CN102561098A - Method of preparing silk rice paper by using silk residuals as raw materials - Google Patents
Method of preparing silk rice paper by using silk residuals as raw materials Download PDFInfo
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- 235000007164 Oryza sativa Nutrition 0.000 title claims abstract description 42
- 235000009566 rice Nutrition 0.000 title claims abstract description 42
- 239000002994 raw material Substances 0.000 title claims abstract description 24
- 240000007594 Oryza sativa Species 0.000 title 1
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- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 8
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- 229920002545 silicone oil Polymers 0.000 claims description 4
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 4
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Abstract
The invention discloses a method of preparing silk rice paper by using silk residuals as raw materials. The method is characterized in that the method comprises the following steps: (1) pretreatment of the raw materials: cooking the silk residuals, removing stains of the silk residuals by adding decontamination agent, adding water to the silk residuals after rinsing, freezing the silk residuals into silk residual ice cakes, performing shaving or slicing on the silk residual ice cakes to form crushed silk residuals, draining the silk residuals after being melted with water, performing degumming and decoloration on the drained silk residuals, rinsing in the water after the silk residuals are drained, and drying the silk residuals to form silk residual raw materials ready for use; and (2), mixing the silk residual raw materials ready for use with rice paper pulp according to the preset raw material mixing proportion to produce the silk rice paper by using the conventional rice paper making process. The production process is simple and very high in operability; on the premise that the fund is not increased, the standard and scale production is achieved; the method is environmentally friendly; and almost no mulberry silk is wasted.
Description
Technical field
The invention belongs to waste silk recycling technical field, being specifically related to a kind of is the method for feedstock production silk rice paper with silk pin silk.
Background technology
In the prior art, silk (like mulberry silk), silk article are weaved loss 2-3%, dyeing loss 3-5%, stamp loss 3-5% according to statistics weaving, producing natural wastage in the dyeing, stamp process.The silk of these losses in the past, silk fabric have silk spinning factory to use raw material as weaving spun silk fabric usually, or are used for cosmetic, for health care through extracting fibroin.The natural wastage of the hundred meters 3-5%s of mulberry silk in silk weaving, dyeing, stamp is a numeral that tool is big, and is in the past the silk of these natural wastage, very big to loss and the direct waste that silk causes through various processing.
Summary of the invention
It is the method for feedstock production silk rice paper with silk pin silk that the object of the invention is to provide a kind of, has solved the problems such as waste of silk pin silk in the prior art.
In order to solve these problems of the prior art, technical scheme provided by the invention is:
A kind of is the method for feedstock production silk rice paper with silk pin silk, it is characterized in that said method comprising the steps of:
(1) preliminary treatment of raw material: after silk pin silk carried out boiling; Add detergent and remove the spot of silk pin silk; In silk pin silk, inject water after the rinsing, the freezing silk pin silk ice cube of processing carries out water ice or slicing treatment to silk pin silk ice cube then; Form the silk pin silk after pulverizing, drain after the water fusion; The processing of coming unstuck earlier, decolour of silk pin silk after draining drains back rinsing in water then, and oven dry forms subsequent use silk pin silk raw material;
(2) subsequent use silk pin silk raw material and rice paper paper pulp are formed the silk rice paper by conventional rice paper preparation technology after by predetermined proportioning raw materials compatibility.
Preferably, the subsequent use silk pin silk raw material described in the said method and the weight ratio of rice paper paper pulp raw material are (3～5): (20～22).
Preferably, it is 100～105 ℃ that the middle silk pin silk of said method step (1) carries out stewing temperature, digestion time 3h ± 20min.
Preferably, the detergent that adds in the said method step (1) is 5% of a silk pin silk weight.
Preferably, the detergent that adds in the said method step (1) is selected from the VSZX-0321 of Jiangsu Province silk Science Institute.
Preferably, after water ice or the slicing treatment, use 100 purpose screen clothes to drain in the said method step (1).
