CN102605675A - Water transfer printing paper and preparation method thereof - Google Patents
Water transfer printing paper and preparation method thereof Download PDFInfo
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- CN102605675A CN102605675A CN2012100447410A CN201210044741A CN102605675A CN 102605675 A CN102605675 A CN 102605675A CN 2012100447410 A CN2012100447410 A CN 2012100447410A CN 201210044741 A CN201210044741 A CN 201210044741A CN 102605675 A CN102605675 A CN 102605675A
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Abstract
The invention discloses water transfer printing paper and a preparation method thereof. The water transfer printing paper comprises a hydrosol layer, a film-forming adhesive layer, carrier backing paper and an opposite colloid layer sequentially from top to bottom, wherein the opposite colloid layer is a starch layer; the film-forming adhesive layer comprises an activity colloid layer and a white colloid layer sequentially from top to bottom; the activity colloid layer is obtained by coating and drying a mixed aqueous solution of a brightening agent and the starch; the mass fractions of the brightening agent and the starch are respectively 0.5%-1% and 35%-45%; and the white colloid layer is a starch layer. The hydrosol layer is obtained by coating and drying a mixed aqueous solution of kaolin, a butylbenzene emulsion, a dispersing agent and polyvinyl alcohol; and the mass fractions of the kaolin, the butylbenzene emulsion, the dispersing agent and the polyvinyl alcohol are respectively 40%-50%, 10%-15%, 1%-3% and 3%-5%. The water transfer printing paper disclosed by the invention has the advantages of a smooth and flat surface, rational thickness of coated glue layers, higher de-molding speed, uniform water absorbability, and uniform and smooth glue surface.
Description
Technical field
The present invention relates to a kind of printing, specifically is a kind of water-transfer printing paper and preparation method thereof.
Background technology
Water-transfer printing paper is also referred to as the membranelle base stock, and it is as the transfer printing thing of intermediate carrier in the water transfer printing technique.Water-transfer printing paper is a kind of special macromolecular material, and general mainly form by three layers, bottom is the carrier ground paper layer, but the middle level is the film forming glue adhesion coating, and the upper strata is a water-soluble adhesive layer.
During use, be printed on needed multicolour pattern on the transfer paper with ink-jet printer spraying dyestuff usually, water-soluble adhesive layer dissolves automatically after meeting water, and colorant is separated with transfer paper, has realized the transfer of picture and text.
Generally there is following defective in present existing water-transfer printing paper:
(1) surface is often smooth inadequately bright and clean, makes that printing patterned layer above that is clear inadequately smooth, also influences the degree of accuracy of transfer printing mantle, and effects such as transfer printing precision and aesthetics are had negative effect;
(2) coating thickness of water-soluble adhesive layer is unreasonable, causes the pattern after the printing to lack high gloss and third dimension;
(3) dissolution velocity of water-soluble adhesive layer in water is slow excessively, causes demoulding to have some setbacks, and influences the transfer printing effect of color pattern;
(4) water imbibition at each position of water-transfer printing paper is inhomogeneous, influences the even smoothness and the demoulding effect of glue face, causes the transfer printing effect undesirable.
Summary of the invention
Technical problem to be solved by this invention is the defective that overcomes prior art, and a kind of water-transfer printing paper and preparation method thereof is provided, and any surface finish of said water-transfer printing paper is smooth, and the thickness of coating glue-line is reasonable, the demoulding rapid speed, and water imbibition is even, and the glue face is evenly level and smooth.
For solving the problems of the technologies described above, water-transfer printing paper of the present invention, but it comprises water-soluble adhesive layer film forming glue adhesion coating, carrier base stock and reverse side colloid layer from top to bottom successively.
Said reverse side colloid layer is located at the below of carrier base stock, and said reverse side colloid layer is a stratum granulosum.
But said film forming glue adhesion coating comprises activity colloid layer and white colloid layer from top to bottom successively; The mixed aqueous solution coating back oven dry that said activity colloid layer is brightening agent and starch obtains; The mass fraction of said brightening agent and starch is respectively 0.5%-1%, 35%-45%, and said white colloid layer is a stratum granulosum.
