CN102599614A - Mould-proof antioxidant capable of increasing pig feed quality - Google Patents

Mould-proof antioxidant capable of increasing pig feed quality Download PDF

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Publication number
CN102599614A
CN102599614A CN2012101051285A CN201210105128A CN102599614A CN 102599614 A CN102599614 A CN 102599614A CN 2012101051285 A CN2012101051285 A CN 2012101051285A CN 201210105128 A CN201210105128 A CN 201210105128A CN 102599614 A CN102599614 A CN 102599614A
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parts
carrier
origanum oil
sepiolite
feed
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CN102599614B (en
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黄春玲
尹荣华
卢普银
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Yulin twin Feed Co.,Ltd.
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ZHANGZHOU TWINS FEED CO Ltd
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Abstract

The invention provides a mould-proof antioxidant capable of increasing pig feed quality. A natural product, namely, soluble chitin, extracted from shrimp and crab shells is taken as a main component of a mould-proof agent and is combined with a composite antioxidant to exert functions, and the mould-proof antioxidant has the characteristics of long mould-proof period, good anti-oxidation effect, no toxic residue, safety and reliability, and can be used for replenishing nutritional ingredients required by the growth of live pigs and increasing the pig feed quality. After eating the feed in which the mould-proof antioxidant is added, the live pigs are increased in feed intake and obviously accelerated in body weight increase, and the slaughtering time is shortened.

Description

A kind of mold-proof oxidation-resistant agent that improves the pig feed quality
Technical field
The present invention relates to the agent of a kind of pig's feed mold-proof oxidation-resistant, relate in particular to a kind of mold-proof oxidation-resistant agent that improves the pig feed quality.
Background technology
Feed mold is the ubiquitous problem in the whole world, it be since in the feed a large amount of breeding of mould cause.Go mouldy easily at high temperature wet season feed, the feed that goes mouldy not only nutritive value reduces, and palatability is affected, and the toxin that produces of bacterium or mould such as aflatoxin can be poisoned live pig and residue in and influenced human health in the pork.Nutriments such as the lipid in the feed constantly carry out oxidation reaction in storage process, cause the photonasty of feed to descend, and nutritive value reduces; Storage life shortens and palatability descends; The feed that can cause that oxidation is serious becomes sour, and protein destroys and pigment oxidation, but also has certain toxicity; Live pig is caused harm to a certain degree, bring bigger loss to the raiser.
Mostly mold-proof oxidation-resistant agent in the market is the simple composite of mould inhibitor and anti-oxidant; The mold-proof oxidation-resistant effect of playing that can only be simple; And be that main mold-proof oxidation-resistant agent also is easy to generate the toxic residue problem with the chemical composition; Exist additivity to poison like benzoic acid, some countries and regions bans use of; Even some is because special smell can cause the repulsion of live pig, reduces the live pig feed intake, influences marketing time.
Summary of the invention
The invention reside in provides a kind of mold-proof oxidation-resistant agent that improves the pig feed quality; Adopt extract soluble chitin and anti-oxidant synergy in the shrimp and crab shells; Not only has good mold-proof oxidation-resistant effect; And can replenish the required nutriment of live pig growth, and accelerate the live pig weightening finish, improve culture efficiency.
The present invention realizes through following technical scheme:
Mould inhibitor: soluble chitin 50-150 part, KI 10-30 part, Potassiumiodate 10-30 part, calcium propionate 10-50 part, origanum oil 1-5 part;
Anti-oxidant: 5-20 part, dibutyl hydroxy toluene 5-20 part, butylated hydroxy anisole 5-20 part, citric acid 1-5 part, inositol 1-5 part;
Totally 1000 parts in mould inhibitor, anti-oxidant and carrier, the residue umber is a carrier;
=1: (1-3): (1-3), the three is beforehand with pulverization process respectively, and making its fineness is 0.1-0.5mm;
Wherein origanum oil obtains through following method:
With putting into supercritical extraction reactor after the pulverizing of 50g wild marjoram herb; Add 200mL75% ethanol as entrainer, the adjusting extracting pressure is 20MPa, and extraction temperature is 55 ℃; The entrainer flow is 0.02mL/min; Carbon dioxide flow is 1.2L/min, extracts and obtains the oily liquids that pale brown look has special aromatic odor after 2 hours, is origanum oil.
