CN102561098B - Method of preparing silk rice paper by using silk residuals as raw materials - Google Patents
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Abstract
The invention discloses a method of preparing silk rice paper by using silk residuals as raw materials. The method is characterized in that the method comprises the following steps: (1) pretreatment of the raw materials: cooking the silk residuals, removing stains of the silk residuals by adding decontamination agent, adding water to the silk residuals after rinsing, freezing the silk residuals into silk residual ice cakes, performing shaving or slicing on the silk residual ice cakes to form crushed silk residuals, draining the silk residuals after being melted with water, performing degumming and decoloration on the drained silk residuals, rinsing in the water after the silk residuals are drained, and drying the silk residuals to form silk residual raw materials ready for use; and (2), mixing the silk residual raw materials ready for use with rice paper pulp according to the preset raw material mixing proportion to produce the silk rice paper by using the conventional rice paper making process. The production process is simple and very high in operability; on the premise that the fund is not increased, the standard and scale production is achieved; the method is environmentally friendly; and almost no mulberry silk is wasted.
Description
Technical field
The invention belongs to waste silk recycling technical field, be specifically related to a kind of method of preparing natural silk rice paper taking silk pin silk as raw material.
Background technology
In prior art, silk (as mulberry silk), silk product produce natural wastage weaving, in dyeing, stamp process, weave according to statistics loss 2-3%, dyeing loss 3-5%, stamp loss 3-5%.The silk of these losses in the past, silk fabric have silk spinning factory conventionally as weaving spun silk fabric raw material, or by extracting fibroin for cosmetic, for health care.The natural wastage of the hundred meters 3-5%s of mulberry silk in silk weaving, dyeing, stamp, is a numeral that tool is large, and in the past the silk of these natural wastage, loss silk being caused by various processing and directly waste are very large.
Summary of the invention
The object of the invention is to provide a kind of method of preparing natural silk rice paper taking silk pin silk as raw material, solved the problems such as the waste of silk pin silk in prior art.
In order to solve these problems of the prior art, technical scheme provided by the invention is:
A method of preparing natural silk rice paper taking silk pin silk as raw material, is characterized in that said method comprising the steps of:
(1) preliminary treatment of raw material: silk pin silk is carried out after boiling, add detergent to remove the spot of silk pin silk, after rinsing in silk pin silk injected water, the freezing silk pin silk ice cube of making, then silk pin silk ice cube is carried out to water ice or slicing treatment, form the silk pin silk after pulverizing, water drains after melting; The processing of first coming unstuck, decolour of silk pin silk after draining, rinsing in water after then draining, dries and forms silk pin silk raw material for subsequent use;
(2) by silk pin silk raw material for subsequent use and rice paper paper pulp by predetermined raw material proportioning compatibility after routinely rice paper preparation technology form natural silk rice paper.
Preferably, silk pin silk raw material for subsequent use described in described method and the weight ratio of rice paper paper pulp raw material are (3～5): (20～22).
Preferably, the temperature that the middle silk pin silk of described method step (1) carries out boiling is 100～105 DEG C, digestion time 3h ± 20min.
Preferably, the detergent adding in described method step (1) is 5% of silk pin silk weight.
Preferably, the detergent adding in described method step (1) is selected from the VSZX-0321 of silk Science Institute of Jiangsu Province.
Preferably, in described method step (1), after water ice or slicing treatment, use 100 object screen clothes to drain.
Preferably, the decolouring treatment step that comes unstuck in described method step (1) is as follows: by the silk pin silk after draining and water by weight bath raio be mix at 1: 20 after, warming while stirring, turn/min of mixing speed 200～250, heat up point two stages: while starting to be warming up to 60-65 DEG C, constant temperature 4h ± 10min; Then the scouring agent that adds the silicone oil of the kerosene of the soda ash of the silk pin silk weight 1% after draining, silk pin silk weight 4% after draining, silk pin silk weight 4% after draining, silk pin silk weight 2% after draining, is warming up to 100～105 DEG C of boiling 3h ± 10min.
Preferably, the middle scouring agent of described method step (1) is selected from the VSSN-0201 of silk Science Institute of Jiangsu Province.