Said water-soluble adhesive layer is that the mixed aqueous solution coating back oven dry of kaolin, styrene-butadiene emulsion, diffusant and polyvinyl alcohol obtains, and the mass fraction of said kaolin, styrene-butadiene emulsion, diffusant and polyvinyl alcohol is respectively 40%-50%, 10%-15%, 1%-3%, 3%-5%.
As preferably, said reverse side colloid layer is a corn synthetic starch layer.
As preferably, said brightening agent is sodium alginate or VBL.
As preferably, the starch of said activity colloid layer is tapioca.
As preferably, said white colloid layer is the para arrowroot bisque.
As preferably, said diffusant is non-ionic surface active agent, anion surfactant or the two mixture.
The preparation method of water-transfer printing paper of the present invention, it adopts following steps---
(1) preparation of coating fluid:
The water-soluble adhesive layer coating fluid: the mixed aqueous solution of preparation kaolin, styrene-butadiene emulsion, diffusant and polyvinyl alcohol, the mass fraction of said kaolin, styrene-butadiene emulsion, diffusant and polyvinyl alcohol is respectively 40%-50%, 10%-15%, 1%-3%, 3%-5%;
The preparation of activity colloid layer coating fluid: the mixed aqueous solution of preparation brightening agent and starch, the mass fraction of said brightening agent and starch is respectively 0.5%-1%, 35%-45%;
The preparation of white colloid layer coating fluid: preparation starch quality mark is the aqueous solution of 35%-45%;
The preparation of reverse side colloid layer coating fluid: preparation starch quality mark is the aqueous solution of 25%-40%;
(2) white colloid layer coating fluid in the coating of the front of carrier base stock, coating thickness is 10g/m
2-15g/m
2, oven dry, bake out temperature is 72 ℃-87 ℃, wind speed 1.2m/s-1.4m/s after the cooling cylinder pressure pastes the cylinder cooling, carries out press polish with felt wrapped roll and handles;
(3) coating activity colloid layer coating fluid on white colloid layer, coating thickness is 3g/m
2-5g/m
2, oven dry, bake out temperature is 90 ℃-95 ℃, wind speed 1.2m/s-1.4m/s;
(4) at the back side of carrier base stock coating reverse side colloid layer coating fluid, coating thickness is 3g/m
2-5g/m
2, oven dry, bake out temperature is 80 ℃-85 ℃, wind speed 1.2m/s-1.4m/s;
(5) coating water-soluble adhesive layer coating fluid on the activity colloid layer, coating thickness is 5g/m
2-10g/m
2, oven dry, bake out temperature is 80 ℃-85 ℃, wind speed 1.0m/s-1.1m/s after the cooling cylinder pressure pastes the cylinder cooling, carries out polishing with polissoir, by the rolling of rolling equipment, can obtain water-transfer printing paper of the present invention.
Preferred as said method, said brightening agent is sodium alginate or VBL.
Preferred as said method, said diffusant is non-ionic surface active agent, anion surfactant or the two mixture.
Preferred as said method, said activity colloid layer coating fluid is tapioca with the starch of white colloid layer coating fluid, and the starch of said reverse side colloid layer coating fluid is the corn synthetic starch.
Water-transfer printing paper of the present invention, each layer acts on as follows:
White colloid layer makes carrier base stock smooth surface, reduces the absorption of base stock to other colloids simultaneously, and the surface smoothness of further having improved water-transfer printing paper is handled in the press polish during preparation;
The activity colloid layer is met water and is dissolved fast; Make water-soluble adhesive layer rapidly and carrier separating, and can make hydrone reside in the paper surface lastingly, the lubricity of paper is kept lastingly; The speed of its separation is demoulding speed just, and the activity colloid layer among the present invention has good separating rate;
The reverse side colloid layer makes the water-transfer printing paper water absorbing capacity more even, has improved the demoulding speed of water-transfer printing paper, has improved the flatness of water-transfer printing paper simultaneously, reduces paper and curls;
Water-soluble adhesive layer is the carrying person of printing-ink, and it meets water-soluble, and the water-soluble adhesive layer dissolution velocity among the present invention is controlled at the optimum range about 30s;
Polishing during preparation has further improved the surface smoothness of water-transfer printing paper, has improved the degree of accuracy of transfer printing mantle, makes that printing precision is higher, the transfer printing product is more attractive in appearance.
