CN102522209B - 一种高能镍碳超级电容器负极负极板浆料的制备方法 - Google Patents
一种高能镍碳超级电容器负极负极板浆料的制备方法 Download PDFInfo
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- CN102522209B CN102522209B CN 201110294419 CN201110294419A CN102522209B CN 102522209 B CN102522209 B CN 102522209B CN 201110294419 CN201110294419 CN 201110294419 CN 201110294419 A CN201110294419 A CN 201110294419A CN 102522209 B CN102522209 B CN 102522209B
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- supercapacitor
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- 238000002360 preparation method Methods 0.000 title claims abstract description 29
- 239000002002 slurry Substances 0.000 title claims abstract description 25
- VMWYVTOHEQQZHQ-UHFFFAOYSA-N methylidynenickel Chemical compound [Ni]#[C] VMWYVTOHEQQZHQ-UHFFFAOYSA-N 0.000 title claims abstract description 11
- 239000000853 adhesive Substances 0.000 claims abstract description 21
- 230000001070 adhesive effect Effects 0.000 claims abstract description 21
- 239000000843 powder Substances 0.000 claims abstract description 16
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000000956 alloy Substances 0.000 claims abstract description 10
- 229910045601 alloy Inorganic materials 0.000 claims abstract description 10
- 239000003575 carbonaceous material Substances 0.000 claims abstract description 10
- 239000001257 hydrogen Substances 0.000 claims abstract description 10
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 10
- 238000003756 stirring Methods 0.000 claims description 30
- 239000008367 deionised water Substances 0.000 claims description 17
- 229910021641 deionized water Inorganic materials 0.000 claims description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- 238000000034 method Methods 0.000 claims description 12
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims description 11
- 239000004810 polytetrafluoroethylene Substances 0.000 claims description 11
- 239000002994 raw material Substances 0.000 claims description 11
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 10
- 239000000839 emulsion Substances 0.000 claims description 10
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims description 8
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims description 8
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 8
- 150000001875 compounds Chemical class 0.000 claims description 5
- 230000015572 biosynthetic process Effects 0.000 claims description 4
- 239000004615 ingredient Substances 0.000 claims description 3
- 239000003990 capacitor Substances 0.000 abstract description 14
- 238000004146 energy storage Methods 0.000 abstract description 9
- 239000003792 electrolyte Substances 0.000 abstract description 7
- BFDHFSHZJLFAMC-UHFFFAOYSA-L nickel(ii) hydroxide Chemical compound [OH-].[OH-].[Ni+2] BFDHFSHZJLFAMC-UHFFFAOYSA-L 0.000 abstract description 7
- 239000013543 active substance Substances 0.000 abstract description 4
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract description 4
- 229920006351 engineering plastic Polymers 0.000 abstract description 4
- 239000000463 material Substances 0.000 abstract description 4
- 239000010935 stainless steel Substances 0.000 abstract description 4
- 229910001220 stainless steel Inorganic materials 0.000 abstract description 4
- 239000010406 cathode material Substances 0.000 abstract 1
- 238000007599 discharging Methods 0.000 abstract 1
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 23
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 19
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical class C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 11
- 229910052759 nickel Inorganic materials 0.000 description 9
- 229910052799 carbon Inorganic materials 0.000 description 7
- 229910021393 carbon nanotube Inorganic materials 0.000 description 6
