CN102528036B - Siphon-type degreasing device and degreasing method thereof - Google Patents

Siphon-type degreasing device and degreasing method thereof Download PDF

Info

Publication number
CN102528036B
CN102528036B CN 201210045758 CN201210045758A CN102528036B CN 102528036 B CN102528036 B CN 102528036B CN 201210045758 CN201210045758 CN 201210045758 CN 201210045758 A CN201210045758 A CN 201210045758A CN 102528036 B CN102528036 B CN 102528036B
Authority
CN
China
Prior art keywords
flue
heater
platform
degreasing
protective gas
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN 201210045758
Other languages
Chinese (zh)
Other versions
CN102528036A (en
Inventor
姬祖春
顾晓明
顾祖良
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
P-TECH POWDER INJECTION MOLDING CHANGSHU PTE LTD
Original Assignee
P-TECH POWDER INJECTION MOLDING CHANGSHU PTE LTD
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by P-TECH POWDER INJECTION MOLDING CHANGSHU PTE LTD filed Critical P-TECH POWDER INJECTION MOLDING CHANGSHU PTE LTD
Priority to CN 201210045758 priority Critical patent/CN102528036B/en
Publication of CN102528036A publication Critical patent/CN102528036A/en
Application granted granted Critical
Publication of CN102528036B publication Critical patent/CN102528036B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Landscapes

  • Powder Metallurgy (AREA)

Abstract

The invention discloses a siphon-type degreasing device and a degreasing method thereof and belongs to the technical field of degreasing devices of powder metallurgy injection molding parts. The siphon-type degreasing device comprises a furnace pipe platform, a furnace pipe, a furnace body, a trap, a vacuumizing mechanism and a protective gas introducing tube, wherein the furnace pipe platform isprovided with one group of hanging legs; the center of one upward side of the furnace pipe platform under a using state is provided with at least one base; the base is provided with a longitudinal through hole; at least one group of lateral through holes are arranged at intervals on the side surface of the base and around the circumstance direction of the base; the furnace pipe is arranged on thefurnace pipe platform; the furnace body is sheathed at the exterior of the furnace pipe; a group of electric heating rods are laid in the inner wall of the furnace body; the trap is fixed on the center part of one side, which faces to the hanging legs, of the furnace pipe platform; the vacuumizing mechanism is arranged on one side of the furnace body; one end of the protective gas introducing tube extends into a furnace pipe cavity via the furnace pipe platform; and the other end of the protective gas introducing tube is connected with a protective gas source device. The siphon-type degreasing device has the advantages that the degreasing speed is improved, and the furnace pipe platform can be conveniently cleaned. By utilizing the siphon-type degreasing device, the safety of operating personnel can be guaranteed, the environmental friendliness is achieved, the production efficiency is improved, and the energy consumption is saved.

