CN102499373A - Siraitia grosvenorii seed oil microcapsule powder and preparation method thereof - Google Patents
Siraitia grosvenorii seed oil microcapsule powder and preparation method thereof Download PDFInfo
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- CN102499373A CN102499373A CN2011103715799A CN201110371579A CN102499373A CN 102499373 A CN102499373 A CN 102499373A CN 2011103715799 A CN2011103715799 A CN 2011103715799A CN 201110371579 A CN201110371579 A CN 201110371579A CN 102499373 A CN102499373 A CN 102499373A
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Abstract
The invention discloses siraitia grosvenorii seed oil microcapsule powder and a preparation method thereof. The siraitia grosvenorii seed oil microcapsule powder mainly comprises raw materials according to a certain weight part ratio, wherein the raw materials comprise beta-cyclodextrin, acacia gum, glycerin monostearate and siraitia grosvenorii seed oil. According to the present invention, the beta-cyclodextrin and the acacia gum are adopted as wall materials, and microencapsulation is performed on the siraitia grosvenorii seed oil at a low temperature. With the present invention, the prepared siraitia grosvenorii seed oil microcapsule is the powder; the encapsulation rate of the siraitia grosvenorii seed oil is more than 85%; the good fluidity is provided; the oxidations of the siraitia grosvenorii seed oil unsaturated fatty acid and squalene are avoided; the activity of the siraitia grosvenorii seed oil can be maintained well; the stability of the siraitia grosvenorii seed oil is increased; the unpleasant odor of the siraitia grosvenorii seed oil is masked; the bioavailability of the siraitia grosvenorii seed oil is improved; the preservation time of the siraitia grosvenorii seed oil can be effectively prolonged; and the microcapsule adopts the edible raw materials as the wall materials, and can be eaten directly, such that the transport and the use of the siraitia grosvenorii seed oil are convenient to perform.
Description
Technical field
The present invention relates to food and field of health care products, be specifically related to Momordica grosvenori seed oil microcapsule powder and preparation method thereof.
Technical background
Momordica grosvenori (Siraitia grosvenorii (Swingle) C.Jeffery), the ripening fruits of Curcurbitaceae (Cucurbitacease) Momordica grosvenori platymiscium mainly is distributed in areas such as Guangdong and Guangxi Provinces, Guizhou, Jiangxi, Hunan.In the Hong Kong and Macao, Southeast Asia and American-European countries have long enjoyed a good reputation, and be rather well received.Momordica grosvenori contains abundant polysaccharide, vitamin, unrighted acid and multiple trace element and amino acid to the human body beneficial; Have treatment coronary heart disease and the angiosclerotic effect of prevention; Be the natural tonic that builds up one's health and prolong one's life among the people, multiple common disease is had magical curative effect, the good reputation of " the refreshing fruit in east; China one is exhausted " is therefore arranged, classified as national famous and precious medicine-food two-purpose medicinal material.Fat content is 27～33% in the Momordica grosvenori seed according to one's analysis, and wherein linoleic acid, oleic acid, palmitic acid account for 77% of TFA, and squalene accounts for seed kernel oil more than 12.5%, is the highest crude vegetal of finding at present of a kind of squalene content.But the easy oxidations of active ingredient such as unrighted acid and squalene in the Momordica grosvenori seed cause the loss of nutrition and quality to descend.
Microcapsules technology is to be the wall material with natural or synthetic macromolecular material, and core substances such as liquid, solid or gas are carried out packing, forms the technology of a kind of microencapsulation with semi permeability or sealing cyst membrane.Microcapsules technology is can make natural or active ingredient be able to keep in the food processing or one of the modern food new and high technology that slowly discharges; Along with reaching its maturity of microcapsules technology; It also enlarges in the Application in Food Industry scope gradually; The heartwood scope of development and application also more and more enlarges, and the while is also constantly developed with the new coating material that various different materials adapt.Many Microencapsulation Method successfully have been applied to flavour of food products composition, food additives, food function property composition; For example in the embedding of polyunsaturated fatty acid such as EPA and DHA; Can reduce the oxidation deterioration of nutritive loss and polyunsaturated fatty acid, but to the oily rarely seen document announcement of Research of Microencapsulation of Momordica grosvenori seed.Because microencapsulation can improve physical propertys such as the color, outward appearance, apparent density, dissolubility of the material that is wrapped; Improve the stability of core substance, improve reactivity, durability, thermal sensitivity and the light sensitivity of the material that is wrapped; Odor barrier; Make medicine have characteristics such as target function, slow-release function; Thereby become current one of many uses and develop new technology rapidly; The application of having succeeded in many fields such as medicine, agricultural, chemical industry, biotechnologys is in the research of field of food industry with use also very extensive.