50-80 ℃ following stirring and adsorbing 3-5 hour, standing adsorption 20-30 hour again, the sepiolite that will be adsorbed with origanum oil then mixed in proportion with other raw materials and carrier, sieving promptly gets;
Add this additive of 0.5-1.5kg in the feed per ton.
Adopt the natural products soluble chitin that from shrimp and crab shells, extracts as the mould inhibitor main component among the present invention; With the composite antioxidant synergy, it is long to have a mildew-resistant phase, and antioxidant effect is good; Avirulence is residual; Safe and reliable characteristics also can be replenished the required nutriment of live pig growth, improve the pig feed quality.Live pig eats has added feed of the present invention, and feed intake increases, and body weight gain is obviously accelerated, and has shortened the time of delivering for sale.
The specific embodiment:
Embodiment 1:
Mould inhibitor: 100 parts of soluble chitins, 20 parts of KIs, 20 parts of Potassiumiodates, 30 parts of calcium propionates, 3 parts of origanum oils;
Anti-oxidant: 15 parts of n-propyl gallates, 15 parts of dibutyl hydroxy toluenes, 10 parts of butylated hydroxy anisoles, 3 parts of citric acids, 3 parts of inositols;
Totally 1000 parts in mould inhibitor, anti-oxidant and carrier, the residue umber is a carrier;
Each weight ratio of constituents is a sepiolite in the carrier: peanut hull meal: defatted rice bran=1:2:2, three are beforehand with pulverization process respectively, and making its fineness is 0.2mm;
Wherein origanum oil obtains through following method:
With putting into supercritical extraction reactor after the pulverizing of 50g wild marjoram herb; Add 200mL75% ethanol as entrainer, the adjusting extracting pressure is 20MPa, and extraction temperature is 55 ℃; The entrainer flow is 0.02mL/min; Carbon dioxide flow is 1.2L/min, extracts and obtains the oily liquids that pale brown look has special aromatic odor after 2 hours, is origanum oil.
Origanum oil is sprayed at uniformly in the sepiolite of pulverization process, and 65 ℃ of following stirring and adsorbing 4 hours, standing adsorption was 25 hours again, and the sepiolite that will be adsorbed with origanum oil then mixes in proportion with other raw materials and carrier, and sieving promptly gets;
Add this additive of 1.0kg in the feed per ton.
Embodiment 2:
Mould inhibitor: 80 parts of soluble chitins, 13 parts of KIs, 14 parts of Potassiumiodates, 20 parts of calcium propionates, 2 parts of origanum oils;
Anti-oxidant: 10 parts of n-propyl gallates, 9 parts of butylated hydroxy-as, 8 parts of butylated hydroxy anisoles, 2 parts of citric acids, 2 parts of inositols;
Totally 1000 parts in mould inhibitor, anti-oxidant and carrier, the residue umber is a carrier;
Each weight ratio of constituents is a sepiolite in the carrier: peanut hull meal: defatted rice bran=1:1:2, three are beforehand with pulverization process respectively, and making its fineness is 0.2mm;
Origanum oil is sprayed at uniformly in the sepiolite of pulverization process, and 55 ℃ of following stirring and adsorbing 3.5 hours, standing adsorption was 22 hours again, and the sepiolite that will be adsorbed with origanum oil then mixes in proportion with other raw materials and carrier, and sieving promptly gets;
Add this additive of 1.4kg in the feed per ton.
All the other are with embodiment 1.
