CN102578364A - Ternary complex peptides powder - Google Patents
Ternary complex peptides powder Download PDFInfo
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- CN102578364A CN102578364A CN2012100676871A CN201210067687A CN102578364A CN 102578364 A CN102578364 A CN 102578364A CN 2012100676871 A CN2012100676871 A CN 2012100676871A CN 201210067687 A CN201210067687 A CN 201210067687A CN 102578364 A CN102578364 A CN 102578364A
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Abstract
The invention discloses a ternary complex peptides powder. The processing steps include: using defatted soybean meal, defatted peanut meal and defatted sesame meal as raw materials, subjecting the raw materials to pretreatment, subjecting suspension to homogeneity, then subjecting the mixture to thermal insulation enzymolysis, high temperature enzymic inactivation, concentration and spray drying, finally obtaining the tri-composite peptides powder after hydrolysis treatment of compound protease. According to the tri-composite peptides powder, the defatted soybean meal, the defatted peanut meal and the defatted sesame meal are used as raw materials, thereby the additional values of the three raw materials are increased; soybean, peanut and sesame are scientifically and reasonably combined, nutritional components of the soybean, the peanut and the sesame are provided and the functions of strengthening human immunity, anti-aging, anti-oxidation and recovering from tiredness are achieved; the prepared tri-composite peptides powder is absorbed by human easily, directly and quickly, and the delivery capacity and the rate of digestibility of protein for human eating are greatly improved.
Description
Technical field
The present invention relates to the compound peptide powder of a kind of ternary, specifically is to be the compound peptide powder of ternary that the prepared using compound protease is produced with defatted soybean meal, the defatted peanut dregs of rice and degreasing sesame seed meal, belongs to food processing field.
Background technology
Human panning protein is after the digestive ferment effect; Be not mainly to absorb with amino acid whose form; But absorb with the form of peptide; Some peptides can not only provide people's bulk-growth, grow required nutriment, have different physiological roles simultaneously, as improve mineral matter transportation and absorption, antibiotic and viral, improve immunity, anti-oxidant norcholesterol, antitumaous effect, the removing free radical is anti-ageing and anti-hypertension and high fat of blood etc.
Defatted soybean meal is present most important vegetable protein source, and its crude protein content is up to 43%-48%, and is made up of the amino acid than balance, but the soybean protein molecular structure is complicated, and molecular weight is bigger, thereby causes digestibility and biological value not high.Handle the various ANFs that can reduce effectively in the removal defatted soybean meal through enzyme, make the protein in the dregs of beans resolve into a large amount of Soybean Peptide simultaneously.Soybean Peptide is the controlled hydrolysis of soybean protein process, the refining one type of active peptide that obtains, and normally is made up of 3-6 amino acid.
Peanut is as one of six big oil crops of China, and the output height occupies first place in the world.And China is many aspect the extraction of edible oil and fat to the utilization of peanut, and is less to utilizing of peanut protein.Contain 50% protein in the peanut meal after the peanut oil expression, peanut protein generates the different peptide section of molecular weight through hydrolysis, and the content that contains human body necessary 8 seed amino acids, especially sulfur-containing amino acid in the peanut peptide is quite high.The dissolubility of peanut peptide, stability all are superior to peanut protein, can supplement the nutrients rapidly and participate in the synthetic of human amino acid and protein directly directly by little intestinal absorption, promote the protein active group to play a role enhance immunity power.
Protein content in the sesame is 20%-22%; Its oil expression back byproduct dregs of linseeds or sesame seeds or grouts contain protein 38%-50%; Sesame protein amino acid is formed and to be compared with beef, except that lysine content is low, all the other all near or reach FAO/WHO suggestion high-quality protein; And be rich in sulfur-containing amino acid, especially methionine content is higher than other vegetable protein.
Therefore, utilizing the compound peptide powder of protein Preparation ternary in these three kinds of raw materials of protease hydrolytic, is a significant research topic.
Summary of the invention
It is raw material with defatted soybean meal, the defatted peanut dregs of rice, degreasing sesame seed meal that the present invention is intended to exploitation, utilizes the compound peptide powder of compound protease production ternary, not only realizes twice laid, also can improve its added value.
The technical scheme that the present invention adopted is following:
The compound peptide powder of this ternary, its raw materials for production comprise defatted soybean meal, the defatted peanut dregs of rice and degreasing sesame seed meal, by homogeneous, insulation enzymolysis, the high temperature of the preliminary treatment of raw material, suspension go out enzyme, concentrate and the drying process with atomizing step is made.
The raw materials for production preferred version of the compound peptide powder of this ternary is: the mass fraction of each component and content thereof is: defatted soybean meal 3, the defatted peanut dregs of rice 2, degreasing sesame seed meal 1, and selected raw material color is normal, free from extraneous odour, nothing go mouldy.