Preferably; The decolouring treatment step that comes unstuck in the said method step (1) is following: the silk pin silk after will draining and water bath raio by weight are after mixing at 1: 20, warming while stirring, mixing speed 200～250 commentaries on classics/min; Heat up and divide two stages: when beginning to be warming up to 60-65 ℃, constant temperature 4h ± 10min; Add the scouring agent of the silicone oil of the kerosene of the soda ash of the silk pin silk weight 1% after draining, the silk pin silk weight 4% after draining, the silk pin silk weight 4% after draining, the silk pin silk weight 2% after draining then, be warming up to 100～105 ℃ of boiling 3h ± 10min.
Preferably, the middle scouring agent of said method step (1) is selected from the VSSN-0201 of Jiangsu Province silk Science Institute.
Preferably; After draining, in water, also to carry out preservative treatment after the rinsing in the said method step (1); Said anticorrosion step is included in the silk pin silk after the adding rinsing in the soak; The weight bath raio of the silk pin silk after soak and the rinsing is 1: 1, and the real silk fabric that contains pin silk weight 0.3% in the soak is prevented microbial inoculum, soak time 3h ± 20min with the real silk fabric of antioxidant, pin silk weight 0.2% with mildew-resistant with the real silk fabric of age resister, pin silk weight 3%.
Real silk fabric can select for use real silk fabric commonly used on the market with age resister such as styrenated phenol (Stgrenated Phenot) with age resister; Said real silk fabric can select for use real silk fabric commonly used on the market with antioxidant such as BHT with antioxidant; Said real silk fabric can select for use real silk fabric commonly used on the market with the anti-microbial inoculum of mildew-resistant with the anti-microbial inoculum of mildew-resistant, prevents microbial inoculum AA-83w like the mildew-resistant that Japan big phase chemistry company releases.
Since the silk of natural wastage, the kind of silk article difference, twist, and the difference of DENIER, color difference thereby technology are also different fully.The object of the invention is to provide a kind of silk rice paper production method, adopts silk pin silk, and after suitably handling, it is essential to meet the production of silk rice paper fully, meets silk rice paper all size.The appropriate location package management is drawn together through freezing, the plane that disappears, shearing, technology such as concise; Make the silk rice paper that produces meet the expert of calligraphy and painting fully; Light, heavy, slow, disease when painting and calligraphy are used painted the wieling the pen of China ink; Burnt, dense, withered, light, wet vary reaches ink or coloring effect with traditional superfine product rice-paper painting.Said silk pin silk is meant 2 percent to three normal foot silk of genus natural wastage in the weaving process: refer in particular to reeling, lead through, rewinding, shake winding, joint, the folding latitude is mended silk pin silks such as shelves.
With respect to scheme of the prior art, advantage of the present invention is:
Pass through in the technical scheme of the present invention silk pin silk is sheared with the water ice making method of environmental protection; The dust that machinery causes when having avoided conventional the recovery; The water of ice making can recycle fully, and silk, silk fabric that the present invention is used strictly say it is not have used new silk; Come unstuck, the decolour auxiliary agent of usefulness, all mildew-resistant of using when soaking, mothproof, anticorrosion, anti-mite, antibiotic; Antiultraviolet, auxiliary agent such as anti-oxidant, antistatic all are environmental protection does not have the product of harm to environment, all is the conventional products that buys easily on the market.
Be used to make the silk rice paper after technical scheme of the present invention reclaims silk pin silk and use raw material; No matter be that it reclaims technology, preparation side; The return-enclosure that comprises leftover pieces in the manufacturing silk rice paper process is reproduced; Its waste all is minimum minimum with loss as far as silk fiber, and mulberry silk is the natural fabric that has life intelligence pure after all, so uses raw material with mulberry silk through the silk rice paper that recovery preparation method of the present invention makes.After the processing, make it and rice paper paper pulp compatibility after become bump that water be prone to disperse, suspension is stable, silk with thread between can adsorpting aggregation, thixotropy, rheological characteristic be good, is to manufacture the superior raw material of high-quality silk rice paper.