Water-transfer printing paper of the present invention compared with prior art, has the following advantages:
(1) any surface finish is smooth, makes printed patterns smooth clear, and the degree of accuracy of transfer printing mantle is high, has improved the aesthetics of transfer printing precision and product;
(2) coating thickness of each glue-line is reasonable, and the pattern after the printing has high gloss and third dimension;
(3) the water-soluble adhesive layer dissolution velocity is controlled at the optimum range about 30s, and demoulding is smooth and easy, has improved the transfer printing effect of color pattern;
(4) the reverse side colloid layer makes the water-transfer printing paper water absorbing capacity more even, has improved the demoulding speed of water-transfer printing paper, has improved the flatness of water-transfer printing paper simultaneously, reduces paper and curls, and has further improved the transfer printing effect.
The specific embodiment
Below in conjunction with embodiment the present invention is done further detailed explanation; But the present invention is not limited to following examples; The technical staff of same area can propose other embodiment in technical scheme framework of the present invention, but these embodiment include in protection scope of the present invention.
Embodiment 1
(1) preparation of coating fluid:
The water-soluble adhesive layer coating fluid: the mixed aqueous solution of preparation kaolin, styrene-butadiene emulsion, diffusant and polyvinyl alcohol, wherein the mass fraction of kaolin, styrene-butadiene emulsion, APES and polyvinyl alcohol is respectively 40%, 10%, 1%, 3%;
The preparation of activity colloid layer coating fluid: the mixed aqueous solution of preparation brightening agent sodium alginate and tapioca, the mass fraction of said brightening agent sodium alginate and tapioca is respectively 0.6%, 42%;
The preparation of white colloid layer coating fluid: preparation tapioca mass fraction is 40% the aqueous solution;
The preparation of reverse side colloid layer coating fluid: preparation corn synthetic starch mass fraction is 30% the aqueous solution;
(2) white colloid layer coating fluid in the coating of the front of carrier base stock, coating thickness is 10g/m
2, oven dry, bake out temperature is 72 ℃, wind speed 1.2m/s after the cooling cylinder pressure pastes the cylinder cooling, carries out press polish with felt wrapped roll and handles;
(3) coating activity colloid layer coating fluid on white colloid layer, coating thickness is 3g/m
2, oven dry, bake out temperature is 90 ℃, wind speed 1.2m/s;
(4) at the back side of carrier base stock coating reverse side colloid layer coating fluid, coating thickness is 3g/m
2, oven dry, bake out temperature is 80 ℃, wind speed 1.2m/s;
(5) coating water-soluble adhesive layer coating fluid on the activity colloid layer, coating thickness is 5g/m
2, oven dry, bake out temperature is 80 ℃, wind speed 1.0m/s after the cooling cylinder pressure pastes the cylinder cooling, carries out polishing with polissoir, by the rolling of rolling equipment, can obtain water-transfer printing paper of the present invention.