The compound peptide powder of this ternary, its manufacturing process steps is following:
1) preliminary treatment of raw material: defatted soybean meal, the defatted peanut dregs of rice and degreasing sesame seed meal are pulverized and cross 40 mesh sieves respectively with pulverizer, the raw material after the pulverizing is mixing in advance in proportion, presses raw material again and mixes with the mass ratio of water=1:4-6, and is subsequent use;
2) homogeneous of suspension: above-mentioned suspension is passed through the high pressure homogenizer homogenization processing through the colloid mill defibrination earlier again, and pressure is 25-30MPa;
3) insulation enzymolysis: the suspension that homogeneous is good places reaction ax; In the raw material suspension, adding earlier alkali protease (the letter Alcalase of Novi) addition is the 0.03%-0.05% of raw material suspension quality; Its enzyme hydrolysis condition is: 50-60 ℃, pH7.0-8.5 after hydrolysis 6-8 hour, add flavor protease (the letter Flavourzyme of Novi) in enzymolysis liquid; Addition is the 0.01%-0.02% of raw material suspension quality; Its enzyme hydrolysis condition is: 50-60 ℃, pH6.0-7.0, continue hydrolysis 2-3 hour, and can finish enzymolysis;
4) the high temperature enzyme that goes out: enzymolysis is warming up to the 90-95 ℃ of enzyme that goes out with the enzymolysis liquid temperature fast, and is incubated 10 minutes after finishing;
5) concentrate: the ternary peptide suspension behind the enzyme that will go out carries out vacuum and concentrates, and making the moisture in the concentrate is 65-70%;
6) spray-drying: concentrate introduced in the drying tower spray, drying tower import hot air temperature is controlled at 160-180 ℃, and the outlet hot air temperature is controlled at 75-90 ℃, and the concentrate charging rate is 10 kilograms/hour, and rotary head speed is 12000 rev/mins.
Useful effect of the present invention: (1) utilizes defatted soybean meal, the defatted peanut dregs of rice and degreasing sesame seed meal to be the compound peptide powder of raw material production ternary, has improved the added value of these three kinds of raw materials; (2) scientific and reasonable collocation soybean, peanut, sesame three kind of plant have the nutritional labeling of soybean, peanut and sesame concurrently, but have enhancing human immune, anti-ageing, anti-oxidant, function such as set up; (3) the prepared compound peptide powder of ternary is easy to by human body directly, absorb rapidly, and these article have improved the conveying capacity and the digestibility of human body edible protein greatly.
The specific embodiment
Embodiment 1
The raw material of the compound peptide powder of this ternary is defatted soybean meal, the defatted peanut dregs of rice and degreasing sesame seed meal, is formed by the compound protease hydrolysis process, and making step is following:
1) preliminary treatment of raw material: defatted soybean meal, the defatted peanut dregs of rice and degreasing sesame seed meal are pulverized and cross 40 mesh sieves respectively with pulverizer; Raw material after the pulverizing is by defatted soybean meal: the defatted peanut dregs of rice: degreasing sesame seed meal=3:2:1 mass ratio mixing of going ahead of the rest; Mass ratio by raw material and water=1:6 mixes again, and require that selected raw material answers that color is normal, free from extraneous odour, nothing go mouldy;
2) homogeneous of suspension: suspension is passed through the high pressure homogenizer homogenization processing through the colloid mill defibrination earlier again, and homogenization pressure is 30MPa;
3) insulation enzymolysis: in the raw material suspension, adding earlier alkali protease (the letter Alcalase of Novi) addition is 0.03% of raw material suspension quality; Its enzyme hydrolysis condition is: 60 ℃, pH8.5, and hydrolysis added flavor protease (the letter Flavourzyme of Novi) after 8 hours in enzymolysis liquid; Addition is 0.01% of a raw material suspension quality; Its enzyme hydrolysis condition is: 60 ℃, pH7.0, continue hydrolysis 3 hours, and can finish enzymolysis;
4) the high temperature enzyme that goes out: enzyme hydrolysis is warming up to 95 ℃ with the enzymolysis liquid temperature fast, and is incubated 10 minutes after finishing;
5) concentrate: enzymolysis liquid is concentrated to reduce moisture wherein through vacuum, make the moisture in the enzymolysis concentrate be reduced to 70%;
6) spray-drying: the enzymolysis concentrate that will reach the water content requirement is introduced in the spray drying tower; And control spray drying tower import hot air temperature is 160 ℃; The outlet hot air temperature is at 90 ℃; The concentrate charging rate is 10 kilograms/hour, and 12000 rev/mins of rotary head speed can obtain the compound peptide powder of ternary.