Description

Hydrocone type degreasing plant and degreasing method thereof
Technical field
The invention belongs to powder metallurgy injection-molded parts degreasing plant technical field, be specifically related to a kind of hydrocone type degreasing plant, and relate to degreasing method
Background technology
Metal powder injection molding technology (Metal Injection Molding, be called for short MIM) be multidisciplinary interpenetrating and the technology of intersecting such as collection plastics molding process, polymer chemistry, powder metallurgy technology and Metal Material Science, utilize mould can disposable injection moulding to go out the product of complicated shape and made the structural member of high density, high accuracy and 3 D complex shape by sintering.This technology takes the lead in being invented in year in last century (1973) by California, USA Parmatech company, and early eighties is used widely America and Europe and Japan etc.This technology have processing step few, need not to cut or cutting and the high strong point of economic benefit on a small quantity, and can overcome that traditional powder metallurgical technique extrudate density is low, material is inhomogeneous, mechanical and physical performance is poor, the shortcoming of the slim and baroque part of easy-formation not.
Metal powder injection molding is realized by adding binding agent, namely give the sufficient flowability of metal dust and use the blank that acquisition has the specific products feature by binding agent, blank removes by the binding agent that follow-up degreasing process will before add, and obtains having the product of metal or ceramic performance again through high temperature sintering.Specifically can be summarized by following flow process: metal dust mixes (abbreviation batch mixing), granulation, the post processing by mold injects moulding, degreasing (industry also claims unsticking), sintering and necessity with binding agent.
The system that is used for the known binding agent of metal powder injection molding mainly contains paraffinic base system and aldehyde resin system.The removal methods of binding agent mainly contains four kinds: the one, and the solvent degreasing method; The 2nd, hot degreasing method; The 3rd, siphon degreasing method; The 4th, the catalysis degreasing method of adhesive special system.The solvent degreasing method is first with the part component in the injection molding blank (also claiming constituent element) sucking-off by the principle of organic solvent extraction, remove all the other components by hot degreasing method again, because this method needs converter, namely need blank is transferred to thermal debinding furnace from the solvent stove, therefore comparatively bother.Siphon degreasing method is that blank is placed on the siphon material, and more than the fusing point of one of them component in being heated to binding agent, this component sucking-off that the capillary force by the siphon material will melt is to reach the purpose that removes the wherein a kind of component in the binding agent.The catalysis degreasing method is to utilize aldehyde resin depolymerization in acid atmosphere to remove most of binding agent for the characteristic of formaldehyde gas, but this method has the fastidious property to binder system, namely be only applicable to the binding agent of aldehyde resin system, and be not suitable for the binding agent of paraffin system.
Above-mentioned four kinds of degreasing methods all need to use corresponding degreasing plant, and in disclosed Chinese patent literature, be no lack of and be seen in, omit " liquid solvent extracting and degreasing device that is used for metal powder injection molded blank " as the CN101653665A recommendation to exemplify, this device is applicable to aforesaid solvent degreasing method; " a kind of powder metallurgy injection moulding fast defat stove " that CN202070764U provides, this debinding furnace is equally applicable to aforesaid solvent degreasing method; " the powder injection forming blank solvent degreasing device " that CN202113637U introduces, this degreasing plant still is applicable to the solvent degreasing method; " a kind of powder injection forming gradient negative pressure hot defatting method " that CN100486737C discloses.
" vacuum degreasing, the sintering integrated furnace " that typical as practical novel license notification number CN2595500Y discloses, this patent scheme belongs to hydrocone type degreasing plant category, has the alleged technique effect of its Instructions Page 2 the 7th to the 9th row, but there is following shortcoming: one, degreasing speed is slow, because only be difficult under negative pressure state the adhesive gas that is volatilized by blank in the body of heater is drawn outside the stove with the exhaust tube in bottom of furnace body is insinuated into body of heater (patent claims the body of heater bleed-off passage); Its two, the blank and take out finished product inconvenience of packing in the body of heater, and patent does not provide the technology enlightenment of the blank of packing in the stove yet; Its three, the structure of body of heater is lost rationally and is not easy to cleaning, because in use, especially in the blank loading furnace process, exists blank to cause the damage situation unavoidably, if can not in time clear up then can influence follow-up use.