The content that contains a large amount of unrighted acids, particularly squalene in the Momordica grosvenori seed oil is higher, but unrighted acid and the easy oxidation of squalene in the Momordica grosvenori seed oil causes the loss of nutrition and quality to descend, even can produce some harmful materials.Microencapsulation can prevent the oxidation of unrighted acid and squalene in the Momordica grosvenori seed oil, prolongs its storage period.
Summary of the invention
The purpose of this invention is to provide a kind of oxidation that prevents unrighted acid and squalene in the Momordica grosvenori seed oil, prolong Momordica grosvenori seed oil microcapsule powder of its storage period and preparation method thereof.
For achieving the above object, technical scheme of the present invention is:
A kind of Momordica grosvenori seed oil microcapsule powder is characterized in that being made up of the raw material of following weight portion:
10～30 parts of beta-schardinger dextrin-s; 150～180 parts of Arabic gums; 5～10 parts of monoglycerides; 50～90 parts of Momordica grosvenori seed oil; Surplus is a water.
The preparation method's of Momordica grosvenori seed oil microcapsule step is following:
(1) beta-schardinger dextrin-with 10～30 parts of weight portions adds in 400～600 parts of water; Under 55～60 ℃ condition, be stirred to the beta-schardinger dextrin-dissolving; The Arabic gum that adds 150～180 parts then continues to be stirred to dissolving fully, forms beta-schardinger dextrin-and Arabic gum water solution A;
(2) 5～10 parts of monoglycerides of weight portion and 50～90 parts of Momordica grosvenori seeds oil are added in 80～120 parts of water, stir, form emulsion B after being heated to 50 ℃ of dissolvings.
(3) with step 1) and step 2) in the beta-schardinger dextrin-and the Arabic gum water solution A that form mix with emulsion B; Adding water to total weight parts is 1000 parts; With cutter at 5000～8000rpm down cut, 3～5min; Under 15～30Mpa pressure, pass through the high pressure homogenizer homogeneous 2～3 times then, form the emulsion C of Momordica grosvenori seed oil average grain diameter less than 1000nm.
(4) the emulsion C that forms in the step 3) is carried out spray-drying process, promptly obtain Momordica grosvenori seed oil microcapsule powder.
Technology simple possible of the present invention is the wall material with beta-schardinger dextrin-and Arabic gum, at a lower temperature Momordica grosvenori seed oil is carried out microencapsulation; Prepared Momordica grosvenori seed oil microcapsule is a kind of powder, and the embedding rate of Momordica grosvenori seed oil has good flowability more than 85%; Avoid the oxidation of Momordica grosvenori seed oil unrighted acid and squalene, can keep Momordica grosvenori seed oil active preferably, increased the stability of Momordica grosvenori seed oil; Covered the offending smell of Momordica grosvenori seed oil; Improved the bioavilability of Momordica grosvenori seed oil, can prolong the holding time of Momordica grosvenori seed oil effectively, microcapsules adopt edible raw material as the wall material; Can directly eat, thereby make things convenient for Momordica grosvenori seed oily transportation and use.
The specific embodiment
Below the present invention is set forth as further through embodiment.
Embodiment 1
(1) 10 parts of beta-schardinger dextrin-s of weight portion is added in 400 parts of water, under the condition of 55 ℃ of temperature, be stirred to the beta-schardinger dextrin-dissolving, add 180 parts of Arabic gums then and continue to be stirred to dissolving fully, form A liquid.
(2) 5 parts of monoglycerides of weight portion and 80 parts of Momordica grosvenori seed oil are added in 80 parts of entry, be heated to and form B liquid after 50 ℃ of stirring and dissolving.
(3) A liquid and B liquid are mixed, adding water to total weight parts is 1000 parts, at 5000rpm down cut 3min, under 25Mpa pressure, passes through the high pressure homogenizer homogeneous 3 times with cutter then, obtains equal emulsion C.
(4) emulsion C is carried out spray-drying process under 190 ℃ of EATs, 60 ℃ of conditions of leaving air temp, promptly obtain Momordica grosvenori seed oil microcapsule powder.Embedding rate can reach 90.4%.
Embodiment 2
(1) beta-schardinger dextrin-with 15 parts of weight portions adds in 450 parts of entry, under 56 ℃ condition, is stirred to the beta-schardinger dextrin-dissolving, adds 165 parts of Arabic gums of weight portion then and continues to be stirred to dissolving fully, forms A liquid.