Embodiment 2
The raw material of the compound peptide powder of this ternary is defatted soybean meal, the defatted peanut dregs of rice and degreasing sesame seed meal, is formed by the compound protease hydrolysis process, and making step is following:
1) preliminary treatment of raw material: defatted soybean meal, the defatted peanut dregs of rice and degreasing sesame seed meal are pulverized and cross 40 mesh sieves respectively with pulverizer; Raw material after the pulverizing is by defatted soybean meal: the defatted peanut dregs of rice: degreasing sesame seed meal=3:2:1 mass ratio mixing of going ahead of the rest; Mass ratio by raw material and water=1:4 mixes again, and require that selected raw material answers that color is normal, free from extraneous odour, nothing go mouldy;
2) homogeneous of suspension: suspension is passed through the high pressure homogenizer homogenization processing through the colloid mill defibrination earlier again, and homogenization pressure is 25MPa;
3) insulation enzymolysis: in the raw material suspension, adding earlier alkali protease (the letter Alcalase of Novi) addition is 0.05% of raw material suspension quality; Its enzyme hydrolysis condition is: 50 ℃, pH7.0, and hydrolysis added flavor protease (the letter Flavourzyme of Novi) after 6 hours in enzymolysis liquid; Addition is 0.02% of a raw material suspension quality; Its enzyme hydrolysis condition is: 50 ℃, pH6.0, continue hydrolysis 2 hours, and can finish enzymolysis;
4) the high temperature enzyme that goes out: enzyme hydrolysis is warming up to 90 ℃ with the enzymolysis liquid temperature fast, and is incubated 10 minutes after finishing;
5) concentrate: enzymolysis liquid is concentrated to reduce moisture wherein through vacuum, make the moisture in the enzymolysis concentrate be reduced to 65%;
6) spray-drying: the enzymolysis concentrate that will reach the water content requirement is introduced in the spray drying tower; And control spray drying tower import hot air temperature is at 180 ℃; The outlet hot air temperature is at 75 ℃; The concentrate charging rate is 10 kilograms/hour, and 12000 rev/mins of rotary head speed can obtain the compound peptide powder of ternary.
Embodiment 3
The raw material of the compound peptide powder of this ternary is defatted soybean meal, the defatted peanut dregs of rice and degreasing sesame seed meal, is formed by the compound protease hydrolysis process, and making step is following:
1) preliminary treatment of raw material: defatted soybean meal, the defatted peanut dregs of rice and degreasing sesame seed meal are pulverized and cross 40 mesh sieves respectively with pulverizer; Raw material after the pulverizing is by defatted soybean meal: the defatted peanut dregs of rice: degreasing sesame seed meal=3:2:1 mass ratio mixing of going ahead of the rest; Mass ratio by raw material and water=1:5 mixes again, and require that selected raw material answers that color is normal, free from extraneous odour, nothing go mouldy;
2) homogeneous of mixed liquor: suspension is passed through the high pressure homogenizer homogenization processing through the colloid mill defibrination earlier again, and homogenization pressure is 28MPa;
3) insulation enzymolysis: in the raw material suspension, adding earlier alkali protease (the letter Alcalase of Novi) addition is 0.04% of raw material suspension quality; Its enzyme hydrolysis condition is: 550 ℃, pH87.0, and hydrolysis added flavor protease (the letter Flavourzyme of Novi) after 7 hours in enzymolysis liquid; Addition is 0.02% of a raw material suspension quality; Its enzyme hydrolysis condition is: 55 ℃, pH6.0, continue hydrolysis 2 hours, and can finish enzymolysis;
4) the high temperature enzyme that goes out: enzyme hydrolysis is warming up to 95 ℃ with the enzymolysis liquid temperature fast, and is incubated 10 minutes after finishing;
5) concentrate: enzymolysis liquid is concentrated to reduce moisture wherein through vacuum, make the moisture in the enzymolysis concentrate be reduced to 65%;
6) spray-drying: the enzymolysis concentrate that will reach the water content requirement is introduced in the spray drying tower; And control spray drying tower import hot air temperature is at 170 ℃; The outlet hot air temperature is at 80 ℃; The concentrate charging rate is 10 kilograms/hour, and 12000 rev/mins of rotary head speed can obtain the compound peptide powder of ternary.
The foregoing description is a preferred implementation of the present invention; But embodiment of the present invention is not restricted to the described embodiments; Other is any not to deviate from change that principle of the present invention and aim done, substitute, combination or simplify; All should be the substitute mode of equivalence, be included within protection scope of the present invention.
Claims (3)
1. compound peptide powder of ternary; It is characterized in that: the raw materials for production of this compound peptide powder comprise defatted soybean meal, the defatted peanut dregs of rice and degreasing sesame seed meal, by homogeneous, insulation enzymolysis, the high temperature of the preliminary treatment of raw material, suspension go out enzyme, concentrate and the drying process with atomizing step is made.
