CN102579275B - Beautifying toothpaste containing aluminum-magnesium silicate and preparation method of beautifying toothpaste - Google Patents
Beautifying toothpaste containing aluminum-magnesium silicate and preparation method of beautifying toothpaste Download PDFInfo
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- CN102579275B CN102579275B CN 201210040114 CN201210040114A CN102579275B CN 102579275 B CN102579275 B CN 102579275B CN 201210040114 CN201210040114 CN 201210040114 CN 201210040114 A CN201210040114 A CN 201210040114A CN 102579275 B CN102579275 B CN 102579275B
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Abstract
The invention discloses a beautifying toothpaste containing aluminum-magnesium silicate and a preparation method of the beautifying toothpaste, wherein the beautifying toothpaste containing aluminum-magnesium silicate adopts natural mineral materials as raw materials and aluminum-magnesium silicate mineral powder of 400-500 meshes obtained by purification and modification as a main component, and is prepared by adopting the following components according to weight: 5-25 percent of aluminum-magnesium silicate, 20-40 percent of calcium carbonate, 0.2-30 percent of sorbitol, 0.5-30 percent of glycerol, 1-5 percent of sodium dodecyl sulfate, 0.3-0.9 percent of sodium carboxy methyl cellulose, 0.3-0.9 percent of hydroxypropyl guar gum, 0.5-1.5 percent of essence, 0.1-0.3 percent of sweetener, 0.1-0.2 percent of methylparaben and the balance of deionized water. The toothpaste not only can whiten teeth, but also can inhibit harmful bacteria in the oral cavity and clear away bad breath, thereby realizing complete beautification of the oral cavity.
Description
Technical field
The present invention relates to a kind of beauty treatment toothpaste that contains aluminium magensium silicate and preparation method thereof, belong to daily chemical product.
Background technology
Along with China strides into well-off society, the people is more and more higher to the requirement of toothpaste quality and function, helps the toothpaste of tooth whitening and oral health more and more to be subject to pursuing of market.As Black people's ultrawhite toothpaste, take whitening silicon (HCS) as active component, the brilliant white tooth; Receive the Ace nutrient toothpaste, take vitamin as active component, the nursing gingiva; The black salubrious toothpaste of younger sister's vigor take organic antibacterial agent and plant extract as active component, suppresses the oral cavity harmful bacteria, fresh breath.They are all star's toothpaste of market manifestation excellence.
The object of the invention is to research and develop a kind of effect type toothpaste that adds aluminium magensium silicate, it both can come tooth-whitening by minimizing tooth stain, dental plaque, tartar; Can alleviate gingivitis, remove halitosis by suppressing the oral cavity harmful bacteria again, thereby bring more aesthetic feelings to life, this toothpaste can be referred to as the toothpaste of improving looks.
The main active aluminium magensium silicate of this toothpaste is a kind of natural minerals (if you would take off stone, meerschaum, foresite etc.) through purification, modification, and this material has been widely used in food decolouring processing, and safety is very good.
The inner porous of aluminium magensium silicate, specific surface area is large, surface activity is high, has excellent absorption property, in the process of brushing teeth can with dental surface on the quick combination of tooth stain, dental plaque, tartar, then through gargling and being eliminated.
The tectosilicate that aluminium magensium silicate is comprised of silicon-oxy tetrahedron and aluminum-oxygen tetrahedron, but the cation of combined belt positive electricity (as magnesium, calcium, potassium, sodium etc.), has open architecture, be conducive to ion exchange, load is to human-body safety and have the metal ion such as nanoscale zinc, titanium of antibacterial activity, can effectively suppress the harmful bacteria in the oral cavity, prevent and alleviate gingivitis, protect the health of one's mouth; Zinc, titanium ion can also with oral cavity bacterium and Organic substance in sulfydryl (SH) and amino (NH) functional group reacts, and decomposes the organic molecule that produces abnormal flavour, fast counteract oral malodour.
Up to the present, also find to produce with the aluminium magensium silicate after purification, modification the report of beauty treatment toothpaste at home and abroad.
Summary of the invention
In order to alleviate shortcomings and deficiencies of the prior art, the object of the present invention is to provide a kind of beauty treatment toothpaste that contains aluminium magensium silicate and preparation method thereof, the beauty treatment toothpaste that contains aluminium magensium silicate provided by the invention can reduce tooth stain, dental plaque, tartar, alleviate gingivitis, remove halitosis, make tooth whitening, gingiva is healthy, breath freshening, thus realize comprehensive beauty treatment in oral cavity.
