CN102617124A - Active crystal ceramic production process - Google Patents
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Abstract
The invention discloses an active crystal ceramic production process, which includes the steps: calcining part of raw materials at a low temperature, preparing petuntse, preparing ceramic glaze, molding, biscuit firing, glazing, firing and the like to produce an active crystal ceramic product. The active crystal ceramic product is natural, nontoxic, harmless, odorless, energy-saving and environment-friendly, and capable of turning daily drinking water into microcluster water which can enter cell water channels of human body, and accordingly physiological and health efficacies on human body of water are improved.
Description
Technical field
The present invention relates to ceramic field, be specifically related to a kind of production technique of the brilliant porcelain of living.
Background technology
Traditional ceramic product only is the effect of playing decoration or storage, and earthenware porcelain receptacle does not play any beneficial effect to the object that it held, and has only the function that holds of container.
Summary of the invention
For promoting the function of ceramic product, the invention provides a kind of production technique of the brilliant porcelain of living.
The brilliant porcelain production technique of work of the present invention comprises following production stage:
One, part material low temperature calcination
1, get potassium felspar sand, albite, sodium aluminum fluoride, ovum phosphorus stone, spinel, mullite, trichroite and ground behind postcooling to the normal temperature in 5.5～6.5 hours respectively at 940～960 ℃ of calcinings, it is subsequent use to cross 90～120 mesh sieves;
2, get periclasite, calcite, lustrous and transparent spar, quartzite, medical stone, tourmalinite and ground behind postcooling to the normal temperature in 5.5～6.5 hours respectively at 840～860 ℃ of calcinings, it is subsequent use to cross 90～120 mesh sieves;
3, get kaolin, wilkinite, clay and ground behind postcooling to the normal temperature in 5.5～6.5 hours respectively at 590～610 ℃ of calcinings, it is subsequent use to cross 90～120 mesh sieves;
This step be the congruent melting property according to raw material fall into three classes temperature carry out base mud before impurity and purification handle; Carry out three kinds of low temperature calcinations by about 950 ℃, 850 ℃, 600 ℃ respectively, purpose is to improve the precision of shaping base substrate and facilitate the polycrystalline clinkering effect in the various crystal raw material melt stage in the calcination process.
Two, porcelain is clay is equipped with
Get kaolin 21～23%, clay 21～23%, quartzite 11～13%, albite 7～9%, bone meal 4～6%, mullite 4～4.5%, trichroite 3～3.5%, tourmalinite 3～3.5%, medical stone 3～3.5%, spinel 3～3.5%, borax 2.8～3.2%, REE 4.8～5.2%, wilkinite 5～7% by weight percentage and knock down ball mill as porcelain mud raw material; The water that adds porcelain mud raw material gross weight 80～100% ground 24～28 hours; Old more dirty 36 hours; Remove hydraulic pressure mud, pugging to pug water cut 19～25% then, it is subsequent use to process porcelain mud.
Three, enamel preparation
Get kaolin 2～2.5%, wilkinite 9～11%, potassium felspar sand 36～40%, calcite 3.5～4.5%, zinc oxide 10～12%, barium carbonate 2～3%, titanium trioxide 0.2～1.4%, quartzite 4.5～5.5%, sodium aluminum fluoride 2.5～3.5%, Quilonum Retard 2.5～3.5%, ovum phosphorus stone 2.5～3.5%, REE 4.8～5.2%, periclasite 2.8～3.2%, tourmalinite 4.8～5.2%, medical stone 4.8～5.2% by weight percentage and knock down ball mill as the enamel raw material; The water that adds enamel raw material gross weight 80～100% ground 24～28 hours; Old more dirty 36 hours; Remove hydraulic pressure mud, pugging to pug water cut 19～25% then, it is subsequent use to process enamel.
Above-mentioned porcelain mud and enamel prepare to have in the process and relate to and the identical component of low temperature calcination raw material, all adopt in the step 1 the subsequent use raw material of low temperature calcination.
Specifically can be that 1 weight part yttrium, 1 weight part lanthanum, 2 weight part praseodymiums and 1 weight part neodymium are mixed form above-mentioned REE.