Embodiment 3:
Mould inhibitor: 120 parts of soluble chitins, 25 parts of KIs, 27 parts of Potassiumiodates, 40 parts of calcium propionates, 4 parts of origanum oils;
Anti-oxidant: 18 parts of n-propyl gallates, 16 parts of dibutyl hydroxy toluenes, 16 parts of butylated hydroxy anisoles, 4 parts of citric acids, 4 parts of inositols;
Totally 1000 parts in mould inhibitor, anti-oxidant and carrier, the residue umber is a carrier;
Each weight ratio of constituents is a sepiolite in the carrier: peanut hull meal: defatted rice bran=1:2:3, three are beforehand with pulverization process respectively, and making its fineness is 0.4mm;
Origanum oil is sprayed at uniformly in the sepiolite of pulverization process, and 75 ℃ of following stirring and adsorbing 4.5 hours, standing adsorption was 28 hours again, and the sepiolite that will be adsorbed with origanum oil then mixes in proportion with other raw materials and carrier, and sieving promptly gets;
Add this additive of 0.8kg in the feed per ton.
All the other are with embodiment 1.
Embodiment 4:
Mould inhibitor: 50 parts of soluble chitins, 10 parts of KIs, 10 parts of Potassiumiodates, 10 parts of calcium propionates, 1 part of origanum oil;
Anti-oxidant: 5 parts of n-propyl gallates, 5 parts of dibutyl hydroxy toluenes, 5 parts of butylated hydroxy anisoles, 1 part of citric acid, 1 part of inositol;
Totally 1000 parts in mould inhibitor, anti-oxidant and carrier, the residue umber is a carrier;
Each weight ratio of constituents is a sepiolite in the carrier: peanut hull meal: defatted rice bran=1:1:1, three are beforehand with pulverization process respectively, and making its fineness is 0.1mm;
Origanum oil is sprayed at uniformly in the sepiolite of pulverization process, and 50 ℃ of following stirring and adsorbing 3 hours, standing adsorption was 20 hours again, and the sepiolite that will be adsorbed with origanum oil then mixes in proportion with other raw materials and carrier, and sieving promptly gets;
Add this additive of 0.5kg in the feed per ton.
All the other are with embodiment 1.
Embodiment 5:
Mould inhibitor: 150 parts of soluble chitins, 30 parts of KIs, 30 parts of Potassiumiodates, 50 parts of calcium propionates, 5 parts of origanum oils;
Anti-oxidant: 20 parts of n-propyl gallates, 20 parts of dibutyl hydroxy toluenes, 20 parts of butylated hydroxy anisoles, 5 parts of citric acids, 5 parts of inositols;
Totally 1000 parts in mould inhibitor, anti-oxidant and carrier, the residue umber is a carrier;
Each weight ratio of constituents is a sepiolite in the carrier: peanut hull meal: defatted rice bran=1:3:3, three are beforehand with pulverization process respectively, and making its fineness is 0.5mm;
Origanum oil is sprayed at uniformly in the sepiolite of pulverization process, and 80 ℃ of following stirring and adsorbing 5 hours, standing adsorption was 30 hours again, and the sepiolite that will be adsorbed with origanum oil then mixes in proportion with other raw materials and carrier, and sieving promptly gets;
Add this additive of 1.5kg in the feed per ton.
All the other are with embodiment 1.
Embodiment 6:
Mould inhibitor: 140 parts of soluble chitins, 12 parts of KIs, 12 parts of Potassiumiodates, 48 parts of calcium propionates, 2 parts of origanum oils;
Anti-oxidant: 18 parts of n-propyl gallates, 19 parts of dibutyl hydroxy toluenes, 6 parts of butylated hydroxy anisoles, 2 parts of citric acids, 4 parts of inositols;
Totally 1000 parts in mould inhibitor, anti-oxidant and carrier, the residue umber is a carrier;
Each weight ratio of constituents is a sepiolite in the carrier: peanut hull meal: defatted rice bran=1:1:3, three are beforehand with pulverization process respectively, and making its fineness is 0.3mm;
Origanum oil is sprayed at uniformly in the sepiolite of pulverization process, and 60 ℃ of following stirring and adsorbing 5 hours, standing adsorption was 20 hours again, and the sepiolite that will be adsorbed with origanum oil then mixes in proportion with other raw materials and carrier, and sieving promptly gets;
Add this additive of 0.9kg in the feed per ton.