2. the compound peptide powder of ternary according to claim 1; It is characterized in that: the mass fraction of each component of the raw materials for production of this compound peptide powder and content thereof is: defatted soybean meal 3, the defatted peanut dregs of rice 2, degreasing sesame seed meal 1, and selected raw material color is normal, free from extraneous odour, nothing go mouldy.
3. the compound peptide powder of ternary according to claim 1 and 2, it is characterized in that: the manufacturing process steps of this compound peptide powder is following:
1) preliminary treatment of raw material: said three kinds of raw materials are pulverized respectively, and crossed 40 mesh sieves, pulverize the back, mix with the mass ratio of water=1:4-6 by raw material again in the said ratio mixing of going ahead of the rest, subsequent use;
2) homogeneous of suspension: above-mentioned suspension is passed through the high pressure homogenizer homogenization processing through the colloid mill defibrination earlier again, and pressure is 25-30MPa;
3) insulation enzymolysis: the suspension that homogeneous is good places reaction ax; In the raw material suspension, add earlier alkali protease (the letter Alcalase of Novi), addition is the 0.03%-0.05% of raw material suspension quality, and its enzyme hydrolysis condition is: 50-60 ℃, pH7.0-8.5; After hydrolysis 6-8 hour; In enzymolysis liquid, add flavor protease (the letter Flavourzyme of Novi), addition is the 0.01%-0.02% of raw material suspension quality, and its enzyme hydrolysis condition is: 50-60 ℃, pH6.0-7.0; Continue hydrolysis 2-3 hour, can finish enzymolysis;
4) the high temperature enzyme that goes out: enzymolysis is warming up to the 90-95 ℃ of enzyme that goes out with the enzymolysis liquid temperature fast, and is incubated 10 minutes after finishing;
5) concentrate: the ternary peptide suspension behind the enzyme that will go out carries out vacuum and concentrates, and makes the moisture in the concentrate be reduced to 65-70%;
6) spray-drying: concentrate introduced carry out spray-drying in the drying tower; Drying tower import hot air temperature is controlled at 160-180 ℃; The outlet hot air temperature is controlled at 75-90 ℃, and the concentrate charging rate is 10 kilograms/hour, and rotary head speed is 12000 rev/mins.
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| CN2012100676871A CN102578364A (en) | 2012-03-15 | 2012-03-15 | Ternary complex peptides powder |
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| CN2012100676871A CN102578364A (en) | 2012-03-15 | 2012-03-15 | Ternary complex peptides powder |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102987275A (en) * | 2012-12-28 | 2013-03-27 | 黑龙江新曙光牧业集团有限公司 | Preparation method of soybean oligo saccharide peptide with high biological value |
| CN102987462A (en) * | 2012-12-28 | 2013-03-27 | 黑龙江新曙光牧业集团有限公司 | Preparation method of instant-dissolving soybean oligosaccharide peptide peanut product |
| CN104544050A (en) * | 2014-12-16 | 2015-04-29 | 山东世纪春食品有限公司 | Method for producing special diet food rich in peanut peptides for patients with hypertension |
| CN104904988A (en) * | 2015-06-17 | 2015-09-16 | 山东省农业科学院农产品研究所 | Method for processing peanut protein powder with high polypeptide content |
| CN109280683A (en) * | 2017-08-15 | 2019-01-29 | 广东丸美生物技术股份有限公司 | Preparation method of composite plant hydrolyzed protein peptide |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102987275A (en) * | 2012-12-28 | 2013-03-27 | 黑龙江新曙光牧业集团有限公司 | Preparation method of soybean oligo saccharide peptide with high biological value |
| CN102987462A (en) * | 2012-12-28 | 2013-03-27 | 黑龙江新曙光牧业集团有限公司 | Preparation method of instant-dissolving soybean oligosaccharide peptide peanut product |
| CN102987275B (en) * | 2012-12-28 | 2018-06-01 | 长春大学 | A kind of preparation method of the soy oligosaccharides glycopeptide of high biological value |
| CN102987462B (en) * | 2012-12-28 | 2018-10-23 | 长春大学 | A kind of preparation method of instant soluble soybean oligosaccharide peptide peanut products |
| CN104544050A (en) * | 2014-12-16 | 2015-04-29 | 山东世纪春食品有限公司 | Method for producing special diet food rich in peanut peptides for patients with hypertension |
| CN104904988A (en) * | 2015-06-17 | 2015-09-16 | 山东省农业科学院农产品研究所 | Method for processing peanut protein powder with high polypeptide content |
| CN109280683A (en) * | 2017-08-15 | 2019-01-29 | 广东丸美生物技术股份有限公司 | Preparation method of composite plant hydrolyzed protein peptide |
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Application publication date: 20120718 |