Four, moulding biscuiting
Get subsequent use porcelain mud and carry out shaping and drying by the traditional ceramics working method, then with moulding product in 880～920 ℃ of biscuitings after 3.5～4.5 hours, it is subsequent use to naturally cool to normal temperature;
Five, glazing is burnt till
1, gets subsequent use enamel by the traditional ceramics working method and carry out glazing to the product after the biscuiting; Place kiln to burn till then; This moment, kiln was a reducing atmosphere, in 3～4 hours, was warming up to 850～900 ℃, was warming up to 1215～1225 ℃ in 5～6 hours again; Controlling kiln again is oxidizing atmosphere, keeps kiln temperature 2 hours (this is the crystal melt stage) in 1215～1225 ℃;
2, carry out quench and handle (being the whole brilliant crux step that forms of living), the adjustment kiln is a neutral atmosphere, in 3 minutes, kiln temperature is cooled to 1160～1170 ℃; This moment, the plunging of temperature impelled host crystal when quench, to form a kind of natural pulling force naturally, was attracted to other low-melting crystal around the host crystal, thereby form a kind of polynary bonded regular in order brilliant the spending of eternal live body that can discharge infrared energy of type arranged.
3, carry crystalline substance and brighten calcining; In 100～120 minutes, kiln temperature is warming up to 1280～1300 ℃ with 50～65 ℃ speed per hour; And keep constant temperature to come out of the stove after 25～35 minutes in 1280～1300 ℃ naturally cooling to normal temperature, process product of the present invention.
Said normal temperature is 20～35 ℃.
The product that the present invention processes has the brilliant characteristic of following work:
1, crystal shape is different with ordinary porcelain, and its crystal is a macrocrystal cover small-crystalline, and small-crystalline cover macrocrystal seems to seem active pure.
2, this crystal intrinsic heat electrically and piezoelectricity, it can make the vibration and cause moment of dipole to change the electromagnetic radiation that produces far infrared band and generate energy is also claimed the anion far infrared rays energy in the equilibrium theory of tide of its polarity ion.
3, detect through national far infrared inspection center, its far infrared rays wavelength is 11mn, and emittance reaches 92%, and the full emission of normal direction reaches 84.
The product that the present invention processes has the brilliant function of following work:
1, can make the macromolecular mass water of tap water become small-micelle water (title running water), existing " national drug and meta-bolites analysis and research " center " detect, and recording the spectrum peak width, to reach NMR be 57.43Hz.
2, through " national general Buddhist nun examines " center " and detects, potential of hydrogen that can the equilibrium water.
3, through " Beijing public health tap water institute " check, the free chlorine residual that can remove in anhydrating reaches 20.09%.
4, through " Beijing public health tap water institute " check, bacteriostasis rate reaches 75.76%.
The brilliant porcelain products of the work that the present invention processes are natural, nontoxic, tasteless, energy-conservation and environmental protection; It can become small-micelle water to daily tap water; Small-micelle water can get into the cellular water channel of human body, thereby improves water to Human Physiology effect and health efficacy.Science proves that ordering and structurized small-micelle water are absorbed by human body cell easily, can better participate in substance metabolism, energy metabolism, the information metabolism of human body, thereby reach the effect that promotes health and improve quality of life.
Description of drawings
Fig. 1 is the crystallographic microscope picture of product of the present invention.
Embodiment
Embodiment: the brilliant porcelain production technique of the work of present embodiment comprises following production stage:
One, part material low temperature calcination
1, get potassium felspar sand, albite, sodium aluminum fluoride, ovum phosphorus stone, spinel, mullite, trichroite and ground behind postcooling to the normal temperature in 6 hours respectively at 950 ℃ of calcinings, it is subsequent use to cross 120 mesh sieves;
2, get periclasite, calcite, lustrous and transparent spar, quartzite, medical stone, tourmalinite and ground behind postcooling to the normal temperature in 6 hours respectively at 850 ℃ of calcinings, it is subsequent use to cross 120 mesh sieves;
3, get kaolin, wilkinite, clay and ground behind postcooling to the normal temperature in 6 hours respectively at 600 ℃ of calcinings, it is subsequent use to cross 120 mesh sieves;
Two, porcelain is clay is equipped with
Get kaolin 22%, clay 22%, quartzite 12%, albite 8%, bone meal 5%, mullite 4.2%, trichroite 3.2%, tourmalinite 3.2%, medical stone 3.2%, spinel 3.2%, borax 3%, yttrium 1%, lanthanum 1%, praseodymium 2%, neodymium 1%, wilkinite 6% by weight percentage and knock down ball mill as porcelain mud raw material; The water that adds porcelain mud raw material gross weight 100% ground 24 hours; Old more dirty 36 hours; Remove hydraulic pressure mud, pugging to pug water cut 20% then, it is subsequent use to process porcelain mud.
