CN102550820A - Garlic skin extract prepared by using petroleum ether and preparation method and application thereof - Google Patents
Garlic skin extract prepared by using petroleum ether and preparation method and application thereof Download PDFInfo
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- CN102550820A CN102550820A CN2012100024242A CN201210002424A CN102550820A CN 102550820 A CN102550820 A CN 102550820A CN 2012100024242 A CN2012100024242 A CN 2012100024242A CN 201210002424 A CN201210002424 A CN 201210002424A CN 102550820 A CN102550820 A CN 102550820A
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- benzinum
- bulbus allii
- cortex bulbus
- medicinal extract
- garlic
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
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Abstract
The invention discloses garlic skin extract prepared by using petroleum ether and a preparation method and application thereof. Garlic skins and the petroleum ether are mixed evenly to obtain required extract through extraction, solid-liquid separation, distillation and concentration. 0.05-0.15% of garlic skin extract prepared by using the petroleum ether is added into feed by weight of daily livestock ration, and a feeding test result shows that the garlic skin extract has good growth promoting and weight increasing effects on broiler chicken, piglets and growing pigs. Due to the fact that the garlic skin extract prepared by using the petroleum ether enables active components to be concentrated, a large quantity of crude fiber and coarse hard materials in the garlic skins are decreased, absorbing and utilization of animals are facilitated, using amount is reduced, and the garlic skin extract is rich in fragrance, better in taste compared with the garlic skins and enables livestock to be happy to eat. A new way is opened for development and utilization of waste garlic skins.
Description
Technical field
The invention belongs to the feed addictive preparing technical field, be specifically related to a kind of Cortex Bulbus Allii benzinum and extract medicinal extract.Simultaneously, the invention still further relates to this extract making method and the application in feed addictive thereof.
Background technology
Garlic has that promoting the circulation of qi stagnates, warming spleen and stomach, detoxifcation, desinsection, end effect such as dysentery, and two conducts of " People's Republic of China's veterinary drug allusion quotation " in 2010 version herbal medicine commonly used records, and is used for the slow grass of livestock and poultry not eat tripe distention and fullness in the abdomen, diarrhea, abdominal pain due to enterositosis, fish enteritis.At present domestic have allicin, garlic products to be used for livestock and poultry and aquaculture, and its food calling, growth promotion effect are obvious, and aquaculture limits the use of antibiotic especially in recent years, and garlic is as the substitute of antiseptic, and research of its development and use garlic is more deep.
Contain nutrients such as very high protein and amino acid and calcium, zinc, iron, copper in the garlic, make it to be not only the special purpose as disease preventing and treating, the utilization of its nutritive value has the double-deck effect of nutrition and disease preventing and treating for livestock and poultry and aquaculture.
Cortex Bulbus Allii to contain composition similar basically with garlic, the accessory substance as garlic processing at present all as offal treatment, not only causes the wasting of resources, causes severe contamination to surrounding enviroment simultaneously.
Find that through Cortex Bulbus Allii being detected the back removing Cortex Bulbus Allii, to be rich in cellulose, protopectin and cutin class material more, other nutritional labelings are similar basically with garlic rice, only in its content difference to some extent, compare through detection Cortex Bulbus Allii and garlic rice, and its result is following:
Cortex Bulbus Allii and garlic rice part composition are relatively
| Project | Cortex Bulbus Allii (aquatic foods) | Garlic rice (aquatic foods) |
| Moisture % | 68.50 | 72.00 |
| Thick protein % | 4.82 | 6.00 |
| Crude fibre % | 1.60 | 0.80 |
| Coarse ash % | 2.20 | 1.40 |
| Total phosphorus % | 0.12 | 0.20 |
| Carbohydrate % | 21.20 | 23.00 |
| Total amino acid % | 2.72 | 2.96 |
| Allicin % | 0.11 | 0.418 |
Except that above-mentioned nutritional labeling, still contain multiple element pledges such as vitamin and calcium, iron, zinc, copper, potassium, sodium, magnesium in the Cortex Bulbus Allii.