All the other are with embodiment 1.
Embodiment 7:
Mould inhibitor: 45 parts of soluble chitins, 8 parts of KIs, 8 parts of Potassiumiodates, 7 parts of calcium propionates, 1 part of origanum oil;
Anti-oxidant: 3 parts of n-propyl gallates, 3 parts of dibutyl hydroxy toluenes, 4 parts of butylated hydroxy anisoles, 1 part of citric acid, 1 part of inositol;
Totally 1000 parts in mould inhibitor, anti-oxidant and carrier, the residue umber is a carrier;
Each weight ratio of constituents is a sepiolite in the carrier: peanut hull meal: defatted rice bran=1:1:1, three are beforehand with pulverization process respectively, and making its fineness is 0.1mm;
Origanum oil is sprayed at uniformly in the sepiolite of pulverization process, and 45 ℃ of following stirring and adsorbing 2.5 hours, standing adsorption was 18 hours again, and the sepiolite that will be adsorbed with origanum oil then mixes in proportion with other raw materials and carrier, and sieving promptly gets;
Add this additive of 0.4kg in the feed per ton.
All the other are with embodiment 1.
Embodiment 8:
Mould inhibitor: 160 parts of soluble chitins, 35 parts of KIs, 35 parts of Potassiumiodates, 60 parts of calcium propionates, 8 parts of origanum oils;
Anti-oxidant: 25 parts of n-propyl gallates, 25 parts of dibutyl hydroxy toluenes, 30 parts of butylated hydroxy anisoles, 8 parts of citric acids, 8 parts of inositols;
Totally 1000 parts in mould inhibitor, anti-oxidant and carrier, the residue umber is a carrier;
Each weight ratio of constituents is a sepiolite in the carrier: peanut hull meal: defatted rice bran=1:3:4, three are beforehand with pulverization process respectively, and making its fineness is 0.5mm;
Origanum oil is sprayed at uniformly in the sepiolite of pulverization process, and 85 ℃ of following stirring and adsorbing 6 hours, standing adsorption was 35 hours again, and the sepiolite that will be adsorbed with origanum oil then mixes in proportion with other raw materials and carrier, and sieving promptly gets;
Add this additive of 1.6kg in the feed per ton.
All the other are with embodiment 1.
Embodiment 9:
Be disclosed a kind of composite mildewproof antioxidant in the patent of 97104323.X according to application number, its prescription and preparation method are following:
Mould inhibitor: DMF 100g;
Antioxidant: EMQ 100g, BHA 1g, BHT 20g;
Synergist: phosphoric acid (containing heavy more than 85%) 100g
Citric acid 100g
Disodium EDTA 1g
Carrier: white carbon 30g
The preparation of antioxidant: above-mentioned three kinds of antioxidant are poured in the beaker, be heated to 80 ℃, stir, BHA, BHT all are dissolved among the EMQ, subsequent use.
The preparation of synergist: disodium EDTA and citric acid and phosphoric acid are poured in the beaker, be heated to 80 ℃ of dissolvings, it is subsequent use to stir the back.
The mixing of material: take by weighing 100gDMF and put in the 500ml beaker, pour 30g white carbon mixing into, take by weighing again and mix in antioxidant 30g and the synergist 15g adding beaker, stir total amount 175g composite mildewproof antioxidant product.
Adding this product of 0.5g in every 1000g feed gets final product.
Embodiment 10:
Be disclosed a kind of composite synergistic antioxidant mildew-retarding agent in 99115498.3 the patent according to application number, its prescription and preparation method are following:
Take by weighing sodium Diacetate 10.5g, dimethyl fumarate 5.5g, ethoxyquinoline 4.5g, citral 10.5g, cloud essential oil 5g, sepiolite 64.0g, pulverize the back mixing and get final product.
Adding this product of 1g in every 1000g feed gets final product.