In view of above-mentioned prior art is necessary rationally to be improved, for this reason, the applicant has done useful design, and technical scheme described below produces under this background
Summary of the invention
Task of the present invention is to provide a kind of and helps to improve degreasing speed, have and be convenient to feed and discharging, the hydrocone type degreasing plant that is conducive to clean.
The degreasing method that also has a task to be to provide a kind of hydrocone type degreasing plant of the present invention, this method need not with an organic solvent to use embodiment safety and environmental protection, plays siphonic effect effectively, makes degreasing and presintering finish in stove and use and raise the efficiency and energy savings.
Top priority of the present invention is finished like this, a kind of hydrocone type degreasing plant, comprise the flue platform with one group of balance leg, this flue platform under the use state towards on the central authorities of a side be provided with at least one base, a spaced apart side that is provided with from base connects the longitudinal hole to opposite side on base, each longitudinal hole is corresponding with the flue platform through hole on being opened in the flue platform and communicate, be provided with one group of cross through hole in the side of base and around the circumferencial direction of base is spaced apart, each cross through hole communicates with described longitudinal hole; One flue, this flue are arranged on the described flue platform, and the flue chamber of this flue is corresponding with described base; One body of heater, this body of heater are set in outside the described flue, flue is sealed, and be laid with for one group of electrically heated rod described flue being implemented radiation heating at the inwall of this body of heater, and this group electrically heated rod arranges at interval along the short transverse of body of heater; One trap, this trap are fixed on described flue platform towards the central part of a side of described balance leg, and corresponding with described base; One vacuum device, this vacuum device are arranged on a side of described body of heater, and are connected with described trap pipeline; One protective gas inlet tube; one end of this protective gas inlet tube is in described flue platform is stretched over described flue chamber; and the other end of protective gas inlet tube is connected with the protective gas compressed air source unit, and described electrically heated rod is connected with the electrical control gear electrical control with described vacuum device.
In a specific embodiment of the present invention, the shape of described flue platform is disc, and is arranged at intervals with one group of tab in the edge of the circumferencial direction of flue platform; The shape of described flue is bell shape, and expand to establish around the circumferencial direction of outer wall at the outer wall of the bottom of flue and constitute a cooperation dish, in the edge of this cooperation dish and around the spaced apart equal locking catching groove of the position quantity corresponding with described tab that is provided with of the circumferencial direction of cooperation dish; On the outer wall of the bottom of described body of heater and around the circumferencial direction of body of heater, constitute a fixed flange, on this fixed flange and around the spaced apart ring flange holddown groove that quantity equates and the position is corresponding that is provided with quantity and described locking catching groove of the circumferencial direction of fixed flange, described tab and described locking catching groove and ring flange holddown groove lock.
In another specific embodiment of the present invention, on the outer wall at the top of described flue and be positioned at middle position one flue hanger is fixedly arranged, described body of heater has a stove, the top seal of this bell and body of heater is fixed, on the outer wall of this bell and be positioned at middle position one bell hanger is fixedly arranged.
In another specific embodiment of the present invention, outside described body of heater, be provided with one group of power supply connecting plate, described electrically heated rod is connected with the power supply connecting plate by power line, and the power line outside being stretched over body of heater is arranged with insulating sleeve.
In another specific embodiment of the present invention, fixedly have one to be used for described power supply connecting plate is covered the insulating protection plate that protects and the position is corresponding with the power supply connecting plate at the outer wall of described body of heater.
Also have in the specific embodiment of the present invention, described trap has a cavity volume, described flue platform through hole communicates with this cavity volume, side at trap is equipped with an exhaust tube interface, this exhaust tube interface communicates with cavity volume, and connect an end of exhaust tube at the exhaust tube interface, and the other end of exhaust tube is connected with described vacuum device.
Of the present invention also have a task to finish like this, a kind of degreasing method of hydrocone type degreasing plant, and it may further comprise the steps:
A) charging, earlier metal dust is mixed afterwards injection molding blank packs into and fills in the siphon vessel of siphon material with binding agent, and blank is buried in the siphon material, again siphon vessel is built and placed on the base, then with flue and body of heater handling successively to the flue platform, and with tab and locking catching groove and the locking of ring flange holddown groove;
B) vacuumize, open vacuum device, the flue chamber of flue is vacuumized, and control vacuum;
C) degreasing and presintering; the electrically heated rod energising; to flue chamber gradient increased temperature and gradient insulation; and in the flue chamber, introduce protective gas by the protective gas inlet tube; the flow of control protective gas; binding agent in blank effusion blank and enter the siphon material under the effect of windstream; the binding agent that enters in the siphon material flows with gaseous form effusion siphon material and towards trap; captured by trap; presintering and control intensification pre-sintering temperature then heat up; cooling obtains degreasing and injection molding powder metallurgy blank presintering after being incubated.
In of the present invention and then specific embodiment, steps A) the siphon material described in is sand; Step B) the control vacuum described in is to be 10-50Pa with vacuum degree control.
Of the present invention again more and in specific embodiment, step C) gradient increased temperature described in and gradient insulation are the insulation 60-180min when rising to 60-80 ℃ of the temperature with the flue chamber, then are warming up to 450-550 ℃ and be incubated 120-240min again; The flow of described control protective gas is to be 0.5-1L/min with flow-control; Described control intensification pre-sintering temperature is that temperature is controlled to be 700-850 ℃, and the time of described insulation is 30-120min.
Technical scheme provided by the invention is owing to be provided with base at the flue platform, and offered the vertical, horizontal through hole at base, longitudinal hole communicates with trap through flue platform through hole, under the effect of the vacuum device that is connected with trap, and under the electrically heated rod heating, the binding agent that the blank in the flue chamber that is arranged in flue is overflowed flows to trap under the effect of windstream fast, thereby can improve degreasing speed; Flue and body of heater are the ceiling-mounted combining structure, therefore are conducive to charging and discharging and have be convenient to the flue platform is implemented cleaning.The method that provides is not because not with an organic solvent; thereby can ensure operating personnel's safety and protect environment; blank is packed in the siphon material; can bring into play siphonic effect effectively; degreasing and presintering are finished with stove; can reduce the intermediate handling process, enhance productivity, but and need not to repeat heating and energy savings consumption.
Description of drawings
Fig. 1 is the embodiments of the invention structure chart.
Fig. 2 is the cutaway view of Fig. 1.
The specific embodiment
For the auditor that the makes Patent Office especially public can be expressly understood technical spirit of the present invention and beneficial effect more, the applicant general elaborates in the mode of embodiment below, but all be not restriction to the present invention program to the description of embodiment, any according to the present invention's design done only for pro forma but not substantial equivalent transformation all should be considered as technical scheme category of the present invention.
Embodiment 1:
Ask for an interview Fig. 1 and Fig. 2, provided a flue platform 1, this flue platform 1 has one group and is used for flue platform 1 is in the balance leg 11 that soars in the terrace of field of employment, that is to say flue platform 1 and terrace are maintained a certain distance, under the flue platform 1 use state towards on a side central spaced apart be provided with one group of flue platform through hole 13(Fig. 2 and show), be stacked with a pair of base 12 at the position corresponding to flue platform through hole 13, certainly the quantity of base 12 is not subjected to illustrating the restriction of quantity, for example may be as few as one also can as many as three or more, its effect is mainly used in regulating height.A spaced apart side that is provided with from base 12 connects one group of longitudinal hole 121 to opposite side on base 12, each longitudinal hole 121 is corresponding with aforesaid flue platform through hole 13, and be provided with one group of cross through hole 122 in the side of base 12 around the circumferencial direction of base 12 is spaced apart, each cross through hole 122 communicates (Fig. 2 shows) with aforesaid longitudinal hole 121.Preferably, between base 12 and flue platform 11, add a sealing ring 123, play the edge of base 12 and the sealing function between the flue platform 1 by sealing circle 123.
The shape of flue platform 1 is disc, in the edge of this flue platform 1 and around the circumferencial direction of the flue platform 1 one group of tab 14 that has been equidistantly spaced, and is furnished with nut on each tab 14.In addition, be extended with the first guide rod seat 15(that quantity is not subjected to illustrating restricted number in the edge one of flue platform 1 and be illustrated as two), on each first guide rod seat 15 guide rod 151 is arranged fixedly.