The present invention adopts following technical scheme to achieve these goals:
The beauty treatment toothpaste that contains aluminium magensium silicate, the percentage by weight that it is characterized in that its constitutive material is: aluminium magensium silicate breeze 5%-25%, calcium carbonate 20%-40%, sorbitol 0.2%-30%, glycerol 0.5%-30%, sodium lauryl sulphate 1%-5%, sodium carboxymethyl cellulose 0.3%-0.9%, hydroxypropyl guar gum 0.3%-0.9%, essence 0.5%-1.5%, sweeting agent 0.1%-0.3%, methyl hydroxybenzoate 0.1%-0.2%, deionized water surplus.
The described beauty treatment toothpaste that contains aluminium magensium silicate is characterized in that: described aluminium magensium silicate breeze obtains by purification, modification take natural minerals as raw material.
The described beauty treatment toothpaste that contains aluminium magensium silicate, it is characterized in that: described aluminium magensium silicate ore powder granularity is the 400-500 order, production technology is: (1) selection whiteness is high, pure raw ore, eluriates, dries, and be crushed to the 400-500 order with connected superfine pulverizer; (2) breeze is added make high-concentration ore slurry in deionized water, the modifier and the dispersant that add again 0.1-1.5% tetrasodium pyrophosphate, 1.0-8.0% aluminium hydroxide, 0.1-1.5% magnesium oxide, 0.1-0.6% zinc citrate, 0.2-2.0% titanium dioxide, high-speed stirred ore pulp 30 minutes, then carry out centrifugal, filter pressing, realize except sand separation; (3) dry the ore pulp of separating, then use tooth-like pulverizer broken, the clean polyethylene plastic bag of packing into is standby.
The described preparation method that contains the beauty treatment toothpaste of aluminium magensium silicate is characterized in that comprising the following steps:
(1) percentage by weight by constitutive material takes each raw material, with the sweeting agent deionized water dissolving, adds the toothpaste Manufacturing medicine extract machine, again sorbitol, glycerol and remaining deionized water are added the toothpaste Manufacturing medicine extract machine, change down speed and stir and vacuum pump, until vacuum reach-during 0.09MPa, close vacuum pump;
(2) open toothpaste Manufacturing medicine extract machine high-speed stirred, utilize successively vacuum to suck the toothpaste Manufacturing medicine extract machine aluminium magensium silicate, calcium carbonate, sodium carboxymethyl cellulose, hydroxypropyl guar gum, sodium lauryl sulphate;
(3) open vacuum pump, until vacuum reach-during 0.094MPa, continued homogenizing 20-30 minute, make mastic reach the state of compacting, then close vacuum, methyl hydroxybenzoate is dissolved in essence, resorb the toothpaste Manufacturing medicine extract machine;
(4) open vacuum and continue emulsifying 10-20 minute, can make needed finished product mastic;
(5) with the toothpaste filling machine, the finished product mastic is poured into aluminium-plastic composite hose, complete preparation.
In the present invention, the purposes of aluminium magensium silicate is teeth whitening, antibacterial, flavorants, the purposes of calcium carbonate is abrasivus, the purposes of sorbitol and glycerol is wetting agent, the purposes of sodium lauryl sulphate is foaming agent, detergent, the purposes of sodium carboxymethyl cellulose and hydroxypropyl guar gum is thickening agent, various types of food flavors such as the optional Herba Menthae of essence, Ilicis Purpureae, Herba Menthae Rotundifoliae, the optional saccharin sodium of sweeting agent, aspartame, methyl hydroxybenzoate are antiseptic.
Compared with prior art, the present invention has following advantage:
(1) utilize natural minerals efficiently to remove tooth stain, dental plaque, tartar on tooth, have the remarkable result of tooth-whitening.
(2) utilize nanoscale zinc, titanium ion in natural minerals effectively to suppress staphylococcus aureus, escherichia coli, Candida albicans, Streptococcus mutans, Aspergillus niger in the oral cavity, have the remarkable result that alleviates with prevention of gingivitis.
(3) utilize natural minerals efficient adsorption halitosis, decompose to produce the sulfydryl of abnormal flavour (SH) and amino (NH) functional group, elimination halitosis, fresh breath.
(4) inorganic nano antiseptic is with respect to organic antibacterial agent, and safety is good, and toxic and side effects is little.
(5) natural minerals wide material sources, cost advantage is obvious, and can drive the development of regional economy.
