrate, its parts by weight are: Pseudobulbus Bletillae (Rhizoma Bletillae) 10-12 part, Caulis et Folium Sinapis albee 10-12 part, Radix Angelicae Dahuricae 16-20 part, shaggy-fruited dittany 6-8 part, hold back 6-8 part, BAIYAO 1.5-2 part, Semen Ginkgo 5-6 part, Herba Artemisiae Sieversianae 6-8 part, Radix Paeoniae Alba 11-13 part, Radix Pulsatillae 5-6 part, Margarita powder 0.1-3.5 part, Santalum album 2-2.5 part and emollient cream substrate in vain; Described emollient cream substrate is sodium carboxymethyl cellulose 3-4 part, TC 2-3 part, triethanolamine 0.5-0.7 part, Tween 80 3-4 part, deionized water 20-30 part.
3. a kind of Chinese medicine 12 white emollient cream according to claim 2, it is characterized in that: made by following Chinese medicinal components and emollient cream substrate, its parts by weight are: 11 parts of Pseudobulbus Bletillae (Rhizoma Bletillae), 11 parts of Caulis et Folium Sinapis albees, 18 parts of the Radixs Angelicae Dahuricae, 7 parts of shaggy-fruited dittanies, hold back 7 parts, 2 parts of BAIYAO, 5 parts of Semen Ginkgoes, 7 parts of Herba Artemisiae Sieversianaes, 12 parts of the Radix Paeoniae Albas, 5 parts of the Radix Pulsatillaes, 2 parts of Margarita powder, 2.5 parts of Santalum albums and emollient cream substrate in vain; Described emollient cream substrate is 3.5 parts of sodium carboxymethyl cellulose, 3 parts of TC, 0.6 part of triethanolamine, 4 parts of Tween 80s, 26 parts of deionized waters.
4. the preparation method of a kind of Chinese medicine 12 white emollient cream according to claim 1, comprise the Chinese medicine extracts active ingredients, decolouring and preparation cream, it is characterized in that: described Chinese medicine extracts active ingredients is to adopt carbon dioxide supercritical fluid extraction and recirculation water to put forward two-step method to extract, earlier with raw material Chinese medicine Pseudobulbus Bletillae (Rhizoma Bletillae) 6-15 part, Caulis et Folium Sinapis albee 6-15 part, Radix Angelicae Dahuricae 10-22 part, shaggy-fruited dittany 5-10 part, hold back 5-10 part in vain, BAIYAO 1.5-3 part, Semen Ginkgo 3-9 part, Herba Artemisiae Sieversianae 5-10 part, Radix Paeoniae Alba 10-15 part, Radix Pulsatillae 1-8 part, Rhizoma Typhonii 0-6 part, Santalum album 1-3 part is ground into coarse powder, obtain supercritical extract through carbon dioxide supercritical fluid extraction, the medicinal residues water refluxes and decocts the back filtration, the filtrate vacuum concentration obtains water extract, merges carbon dioxide supercritical fluid extraction thing and water extract and obtains Chinese medicine extract; Described decolouring is that Chinese medicine extract is dissolved in the ethanol water, adds activated carbon decolorizing, filters, and vacuum concentration obtains the Chinese medicine clear paste; Described preparation cream is that the Chinese medicine clear paste is added emollient cream substrate, uses conventional method emulsifying, and homogenizing obtains Chinese medicine 12 white emollient cream, and its step is as follows:
(1) pulverize: it is standby that medicinal pulverizer in the clean raw material is ground into 30-60 order Chinese medicine coarse powder;
(2) supercritical extraction: obtain supercritical extract with carrying out carbon dioxide supercritical fluid extraction in the Chinese medicine coarse powder input supercritical extraction device;
(3) water is carried: drop in the backflow digester through the medicinal residues of supercritical extraction, after adding the water recirculation water and carrying, cooling is filtered, and 55-80 ℃ of vacuum concentration of control temperature obtains the decocting in water extract;
(4) decolouring: Chinese medicine supercritical extract and decocting in water extract are dissolved in the ethanol water, add activated carbon decolorizing, filter, 55-80 ℃ of vacuum concentration of control temperature obtains the Chinese medicine clear paste, recovered carbon and alcoholic solution;
(5) mix: with Chinese medicine clear paste and emollient cream base starting material sodium carboxymethyl cellulose 1-6 part, TC 1-5 part, triethanolamine 0.5-1 part, Tween 80 1-5 part and deionized water 15-35 part, use conventional method emulsifying, homogenizing obtains Chinese medicine 12 white emollient cream.