One shape is arranged on the flue platform 1 just as the flue 2 of bell jar, and the flue chamber 21 of this flue 2 is corresponding with aforesaid base 12, that is to say, along with flue 2 is set to flue platform 1 and makes base 12 be positioned at flue chamber 21.Shown in figure, outer wall in the bottom of flue 2 extends and constitutes one and connect dish 22, connect dish 22 edge and be provided with one group of locking catching groove 221 around the circumferencial direction that connects dish 22 is spaced apart at this, the quantity of locking catching groove 221 is equal with the quantity of aforesaid tab 14 and the position is corresponding.Solid welding has a flue hanger 23 on the outer wall at the top of flue 2, in addition, is extended with the second guide rod seat 222 that quantity equates with the quantity of the first guide rod seat 15 in the edge of cooperation dish 22 and in the position corresponding to the aforesaid first guide rod seat 15.
One body of heater, 3 covers are put outside aforesaid flue 2, be laid with electrically heated rod 31 at interval at the inwall of this body of heater 3 and along the short transverse of body of heater 3, by 31 pairs of flue 2 radiation heatings of electrically heated rod, the power line 311 of electrically heated rod 31 is connected with body of heater 3 power supply connecting plate 34 power supplys outward, and the power line outside being stretched over body of heater 3 311 is arranged with insulating sleeve 3111.Body of heater 32 has a chuck 36, is equipped with at chuck 36 that cooling medium is introduced interface 361 and cooling medium is drawn interface 362, and wherein, cooling medium is introduced interface 361 is drawn interface 362 corresponding to cooling medium below.Cooling medium (water) is drawn interface 362 by cooling medium and is drawn after also cooling medium is introduced interface 361 introducing chucks 36, to form circulating reflux.Top at body of heater 3 is equipped with a bell 33 with one group of securing member (cooperations of bolts and nuts), bell 33 has bell chuck 332, be provided with at bell chuck 332 that bell chuck cooling medium is introduced interface 3321 and bell chuck cooling medium is drawn interface 3322, the introducing of bell chuck cooling medium, outgoing interface 3321,3322 communicate with bell chuck 332.In addition, at the top of bell 33 a bell hanger 331 is arranged fixedly.
Outer wall in the bottom of body of heater 3 is outward extended with a fixed flange 32, be provided with the ring flange holddown groove 321 that quantity and aforesaid locking catching groove 221 are equal and the position is corresponding at the edge of this fixed flange 32 and around the circumferencial direction of fixed flange 32 is spaced apart, and on fixed flange 32, be extended with the 3rd guide pillar seat 322 that quantity equates with the second guide pillar seat 222 in the position corresponding to the aforesaid second guide pillar seat 222.Preferably, the inwall of body of heater 3 arranges furnace insulation flame retardant coating 37, and the inwall of same bell 33 arranges bell thermal insulation fire-resistant layer 333.
After the cooperation dish hole 2221 that flue 2 is offered on by the second guide pillar seat 222 on the cooperation dish 22 is aimed at guide rods 151 and is arranged on the flue platform 1, and when guide rods 151 are aimed at and after cover places outside the flue 2 in the ring flange hole of offering on the 3rd guide rod seat 322 of the fixed flange 32 of body of heater 3 3221, flue 2 and body of heater 3 are locked on the flue platform 1 reliably in the position corresponding to the ring flange holddown groove 321 that locks catching groove 221 and overlap with locking catching groove 221 by tab 14, vice versa.Preferably, in order to ensure safety, can arrange one outside body of heater 3 and in the position corresponding to aforesaid power supply connecting plate 34 is used for power supply connecting plate 34 is covered the insulating protection plate 35 that protects, figure 2 illustrates a pair of cramp bar 351 for supporting insulating protection plate 35, cramp bar 351 is fixing with body of heater 3.
Please continue to see Fig. 1 and Fig. 2, provided a trap 4, this trap 4 has a cavity volume 41, and it is the steel wire pelletizing that first cleaning ball, 411, the first cleaning balls 411 are set in the cavity volume 41.When with screw 43 and aforesaid flue platform 1 towards under a side and after the fixed-site corresponding to base 12, cavity volume 41 just communicates with aforesaid flue platform through hole 13.Preferably, trap 4 constitutes a trap chuck 44, has connected into water interface 441 and water outlet interface 442 at this trap chuck 44, and the interface 441 of wherein intaking is positioned at the sidepiece of trap chuck 44, and water outlet interface 442 is positioned at the bottom of trap chuck 44.Preferably, also be equipped with a row's fat mouth 45 that communicates with cavity volume 41 in the bottom of trap 4, be equipped with valve 451 at row's fat mouth 45.Side at trap 4 is equipped with an exhaust tube interface 42, connect an end of an exhaust tube 421 at this exhaust tube interface 42, and the other end of exhaust tube 421 is connected with the vacuum device 5 of a side that is arranged on body of heater 3.
One end of the protective gas inlet tube of illustrating among the figure 6 is being stretched over behind flue platform 1 in the aforesaid flue chamber 21, and corresponding to the top in flue chamber 21, and the other end of protective gas inlet tube 6 is connected with the protective gas compressed air source unit.