- 239000002041 carbon nanotube Substances 0.000 description 6
- 239000003610 charcoal Substances 0.000 description 5
- 239000006260 foam Substances 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 239000000758 substrate Substances 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000000465 moulding Methods 0.000 description 3
- 239000011148 porous material Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000011257 shell material Substances 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 2
- 230000004888 barrier function Effects 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 238000003487 electrochemical reaction Methods 0.000 description 2
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 238000005187 foaming Methods 0.000 description 2
- 239000010439 graphite Substances 0.000 description 2
- 229910002804 graphite Inorganic materials 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 239000011159 matrix material Substances 0.000 description 2
- -1 polytetrafluoroethylene Polymers 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910010413 TiO 2 Inorganic materials 0.000 description 1
- 229910003075 TiO2-B Inorganic materials 0.000 description 1
- 229910021536 Zeolite Inorganic materials 0.000 description 1
- OSOVKCSKTAIGGF-UHFFFAOYSA-N [Ni].OOO Chemical compound [Ni].OOO OSOVKCSKTAIGGF-UHFFFAOYSA-N 0.000 description 1
- 239000011149 active material Substances 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 239000012300 argon atmosphere Substances 0.000 description 1
- 239000012298 atmosphere Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000000498 ball milling Methods 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 239000002134 carbon nanofiber Substances 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000005229 chemical vapour deposition Methods 0.000 description 1
- 239000006258 conductive agent Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 239000011258 core-shell material Substances 0.000 description 1
- 239000003431 cross linking reagent Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- IPJKJLXEVHOKSE-UHFFFAOYSA-L manganese dihydroxide Chemical compound [OH-].[OH-].[Mn+2] IPJKJLXEVHOKSE-UHFFFAOYSA-L 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000002808 molecular sieve Substances 0.000 description 1
- GDXTWKJNMJAERW-UHFFFAOYSA-J molybdenum(4+);tetrahydroxide Chemical compound [OH-].[OH-].[OH-].[OH-].[Mo+4] GDXTWKJNMJAERW-UHFFFAOYSA-J 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 229910000483 nickel oxide hydroxide Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000007774 positive electrode material Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
- 229910001928 zirconium oxide Inorganic materials 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/30—Electrodes characterised by their material
- H01G11/32—Carbon-based
- H01G11/38—Carbon pastes or blends; Binders or additives therein
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/26—Electrodes characterised by their structure, e.g. multi-layered, porosity or surface features
- H01G11/28—Electrodes characterised by their structure, e.g. multi-layered, porosity or surface features arranged or disposed on a current collector; Layers or phases between electrodes and current collectors, e.g. adhesives
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/13—Energy storage using capacitors
Landscapes
- Engineering & Computer Science (AREA)
- Power Engineering (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Electric Double-Layer Capacitors Or The Like (AREA)
- Battery Electrode And Active Subsutance (AREA)
Abstract
Description
Claims (2)
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
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CN 201110294419 CN102522209B (zh) | 2011-09-30 | 2011-09-30 | 一种高能镍碳超级电容器负极负极板浆料的制备方法 |