Cortex Bulbus Allii among the people have it is minced the custom of feeding chicken, feeding fish; Observe its chicken crowd and can find out that to the voracity property of garlic skin its food calling effect is no less than garlic products, Cortex Bulbus Allii is as the discarded object of deep processing; Remain it is fully developed, the report of this respect is also seldom arranged at present.Number of patent application: 201110207889.7 have invented a kind of Cortex Bulbus Allii feed addictive and preparation method thereof; Be to adopt Cortex Bulbus Allii and active dry yeasr through fermented and cultured, drying, the feed addictive that sieves and process; Addition in the animal daily ration is 2-5%, and this invention develops Cortex Bulbus Allii and played beneficial effect.
Summary of the invention
The objective of the invention is to deficiency to existing application technology; Provide a kind of benzinum to extract Cortex Bulbus Allii medicinal extract; Use it for additive for farm animal feed, so that the active ingredient of Cortex Bulbus Allii is fully extracted, and use amount reduces; Easy to use, be more conducive to the purpose that animal absorbs and improve product efficacy.
Another object of the present invention is to provide a kind of method that said benzinum extracts Cortex Bulbus Allii medicinal extract for preparing.
The present invention also aims to provide a kind of described benzinum to extract Cortex Bulbus Allii medicinal extract as the application in animal and fowl fodder in the feed addictive.
Except as otherwise noted, the percentage that the present invention adopted is percetage by weight.
The object of the invention is achieved through following technical scheme.
A kind of benzinum extracts Cortex Bulbus Allii medicinal extract, is prepared by following method: Cortex Bulbus Allii and benzinum are mixed, obtain required Cortex Bulbus Allii medicinal extract through extraction, Separation of Solid and Liquid, distillation after concentrating.
The invention provides a kind of method that benzinum extracts Cortex Bulbus Allii medicinal extract for preparing, this method comprises the step of following order:
(1) meal is cleaned, drains, is ground into to Cortex Bulbus Allii;
(2) Cortex Bulbus Allii after will pulverizing mixes with benzinum, the mixed weight ratio is 1: 5-15
(3) extract 18-36h at ambient temperature;
(4) Separation of Solid and Liquid is collected supernatant liquid;
(5) decompression distillation 0.5-2.0h under vacuum 0.02-0.15Mpa, 22 ℃ of-28 ℃ of conditions of vapo(u)rizing temperature promptly obtains required medicinal extract except that after desolvating.
The preferred medical grade benzinum of described benzinum.
When described medical grade benzinum boiling point is 30 ℃-60 ℃, preferred 18h of extraction time.
When described medical grade benzinum boiling point is 60 ℃-90 ℃, preferred 36h. of extraction time
Wherein, described Cortex Bulbus Allii is fresh garlic skin or dried Cortex Bulbus Allii.
The invention provides a kind of benzinum and extract the application of Cortex Bulbus Allii medicinal extract as additive for farm animal feed, be specially: the 0.05-0.15% by livestock and poultry diet weight adds in the feed with benzinum extraction garlic medicinal extract of the present invention.
Preferably the 0.05% benzinum extraction Cortex Bulbus Allii medicinal extract by feed weight adds in the chicken feed.
Preferably the 0.1% benzinum extraction Cortex Bulbus Allii medicinal extract by feed weight adds in the pig starter feed.
Preferably add to and breed in the pig feed by the 0.15% benzinum extraction Cortex Bulbus Allii medicinal extract of raising weight.
Preferably equably benzinum being extracted Cortex Bulbus Allii medicinal extract with " equivalent is progressively increased " mode is added in the feed.
Beneficial effect of the present invention:
1, contains many effective ingredients identical in the Cortex Bulbus Allii, extract effectively its composition to be added in the animal and fowl fodder through benzinum and use with garlic;
2, in the process of Cortex Bulbus Allii extracts active ingredients and application, reduced crude fibre and coarse hard material a large amount of in the garlic skin, be more conducive to absorbing of animal;
3, because benzinum extracts Cortex Bulbus Allii medicinal extract effective ingredient is concentrated, use amount reduces, and gives off a strong fragrance, and compares with the Cortex Bulbus Allii powder, and its mouthfeel is good, makes livestock and poultry glad feeding;
4, benzinum can fully extract organic principle in the Cortex Bulbus Allii, and particularly fat-soluble allicin composition can fully be extracted, and the health-care efficacy of its medicinal extract is guaranteed, and solvent can recycle and reuse, and there is not solvent contamination in process of producing product;
5, production technology of the present invention is simple, and is easy and simple to handle, suitability for industrialized production;
6, the present invention be advantageous in that the discarded Cortex Bulbus Allii that utilizes in the garlic process is raw material, reduce cost of material, the preparation yield of extract is high, for new approach has been opened up in the development and use of discarded Cortex Bulbus Allii.