Aforesaid vacuum device 5 comprises vavuum pump 51 and capture tank 52, vavuum pump 51 is arranged on the terrace of field of employment, the air inlet of capture tank 52 is connected with aforesaid exhaust tube 421, and this exhaust tube 421 is provided with valve 4211, vacuum meter 4212 and Pressure gauge 4213, wherein, vacuum meter 4212 is between valve 4211 and Pressure gauge 4213, and the gas outlet of capture tank 52 is connected with vavuum pump 51 by pipeline 521.Second cleaning ball 522 that is equivalent to aforesaid first cleaning ball 411 is set in capture tank 52.
Use when of the present invention, table platform 1 is arranged in the melt pit 81 of excavation on the terrace 8 together with flue 2 and body of heater 3.
The step of the degreasing method of the hydrocone type degreasing plant of said structure is as follows:
A) charging, to mix the injection molding diameter in back with the adhesive of paraffinic base system by the stainless steel metal powder earlier is that 10 ㎜ and thickness are that the blank of the oblate body of 1 ㎜ is packed in the siphon vessel 7 that fills siphon material 71, and by siphon material 71 blank is buried, namely buried by 71 pairs of blanks of siphon material, again siphon vessel 7 is built on base 12 together with blank, then flue 2 and body of heater 3 are passed through the hoist tool handling to flue platform 1, and with tab 14 and locking catching groove 222 and 321 lockings of ring flange holddown groove, the binding agent of the paraffinic base system described in this step is known by paraffin, polyethylene and stearic acid are formulated, and described siphon material 71 is sand (for example common emergy or quartz sand);
B) take out straight sky, by the operation to electrical control gear such as electric control box, open the vavuum pump 51 of vacuum device 5, the flue chamber 21 of flue 2 is evacuated to 10Pa;
C) degreasing and presintering; same by the operation to electrical control gear such as electric control box; make electrically heated rod 31 switch on and work; insulation 60min when the temperature in the flue chamber 21 rises to 60 ℃; introduce hydrogen or argon gas by protective gas inlet tube 6 simultaneously; the flow of hydrogen or argon gas is 0.5L/min; this moment, first component (also can claim first constituent element) of the binding agent in the blank under the effect of vacuum device 5 was that paraffin effusion blank under the effect of windstream enters formation capillary channel in the siphon material 71; aforementioned first component that enters in the siphon material 71 flows with gaseous form effusion siphon material 71 and towards trap 4; specifically be that gap and the cross through hole on base 12 122 through adjacent siphon vessel 7 enters in the cavity volume 41 of trap 4 by flue platform through hole 13; and making first component that enters in the cavity volume 41 under the state of cold water is introduced in trap chuck 44 circulation of trap 4 is that paraffin build is placing on first cleaning ball 411 in the cavity volume 41; first component that makes the binding agent in the blank by this is that paraffin removes; continue to be warming up to 450 ℃ and insulation 120min; making essentially identical second component of fusing point each other in the binding agent is that polyethylene and the 3rd component are that stearic acid removes; presintering then heats up; the intensification temperature is 750 ℃; after the insulation of 60min; cooling; remove body of heater 3 and flue 2 successively; obtain degreasing and injection molding powder metallurgy blank presintering, namely obtaining diameter is 10 ㎜; thickness is the stainless steel blank of the oblate body of 1 ㎜.In above-mentioned degreasing and presintering process, feed cold water all the time to the chuck 36 of body of heater 3 and to the bell chuck 332 of bell 33, same, trap chuck 44 is also fed cold water.In the time will implementing cleaning to first cleaning ball 411 in the cavity volume 41 of trap 4, then feed 70-80 ℃ hot water so that with the binding agent of productive set on first cleaning ball 411 molten except and discharge (open valve 451) from row's fat mouth 45.
Embodiment 2:
Only with steps A) the material of blank change iron powder into, and diameter is 10 ㎜, and thickness is 1.5 ㎜; With step B) vacuum change 50Pa into; With step C) the temperature in flue chamber 21 change into and rise to 70 ℃; temperature retention time changes 120min into; use protective gas instead nitrogen; flow changes 0.75L/min into; change the temperature that continue to heat up into 550 ℃, temperature retention time changes 180min into, changes the intensification temperature of intensification presintering into 700 ℃; temperature retention time changes 30min into, and all the other are all with the description to embodiment 1.
Embodiment 3:
Only with steps A) the material of blank change cemented carbide powder into, diameter changes 20 ㎜ into, thickness changes 3 ㎜ into; With step B) vacuum change 30Pa into; With step C) the temperature in flue chamber 21 change into and rise to 80 ℃; temperature retention time changes 180min into; use protective gas instead nitrogen; the flow of protective gas changes 1L/min into; change the temperature that continue to heat up into 500 ℃, temperature retention time changes 200min into, changes the intensification temperature of intensification presintering into 850 ℃; temperature retention time changes 120min into, and all the other are all with the description to embodiment 1