Preferably, in described method step (1), after draining, in water, after rinsing, also to carry out preservative treatment, described anticorrosion step is included in and in soak, adds the silk pin silk after rinsing, the weight bath raio of the silk pin silk after soak and rinsing is 1: 1, in soak, contain the real silk fabric germproof matter of antioxidant, pin silk weight 0.2% for real silk fabric of age resister, pin silk weight 3% for real silk fabric of pin silk weight 0.3%, soak time 3h ± 20min.
Real silk fabric can select conventional on the market real silk fabric age resister as styrenated phenol (Stgrenated Phenot) with age resister; Described real silk fabric can select conventional on the market real silk fabric antioxidant as BHT with antioxidant; Described real silk fabric can be selected on the market conventional real silk fabric germproof matter with germproof matter, the germproof matter AA-83w that as large in Japan phase chemistry company releases.
Due to the silk of natural wastage, the kind difference of silk product, twist, the difference of DENIER, color difference thereby technique are also completely different.The object of the invention is to provide a kind of natural silk rice paper production method, adopts silk pin silk, after suitably processing, meets natural silk rice paper production completely essential, meets natural silk rice paper all size.Suitably process and comprise by freezing, the plane that disappears, shearing, the technique such as concise, make the natural silk rice paper producing meet expert of calligraphy and painting completely, painting and calligraphy are light, heavy, slow, disease when painted wieling the pen with China ink, burnt, dense, withered, light, wet random variation, reaches ink or coloring effect with traditional superfine product rice-paper painting.Described silk pin silk refers to 2 percent to three normal foot silk of genus natural wastage in weaving process: refer in particular to reeling, lead through, rewinding, shake winding, joint, folding latitude is mended the silk pin silks such as shelves.
With respect to scheme of the prior art, advantage of the present invention is:
In technical solution of the present invention, pass through silk pin silk to shear with the water ice making method of environmental protection, the dust that while having avoided conventional recovery, machinery causes, the water of ice making can recycle completely, silk, silk fabric that the present invention is used, strictly say it is there is no used new silk, come unstuck, the decolour auxiliary agent of use, all mildew-resistant, mothproof, anticorrosion, the anti-mite, antibacterial used while soaking, antiultraviolet, the auxiliary agent such as anti-oxidant, antistatic, the product without harm that is all environmental protection to environment is all the conventional products easily buying on market.
Technical solution of the present invention by silk pin silk reclaim after for the manufacture of natural silk rice paper raw material, no matter be its recovery process, preparation side, the return-enclosure that comprises leftover pieces in manufacture natural silk rice paper process is reproduced, all minimum minimum for its waste of silk fiber and loss, mulberry silk is the natural fabric that has life intelligence pure after all, the natural silk rice paper raw material therefore making by recovery preparation method of the present invention with mulberry silk.After processing, make it and rice paper paper pulp compatibility after become touch that water easily disperses, suspension is stable, silk with thread between can adsorpting aggregation, thixotropy, rheological characteristic be good, is to manufacture the superior raw material of high-quality natural silk rice paper.
The simple operability extra-heavy of production technology of the present invention, without increasing under the prerequisite of fund, realizes standardization, large-scale production, environmental protection, and the loss of mulberry silk is almost nil.Both fundamentally solved serious waste problem of pin filament length phase, also met the requirement of painting and calligraphy Xuan paper technique from material, no matter in superior rice paper, injected again the intelligence of silk fiber, be energy-conserving and environment-protective, cultureal value, painting and calligraphy quality, or all unlimited potentiality of tool of market prospects.
Detailed description of the invention
Below in conjunction with specific embodiment, such scheme is described further.Should be understood that these embodiment are not limited to limit the scope of the invention for the present invention is described.The implementation condition adopting in embodiment can be done further adjustment according to the condition of concrete producer, and not marked implementation condition is generally the condition in normal experiment.
The preparation of embodiment 1 natural silk rice paper
The present embodiment is prepared natural silk rice paper in accordance with the following steps:
(1) boiling, rinse step:
The pin silk that is 20% by bath raio (weight ratio): 80% water, mulberry silk is placed on to boiling in rustless steel container, digestion time 3h ± 20min, boiling temperature 100-105 DEG C, stir on boiling limit, limit, and turn/min of mixing speed 200-250, adds detergent VSZX-0321 according to 5% of pin silk weight, naturally, after cooling, pull silk fabrics out by water extruding stem.The pin silk that is 20% by bath raio (weight ratio) again: 80% water, be placed on rinsing 30-50min in clear water, pull out and extract after water, shear the rectangle of growth 19cm × wide 15cm, prepare water filling clamp dog and use.