Three, enamel preparation
Get kaolin 2.2%, wilkinite 10%, potassium felspar sand 38%, calcite 4%, zinc oxide 11%, barium carbonate 2.5%, titanium trioxide 0.3%, quartzite 5%, sodium aluminum fluoride 3%, Quilonum Retard 3%, ovum phosphorus stone 3%, yttrium 1%, lanthanum 1%, praseodymium 2%, neodymium 1%, periclasite 3%, tourmalinite 5%, medical stone 5% by weight percentage and knock down ball mill as the enamel raw material; The water that adds enamel raw material gross weight 80% ground 28 hours; Old more dirty 36 hours; Remove hydraulic pressure mud, pugging to pug water cut 24% then, it is subsequent use to process enamel.
Above-mentioned porcelain mud and enamel prepare to have in the process and relate to and the identical component of low temperature calcination raw material, all adopt in the step 1 the subsequent use raw material of low temperature calcination.
Four, moulding biscuiting
Get subsequent use porcelain mud and carry out shaping and drying by the traditional ceramics working method, then with moulding product in 900 ℃ of biscuitings after 4 hours, it is subsequent use to naturally cool to normal temperature;
Five, glazing is burnt till
1, get subsequent use enamel by the traditional ceramics working method and carry out glazing to the product after the biscuiting, place kiln to burn till then, this moment, kiln was a reducing atmosphere, in 4 hours, was warming up to 900 ℃, was warming up to 1220 ℃ in 5 hours again; Controlling kiln again is oxidizing atmosphere, keeps kiln temperature in 1220 ℃ 2 hours;
2, the adjustment kiln is a neutral atmosphere, in 3 minutes, kiln temperature is cooled to 1160 ℃;
3, in 120 minutes, kiln temperature is warming up to 1280 ℃, and keeps constant temperature to come out of the stove after 30 minutes in 1280 ℃ naturally cooling to normal temperature, process the product of embodiment with 60 ℃ speed per hour.
The present embodiment formed product is good, and the rate of burning till reaches 99%, at the microscopically crystal shape shown in accompanying drawing 1. through detecting; Its far infrared rays wavelength is 11mn; Emittance reaches 92%, and the full emission of normal direction reaches 84, and it is 57.43Hz that the spectrum peak width reaches NMR; The free chlorine residual that can remove in anhydrating reaches 20.09%, and bacteriostasis rate reaches 75.76%.
Comparative Examples 1: different with embodiment is, omits step 1 " part material low temperature calcination ", processes the product of Comparative Examples 1.The technology of Comparative Examples 1 makes raw material have the organism residue, and the carbide that produces can influence crystalline and flows in sintering process, can't form uniform crystal, and the formed product qualification rate is low.
Comparative Examples 2: different with embodiment is that step 1 " part material low temperature calcination " all adopts 800 ℃ of calcinings 6 hours, processes the product of Comparative Examples 2.The technology of Comparative Examples 2 produces the surface interruptions thing around making crystal, and the product crystal size of processing is inhomogeneous.
Comparative Examples 3: different with embodiment is; Step 5 " glazing is burnt till " is revised as gets subsequent use enamel by the traditional ceramics working method and carries out glazing for the product after the biscuiting; Place kiln to burn till then; This moment, kiln was a reducing atmosphere, in 4 hours, was warming up to 900 ℃, was warming up to 1220 ℃ in 5 hours again; Controlling kiln again is oxidizing atmosphere, keeps kiln temperature in 1220 ℃, directly to come out of the stove after 2.5 hours and naturally cools to normal temperature, processes the product of Comparative Examples 3.The technogenic influence crystalline of Comparative Examples 3 forms, and the crystal of the product of processing is irregular or half of crystal block, influences the radiation quantity of far infrared rays.