The simple operability extra-heavy of production technology of the present invention need not to increase under the prerequisite of fund, realizes standardization, large-scale production, environmental protection, and the loss of mulberry silk is almost nil.Both fundamentally solved serious waste problem of pin filament length phase; Also met the requirement of painting and calligraphy rice paper papermaking process from material; No matter in superior rice paper, injected the intelligence of silk fiber again, be energy-conserving and environment-protective, cultureal value, painting and calligraphy quality, or market prospects unlimited potentiality of tool all.
The specific embodiment
Below in conjunction with specific embodiment such scheme is further specified.Should be understood that these embodiment are used to the present invention is described and are not limited to limit scope of the present invention.The implementation condition that adopts among the embodiment can be done further adjustment according to the condition of concrete producer, and not marked implementation condition is generally the condition in the normal experiment.
The preparation of embodiment 1 silk rice paper
Present embodiment prepares the silk rice paper according to following steps:
(1) boiling, rinse step:
Be 20% pin silk by bath raio (weight ratio): 80% water is placed on boiling in the rustless steel container with mulberry silk, digestion time 3h ± 20min; Boiling temperature 100-105 ℃; Stir on boiling limit, limit, and mixing speed 200-250 commentaries on classics/min adds detergent VSZX-0321 according to 5% of pin silk weight; Naturally after the cooling, pull silk fabrics out with the water extruding stem.Be 20% pin silk again by bath raio (weight ratio): 80% water, be placed on rinsing 30-50min in the clear water, pull out extract water after, shear the rectangle of growth 19cm * wide 15cm, prepare the water filling clamp dog and use.
(2) ice making, shearing step:
Earlier the pin silk is placed in the rustless steel container of long 19cm, wide 15cm, high 6cm, injects and put into the ice making refrigerator behind the clear water and process ice, take out the back and exempt to refuel luxury quick vertical full-automatic slicing machine with electric planer or 360FA; The bar that digs or be cut into thick 1.5m, long 19cm, wide 15cm is put into rustless steel container like ice cube, after waiting to ice nature and dissolving; Pick up with 100 purpose screen clothes filter solid carbon dioxide, be placed on again in the rustless steel container of long 19cm, wide 15cm, high 6cm, carry out ice making behind the injection clear water; The ice cube that will contain silk exempts to refuel luxury quick vertical full-automatic slicing machine with electric planer or 360FA, and the bar that digs or be cut into thick 1m, long 19cm, wide 15cm is put into rustless steel container like ice cube; After waiting to ice the nature dissolving, pick up, be placed on again in the rustless steel container of long 19cm, wide 15cm, high 6cm with 100 purpose screen clothes filter solid carbon dioxide; Carry out ice making after injecting clear water; The bar that digs or be cut into thick 0.5m, long 19cm, wide 15cm is put into rustless steel container like ice cube, after waiting to ice nature and fusing; Pick up with 100 purpose screen clothes filter solid carbon dioxide, prepare to come unstuck, decolour after all filter is done with water.
(3) step of decolouring, come unstuck:
The silk that filter is dried is 20% pin silk by bath raio (weight ratio): 80% water is placed on silk in the rustless steel container warming while stirring; Mixing speed 200-250 commentaries on classics/min; Heat up to divide two stages, the phase I is when being warming up to 60-65 ℃, constant temperature 4h ± 10min; The weight ratio that second stage adds auxiliary agent is to calculate according to the ratio of 20% pin silk and 80% water.Add soda ash (1%), kerosene (4%), silicone oil (4%), scouring agent (2%) in the ratio that accounts for pin silk percentage by weight successively, be warming up to 100-105 ℃ of boiling 3h ± 10min, pour into and treat nature filter solid carbon dioxide preparation rinsing in the stainless screen cloth.