5. according to the preparation method of claim 2 or 3 described a kind of Chinese medicine 12 white emollient cream, comprise the Chinese medicine extracts active ingredients, decolouring and preparation cream, it is characterized in that: described Chinese medicine extracts active ingredients is to adopt carbon dioxide supercritical fluid extraction and recirculation water to put forward two-step method to extract, earlier with raw material Chinese medicine Pseudobulbus Bletillae (Rhizoma Bletillae) 10-12 part, Caulis et Folium Sinapis albee 10-12 part, Radix Angelicae Dahuricae 16-20 part, shaggy-fruited dittany 6-8 part, hold back 6-8 part in vain, BAIYAO 1.5-2 part, Semen Ginkgo 5-6 part, Herba Artemisiae Sieversianae 6-8 part, Radix Paeoniae Alba 11-13 part, Radix Pulsatillae 5-6 part, Santalum album 2-2.5 part is ground into coarse powder, obtain supercritical extract through carbon dioxide supercritical fluid extraction, the medicinal residues water refluxes and decocts the back filtration, the filtrate vacuum concentration obtains water extract, merges carbon dioxide supercritical fluid extraction thing and water extract and obtains Chinese medicine extract; Described decolouring is that Chinese medicine extract is dissolved in the ethanol water, adds activated carbon decolorizing, filters, and vacuum concentration obtains the Chinese medicine clear paste; Described preparation cream is that the Chinese medicine clear paste is added emollient cream substrate and Chinese medicine Margarita powder, uses conventional method emulsifying, and homogenizing obtains Chinese medicine 12 white emollient cream, and its step is as follows:
(1) pulverize: it is standby that medicinal pulverizer in the clean raw material is ground into 30-60 order Chinese medicine coarse powder;
(2) supercritical extraction: obtain supercritical extract with carrying out carbon dioxide supercritical fluid extraction in the Chinese medicine coarse powder input supercritical extraction device;
(3) water is carried: drop in the backflow digester through the medicinal residues of supercritical extraction, after adding the water recirculation water and carrying, cooling is filtered, and 55-80 ℃ of vacuum concentration of control temperature obtains the decocting in water extract;
(4) decolouring: Chinese medicine supercritical extract and decocting in water extract are dissolved in the ethanol water, add activated carbon decolorizing, filter, 55-80 ℃ of vacuum concentration of control temperature obtains the Chinese medicine clear paste, recovered carbon and alcoholic solution;
(5) mix: with Chinese medicine clear paste and emollient cream base starting material sodium carboxymethyl cellulose 3-4 part, TC 2-3 part, triethanolamine 0.5-0.7 part, Tween 80 3-4 part, deionized water 20-30 part and Margarita powder 0.1-3.5 part, use conventional method emulsifying, homogenizing obtains Chinese medicine 12 white emollient cream.
6. according to claim 4 or 5 described preparation methoies, it is characterized in that: the extracting pressure of described carbon dioxide supercritical fluid extraction is 12-35Mpa, and extraction temperature is 30-50 ℃, and the extraction time is 0.5-2 hour, and carbon dioxide flow is 16-40kg/ hour.
7. according to claim 4 or 5 described preparation methoies, it is characterized in that: described recirculation water is put forward 85-100 ℃ of control temperature, and the decocting in water time is 1-2.5 hour.
8. according to claim 4 or 5 described preparation methoies, it is characterized in that: the determining alcohol of described ethanol water is 45-80%.
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