Comparative Examples 4: different with embodiment is that step 5 " glazing is burnt till " all adopts neutral atmosphere to burn till, and processes the product of Comparative Examples 4.The technology of Comparative Examples 4 effectively catalysis crystalline forms the invisible crystal of processing of product microscopically.
Claims (3)
1. the brilliant porcelain production technique of work is characterized in that, comprises following production stage:
(1), part material low temperature calcination
(1), get potassium felspar sand, albite, sodium aluminum fluoride, ovum phosphorus stone, spinel, mullite, trichroite and ground behind postcooling to the normal temperature in 5.5～6.5 hours respectively at 940～960 ℃ of calcinings, it is subsequent use to cross 90～120 mesh sieves;
(2), get periclasite, calcite, lustrous and transparent spar, quartzite, medical stone, tourmalinite and ground behind postcooling to the normal temperature in 5.5～6.5 hours respectively at 840～860 ℃ of calcinings, it is subsequent use to cross 90～120 mesh sieves;
(3), get kaolin, wilkinite, clay and ground behind postcooling to the normal temperature in 5.5～6.5 hours respectively at 590～610 ℃ of calcinings, it is subsequent use to cross 90～120 mesh sieves;
(2), porcelain is clay is equipped with
Get kaolin 21～23%, clay 21～23%, quartzite 11～13%, albite 7～9%, bone meal 4～6%, mullite 4～4.5%, trichroite 3～3.5%, tourmalinite 3～3.5%, medical stone 3～3.5%, spinel 3～3.5%, borax 2.8～3.2%, REE 4.8～5.2%, wilkinite 5～7% by weight percentage and knock down ball mill as porcelain mud raw material; The water that adds porcelain mud raw material gross weight 80～100% ground 24～28 hours; Old more dirty 36 hours; Remove hydraulic pressure mud, pugging to pug water cut 19～25% then, it is subsequent use to process porcelain mud;
(3), enamel preparation
Get kaolin 2～2.5%, wilkinite 9～11%, potassium felspar sand 36～40%, calcite 3.5～4.5%, zinc oxide 10～12%, barium carbonate 2～3%, titanium trioxide 0.2～1.4%, quartzite 4.5～5.5%, sodium aluminum fluoride 2.5～3.5%, Quilonum Retard 2.5～3.5%, ovum phosphorus stone 2.5～3.5%, REE 4.8～5.2%, periclasite 2.8～3.2%, tourmalinite 4.8～5.2%, medical stone 4.8～5.2% by weight percentage and knock down ball mill as the enamel raw material; The water that adds enamel raw material gross weight 80～100% ground 24～28 hours; Old more dirty 36 hours; Remove hydraulic pressure mud, pugging to pug water cut 19～25% then, it is subsequent use to process enamel;
Above-mentioned porcelain mud and enamel prepare to have in the process and relate to and the identical component of low temperature calcination raw material, all adopt in the step () the subsequent use raw material of low temperature calcination;
(4), moulding biscuiting
Get subsequent use porcelain mud and carry out shaping and drying by the traditional ceramics working method, then with moulding product in 880～920 ℃ of biscuitings after 3.5～4.5 hours, it is subsequent use to naturally cool to normal temperature;
(5), glazing is burnt till
(1), gets subsequent use enamel by the traditional ceramics working method and carry out glazing to the product after the biscuiting; Place kiln to burn till then; This moment, kiln was a reducing atmosphere, in 3～4 hours, was warming up to 850～900 ℃, was warming up to 1215～1225 ℃ in 5～6 hours again; Controlling kiln again is oxidizing atmosphere, keeps kiln temperature in 1215～1225 ℃ 2 hours;
(2), the adjustment kiln is neutral atmosphere, in 3 minutes, kiln temperature is cooled to 1160～1170 ℃;
(3), in 100～120 minutes, kiln temperature is warming up to 1280～1300 ℃, and keep constant temperature to come out of the stove after 25～35 minutes in 1280～1300 ℃ naturally cooling to normal temperature, process product of the present invention with 50～65 ℃ speed per hour.