(4) rinse step:
The silk that filter is dried is 10% pin silk by bath raio (weight ratio): 90% water; Rinsing 1h ± 10min in clear water,, pour into and treat nature filter solid carbon dioxide in the stainless screen cloth; Be 10% pin silk again by bath raio (weight ratio): 90% water; Silk is placed in the rustless steel container, is warming up to 100-105 ℃ of boiling 1h ± 10min, pour into and treat nature filter solid carbon dioxide preparation immersion in the stainless screen cloth.
(5) soaking step:
Soaking step is by the pin silk that by bath raio (weight ratio) is 50%: 50% water soaks; The silk that drains is immersed in the rustless steel container; Institute's adding assistant weight ratio is the percentage calculation according to pin silk weight, add successively 0.3% real silk fabric with age resister, 3% real silk fabric with antioxidant, 0.2% real silk fabric with the anti-microbial inoculum of mildew-resistant.Soak time 3h ± 20min pours in the stainless silk piece mould water squeezed to do and prepares to dry.
(6) bake step:
Water is squeezed dried spinning cake or silk piece, send in the baking oven and bake, baking temperature 40-50 ℃, bake time 3h ± 20min, the spinning cake that takes out drying and moulding is prepared slurrying and is used.
(7) slurrying step:
The raw material components of silk rice paper adopts by weight percentage:
Jingxian County rice paper paper pulp 65.00%;
Silk pin silk spinning cake 25.00%;
Deionized water 10.00%.
Composite stirring is a stirring at low speed, stirs speed of a motor vehicle 1min/200 and changes, and mixing time 10min ± 5min, composite good silk rice paper paper pulp is placed in the rustless steel container subsequent use.
(8) copy the paper step:
With silk rice paper paper pulp by 1% with the part by weight of water 99%, the manual limit blowing that stirs in limit is gone in the papermaking groove, copying paper, wet pressing, lead paper, airing by routine; Scald through pressing again; Pressure is scalded 100 ℃ ± 10 ℃ of temperature, and the boiling hot speed of a motor vehicle 1min/ of pressure (8m ± 2m), the boiling hot pressure of pressure (3kg ± 2kg)/m
2, be cut on the receipts limit need big or small silk rice paper be finished product.
The preparation of embodiment 2 silk rice paper
Present embodiment prepares the silk rice paper according to following steps:
(1) boiling, rinsing
Be 10% pin silk by bath raio (weight ratio): 90% water is placed on boiling in the rustless steel container, digestion time 3h ± 20min with the Saunas silk fabric of dyeing, stamp normal loss; Boiling temperature 100-105 ℃; Stir on boiling limit, limit, and mixing speed 200-250 commentaries on classics/min adds detergent VSZX-0321 according to 5% of silk pin silk weight; Naturally after the cooling, pull silk fabrics out with the water extruding stem.Be 50% pin silk again by bath raio (weight ratio): 50% water, be placed on rinsing 30-50min in the clear water, pull out extract water after, shear the rectangle of growth 19cm, wide 15cm, prepare the water filling clamp dog and use.
(2) ice making, shearing step
Be placed in the rustless steel container of long 19cm, wide 15cm, high 6cm shearing good fabric, inject and put into ice machine behind the clear water and process ice, take out the back and exempt to refuel luxury quick vertical full-automatic slicing machine with electric planer or 360FA; The bar that digs or be cut into thick 1.5m, long 19cm, wide 15cm is put into rustless steel container like ice cube, after waiting to ice nature and dissolving; Pick up with 100 purpose screen clothes filter solid carbon dioxide, be placed on again in the rustless steel container of long 19cm, wide 15cm, high 6cm, carry out ice making behind the injection clear water; The ice cube that will contain silk exempts to refuel luxury quick vertical full-automatic slicing machine with electric planer or 360FA, and the bar that digs or be cut into thick 1m, long 19cm, wide 15cm is put into rustless steel container like ice cube; After waiting to ice the nature dissolving, pick up, be placed on again in the rustless steel container of long 19cm, wide 15cm, high 6cm with 100 purpose screen clothes filter solid carbon dioxide; Carry out ice making after injecting clear water; Dig or 360FA exempts to refuel bar that luxury quick vertical full-automatic slicing machine is cut into thick 0.5m, long 19cm, wide 15cm like ice cube, put into rustless steel container, after waiting to ice nature and fusing; Pick up with 100 purpose screen clothes filter solid carbon dioxide, prepare to come unstuck, decolour after all filter is done with water.