(2) ice making, shearing step:
First pin silk is placed on to long 19cm, wide 15cm, in the rustless steel container of high 6cm, inject and put into ice making refrigerator after clear water and make ice, after taking-up, exempt to refuel luxury quick vertical type full automatic slicer with electric planer or 360FA, dig or be cut into thick 1.5m, long 19cm, the bar of wide 15cm, like ice cube, is put into rustless steel container, after ice dissolves naturally, is filtered dry water picks up with 100 object screen clothes, then be placed on long 19cm, wide 15cm, in the rustless steel container of high 6cm, inject after clear water and carry out ice making, the ice cube that contains silk is exempted to refuel luxury quick vertical type full automatic slicer with electric planer or 360FA, dig or be cut into thick 1m, long 19cm, the bar of wide 15cm, like ice cube, is put into rustless steel container, after ice dissolves naturally, is filtered dry water picks up with 100 object screen clothes, then be placed on long 19cm, wide 15cm, in the rustless steel container of high 6cm, after injection clear water, carry out ice making, dig or be cut into thick 0.5m, long 19cm, the bar of wide 15cm, like ice cube, is put into rustless steel container, after ice melts naturally, is filtered dry water picks up with 100 object screen clothes, water is all filtered dry to rear preparation and comes unstuck, decolouring.
(3) step of decolouring, come unstuck:
The pin silk that is 20% by bath raio (weight ratio) by the silk being filtered dry: 80% water, is placed on silk in rustless steel container warming while stirring, turn/min of mixing speed 200-250, in point two stages of intensification, the first stage is while being warming up to 60-65 DEG C, constant temperature 4h ± 10min; It is to calculate according to the ratio of 20% pin silk and 80% water that second stage adds the weight ratio of auxiliary agent.Add soda ash (1%), kerosene (4%), silicone oil (4%), scouring agent (2%) in the ratio that accounts for pin silk percentage by weight successively, be warming up to 100-105 DEG C of boiling 3h ± 10min, pour in stainless screen cloth and treat that nature is filtered dry level for rinsing.
(4) rinse step:
The pin silk that is 10% by bath raio (weight ratio) by the silk being filtered dry: 90% water, rinsing 1h ± 10min in clear water, pour in stainless screen cloth and treat that nature is filtered dry water, the pin silk that is 10% by bath raio (weight ratio) again: 90% water, silk is placed in rustless steel container, is warming up to 100-105 DEG C of boiling 1h ± 10min, pour in stainless screen cloth and treat that nature is filtered dry the standby immersion of level.
(5) soaking step:
Soaking step is by the pin silk that is 50% by bath raio (weight ratio): 50% water soaks, by the Silk Soaking draining in rustless steel container, institute's adding assistant weight ratio is the percentage calculation according to pin silk weight, adds successively 0.3% age resister for real silk fabric, 3% antioxidant for real silk fabric, 0.2% real silk fabric germproof matter.Soak time 3h ± 20min, pours into and in stainless silk piece mould, water is squeezed to dry preparation and dry.
(6) bake step:
Water is squeezed to dry spinning cake or silk piece, send in baking oven and bake, baking temperature 40-50 DEG C, bakes time 3h ± 20min, takes out the spinning cake of drying and moulding and prepares slurrying use.
(7) slurrying step:
The raw material components of natural silk rice paper adopts by weight percentage:
Jingxian County rice paper paper pulp 65.00%;
Silk pin silk spinning cake 25.00%;
Deionized water 10.00%.
Composite stirring is stirring at low speed, stirs speed of a motor vehicle 1min/200 and turns, and mixing time 10min ± 5min, composite good natural silk rice paper paper pulp, is placed in rustless steel container for subsequent use.
(8) copy paper step:
By natural silk rice paper paper pulp by 1% and the part by weight of water 99%, the manual limit blowing that stirs in limit enters in papermaking groove, copy paper, wet pressing routinely, lead paper, airing, again through pressing, 100 DEG C ± 10 DEG C of pressing temperature, pressing speed of a motor vehicle 1min/ (8m ± 2m), pressing pressure (3kg ± 2kg)/m
2, be cut on receipts limit need to big or small natural silk rice paper be finished product.