2. according to the said production technique of claim 1, it is characterized in that to be that 1 weight part yttrium, 1 weight part lanthanum, 2 weight part praseodymiums and 1 weight part neodymium are mixed form said REE.
3. according to claim 1 or 2 said production technique, it is characterized in that said normal temperature is 20～35 ℃.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
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| CN2012100830253A CN102617124A (en) | 2012-03-27 | 2012-03-27 | Active crystal ceramic production process |
| CN2013100986321A CN103172350A (en) | 2012-03-27 | 2013-03-25 | Production technology of live crystal porcelain |
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| CN2012100830253A CN102617124A (en) | 2012-03-27 | 2012-03-27 | Active crystal ceramic production process |
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| CN2013100986321A Pending CN103172350A (en) | 2012-03-27 | 2013-03-25 | Production technology of live crystal porcelain |
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Cited By (12)
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| CN102795835A (en) * | 2011-05-23 | 2012-11-28 | 凌邦方 | Specialized porcelain clay for Mao porcelain/underglazed five-color porcelain, and preparation method thereof |
| CN103172350A (en) * | 2012-03-27 | 2013-06-26 | 林俊生 | Production technology of live crystal porcelain |
| CN103396164A (en) * | 2013-07-25 | 2013-11-20 | 郑州大学 | High-temperature stereoscopic glaze and preparation method thereof |
| CN105016708A (en) * | 2015-08-11 | 2015-11-04 | 林俊生 | Functional live crystal porcelain and preparation method and application thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102617124A (en) * | 2012-03-27 | 2012-08-01 | 林俊生 | Active crystal ceramic production process |
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2012
- 2012-03-27 CN CN2012100830253A patent/CN102617124A/en active Pending
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2013
- 2013-03-25 CN CN2013100986321A patent/CN103172350A/en active Pending
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| CN102795835A (en) * | 2011-05-23 | 2012-11-28 | 凌邦方 | Specialized porcelain clay for Mao porcelain/underglazed five-color porcelain, and preparation method thereof |
| CN102795835B (en) * | 2011-05-23 | 2015-09-09 | 凌邦方 | Special porcelain mud of a kind of hair porcelain/five color painting in the glaze porcelain and preparation method thereof |
| CN103172350A (en) * | 2012-03-27 | 2013-06-26 | 林俊生 | Production technology of live crystal porcelain |
| CN103396164A (en) * | 2013-07-25 | 2013-11-20 | 郑州大学 | High-temperature stereoscopic glaze and preparation method thereof |
| CN103396164B (en) * | 2013-07-25 | 2014-10-08 | 郑州大学 | High-temperature stereoscopic glaze and preparation method thereof |
| CN105016708A (en) * | 2015-08-11 | 2015-11-04 | 林俊生 | Functional live crystal porcelain and preparation method and application thereof |
| CN105948505A (en) * | 2016-06-23 | 2016-09-21 | 叶国强 | Preparation method for lead-zinc-silver tailing low-temperature-sintered encaustic brick glaze |
| CN106116153A (en) * | 2016-06-30 | 2016-11-16 | 安徽省德邦瓷业有限公司 | A kind of ceramic wine bottle glaze and preparation method thereof |
| CN106348738A (en) * | 2016-08-31 | 2017-01-25 | 揭阳市揭东恒成陶瓷实业有限公司 | Health-maintaining ceramics and preparing method thereof |
| CN107244939A (en) * | 2017-04-20 | 2017-10-13 | 林俊生 | A kind of porous closure material and preparation method thereof |
| CN107858603A (en) * | 2017-09-26 | 2018-03-30 | 陈薇羽 | DNI sheet of energy |
| CN108727065A (en) * | 2018-04-23 | 2018-11-02 | 卢群海 | A kind of preparation method of blooming period prolonging ceramic glaze |
| CN108793960A (en) * | 2018-08-23 | 2018-11-13 | 广西亚欧瓷业有限公司 | A kind of preparation method of wear-resistant ceramic brick capable of releasing negative ion |
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Application publication date: 20120801 |