CN102429835B - Keratin hairspray for hair and modeling products for hair - Google Patents
Keratin hairspray for hair and modeling products for hair Download PDFInfo
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- CN102429835B CN102429835B CN 201110390600 CN201110390600A CN102429835B CN 102429835 B CN102429835 B CN 102429835B CN 201110390600 CN201110390600 CN 201110390600 CN 201110390600 A CN201110390600 A CN 201110390600A CN 102429835 B CN102429835 B CN 102429835B
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Abstract
The invention discloses a keratin hairspray for hair, which consists of a keratin extracted from human hair or animal hair and having a molecular weight of 60,000-150,000 daltons and a vinyl pyrrolidone/vinyl acetate copolymer. The weight ratio of the keratin to the vinyl pyrrolidone/vinyl acetate copolymer is 0.2-3: 1. Modeling products for the hair, which are provided by the invention, comprise gel water, fixature and mousse, and the gel water, the fixature and the mousse all comprise the keratin hairspray for the hair.
Description
Technical field
The invention belongs to the hair-dressing article field, particularly for setting agent and the product of hair fixing.
Background technology
Along with the day by day raising of living standard, people are more and more higher to the requirement of U.S., more pursue natural beauty, require it more natural to hair-dressing article.Many researcheres have also been carried out many researchs, wish to obtain more near the beauty of nature hair care product.Hou Huiyu (Chemical Industry in Guangzhou; 2 (38), 2010 :) studied the character of vinyl pyrrolidone, the synthetic and character of homopolymer, and the film forming in the hair conditioning style series products, lubricated in the skin type product, the application in moisturizing and the film forming.Patent ZL200510007990.2 discloses a kind of method and composition of shaping of keratin fibers, preferred human keratin fiber, the method of hair particularly, it comprises following two key steps: use the cosmetic composition that comprises at least a anionic shaped polymer and at least a non-ionic compound to keratin fiber, described non-ionic compound is selected from aliphatic alcohol, polyhydric alcohol and siloxanes are so that the ratio of anionic shaped polymer/non-ionic compound is greater than 1; And after one period optional action time, keratin fiber is contacted with the heater of the described keratin fiber of can finalizing the design; This patent application also relates to employed compositions.CN101955566A discloses a kind of ternary amphoteric ion type hair styling polymer and preparation method thereof, described hair styling polymer is acrylic acid (salt) class monomer and 15～30% nitrogenous class reactive monomers that the function of anion is provided by 40～70% vinyl pyrrolidone main body reactive monomers, 15～30%, take hydroxyl micromolecule polar compound as reaction medium, take azo-bis-isobutyl cyanide or organic peroxide as catalyst, by the polymerisation in solution of free radical, and polymer is carried out the season ammonification process and form.CN1391882A discloses a kind of natural keratin hair shaping liquid, described style keeping liquid by hydrolysis of keratin, siloxanes, glycerol, carbamide, fruit acid, pure water through mixing.Although above-mentioned hair styling agent, approved product respectively have its characteristics, but still remain further to be improved its performance, to satisfy the demand of people's hair caring and protection hair.
Summary of the invention
The object of the present invention is to provide a kind of hair keratin setting agent and use the hair styling product of its preparation, so that make human hair at aspects such as gloss, elasticity, feels more near the nature kenel, and to because of the hair-waving, hair dyeing, ultraviolet light, the damage that air pollution etc. cause human hair has certain repair function.
Hair keratin setting agent of the present invention, be that the daltonian keratin of 60000-150000 and vinyl pyrrolidone/vinyl acetate copolymer form by the molecular weight that extracts in Crinis Carbonisatus or the animal hair, the weight ratio of described keratin and vinyl pyrrolidone/vinyl acetate copolymer is 0.2～3: 1.Described keratin both can be bought by market, also can prepare voluntarily; Described vinyl pyrrolidone/vinyl acetate copolymer is bought by market.
Hair styling product of the present invention comprise hair gel, hair jelly and mousse, and are formulated by above-mentioned hair keratin setting agent and other component.
1, hair gel
The component of hair gel of the present invention comprises keratin setting agent, triethanolamine, surfactant, ethanol and pure water, and the percetage by weight of each component is as follows:
Hair gel of the present invention, its component also comprises antiseptic and essence, the percetage by weight of each component is as follows:
In the hair gel of the present invention, described keratin setting agent is above-mentioned hair keratin setting agent; Described surfactant is at least a in laureth-9, nonyl phenol polyethers-10, castor oil hydrogenated, sodium laureth sulfate, the lauryl glucoside; Described pure water is deionized water or distilled water.