(3) step of decolouring, come unstuck
The silk fabrics that filter is dried is 10% pin silk by bath raio (weight ratio): 90% water; Be placed in the rustless steel container warming while stirring, mixing speed 200-250 commentaries on classics/min; Heat up and divide two stages: the phase I: when being warming up to 60-65 ℃, constant temperature 4h ± 10min; Second stage: according to silk pin silk weight; Add soda ash (1%), kerosene (4%), silicone oil (4%), scouring agent (2%) in the ratio that accounts for pin silk percentage by weight; Be warming up to 100-105 ℃ of boiling 3h ± 10min, pour into and treat nature filter solid carbon dioxide preparation rinsing in the stainless screen cloth.
(4) rinse step
The silk that filter is dried is 10% pin silk by bath raio (weight ratio): 90% water; Rinsing 1h ± 10min in clear water,, pour into and treat nature filter solid carbon dioxide in the stainless screen cloth; Be 10% pin silk again by bath raio (weight ratio): 90% water; Silk is placed in the rustless steel container, is warming up to 100-105 ℃ of boiling 1h ± 10min, pour into and treat nature filter solid carbon dioxide preparation immersion in the stainless screen cloth.
(5) soaking step
Be 50% pin silk by bath raio (weight ratio): 50% water soaks; The silk that drains is immersed in the rustless steel container; Institute's adding assistant weight ratio is the percentage calculation according to pin silk weight, adds 0.3% real silk fabric successively and prevents microbial inoculum with antioxidant, 0.2% real silk fabric with mildew-resistant with age resister, 3% real silk fabric.Soak time 3h ± 20min pours in the stainless silk piece mould water squeezed to do and prepares to dry.
(6) bake step
Water is squeezed dried spinning cake or silk piece, send in the baking oven and bake, baking temperature 40-50 ℃, bake time 3h ± 20min, the spinning cake that takes out drying and moulding is prepared slurrying and is used.
(7) slurrying step
The raw material components of silk rice paper adopts by weight percentage:
Jingxian County rice paper paper pulp 80.00%;
Silk pin silk spinning cake 15.00%;
Deionized water 5.00%.
(8) copy the paper step
With silk rice paper paper pulp in 1% with the ratio of water 99%, the manual limit blowing that stirs in limit is gone in the papermaking groove, copying paper, wet pressing, lead paper, airing by routine; Scald through pressing again; Pressure is scalded 100 ℃ ± 10 ℃ of temperature, and the boiling hot speed of a motor vehicle 1min/ of pressure (8m ± 2m), the boiling hot pressure of pressure (3kg ± 2kg)/m
2, be cut on the receipts limit need big or small silk rice paper be finished product.
Above-mentioned instance only is explanation technical conceive of the present invention and characteristics, and its purpose is to let the people who is familiar with this technology can understand content of the present invention and enforcement according to this, can not limit protection scope of the present invention with this.All equivalent transformations that spirit is done according to the present invention or modification all should be encompassed within protection scope of the present invention.
Claims (9)
1. one kind is the method for feedstock production silk rice paper with silk pin silk, it is characterized in that said method comprising the steps of:
(1) preliminary treatment of raw material: after silk pin silk carried out boiling; Add detergent and remove the spot of silk pin silk; In silk pin silk, inject water after the rinsing, the freezing silk pin silk ice cube of processing carries out water ice or slicing treatment to silk pin silk ice cube then; Form the silk pin silk after pulverizing, drain after the water fusion; The processing of coming unstuck earlier, decolour of silk pin silk after draining drains back rinsing in water then, and oven dry forms subsequent use silk pin silk raw material;
(2) subsequent use silk pin silk raw material and rice paper paper pulp are formed the silk rice paper by conventional rice paper preparation technology after by predetermined proportioning raw materials compatibility.