Test Example 1: anti-mold effect is investigated
Test feed is the conventional feed that ZhangZhou twins feed corporation,Ltd produces, and takes by weighing 10 groups of feeds, every group of 1000g; 10 experimental group add the mold-proof oxidation-resistant agent that makes among the embodiment 1-10 respectively; Pack behind the mixing, put in the chamber, in the condition held of 26~30 ℃ of temperature, relative humidity about 75%; The 20th heaven-made outward appearance observation first time, after this every growing state of observing mould at a distance from 5 days; The blank group is not added any mold-proof oxidation-resistant agent, other same experimental group.Experimental result is seen table 2.
Deposit to 55d and take a sample, strict press " mensuration of total number of molds in State Standard of the People's Republic of China G B/T13092-2006 feed " is measured total number of molds in each processed group feed.With each processed group feed mixing, the caking feed need be pulverized, and fully samples behind the mixing before the sampling.Experimental result is seen table 3.
Table 1 feed is in the characteristic that difference is deposited the stage
The feed state Criterion Result of determination
Not mouldy The feed color is normal, can smell tangible feed fragrance
Indistinctly mouldy The feed color is normal, and feed fragrance is lighter, and a musty is indistinctly arranged
Slightly mouldy The feed color shows slightly gloomy, can smell tangible musty ++
Moderate is mouldy A small amount of point-like mildew is arranged, do not lump, musty is heavier +++
Seriously mouldy Outward appearance has tangible point-like mildew, caking, and musty is very heavy ++++
Each processed group difference of table 2 is deposited the observed result in stage
Figure 2012101051285100002DEST_PATH_IMAGE001
Each processed group of table 3 is deposited the mould quantity to the 55d
Processed group Total plate count in the feed (individual/g)
Control group 75×10 4
Embodiment 1 16×10 4
Embodiment 2 25×10 4
Embodiment 3 38×10 4
Embodiment 4 41×10 4
Embodiment 5 49×10 4
Embodiment 6 52×10 4
Embodiment 7 62×10 4
Embodiment 8 66×10 4
Embodiment 9 54×10 4
Embodiment 10 57×10 4
Test Example 2: antioxidant effect is investigated
Test feed is the conventional feed that ZhangZhou twins feed corporation,Ltd produces, and takes by weighing 10 groups of feeds, every group of 1000g; 10 experimental group add the mold-proof oxidation-resistant agent that makes among the embodiment 1-10 respectively; Pack behind the mixing, put in the chamber, keeping temperature is 35-40 ℃; For guaranteeing that sample fully contacts with airborne oxygen, every day, biased sample was 2 times.Carry out the mensuration of peroxide value in 0d, 7d, 20d, 40d, 60d sampling; The blank group is not added any mold-proof oxidation-resistant agent, other same experimental group.Experimental result is seen table 4.
Table 4 oxidation resistance testing result
Figure 2012101051285100002DEST_PATH_IMAGE002
Test Example 3: the investigation of live pig growing state
Test and Selection ZhangZhou twins feed corporation,Ltd subordinate pig farm average weight is 660 of the health pig of (38.7 ± 2.3) kg, and is not remarkable through statistical analysis body weight difference.Be divided into 11 groups at random, every group of 6 repetitions, each repeats 10.Experimental group has been added the feed of the mold-proof oxidation-resistant agent that embodiment 1-10 makes, and live pig free choice feeding and drinking-water carry out immunity and expelling parasite by routine, and ramming material and weighing after 30 days calculates daily gain, daily ingestion amount, feedstuff-meat ratio (feed intake/weightening finish); The blank group is not added any mold-proof oxidation-resistant agent, other same experimental group.Experimental result is seen table 5.
Table 5 live pig growing state
Figure 2012101051285100002DEST_PATH_IMAGE003
Can find out from above-mentioned test, compare with the blank group, add the feed of the mold-proof oxidation-resistant agent that the present invention makes and compared with conventional feed that it is long to have a mildew-resistant phase, anti-mold effect is good; Peroxide value is lower, the characteristics that antioxidant effect is good; Edible live pig daily gain and the daily ingestion amount that has added the feed of the mold-proof oxidation-resistant agent that the present invention makes significantly increases, and feedstuff-meat ratio obviously descends; And the effect of the test group that embodiment 1-6 is corresponding generally is superior to the corresponding test group of embodiment 9-10, especially with the best results of embodiment 1.So the mold-proof oxidation-resistant agent that the present invention makes can significantly improve the culture efficiency of live pig, utilization is worthy to be popularized.