The preparation of embodiment 2 natural silk rice papers
The present embodiment is prepared natural silk rice paper in accordance with the following steps:
(1) boiling, rinsing
The pin silk that is 10% by bath raio (weight ratio): 90% water, the Saunas silk fabric of dyeing, stamp normal loss is placed on to boiling in rustless steel container, digestion time 3h ± 20min, boiling temperature 100-105 DEG C, stir on boiling limit, limit, and turn/min of mixing speed 200-250, adds detergent VSZX-0321 according to 5% of silk pin silk weight, naturally, after cooling, pull silk fabrics out by water extruding stem.The pin silk that is 50% by bath raio (weight ratio) again: 50% water, be placed on rinsing 30-50min in clear water, pull out and extract after water, shear the rectangle of growth 19cm, wide 15cm, prepare water filling clamp dog and use.
(2) ice making, shearing step
The fabric of having sheared is placed on to long 19cm, wide 15cm, in the rustless steel container of high 6cm, inject and put into ice machine after clear water and make ice, after taking-up, exempt to refuel luxury quick vertical type full automatic slicer with electric planer or 360FA, dig or be cut into thick 1.5m, long 19cm, the bar of wide 15cm, like ice cube, is put into rustless steel container, after ice dissolves naturally, is filtered dry water picks up with 100 object screen clothes, then be placed on long 19cm, wide 15cm, in the rustless steel container of high 6cm, inject after clear water and carry out ice making, the ice cube that contains silk is exempted to refuel luxury quick vertical type full automatic slicer with electric planer or 360FA, dig or be cut into thick 1m, long 19cm, the bar of wide 15cm, like ice cube, is put into rustless steel container, after ice dissolves naturally, is filtered dry water picks up with 100 object screen clothes, then be placed on long 19cm, wide 15cm, in the rustless steel container of high 6cm, inject after clear water and carry out ice making, plane or 360FA exempt to refuel luxury quick vertical type full automatic slicer and are cut into thick 0.5m, long 19cm, the bar of wide 15cm, like ice cube, is put into rustless steel container, after ice melts naturally, is filtered dry water picks up with 100 object screen clothes, water is all filtered dry to rear preparation and comes unstuck, decolouring.
(3) step of decolouring, come unstuck
The pin silk that is 10% by bath raio (weight ratio) by the silk fabrics being filtered dry: 90% water, be placed in rustless steel container warming while stirring, turn/min of mixing speed 200-250, heat up point two stages: the first stage: while being warming up to 60-65 DEG C, constant temperature 4h ± 10min; Second stage: according to silk pin silk weight, add soda ash (1%), kerosene (4%), silicone oil (4%), scouring agent (2%) in the ratio that accounts for pin silk percentage by weight, be warming up to 100-105 DEG C of boiling 3h ± 10min, pour in stainless screen cloth and treat that nature is filtered dry level for rinsing.
(4) rinse step
The pin silk that is 10% by bath raio (weight ratio) by the silk being filtered dry: 90% water, rinsing 1h ± 10min in clear water, pour in stainless screen cloth and treat that nature is filtered dry water, the pin silk that is 10% by bath raio (weight ratio) again: 90% water, silk is placed in rustless steel container, is warming up to 100-105 DEG C of boiling 1h ± 10min, pour in stainless screen cloth and treat that nature is filtered dry the standby immersion of level.
(5) soaking step
The pin silk that is 50% by bath raio (weight ratio): 50% water soaks, by the Silk Soaking draining in rustless steel container, institute's adding assistant weight ratio is the percentage calculation according to pin silk weight, adds successively 0.3% age resister for real silk fabric, 3% antioxidant for real silk fabric, 0.2% real silk fabric germproof matter.Soak time 3h ± 20min, pours into and in stainless silk piece mould, water is squeezed to dry preparation and dry.
(6) bake step
Water is squeezed to dry spinning cake or silk piece, send in baking oven and bake, baking temperature 40-50 DEG C, bakes time 3h ± 20min, takes out the spinning cake of drying and moulding and prepares slurrying use.
(7) slurrying step
The raw material components of natural silk rice paper adopts by weight percentage:
Jingxian County rice paper paper pulp 80.00%;
Silk pin silk spinning cake 15.00%;
Deionized water 5.00%.