The specific embodiment
Embodiment 1:
(1) aluminium magensium silicate is passed through to purify by natural foresite, then adds 0.1-1.5% magnesium oxide, 0.1-0.6% zinc citrate, 0.2-2.0% titanium dioxide, gets by the high-speed stirred process modification, selects 400 order breezes;
(2) with 15g saccharin sodium 150ml deionized water dissolving, add the toothpaste Manufacturing medicine extract machine, then 1500g sorbitol and 850ml deionized water are added the toothpaste Manufacturing medicine extract machine.Change down speed and stir and vacuum pump, until vacuum reach-during 0.09MPa, close vacuum pump;
(3) open toothpaste Manufacturing medicine extract machine high-speed stirred, utilize successively vacuum to suck the toothpaste Manufacturing medicine extract machine 750g aluminium magensium silicate, 1500g calcium carbonate, 25g sodium carboxymethyl cellulose, 35g hydroxypropyl guar gum, 120g sodium lauryl sulphate;
(4) open vacuum pump, until vacuum reach-during 0.094MPa, continued homogenizing 20-30 minute, make mastic reach the state of compacting, then close vacuum, the 7.5g methyl hydroxybenzoate is dissolved in 60g essence, resorb the toothpaste Manufacturing medicine extract machine;
(5) open vacuum and continue emulsifying 10-20 minute, can make needed finished product mastic;
(6) with the toothpaste filling machine, the finished product mastic is poured into aluminium-plastic composite hose, complete production.
Embodiment 2:
(1) aluminium magensium silicate is passed through to purify by the natural sea afrodite, then adds 1.0-8.0% aluminium hydroxide, 0.1-0.6% zinc citrate, 0.2-2.0% titanium dioxide, gets by the high-speed stirred process modification, selects 500 order breezes;
(2) with 15g saccharin sodium 150ml deionized water dissolving, add the toothpaste Manufacturing medicine extract machine, then 1250g glycerol and 1100ml deionized water are added the toothpaste Manufacturing medicine extract machine.Change down speed and stir and vacuum pump, until vacuum reach-during 0.09MPa, close vacuum pump;
(3) open toothpaste Manufacturing medicine extract machine high-speed stirred, utilize successively vacuum to suck the toothpaste Manufacturing medicine extract machine 1250g aluminium magensium silicate, 1000g calcium carbonate, 15g sodium carboxymethyl cellulose, 45g hydroxypropyl guar gum, 130g sodium lauryl sulphate;
(4) open vacuum pump, until vacuum reach-during 0.094MPa, continued homogenizing 20-30 minute, make mastic reach the state of compacting, then close vacuum, the 7.5g methyl hydroxybenzoate is dissolved in 67.5g essence, resorb the toothpaste Manufacturing medicine extract machine;
(5) open vacuum and continue emulsifying 10-20 minute, can make needed finished product mastic;
(6) with the toothpaste filling machine, the finished product mastic is poured into aluminium-plastic composite hose, complete production.
Embodiment 3:
(1) aluminium magensium silicate is passed through to purify by natural Montmorillonitum, then adds 0.1-0.6% zinc citrate, 0.2-2.0% titanium dioxide, gets by the high-speed stirred process modification, selects 400 order breezes;
(2) with 15g saccharin sodium 150ml deionized water dissolving, add the toothpaste Manufacturing medicine extract machine, then 500g glycerol, 1000g sorbitol and 850ml deionized water are added the toothpaste Manufacturing medicine extract machine.Change down speed and stir and vacuum pump, until vacuum reach-during 0.09MPa, close vacuum pump;
(3) open toothpaste Manufacturing medicine extract machine high-speed stirred, utilize successively vacuum to suck the toothpaste Manufacturing medicine extract machine 250g aluminium magensium silicate, 2000g calcium carbonate, 35g sodium carboxymethyl cellulose, 25g hydroxypropyl guar gum, 120g sodium lauryl sulphate;
(4) open vacuum pump, until vacuum reach-during 0.094MPa, continued homogenizing 20-30 minute, make mastic reach the state of compacting, then close vacuum, the 7.5g methyl hydroxybenzoate is dissolved in 60g essence, resorb the toothpaste Manufacturing medicine extract machine;
(5) open vacuum and continue emulsifying 10-20 minute, can make needed finished product mastic;
(6) with the toothpaste filling machine, the finished product mastic is poured into aluminium-plastic composite hose, complete production.
Result: the prepared lotion of toothpaste of embodiment 1-3, through the examination and test of products, all meet the requirement of toothpaste GB GB8372-2008, through bacteriostatic test, to the bacteriostasis rate of staphylococcus aureus, escherichia coli, Candida albicans, Streptococcus mutans, Aspergillus niger all more than 99%; Person's test that direct oral cavity has the abnormal flavour, embodiment 1 no longer includes abnormal flavour in the oral cavity after average 10 days, and embodiment 2 no longer includes abnormal flavour in the oral cavity after average 7 days, and embodiment 3 no longer includes abnormal flavour in the oral cavity after average 14 days; Through tooth, cigarette stain person test is arranged, embodiment 1 after average 21 days tooth bleach, embodiment 2 after average 14 days tooth bleach, embodiment 3 after average 30 days tooth bleach; Toothpaste has substantial connection to effect and the consumption of aluminium magensium silicate in formula of removing halitosis and tooth whitening.