PCT/CN2012/079634 WO2013044684A1 (zh) | 2011-09-30 | 2012-08-03 | 一种高能镍碳超级电容器负极负极板浆料的制备方法 |
Applications Claiming Priority (1)
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CN 201110294419 CN102522209B (zh) | 2011-09-30 | 2011-09-30 | 一种高能镍碳超级电容器负极负极板浆料的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN102522209A CN102522209A (zh) | 2012-06-27 |
CN102522209B true CN102522209B (zh) | 2013-09-25 |
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Country Status (2)
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CN (1) | CN102522209B (zh) |
WO (1) | WO2013044684A1 (zh) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102522209B (zh) * | 2011-09-30 | 2013-09-25 | 天津国泰之光新材料技术研究院有限公司 | 一种高能镍碳超级电容器负极负极板浆料的制备方法 |
CN104733701A (zh) * | 2015-02-16 | 2015-06-24 | 徐象华 | 一种镍基高能二次电池负极浆料 |
CN105742578B (zh) * | 2016-03-22 | 2018-11-13 | 中国科学院理化技术研究所 | 一种添加碳纳米管的镍氢电池负极浆料制备方法 |
CN109390639A (zh) * | 2018-09-03 | 2019-02-26 | 中车青岛四方车辆研究所有限公司 | 富液式储能型镍氢电池及其在轨道车辆辅助供电系统上的应用 |
Citations (7)
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CN1277444A (zh) * | 2000-07-21 | 2000-12-20 | 中国科学院上海冶金研究所 | 电化学超电容器及其制造方法 |
CN1832068A (zh) * | 2006-03-10 | 2006-09-13 | 潮州三环(集团)股份有限公司 | 陶瓷电容器的内电极浆料及其制备方法 |
CN101159192A (zh) * | 2007-10-29 | 2008-04-09 | 上海中上汽车科技有限公司 | 牵引型超级电容器 |
CN101241803A (zh) * | 2008-03-11 | 2008-08-13 | 清华大学 | 一种聚吡咯混合式超级电容器及其制造方法 |
CN101710537A (zh) * | 2009-12-09 | 2010-05-19 | 上海奥威科技开发有限公司 | 一种超级电容器用电极及其制造方法 |
KR20110075561A (ko) * | 2009-12-28 | 2011-07-06 | 한국세라믹기술원 | 탄소니켈복합 에어로젤의 제조방법 및 이를 이용한 수퍼커패시터 전극의 제조방법 |
CN102201565A (zh) * | 2011-04-14 | 2011-09-28 | 杭州万好万家动力电池有限公司 | 一种高容量金属锂粉复合负极及制备方法和多层复合电极 |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100576390C (zh) * | 2003-01-20 | 2009-12-30 | 北京理工大学 | 绿色复合双电层电化学电容器 |
US7201857B2 (en) * | 2003-03-03 | 2007-04-10 | Texaco Ovonic Battery Systems, Llc | Performance enhancing additive material for the nickel hydroxide positive electrode in rechargeable alkaline cells |
CN102522209B (zh) * | 2011-09-30 | 2013-09-25 | 天津国泰之光新材料技术研究院有限公司 | 一种高能镍碳超级电容器负极负极板浆料的制备方法 |
-
2011
- 2011-09-30 CN CN 201110294419 patent/CN102522209B/zh active Active
-
2012
- 2012-08-03 WO PCT/CN2012/079634 patent/WO2013044684A1/zh active Application Filing
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1277444A (zh) * | 2000-07-21 | 2000-12-20 | 中国科学院上海冶金研究所 | 电化学超电容器及其制造方法 |
CN1832068A (zh) * | 2006-03-10 | 2006-09-13 | 潮州三环(集团)股份有限公司 | 陶瓷电容器的内电极浆料及其制备方法 |
CN101159192A (zh) * | 2007-10-29 | 2008-04-09 | 上海中上汽车科技有限公司 | 牵引型超级电容器 |
CN101241803A (zh) * | 2008-03-11 | 2008-08-13 | 清华大学 | 一种聚吡咯混合式超级电容器及其制造方法 |
CN101710537A (zh) * | 2009-12-09 | 2010-05-19 | 上海奥威科技开发有限公司 | 一种超级电容器用电极及其制造方法 |
KR20110075561A (ko) * | 2009-12-28 | 2011-07-06 | 한국세라믹기술원 | 탄소니켈복합 에어로젤의 제조방법 및 이를 이용한 수퍼커패시터 전극의 제조방법 |
CN102201565A (zh) * | 2011-04-14 | 2011-09-28 | 杭州万好万家动力电池有限公司 | 一种高容量金属锂粉复合负极及制备方法和多层复合电极 |
Non-Patent Citations (2)
Title |
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Magneli phase Ti4O7 electrode for oxygen reduction reaction and its implication for zinc-air rechargeable batteries;Xiaoxia Li, et al.;《Electrochimica Acta》;20100516;参见摘要,结论部分 * |
Xiaoxia Li, et al..Magneli phase Ti4O7 electrode for oxygen reduction reaction and its implication for zinc-air rechargeable batteries.《Electrochimica Acta》.2010,参见摘要,结论部分. |
Also Published As
Publication number | Publication date |
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WO2013044684A1 (zh) | 2013-04-04 |
CN102522209A (zh) | 2012-06-27 |
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Address after: 100038 Beijing city Xicheng District nancaiyuan Street No. 2, building 2, room 491 Patentee after: Beijing Zhongke taineng Technology Group Co. Ltd. Address before: 100038 Beijing city Xicheng District nancaiyuan Street No. 2, building 2, room 491 Patentee before: Zhongke Tienam (Beijing) Technology Development Co. Ltd. |