2. method according to claim 1 is characterized in that the weight ratio of silk pin silk raw material subsequent use described in the said method and rice paper paper pulp raw material is (3～5): (20～22).
3. method according to claim 1 is characterized in that it is 100～105 ℃ that the middle silk pin silk of said method step (1) carries out stewing temperature, digestion time 3h ± 20min.
4. method according to claim 1 is characterized in that the detergent that adds in the said method step (1) is 5% of a silk pin silk weight.
5. method according to claim 1 is characterized in that the detergent that adds in the said method step (1) is selected from the VSZX-0321 of Jiangsu Province silk Science Institute.
6. method according to claim 1, it is characterized in that in the said method step (1) water ice or slicing treatment after, use 100 purpose screen clothes to drain.
7. method according to claim 1; The decolouring treatment step that it is characterized in that coming unstuck in the said method step (1) is following: the silk pin silk after will draining and water bath raio by weight are after 1:20 mixes; Warming while stirring; Mixing speed 200～250 commentaries on classics/min, heat up and divide two stages: when beginning to be warming up to 60-65 ℃, constant temperature 4h ± 10min; Add the scouring agent of the silicone oil of the kerosene of the soda ash of the silk pin silk weight 1% after draining, the silk pin silk weight 4% after draining, the silk pin silk weight 4% after draining, the silk pin silk weight 2% after draining then, be warming up to 100～105 ℃ of boiling 3h ± 10min.
8. method according to claim 7 is characterized in that the middle scouring agent of said method step (1) is selected from the VSSN-0201 of Jiangsu Province silk Science Institute.
9. method according to claim 7; It is characterized in that after draining, in water, also will carrying out preservative treatment after the rinsing in the said method step (1); Said anticorrosion step is included in the silk pin silk after the adding rinsing in the soak; The weight bath raio of the silk pin silk after soak and the rinsing is 1:1; The real silk fabric that contains pin silk weight 0.3% in the soak is prevented microbial inoculum, soak time 3h ± 20min with the real silk fabric of antioxidant, pin silk weight 0.2% with mildew-resistant with the real silk fabric of age resister, pin silk weight 3%.
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| CN106930132A (en) * | 2017-04-24 | 2017-07-07 | 济南大学 | It is a kind of based on the pulping equipment without water injection type materialization pulping |
| CN105544284B (en) * | 2015-12-15 | 2017-07-11 | 浙江理工大学 | A kind of medical silk paper and preparation method thereof |
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| CN111254734A (en) * | 2020-03-17 | 2020-06-09 | 四川工商职业技术学院 | Process technology for producing painting and calligraphy paper by using waste silk |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105544284B (en) * | 2015-12-15 | 2017-07-11 | 浙江理工大学 | A kind of medical silk paper and preparation method thereof |
| CN106283837A (en) * | 2016-07-29 | 2017-01-04 | 浙江商业职业技术学院 | China picture-character paper and processing technology thereof |
| CN106283837B (en) * | 2016-07-29 | 2017-11-10 | 浙江商业职业技术学院 | China picture-character paper and its manufacture craft |
| CN106930132A (en) * | 2017-04-24 | 2017-07-07 | 济南大学 | It is a kind of based on the pulping equipment without water injection type materialization pulping |
| CN106930132B (en) * | 2017-04-24 | 2023-07-04 | 济南大学 | Pulping equipment based on water-injection-free materialized pulping |
| CN108221119A (en) * | 2017-12-26 | 2018-06-29 | 杭州万事利丝绸文化股份有限公司 | A kind of method of manufacturing technology of the no alum silkworm tiffany silk fabric of painting and calligraphy |
| CN111254734A (en) * | 2020-03-17 | 2020-06-09 | 四川工商职业技术学院 | Process technology for producing painting and calligraphy paper by using waste silk |
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