(2) 6 parts of monoglycerides of weight portion and 60 parts of Momordica grosvenori seed oil are added in 85 parts of entry, be heated to and form B liquid after 50 ℃ of stirring and dissolving.
(3) A liquid and B liquid are mixed, adding water to total weight parts is 1000 parts, at 8000rpm down cut 3min, under 30Mpa pressure, passes through the high pressure homogenizer homogeneous 3 times with cutter then, obtains equal emulsion C.
(4) emulsion C is carried out spray-drying process under 180 ℃ of EATs, 60 ℃ of conditions of leaving air temp, promptly obtain Momordica grosvenori seed oil microcapsule powder.Embedding rate can reach 88.08%.
Embodiment 3
(1) 30 parts of beta-schardinger dextrin-s of weight portion is added in 470 parts of water, under 67 ℃ condition, be stirred to the beta-schardinger dextrin-dissolving, add 180 parts of Arabic gums of weight portion then and continue to be stirred to dissolving fully, form A liquid.
(2) 7 parts of monoglycerides of weight portion and 90 parts of Momordica grosvenori seeds oil are added in 90 parts of water, form B liquid after being heated to 50 ℃ of stirring and dissolving.
(3) A liquid and B liquid are mixed, adding water to total weight parts is 1000 parts, at 8000rpm down cut 3min, under 20Mpa pressure, passes through the high pressure homogenizer homogeneous 3 times with cutter then, obtains equal emulsion C.
(4) emulsion C is carried out spray-drying process under 170 ℃ of EATs, 50 ℃ of conditions of leaving air temp, promptly obtain Momordica grosvenori seed oil microcapsule powder.Embedding rate can reach 85.5%.
Embodiment 4
(1) 10 parts of beta-schardinger dextrin-s of weight portion is added in 500 parts of water, under 60 ℃ condition, be stirred to the beta-schardinger dextrin-dissolving, add 160 parts of Arabic gums of weight portion then and continue to be stirred to dissolving fully, form A liquid.
(2) 10 parts of monoglycerides of weight portion and 90 parts of Momordica grosvenori seed oil are added in 100 parts of entry, be heated to and form B liquid after 50 ℃ of stirring and dissolving.
(3) A liquid and B liquid are mixed, adding water to total weight parts is 1000 parts, at 6000rpm down cut 5min, under 15Mpa pressure, passes through the high pressure homogenizer homogeneous 3 times with cutter then, obtains equal emulsion C.
(4) emulsion C is carried out spray-drying process under 170 ℃ of EATs, 60 ℃ of conditions of leaving air temp, promptly obtain Momordica grosvenori seed oil microcapsule powder.Embedding rate can reach 95.45%.
Embodiment 5
(1) 20 parts of beta-schardinger dextrin-s of weight portion is added in 550 parts of water, under 60 ℃ condition, be stirred to the beta-schardinger dextrin-dissolving, add 170 parts of Arabic gums of weight portion then and continue to be stirred to dissolving fully, form A liquid.
(2) 9 parts of monoglycerides of weight portion and 50 parts of Momordica grosvenori seed oil are added in 110 parts of entry, be heated to and form B liquid after 50 ℃ of stirring and dissolving.
(3) A liquid and B liquid are mixed, adding water to total weight parts is 1000 parts, at 5000rpm down cut 5min, under 25Mpa pressure, passes through the high pressure homogenizer homogeneous 3 times with cutter then, obtains equal emulsion C.
(4) emulsion C is carried out spray-drying process under 175 ℃ of EATs, 50 ℃ of conditions of leaving air temp, promptly obtain Momordica grosvenori seed oil microcapsule powder.Embedding rate can reach 88.67%.
Embodiment 6
(1) 15 parts of beta-schardinger dextrin-s of weight portion is added in 600 parts of entry, under 60 ℃ condition, be stirred to the beta-schardinger dextrin-dissolving, add 180 parts of Arabic gums of weight portion then and continue to be stirred to dissolving fully, form A liquid.
(2) with weight portion 5g monoglyceride, 60g Momordica grosvenori seed oil adds in 120 parts of entry, is heated to and forms B liquid after 50 ℃ of stirring and dissolving.
(3) A liquid and B liquid are mixed, adding water to total weight parts is 1000 parts, at 8000rpm down cut 4min, under 30Mpa pressure, passes through the high pressure homogenizer homogeneous 3 times with cutter then, obtains equal emulsion C.
(4) emulsion C is carried out spray-drying process under 180 ℃ of EATs, 50 ℃ of conditions of leaving air temp, promptly obtain Momordica grosvenori seed oil microcapsule powder.Embedding rate can reach 87.4%.