Embodiment 2
(1) preparation of coating fluid:
The water-soluble adhesive layer coating fluid: the mixed aqueous solution of preparation kaolin, styrene-butadiene emulsion, diffusant and polyvinyl alcohol, wherein the mass fraction of kaolin, styrene-butadiene emulsion, di-2-ethylhexylphosphine oxide bitter edible plant sodium sulfonate and polyvinyl alcohol is respectively 43%, 15%, 1%, 3%;
The preparation of activity colloid layer coating fluid: the mixed aqueous solution of preparation brightening agent VBL and tapioca, the mass fraction of said brightening agent VBL and tapioca is respectively 0.5%, 35%;
The preparation of white colloid layer coating fluid: preparation tapioca mass fraction is 35% the aqueous solution;
The preparation of reverse side colloid layer coating fluid: preparation corn synthetic starch mass fraction is 40% the aqueous solution;
(2) white colloid layer coating fluid in the coating of the front of carrier base stock, coating thickness is 12g/m
2, oven dry, bake out temperature is 82 ℃, wind speed 1.2m/s after the cooling cylinder pressure pastes the cylinder cooling, carries out press polish with felt wrapped roll and handles;
(3) coating activity colloid layer coating fluid on white colloid layer, coating thickness is 3g/m
2, oven dry, bake out temperature is 90 ℃, wind speed 1.2m/s;
(4) at the back side of carrier base stock coating reverse side colloid layer coating fluid, coating thickness is 3.2g/m
2, bake out temperature is 80 ℃, wind speed 1.2m/s;
(5) coating water-soluble adhesive layer coating fluid on the activity colloid layer, coating thickness is 5.2g/m
2, oven dry, bake out temperature is 80 ℃, wind speed 1.0m/s after the cooling cylinder pressure pastes the cylinder cooling, carries out polishing with polissoir, by the rolling of rolling equipment, can obtain water-transfer printing paper of the present invention.
Embodiment 3
(1) preparation of coating fluid:
The water-soluble adhesive layer coating fluid: the mixed aqueous solution of preparation kaolin, styrene-butadiene emulsion, diffusant and polyvinyl alcohol, wherein the mass fraction of kaolin, styrene-butadiene emulsion, di-2-ethylhexylphosphine oxide bitter edible plant sodium sulfonate and polyvinyl alcohol is respectively 45%, 15%, 1.2%, 3%;
The preparation of activity colloid layer coating fluid: the mixed aqueous solution of preparation brightening agent VBL and tapioca, the mass fraction of said brightening agent VBL and tapioca is respectively 0.5%, 40%;
The preparation of white colloid layer coating fluid: preparation tapioca mass fraction is 45% the aqueous solution;
The preparation of reverse side colloid layer coating fluid: preparation corn synthetic starch mass fraction is 35% the aqueous solution;
(2) white colloid layer coating fluid in the coating of the front of carrier base stock, coating thickness is 14g/m
2, oven dry, bake out temperature is 80 ℃, wind speed 1.3m/s after the cooling cylinder pressure pastes the cylinder cooling, carries out press polish with felt wrapped roll and handles;
(3) coating activity colloid layer coating fluid on white colloid layer, coating thickness is 3.5g/m
2, oven dry, bake out temperature is 95 ℃, wind speed 1.4m/s;
(4) at the back side of carrier base stock coating reverse side colloid layer coating fluid, coating thickness is 4.5g/m
2, bake out temperature is 85 ℃, wind speed 1.3m/s;
(5) coating water-soluble adhesive layer coating fluid on the activity colloid layer, coating thickness is 7.5g/m
2, oven dry, bake out temperature is 85 ℃, wind speed 1.1m/s after the cooling cylinder pressure pastes the cylinder cooling, carries out polishing with polissoir, by the rolling of rolling equipment, can obtain water-transfer printing paper of the present invention.
Respectively the water-transfer printing paper of embodiment 1-embodiment 3 is tried out:
Be printed on needed multicolour pattern on the transfer paper with ink-jet printer spraying dyestuff, carry out transfer printing then; During transfer printing, water-transfer printing paper is immersed in the water, the live body colloid layer dissolves fast, makes water-soluble adhesive layer rapidly and carrier separating; Water-soluble adhesive layer also begins automatic dissolving, and dissolution velocity is controlled at the optimum range about 30s, and colorant is separated with transfer paper; Stock is inserted in the water, press close to be the printed patterns of free state gradually along its curved surface profile, owing to the intrinsic adhesive attraction of printing-ink and stock surface produces adhesive force, pattern is slowly transferred to the stock surface, has realized the transfer of picture and text; Then stock is taken out and dry solidification, pattern stays on stock, and pattern effect is clear, true to nature.