Claims (9)

1. A kind of hydrocone type degreasing plant, it is characterized in that comprising the flue platform (1) with one group of balance leg (11), this flue platform (1) under the use state towards on the central authorities of a side be provided with at least one base (12), go up a spaced apart side that is provided with from base (12) at base (12) and connect longitudinal hole (121) to opposite side, each longitudinal hole (121) is corresponding with the flue platform through hole (13) on being opened in flue platform (1) and communicate, in the side of base (12) and around the spaced apart one group of cross through hole (122) that is provided with of circumferencial direction of base (12), each cross through hole (122) communicates with described longitudinal hole (121); One flue (2), this flue (2) is arranged on the described flue platform (1), and the flue chamber (21) of this flue (2) is corresponding with described base (12); One body of heater (3), this body of heater (3) is set in outside the described flue (2), flue (2) is sealed, and the inwall at this body of heater (3) is laid with for one group of electrically heated rod (31) of described flue (2) being implemented radiation heating, and this group electrically heated rod (31) arranges at interval along the short transverse of body of heater (3); One trap (4), this trap (4) are fixed on described flue platform (1) towards the central part of a side of described balance leg (11), and corresponding with described base (12); One vacuum device (5), this vacuum device (5) is arranged on a side of described body of heater (3), and is connected with described trap (4) pipeline; One protective gas inlet tube (6); one end of this protective gas inlet tube (6) is in described flue platform (1) is stretched over described flue chamber (21); and the other end of protective gas inlet tube (6) is connected with the protective gas compressed air source unit, and described electrically heated rod (31) is connected with the electrical control gear electrical control with described vacuum device (5).
2. Hydrocone type degreasing plant according to claim 1 is characterized in that the shape of described flue platform (1) is disc, and is arranged at intervals with one group of tab (14) in the edge of the circumferencial direction of flue platform (1); The shape of described flue (2) is bell shape, and expand to establish around the circumferencial direction of outer wall at the outer wall of the bottom of flue (2) and constitute a cooperation dish (22), in the edge of this cooperation dish (22) and around the spaced apart equal locking catching groove (221) of the position quantity corresponding with described tab (14) that is provided with of the circumferencial direction of cooperation dish (22); On the outer wall of the bottom of described body of heater (3) and around the circumferencial direction of body of heater (3), constitute a fixed flange (32), go up and around the spaced apart ring flange holddown groove (321) that quantity equates and the position is corresponding that is provided with quantity and described locking catching groove (221) of the circumferencial direction of fixed flange (32), described tab (14) locks with described locking catching groove (221) and ring flange holddown groove (321) at this fixed flange (32).
3. Hydrocone type degreasing plant according to claim 1, it is characterized in that on the outer wall at the top of described flue (2) and be positioned at middle position that one flue hanger (23) is fixedly arranged, described body of heater (3) has a bell (33), the top seal of this bell (33) and body of heater (3) is fixed, on the outer wall of this bell (33) and be positioned at middle position one bell hanger (331) is fixedly arranged.
4. Hydrocone type degreasing plant according to claim 1, it is characterized in that outside described body of heater (3), being provided with one group of power supply connecting plate (34), described electrically heated rod (31) is connected with power supply connecting plate (34) by power line (311), and the power line (311) outside being stretched over body of heater (3) is arranged with insulating sleeve (3111).
5. Hydrocone type degreasing plant according to claim 4 is characterized in that fixedly having one to be used for described power supply connecting plate (34) is covered the insulating protection plate (35) that protects and the position is corresponding with power supply connecting plate (34) at the outer wall of described body of heater (3).
6. Hydrocone type degreasing plant according to claim 1, it is characterized in that described trap (4) has a cavity volume (41), described flue platform through hole (13) communicates with this cavity volume (41), side at trap (4) is equipped with an exhaust tube interface (42), this exhaust tube interface (42) communicates with cavity volume (41), and connect an end of exhaust tube (421) at exhaust tube interface (42), and the other end of exhaust tube (421) is connected with described vacuum device (5).
7. A kind of degreasing method of hydrocone type degreasing plant as claimed in claim 1 is characterized in that it may further comprise the steps:
A) charging, earlier metal dust is mixed afterwards injection molding blank packs in the siphon vessel (7) that fills siphon material (71) with binding agent, and blank is buried in siphon material (71), again siphon vessel (7) is built and placed on the base (12), then with flue (2) and body of heater (3) handling successively to flue platform (1), wherein, edge at the circumferencial direction of flue platform (1) is arranged at intervals with one group of tab (14), on the outer wall of the bottom of described flue (2) and around the circumferencial direction of outer wall, expand to establish and constitute a cooperation dish (22), in the edge of this cooperation dish (22) and around the spaced apart equal locking catching groove (221) of the position quantity corresponding with described tab (14) that is provided with of the circumferencial direction of cooperation dish (22), on the outer wall of the bottom of described body of heater (3) and around the circumferencial direction of body of heater (3), constitute a fixed flange (32), go up and around the spaced apart ring flange holddown groove (321) that quantity equates and the position is corresponding that is provided with quantity and described locking catching groove (221) of the circumferencial direction of fixed flange (32), described tab (14) locks with described locking catching groove (221) and ring flange holddown groove (321) at this fixed flange (32);
B) vacuumize, open vacuum device (5), the flue chamber (21) of flue (2) is vacuumized, and control vacuum;
C) degreasing and presintering; electrically heated rod (31) energising; to flue chamber (21) gradient increased temperature and gradient insulation; and in flue chamber (21), introduce protective gas by protective gas inlet tube (6); the flow of control protective gas; binding agent in blank effusion blank and enter siphon material (71) under the effect of windstream; the binding agent that enters in the siphon material (71) flows with gaseous form effusion siphon material and towards trap (4); captured by trap (4); presintering and control intensification pre-sintering temperature then heat up; cooling obtains degreasing and injection molding powder metallurgy blank presintering after being incubated.
8. The degreasing method of hydrocone type degreasing plant according to claim 7 is characterized in that steps A) described in siphon material (71) be sand; Step B) the control vacuum described in is to be 10-50Pa with vacuum degree control.
9. The degreasing method of hydrocone type degreasing plant according to claim 7, it is characterized in that step C) described in gradient increased temperature and gradient insulation be temperature with flue chamber (21) insulation 60-180min when rising to 60-80 ℃, then be warming up to 450-550 ℃ and be incubated 120-240min again; The flow of described control protective gas is to be 0.5-1L/min with flow-control; Described control intensification pre-sintering temperature is that temperature is controlled to be 700-850 ℃, and the time of described insulation is 30-120min
CN 201210045758 2012-02-27 2012-02-27 Siphon-type degreasing device and degreasing method thereof Expired - Fee Related CN102528036B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201210045758 CN102528036B (en) 2012-02-27 2012-02-27 Siphon-type degreasing device and degreasing method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201210045758 CN102528036B (en) 2012-02-27 2012-02-27 Siphon-type degreasing device and degreasing method thereof