Claims (3)

1. mold-proof oxidation-resistant agent that can improve the pig feed quality is characterized by:
Mould inhibitor: soluble chitin, KI, Potassiumiodate, calcium propionate, origanum oil;
Anti-oxidant: n-propyl gallate, dibutyl hydroxy toluene, butylated hydroxy anisole, citric acid, inositol;
Each weight ratio of constituents is a sepiolite in the carrier: peanut hull meal: defatted rice bran=1:1-3:1-3, three are beforehand with pulverization process respectively, and making its fineness is 0.1-0.5mm;
Wherein origanum oil obtains through following method:
With putting into supercritical extraction reactor after the pulverizing of 50g wild marjoram herb; Add 200mL75% ethanol as entrainer, the adjusting extracting pressure is 20MPa, and extraction temperature is 55 ℃; The entrainer flow is 0.02mL/min; Carbon dioxide flow is 1.2L/min, extracts and obtains the oily liquids that pale brown look has special aromatic odor after 2 hours, is origanum oil;
Origanum oil is sprayed at uniformly in the sepiolite of pulverization process, and at 50-80 ℃ of following stirring and adsorbing 3-5 hour, standing adsorption 20-30 hour again, the sepiolite that will be adsorbed with origanum oil then mixed in proportion with other raw materials and carrier, and sieving promptly gets;
Add this additive of 0.5-1.5kg in the feed per ton.
2. mold-proof oxidation-resistant agent that can improve the pig feed quality is characterized by:
Mould inhibitor: soluble chitin 50-150 part, KI 10-30 part, Potassiumiodate 10-30 part, calcium propionate 10-50 part, origanum oil 1-5 part;
Anti-oxidant: n-propyl gallate 5-20 part, dibutyl hydroxy toluene 5-20 part, butylated hydroxy anisole 5-20 part, citric acid 1-5 part, inositol 1-5 part;
Totally 1000 parts in mould inhibitor, anti-oxidant and carrier, the residue umber is a carrier;
Each weight ratio of constituents is a sepiolite in the carrier: peanut hull meal: defatted rice bran=1:1-3:1-3, three are beforehand with pulverization process respectively, and making its fineness is 0.1-0.5mm;
Wherein origanum oil obtains through following method:
With putting into supercritical extraction reactor after the pulverizing of 50g wild marjoram herb; Add 200mL75% ethanol as entrainer, the adjusting extracting pressure is 20MPa, and extraction temperature is 55 ℃; The entrainer flow is 0.02mL/min; Carbon dioxide flow is 1.2L/min, extracts and obtains the oily liquids that pale brown look has special aromatic odor after 2 hours, is origanum oil;
Origanum oil is sprayed at uniformly in the sepiolite of pulverization process, and at 50-80 ℃ of following stirring and adsorbing 3-5 hour, standing adsorption 20-30 hour again, the sepiolite that will be adsorbed with origanum oil then mixed in proportion with other raw materials and carrier, and sieving promptly gets;
Add this additive of 0.5-1.5kg in the feed per ton.