Claims (10)
1. water-transfer printing paper, but it comprises water-soluble adhesive layer film forming glue adhesion coating and carrier base stock from top to bottom successively, it is characterized in that: and it also comprises the reverse side colloid layer, and said reverse side colloid layer is located at the below of carrier base stock, and said reverse side colloid layer is a stratum granulosum; But said film forming glue adhesion coating comprises activity colloid layer and white colloid layer from top to bottom successively; The mixed aqueous solution coating back oven dry that said activity colloid layer is brightening agent and starch obtains; The mass fraction of said brightening agent and starch is respectively 0.5%-1%, 35%-45%, and said white colloid layer is a stratum granulosum; Said water-soluble adhesive layer is that the mixed aqueous solution coating back oven dry of kaolin, styrene-butadiene emulsion, diffusant and polyvinyl alcohol obtains, and the mass fraction of said kaolin, styrene-butadiene emulsion, diffusant and polyvinyl alcohol is respectively 40%-50%, 10%-15%, 1%-3%, 3%-5%.
2. water-transfer printing paper according to claim 1 is characterized in that: said reverse side colloid layer is a corn synthetic starch layer.
3. water-transfer printing paper according to claim 1 is characterized in that: said brightening agent is sodium alginate or VBL.
4. water-transfer printing paper according to claim 1 is characterized in that: the starch of said activity colloid layer is tapioca.
5. water-transfer printing paper according to claim 1 is characterized in that: said white colloid layer is the para arrowroot bisque.
6. water-transfer printing paper according to claim 1 is characterized in that: said diffusant is non-ionic surface active agent, anion surfactant or the two mixture.
7. the preparation method of a water-transfer printing paper according to claim 1, it is characterized in that: it adopts following steps---
(1) preparation of coating fluid:
The water-soluble adhesive layer coating fluid: the mixed aqueous solution of preparation kaolin, styrene-butadiene emulsion, diffusant and polyvinyl alcohol, the mass fraction of said kaolin, styrene-butadiene emulsion, diffusant and polyvinyl alcohol is respectively 40%-50%, 10%-15%, 1%-3%, 3%-5%;
The preparation of activity colloid layer coating fluid: the mixed aqueous solution of preparation brightening agent and starch, the mass fraction of said brightening agent and starch is respectively 0.5%-1%, 35%-45%;
The preparation of white colloid layer coating fluid: preparation starch quality mark is the aqueous solution of 35%-45%;
The preparation of reverse side colloid layer coating fluid: preparation starch quality mark is the aqueous solution of 25%-40%;
(2) white colloid layer coating fluid in the coating of the front of carrier base stock, coating thickness is 10g/m
2-15g/m
2, oven dry, bake out temperature is 72 ℃-87 ℃, wind speed 1.2m/s-1.4m/s after the cooling cylinder pressure pastes the cylinder cooling, carries out press polish with felt wrapped roll and handles;
(3) coating activity colloid layer coating fluid on white colloid layer, coating thickness is 3g/m
2-5g/m
2, oven dry, bake out temperature is 90 ℃-95 ℃, wind speed 1.2m/s-1.4m/s;
(4) at the back side of carrier base stock coating reverse side colloid layer coating fluid, coating thickness is 3g/m
2-5g/m
2, oven dry, bake out temperature is 80 ℃-85 ℃, wind speed 1.2m/s-1.4m/s;
(5) coating water-soluble adhesive layer coating fluid on the activity colloid layer, coating thickness is 5g/m
2-10g/m
2, oven dry, bake out temperature is 80 ℃-85 ℃, wind speed 1.0m/s-1.1m/s after the cooling cylinder pressure pastes the cylinder cooling, carries out polishing with polissoir, by the rolling of rolling equipment, can obtain water-transfer printing paper of the present invention.
8. the preparation method of water-transfer printing paper according to claim 7, it is characterized in that: said brightening agent is sodium alginate or VBL.
9. the preparation method of water-transfer printing paper according to claim 7, it is characterized in that: said diffusant is non-ionic surface active agent, anion surfactant or the two mixture.