The specific embodiment:
Below comprehensive embodiment and application implementation example the present invention is done further detailed description, but they are not to qualification of the present invention.
Embodiment 1
Take by weighing 100 kilograms of Cortex Bulbus Alliis, clean, drain away the water with purified water; Be ground into meal, the extractor of packing into adds 500 liters of boiling points and is 30-60 ℃ medical grade benzinum; Under 25 ℃ of conditions, soak 18h, carry out Separation of Solid and Liquid, collect supernatant liquid with industrial filter cloth; The liquid that obtains is to distill 2.0h under 25 ℃ of conditions in vacuum 0.02Mpa, vapo(u)rizing temperature, remove desolvate 3.9 kilograms of medicinal extract.
Embodiment 2
Take by weighing 100 kilograms of Cortex Bulbus Alliis, clean, drain away the water with pure water; Be ground into meal, the extractor of packing into adds 1000 liters of boiling points and is 60 ℃-90 ℃ medical grade benzinum; Under 25 ℃ of conditions, soak 36h, carry out Separation of Solid and Liquid, collect supernatant liquid with industrial filter cloth; The liquid that obtains is to distill 1.0h under 28 ℃ of conditions in vacuum 0.1Mpa, distillation, remove desolvate 4.6 kilograms of medicinal extract.
Embodiment 3
Take by weighing 100 kilograms of Cortex Bulbus Alliis, clean, drain away the water with pure water; Be ground into meal, the extractor of packing into adds 1500 liters of boiling points and is 30 ℃-60 ℃ medical grade benzinum; Under 18 ℃ of conditions, soak 24h, carry out Separation of Solid and Liquid with industrial filter cloth; Collect supernatant liquid, obtaining liquid is to distill 1.5h under 22 ℃ of conditions in vacuum 0.15Mpa, vapo(u)rizing temperature, remove desolvate 4.3 kilograms of medicinal extract.
Application implementation example 1
The benzinum of embodiment 1 gained is extracted Cortex Bulbus Allii medicinal extract; Press 0.05% of meat chick perfect compound feed weight, evenly add, select each 300 of test group and control groups respectively by " equivalent is progressively increased " method; The feedstuff feeding number of times; Feeding volume, drinking times, feeding environment are identical, and control group does not add the Cortex Bulbus Allii benzinum and extracts medicinal extract, feeds 30 days; Test group is than average weightening finish of control group 120 grams, and the result shows that the Cortex Bulbus Allii benzinum extracts medicinal extract the meat chick is had growth promotion and gaining effect preferably.
Application implementation example 2
The benzinum of embodiment 2 gained is extracted Cortex Bulbus Allii medicinal extract,, evenly add by " equivalent is progressively increased " method by 0.1% of piglet (15kg-30kg/ body weight) perfect compound feed weight; Select each 20 of test group and control group piglets respectively,, adopt identical basal feed at identical feeding environment; Number of times, scale of feeding, the drinking times of feeding is all identical; Control group does not add the Cortex Bulbus Allii benzinum and extracts medicinal extract, carries out check experiment, feeds 22 days; Test group proves that than average head weightening finish 1800 grams of control group the Cortex Bulbus Allii benzinum extracts medicinal extract piglet is had growth promoting function preferably as a result.
Application implementation example 3
The Cortex Bulbus Allii benzinum of embodiment 3 gained is extracted medicinal extract,, evenly add by " equivalent is progressively increased " method by breeding 0.15% of pig (30kg-60kg/ body weight) perfect compound feed weight; Select each 25 of test group and control group growing and fattening pigs respectively,, adopt identical basal feed at identical feeding environment; Number of times, scale of feeding, the drinking times of feeding is all identical; Control group does not add the Cortex Bulbus Allii benzinum and extracts medicinal extract, carries out check experiment, feeds 20 days; Test group shows that than average head weightening finish 2200 grams of control group the Cortex Bulbus Allii benzinum extracts medicinal extract and to breeding pig growth promotion and effect of gain preferably arranged as a result.