3. a kind of mold-proof oxidation-resistant agent that replenishes nutritional labeling in the pig feed as claimed in claim 2 is characterized by:
Mould inhibitor: 100 parts of soluble chitins, 20 parts of KIs, 20 parts of Potassiumiodates, 30 parts of calcium propionates, 3 parts of origanum oils;
Anti-oxidant: 15 parts of n-propyl gallates, 15 parts of dibutyl hydroxy toluenes, 10 parts of butylated hydroxy anisoles, 3 parts of citric acids, 3 parts of inositols;
Totally 1000 parts in mould inhibitor, anti-oxidant and carrier, the residue umber is a carrier;
Each weight ratio of constituents is a sepiolite in the carrier: peanut hull meal: defatted rice bran=1:2:2, three are beforehand with pulverization process respectively, and making its fineness is 0.2mm;
Wherein origanum oil obtains through following method:
With putting into supercritical extraction reactor after the pulverizing of 50g wild marjoram herb; Add 200mL75% ethanol as entrainer, the adjusting extracting pressure is 20MPa, and extraction temperature is 55 ℃; The entrainer flow is 0.02mL/min; Carbon dioxide flow is 1.2L/min, extracts and obtains the oily liquids that pale brown look has special aromatic odor after 2 hours, is origanum oil;
Origanum oil is sprayed at uniformly in the sepiolite of pulverization process, and 65 ℃ of following stirring and adsorbing 4 hours, standing adsorption was 25 hours again, and the sepiolite that will be adsorbed with origanum oil then mixes in proportion with other raw materials and carrier, and sieving promptly gets;
Add this additive of 1.0kg in the feed per ton.
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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103798514A (en) * 2012-11-07 2014-05-21 天津市中敖饲料有限公司 Feed additive with antioxidation function and preparation method thereof
CN104970258A (en) * 2015-07-17 2015-10-14 四川农业大学 Compound feed additive with antioxidant function capable of relieving mycotoxicosis of piggy
CN105010868A (en) * 2015-07-29 2015-11-04 宿迁普朗克生物科技有限公司 Preparation for preventing piglet feed from deteriorating and preparation method thereof
CN108094680A (en) * 2017-12-18 2018-06-01 广州美瑞泰科生物工程技术有限公司 A kind of feed detoxifying agent and preparation method and application
CN108175027A (en) * 2017-12-26 2018-06-19 广州美瑞泰科生物工程技术有限公司 A kind of Midew preventive for feed and preparation method and application
CN109090359A (en) * 2018-08-07 2018-12-28 四川英格瑞生物科技有限公司 A kind of trophism addition pulvis improving sow fertility
CN113662102A (en) * 2021-09-01 2021-11-19 山东富华伟农农牧科技有限公司 Pig feed for improving feed intake and processing method

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1173998A (en) * 1997-05-21 1998-02-25 李侯根 Compound feed antifermenting and antioxidizing agent and its production process
CN1961720A (en) * 2006-11-30 2007-05-16 上海交通大学 Mold-proof oxidation-resistant compound additive
CN102084941A (en) * 2009-12-07 2011-06-08 戚冬梅 mildewproof agent for feed

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1173998A (en) * 1997-05-21 1998-02-25 李侯根 Compound feed antifermenting and antioxidizing agent and its production process
CN1961720A (en) * 2006-11-30 2007-05-16 上海交通大学 Mold-proof oxidation-resistant compound additive
CN102084941A (en) * 2009-12-07 2011-06-08 戚冬梅 mildewproof agent for feed

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103798514A (en) * 2012-11-07 2014-05-21 天津市中敖饲料有限公司 Feed additive with antioxidation function and preparation method thereof
CN104970258A (en) * 2015-07-17 2015-10-14 四川农业大学 Compound feed additive with antioxidant function capable of relieving mycotoxicosis of piggy
CN105010868A (en) * 2015-07-29 2015-11-04 宿迁普朗克生物科技有限公司 Preparation for preventing piglet feed from deteriorating and preparation method thereof
CN108094680A (en) * 2017-12-18 2018-06-01 广州美瑞泰科生物工程技术有限公司 A kind of feed detoxifying agent and preparation method and application
CN108175027A (en) * 2017-12-26 2018-06-19 广州美瑞泰科生物工程技术有限公司 A kind of Midew preventive for feed and preparation method and application
CN109090359A (en) * 2018-08-07 2018-12-28 四川英格瑞生物科技有限公司 A kind of trophism addition pulvis improving sow fertility
CN113662102A (en) * 2021-09-01 2021-11-19 山东富华伟农农牧科技有限公司 Pig feed for improving feed intake and processing method

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