10. the preparation method of water-transfer printing paper according to claim 7 is characterized in that: said activity colloid layer coating fluid is tapioca with the starch of white colloid layer coating fluid, and the starch of said reverse side colloid layer coating fluid is the corn synthetic starch.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012100447410A CN102605675A (en) | 2012-02-24 | 2012-02-24 | Water transfer printing paper and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012100447410A CN102605675A (en) | 2012-02-24 | 2012-02-24 | Water transfer printing paper and preparation method thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103726396A (en) * | 2013-12-18 | 2014-04-16 | 安徽华邦特种纸业有限公司 | Production method of high stiffness heat transfer raw paper |
| CN104652171A (en) * | 2013-11-25 | 2015-05-27 | 中国制浆造纸研究院 | Manufacturing method of quick-dry heat sublimation transfer paper with high transfer rate |
| CN105082856A (en) * | 2015-07-22 | 2015-11-25 | 佛山荷韵特种材料有限公司 | Method for manufacturing water transfer printing paper capable of being directly transferred |
| CN105500983A (en) * | 2016-01-11 | 2016-04-20 | 刘文华 | Polyurethane foam decorating plate and manufacturing technology thereof |
| CN105544305A (en) * | 2015-12-10 | 2016-05-04 | 深圳市万极科技股份有限公司 | Full-degradable water transfer printing paper and production process of surface coating film thereof |
| CN105568755A (en) * | 2015-12-10 | 2016-05-11 | 惠州市万极新材料科技有限公司 | Fully-degraded water-transfer paper and production process for back coating film thereof |
| CN108274914A (en) * | 2018-02-09 | 2018-07-13 | 佛山荷韵特种材料有限公司 | Environment-friendly type, which is pasted, shifts straight calico paper complex printing paper membrane and preparation method thereof |
| CN114481700A (en) * | 2022-01-25 | 2022-05-13 | 佛山荷韵特种材料有限公司 | Water transfer printing base paper and preparation method thereof |
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- 2012-02-24 CN CN2012100447410A patent/CN102605675A/en active Pending
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104652171A (en) * | 2013-11-25 | 2015-05-27 | 中国制浆造纸研究院 | Manufacturing method of quick-dry heat sublimation transfer paper with high transfer rate |
| CN103726396A (en) * | 2013-12-18 | 2014-04-16 | 安徽华邦特种纸业有限公司 | Production method of high stiffness heat transfer raw paper |
| CN103726396B (en) * | 2013-12-18 | 2016-08-17 | 安徽华邦特种材料有限公司 | A kind of production method of high-stiffness thermal transfer body paper |
| CN105082856A (en) * | 2015-07-22 | 2015-11-25 | 佛山荷韵特种材料有限公司 | Method for manufacturing water transfer printing paper capable of being directly transferred |
| CN105544305A (en) * | 2015-12-10 | 2016-05-04 | 深圳市万极科技股份有限公司 | Full-degradable water transfer printing paper and production process of surface coating film thereof |
| CN105568755A (en) * | 2015-12-10 | 2016-05-11 | 惠州市万极新材料科技有限公司 | Fully-degraded water-transfer paper and production process for back coating film thereof |
| CN105500983A (en) * | 2016-01-11 | 2016-04-20 | 刘文华 | Polyurethane foam decorating plate and manufacturing technology thereof |
| CN108274914A (en) * | 2018-02-09 | 2018-07-13 | 佛山荷韵特种材料有限公司 | Environment-friendly type, which is pasted, shifts straight calico paper complex printing paper membrane and preparation method thereof |
| WO2019154251A1 (en) * | 2018-02-09 | 2019-08-15 | 佛山荷韵特种材料有限公司 | Composite printing paper film for environmentally friendly pasting transfer direct-printing patterned paper and preparation method therefor |
| CN114481700A (en) * | 2022-01-25 | 2022-05-13 | 佛山荷韵特种材料有限公司 | Water transfer printing base paper and preparation method thereof |
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Application publication date: 20120725 |