(8) copy paper step
By natural silk rice paper paper pulp in 1% and the ratio of water 99%, the manual limit blowing that stirs in limit enters in papermaking groove, copy paper, wet pressing routinely, lead paper, airing, again through pressing, 100 DEG C ± 10 DEG C of pressing temperature, pressing speed of a motor vehicle 1min/ (8m ± 2m), pressing pressure (3kg ± 2kg)/m
2, be cut on receipts limit need to big or small natural silk rice paper be finished product.
Above-mentioned example is only explanation technical conceive of the present invention and feature, and its object is to allow person skilled in the art can understand content of the present invention and implement according to this, can not limit the scope of the invention with this.All equivalent transformations that Spirit Essence does according to the present invention or modification, within all should being encompassed in protection scope of the present invention.
Claims (5)
1. a method of preparing natural silk rice paper taking silk pin silk as raw material, is characterized in that said method comprising the steps of:
(1) preliminary treatment of raw material: silk pin silk is carried out after boiling, add detergent to remove the spot of silk pin silk, after rinsing in silk pin silk injected water, the freezing silk pin silk ice cube of making, then silk pin silk ice cube is carried out to water ice or slicing treatment, form the silk pin silk after pulverizing, water drains after melting; The processing of first coming unstuck, decolour of silk pin silk after draining, rinsing in water after then draining, dries and forms silk pin silk raw material for subsequent use; Wherein silk pin silk ice cube, after water ice or slicing treatment, uses 100 object screen clothes to drain; The decolouring treatment step that wherein comes unstuck is as follows: by the silk pin silk after draining and water by weight bath raio be after 1:20 mixes, warming while stirring, turn/min of mixing speed 200～250, intensification divides two stages: while starting to be warming up to 60-65 DEG C, constant temperature 4h ± 10min; Then the scouring agent that adds the silicone oil of the kerosene of the soda ash of the silk pin silk weight 1% after draining, silk pin silk weight 4% after draining, silk pin silk weight 4% after draining, silk pin silk weight 2% after draining, is warming up to 100～105 DEG C of boiling 3h ± 10min;
(2) by silk pin silk raw material for subsequent use and rice paper paper pulp by predetermined raw material proportioning compatibility after routinely rice paper preparation technology form natural silk rice paper.
2. method according to claim 1, the weight ratio that it is characterized in that silk pin silk raw material for subsequent use described in described method and rice paper paper pulp raw material is (3～5): (20～22).
3. method according to claim 1, is characterized in that the temperature that the middle silk pin silk of described method step (1) carries out boiling is 100～105 DEG C, digestion time 3h ± 20min.
4. method according to claim 1, is characterized in that the detergent adding in described method step (1) is 5% of silk pin silk weight.
5. method according to claim 1, it is characterized in that after draining, in water, after rinsing, also will carrying out in described method step (1) preservative treatment, described anticorrosion step is included in and in soak, adds the silk pin silk after rinsing, the weight bath raio of the silk pin silk after soak and rinsing is 1:1, in soak, contain the real silk fabric germproof matter of antioxidant, pin silk weight 0.2% for real silk fabric of age resister, pin silk weight 3% for real silk fabric of pin silk weight 0.3%, soak time 3h ± 20min.
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| CN105544284B (en) * | 2015-12-15 | 2017-07-11 | 浙江理工大学 | A kind of medical silk paper and preparation method thereof |
| CN106283837B (en) * | 2016-07-29 | 2017-11-10 | 浙江商业职业技术学院 | China picture-character paper and its manufacture craft |
| CN106930132B (en) * | 2017-04-24 | 2023-07-04 | 济南大学 | Pulping equipment based on water-injection-free materialized pulping |
| CN108221119B (en) * | 2017-12-26 | 2021-02-26 | 杭州万事利丝绸文化股份有限公司 | Method for manufacturing alum-free mulberry silk for painting and calligraphy |
| CN111254734A (en) * | 2020-03-17 | 2020-06-09 | 四川工商职业技术学院 | Process technology for producing painting and calligraphy paper by using waste silk |
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| CN101892608A (en) * | 2010-04-22 | 2010-11-24 | 浙江科技学院 | Process for producing sterilization mask paper by using silk offcut |
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| Publication number | Priority date | Publication date | Assignee | Title |
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