Publications (2)

Publication Number Publication Date
CN102528036A CN102528036A (en) 2012-07-04
CN102528036B true CN102528036B (en) 2013-09-25

Family

ID=46336752

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 201210045758 Expired - Fee Related CN102528036B (en) 2012-02-27 2012-02-27 Siphon-type degreasing device and degreasing method thereof

Country Status (1)

Country Link
CN (1) CN102528036B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109332656A (en) * 2018-12-10 2019-02-15 东北大学 A kind of prefabricated roller core heating device of continuous casting compound high speed steel roll and its application method

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106440807A (en) * 2016-11-30 2017-02-22 广西大学 Nixing pottery electronically-controlled airflow sintering device

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS59224306A (en) * 1983-05-13 1984-12-17 日本碍子株式会社 Manufacture of ceramic part
CN100364929C (en) * 2006-07-27 2008-01-30 淮海工学院 Mixed defatting stove and its mixed defatting process
JP5265475B2 (en) * 2009-07-17 2013-08-14 株式会社トウネツ One-chamber vacuum furnace
CN202070764U (en) * 2011-04-06 2011-12-14 山东金聚粉末冶金有限公司 Quick solvent degreasing furnace in powder metallurgic injection molding
CN202109775U (en) * 2011-05-27 2012-01-11 合肥高歌热处理应用技术有限公司 Tail gas purification device for degreasing furnace

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109332656A (en) * 2018-12-10 2019-02-15 东北大学 A kind of prefabricated roller core heating device of continuous casting compound high speed steel roll and its application method

Also Published As

Publication number Publication date
CN102528036A (en) 2012-07-04

Similar Documents

Publication Publication Date Title
CN102923699B (en) Continuous pyrographite purifying device
CN103978210B (en) The dual-purpose sintering furnace of vacuum protection atmosphere of metal powder injection molded part
CN104308163A (en) Screw and powder injection molding method thereof
CN102528044B (en) Degreasing device
CN102528036B (en) Siphon-type degreasing device and degreasing method thereof
CN101754497B (en) Silicon nitride heat generator and manufacturing method thereof
CN204159874U (en) The dual-purpose sintering furnace of vacuum protection atmosphere of metal powder injection molded part
CN103331447B (en) Gel discharging and degreasing technology for powder metallurgical vacuum sintering furnace
CN106041025A (en) Inert gas shielding immersion type heating difunctional low-pressure casting furnace
CN102528042B (en) Siphon-type degreasing furnace
CN102172957B (en) Platform for hanging, turning, slip casting of black porcelain composite ceramic solar panel
CN102433422A (en) Model correcting method for high-temperature alloy thin-wall casting
CN102581283B (en) Siphon type degreasing and pre-sintering device
CN202479496U (en) Siphon degreasing device
CN102554233B (en) Energy-saving syphon type degreasing device
CN102528043B (en) Degreasing furnace
CN102554232B (en) Siphon degreasing plant
CN102528041B (en) Energy-saving degreasing device
CN204449303U (en) A kind of constant temperature trace circular water degreasing equipment
CN210512622U (en) Device suitable for preparing ceramic powder material by self-propagating high-temperature synthesis method
CN204413153U (en) A kind of degreasing plant
CN103290237A (en) Arsenic lead alloy synthesis and sublimation integral furnace used for producing high-purity arsenic
CN203411349U (en) Uranium dioxide core roasting-reduction integration furnace
CN106508060B (en) A kind of compressed water reactor nuclear power fuel assembly base mould and its casting method
CN102179498A (en) Energy-saving device of liquid rising pipe of low-pressure casting machine

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20130925

CF01 Termination of patent right due to non-payment of annual fee