Claims (2)
1. beauty treatment toothpaste that contains aluminium magensium silicate, the percentage by weight that it is characterized in that its constitutive material is: aluminium magensium silicate breeze 5%-25%, calcium carbonate 20%-40%, sorbitol 0.2%-30%, glycerol 0.5%-30%, sodium lauryl sulphate 1%-5%, sodium carboxymethyl cellulose 0.3%-0.9%, hydroxypropyl guar gum 0.3%-0.9%, essence 0.5%-1.5%, sweeting agent 0.1%-0.3%, methyl hydroxybenzoate 0.1%-0.2%, deionized water surplus; Described aluminium magensium silicate breeze obtains by purification, modification take natural minerals as raw material; Described aluminium magensium silicate ore powder granularity is the 400-500 order, and production technology is: (1) selection whiteness is high, pure aluminium magensium silicate raw ore, eluriates, dries, and be crushed to the 400-500 order with connected superfine pulverizer; (2) breeze is added make high-concentration ore slurry in deionized water, add again 0.1-1.5% tetrasodium pyrophosphate, 1.0-8.0% aluminium hydroxide, 0.1-1.5% magnesium oxide, 0.1-0.6% zinc citrate, titania modified dose of 0.2-2.0% and dispersant, high-speed stirred ore pulp 30 minutes, then carry out centrifugal, filter pressing, realize except sand separation; (3) dry the ore pulp of separating, then use tooth-like pulverizer broken, the clean polyethylene plastic bag of packing into is standby.
2. preparation method that contains the beauty treatment toothpaste of aluminium magensium silicate as claimed in claim 1 is characterized in that comprising the following steps:
(1) percentage by weight by constitutive material takes each raw material, with the sweeting agent deionized water dissolving, adds the toothpaste Manufacturing medicine extract machine, again sorbitol, glycerol and remaining deionized water are added the toothpaste Manufacturing medicine extract machine, change down speed and stir and vacuum pump, until vacuum reach-during 0.09MPa, close vacuum pump;
(2) open toothpaste Manufacturing medicine extract machine high-speed stirred, utilize successively vacuum to suck the toothpaste Manufacturing medicine extract machine aluminium magensium silicate breeze, calcium carbonate, sodium carboxymethyl cellulose, hydroxypropyl guar gum, sodium lauryl sulphate;
(3) open vacuum pump, until vacuum reach-during 0.094MPa, continued homogenizing 20-30 minute, make mastic reach the state of compacting, then close vacuum, methyl hydroxybenzoate is dissolved in essence, resorb the toothpaste Manufacturing medicine extract machine;
(4) open vacuum and continue emulsifying 10-20 minute, can make needed finished product mastic;
(5) with the toothpaste filling machine, the finished product mastic is poured into aluminium-plastic composite hose, complete preparation.
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Families Citing this family (6)
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| WO2014170096A1 (en) * | 2013-04-15 | 2014-10-23 | Unilever N.V. | Toothpaste containing smectite clay |
| CN107184403A (en) * | 2017-06-22 | 2017-09-22 | 缪来耿 | A kind of toothpaste and preparation method thereof |
| CN107308077A (en) * | 2017-07-04 | 2017-11-03 | 湖南云从科技有限公司 | A kind of formulation of tooth-paste of clean tooth-whitening and preparation method thereof |
| CN107661228A (en) * | 2017-10-20 | 2018-02-06 | 广州市西瑶玉池科技有限公司 | A kind of multiple-effect toothpaste of the mineral element containing the tremolite |
| CN108852953A (en) * | 2018-09-28 | 2018-11-23 | 广东温和堂健康科学有限公司 | A kind of formula and technique of Xinhui citrus reticulata unshiu peel extract production toothpaste |
| CN110547977B (en) * | 2019-08-30 | 2022-07-15 | 广州悦创实业有限公司 | Oral care composition containing baking soda as well as preparation method and application thereof |
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Effective date of registration: 20171221 Address after: 510890 Huadu Town, Huadu District, Huadu District, Guangdong, Guangzhou Patentee after: Guangzhou Qian Cai cosmetics company limited Address before: 230022 No. 373, Mount Huangshan Road, Hefei, Anhui Patentee before: Hefei College |