Claims (4)
1. Momordica grosvenori seed oil microcapsule powder is characterized in that being made up of the raw material of following weight portion:
10～30 parts of beta-schardinger dextrin-s; 150～180 parts of Arabic gums; 5～10 parts of monoglycerides; 50～90 parts of Momordica grosvenori seed oil; Surplus is a water.
2. Momordica grosvenori seed oil microcapsule powder according to claim 1 is characterized in that the step of its preparation method is following:
(1) beta-schardinger dextrin-with 10～30 parts of weight portions adds in 400～600 parts of water; Under 55～60 ℃ condition, be stirred to the beta-schardinger dextrin-dissolving; The Arabic gum that adds 150～180 parts then continues to be stirred to dissolving fully, forms beta-schardinger dextrin-and Arabic gum water solution A;
(2) 5～10 parts of monoglycerides of weight portion and 50～90 parts of Momordica grosvenori seeds oil are added in 800～120 parts of water, stir, form emulsion B after being heated to 50 ℃ of dissolvings;
(3) with step 1) and step 2) in the beta-schardinger dextrin-and the Arabic gum water solution A that form mix with emulsion B; Adding water to total weight parts is 1000 parts; With cutter at 5000～8000rpm down cut, 3～5min; Under 15～30Mpa pressure, pass through the high pressure homogenizer homogeneous 2～3 times then, form the emulsion C of Momordica grosvenori seed oil average grain diameter less than 1000nm;
(4) the emulsion C that forms in the step 3) is carried out spray-drying process, promptly obtain Momordica grosvenori seed oil microcapsule powder.
3. Momordica grosvenori seed oil microcapsule powder according to claim 1 is characterized in that being made up of the raw material of following weight portion:
10 parts of beta-schardinger dextrin-s; 160 parts of Arabic gums, 10 parts of monoglycerides; 90 parts of Momordica grosvenori seed oil; Surplus is a water.
4. Momordica grosvenori seed oil microcapsule powder according to claim 1 is characterized in that its preparation method comprises the steps:
(1) 10 parts of beta-schardinger dextrin-s of weight portion is added in 500 parts of water, under 60 ℃ condition, be stirred to the beta-schardinger dextrin-dissolving, add 160 parts of Arabic gums of weight portion then and continue to be stirred to dissolving fully, form A liquid;
(2) 10 parts of monoglycerides of weight portion and 90 parts of Momordica grosvenori seed oil are added in 100 parts of entry, be heated to and form B liquid after 50 ℃ of stirring and dissolving.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2011103715799A CN102499373B (en) | 2011-11-21 | 2011-11-21 | Siraitia grosvenorii seed oil microcapsule powder and preparation method thereof |
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| CN2011103715799A CN102499373B (en) | 2011-11-21 | 2011-11-21 | Siraitia grosvenorii seed oil microcapsule powder and preparation method thereof |
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| CN102499373B CN102499373B (en) | 2013-07-10 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103571625A (en) * | 2013-06-21 | 2014-02-12 | 伊犁紫苏丽人生物科技有限公司 | Lavender essential oil microcapsule and preparation process thereof |
| CN106262933A (en) * | 2016-11-08 | 2017-01-04 | 浙江工业大学 | A kind of preparation method of Vitamin E contained micro capsule |
| CN106579448A (en) * | 2016-12-26 | 2017-04-26 | 齐齐哈尔大学 | Preparation method of groundcherry seed oil microcapsule |
| CN115227624A (en) * | 2022-08-30 | 2022-10-25 | 北京臻味坊食品有限公司 | Infant skin care oil containing nut oil |
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| CN101703491A (en) * | 2009-08-10 | 2010-05-12 | 北京市金康普食品添加剂科技有限公司 | Vitamin a powder and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103571625A (en) * | 2013-06-21 | 2014-02-12 | 伊犁紫苏丽人生物科技有限公司 | Lavender essential oil microcapsule and preparation process thereof |
| CN106262933A (en) * | 2016-11-08 | 2017-01-04 | 浙江工业大学 | A kind of preparation method of Vitamin E contained micro capsule |
| CN106579448A (en) * | 2016-12-26 | 2017-04-26 | 齐齐哈尔大学 | Preparation method of groundcherry seed oil microcapsule |
| CN115227624A (en) * | 2022-08-30 | 2022-10-25 | 北京臻味坊食品有限公司 | Infant skin care oil containing nut oil |
| CN115227624B (en) * | 2022-08-30 | 2023-11-14 | 北京臻味坊食品有限公司 | Infant skin care oil containing nut oil |
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| Publication number | Publication date |
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| CN102499373B (en) | 2013-07-10 |
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