Claims (10)
1. a benzinum extracts Cortex Bulbus Allii medicinal extract, and it is characterized in that: Cortex Bulbus Allii and benzinum are mixed, and the mixed weight ratio is 1: 5-15; Extract 18-36h at ambient temperature; Separation of Solid and Liquid is collected supernatant liquid; Decompression distillation 0.5-2.0h under vacuum 0.02-0.15Mpa, 22 ℃ of-28 ℃ of conditions of vapo(u)rizing temperature had both obtained required medicinal extract except that after desolvating.
2. one kind prepares the preparation method that the described benzinum of claim 1 extracts Cortex Bulbus Allii medicinal extract, and it is characterized in that: this method comprises the step of following order: meal is cleaned, drains, is ground in (1) with Cortex Bulbus Allii; (2) Cortex Bulbus Allii after will pulverizing mixes with benzinum, the mixed weight ratio is 1: 5-15 (3) extracts 18-36h at ambient temperature; (4) Separation of Solid and Liquid is collected supernatant liquid; (5) decompression distillation 0.5-2.0h under vacuum 0.02-0.15Mpa, 22 ℃ of-28 ℃ of conditions of vapo(u)rizing temperature promptly obtains required medicinal extract except that after desolvating.
3. extract Cortex Bulbus Allii medicinal extract according to the desirable 1 and 2 described benzinums that require, it is characterized in that: described Cortex Bulbus Allii is fresh garlic skin or dried Cortex Bulbus Allii.
4. method according to claim 2 is characterized in that: described benzinum is the medical grade benzinum.
5. method according to claim 2 is characterized in that: when described medical grade benzinum boiling point was 30 ℃-60 ℃, the extraction time was 18h.
6. method according to claim 2 is characterized in that: when described medical grade benzinum boiling point was 60 ℃-90 ℃, the extraction time was 36h.
7. benzinum according to claim 1 extracts Cortex Bulbus Allii medicinal extract and it is characterized in that: as the application of additive for farm animal feed, add in the feed by the 0.05-0.15% of livestock and poultry diet weight.
8. application according to claim 7 is characterized in that: the 0.05% benzinum extraction Cortex Bulbus Allii medicinal extract by feed weight adds in the chicken feed.
9. application according to claim 7 is characterized in that: the 0.1% benzinum extraction Cortex Bulbus Allii medicinal extract by feed weight adds in the pig starter feed.
10. application according to claim 7 is characterized in that: extract Cortex Bulbus Allii medicinal extract by 0.15% benzinum of feed weight and add to and breed in the pig feed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012100024242A CN102550820A (en) | 2012-01-01 | 2012-01-01 | Garlic skin extract prepared by using petroleum ether and preparation method and application thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012100024242A CN102550820A (en) | 2012-01-01 | 2012-01-01 | Garlic skin extract prepared by using petroleum ether and preparation method and application thereof |
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| CN102550820A true CN102550820A (en) | 2012-07-11 |
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| CN2012100024242A Pending CN102550820A (en) | 2012-01-01 | 2012-01-01 | Garlic skin extract prepared by using petroleum ether and preparation method and application thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103704700A (en) * | 2013-12-30 | 2014-04-09 | 徐州绿之野生物食品有限公司 | Petroleum ether extraction type lycium barbarum extract and preparation method and application thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101243871A (en) * | 2008-03-21 | 2008-08-20 | 南京工业大学 | Method for extracting garlic oil |
| CN102217710A (en) * | 2011-07-20 | 2011-10-19 | 张奎昌 | Garlic skin feed additive and preparation method thereof |
-
2012
- 2012-01-01 CN CN2012100024242A patent/CN102550820A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101243871A (en) * | 2008-03-21 | 2008-08-20 | 南京工业大学 | Method for extracting garlic oil |
| CN102217710A (en) * | 2011-07-20 | 2011-10-19 | 张奎昌 | Garlic skin feed additive and preparation method thereof |
Non-Patent Citations (3)
| Title |
|---|
| 《食品工业》 20111231 韩海旺 大蒜精油树脂的提取工艺研究 37-39页 1-10 , 第3期 * |
| 王摇风等: "大蒜油提取技术的研究进展", 《中国调味品》 * |
| 韩海旺: "大蒜精油树脂的提取工艺研究", 《食品工业》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103704700A (en) * | 2013-12-30 | 2014-04-09 | 徐州绿之野生物食品有限公司 | Petroleum ether extraction type lycium barbarum extract and preparation method and application thereof |
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Application publication date: 20120711 |