The preparation method of hair gel of the present invention: pure water is joined in the ingredients pot, then under agitation add ethanol, surfactant, triethanolamine, keratin setting agent and antiseptic in room temperature, normal pressure, after mixing equal Uniform, essence is added in the ingredients pot after with dissolve with ethanol, continue to stir at least 1 hour, continue after usefulness 300 mesh filter screens filter the discharging bottling.
2, hair jelly
Hair jelly of the present invention, its component comprises keratin setting agent and ethanol, and the percetage by weight of keratin setting agent is 5%～15%, and the percetage by weight of ethanol is 85%～95%.
Hair jelly of the present invention also comprises essence, and described essence is 0.5%～1% of ethanol weight.。
In the hair jelly of the present invention, described keratin setting agent is above-mentioned hair keratin setting agent.
Hair jelly preparation method of the present invention is: keratin setting agent and ethanol are added in the ingredients pot, be stirred to dissolving under room temperature, normal pressure, then add essence, continue to stir again and can bottle at least 30 minutes.
3, mousse
The component of mousse of the present invention comprises keratin setting agent, triethanolamine, surfactant and pure water, and the percetage by weight of each component is as follows:
Mousse of the present invention, its component also comprises antiseptic and essence, the percetage by weight of each component is as follows:
In the mousse of the present invention, described keratin setting agent is above-mentioned hair keratin setting agent; Described surfactant is at least a in laureth-9, nonyl phenol polyethers-10, castor oil hydrogenated, sodium laureth sulfate, the lauryl glucoside; Described pure water is deionized water or distilled water.
The preparation method of mousse of the present invention is: pure water is joined in the ingredients pot, then under agitation add keratin setting agent, triethanolamine, surfactant, essence and antiseptic in room temperature, normal pressure, stir bottling after at least 2 hours.
The present invention has following beneficial effect:
1, hair keratin setting agent of the present invention and approved product thereof energy holding head is from right bending, make hair have gloss and keep suitable moisture and (contain hydroxyl owing in the keratin, hydrone there is certain affinity, thereby make the hair after its typing keep certain moisture, more near the nature hair quality).
2, because approved product of the present invention all contains hair keratin setting agent of the present invention, thereby approved product of the present invention can be in the hair surface film forming, and the human hair damage that hair-waving, hair dyeing, ultraviolet light, air pollution etc. are caused has certain repair.
3, use approved product of the present invention to hair fixing, not only shaping time is longer, and hair hardness is moderate, and is easy to be cleaned by shampoo.
4, through check, approved product of the present invention meets sanitary index, and concrete data see the following form:
Sanitary index
Hair gel organoleptic indicator, physical and chemical index
Mousse sense organ, physical and chemical index
Hair jelly sense organ, physical and chemical index
The specific embodiment
Below by embodiment hair keratin setting agent of the present invention and approved product are described further.Among following each embodiment, vinyl pyrrolidone/vinyl acetate copolymer is available from ISP (international special product company).
Embodiment 1: the preparation keratin
Human hair's (or Pilus Caprae seu Ovis) is cleaned up rear pulverizing, be 11 with pH value, the TGA sodium solution of concentration 0.5mol/L (sodium hydroxide is regulated pH) is at normal pressure, room temperature (20 ℃～30 ℃) pretreatment 3 hours, then in solution, add carbamide, the addition of carbamide reaches 7mol/L for the concentration in solution, continue after at normal pressure, room temperature (20 ℃～30 ℃) reduction reaction 25 hours, after response time expires, splash into the pH value to 6 of acetic acid conditioned reaction liquid～8, then in solution, pass into oxygen, room temperature (20 ℃～30 ℃) reaction 0.5 hour, after response time expires, normal pressure filters, filtrate is carried out dialysis with the dialysis bag of holding back relative molecular weight 20～80kD, it is 60000～150000 daltonian keratin solution first products that centrifugalize obtains molecular weight, the keratin solution first product saltoutd obtain the keratin solid, drying at room temperature is 6 hours under vacuum (5-10mmHg post) condition, namely obtaining molecular weight is 60000～150000 daltonian keratin, yield 42%.
Embodiment 2: the preparation hair gel
In the present embodiment, hair gel is prepared from by hair keratin setting agent, triethanolamine, laureth-9, castor oil hydrogenated, ethanol, essence, methylchloroisothiazandnone and deionized water, and the percetage by weight of above-mentioned each component is as follows:
Preparation method:
1, the preparation of hair keratin setting agent
Keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 1: 4 (weight ratio), under room temperature, normal pressure, with described keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously, namely form hair keratin setting agent;
2, the preparation of hair gel
Under room temperature, normal pressure, the 824.5Kg deionized water is joined in the ingredients pot, then add ethanol 80Kg, hair keratin setting agent 50Kg, laureth-9 10Kg, castor oil hydrogenated 10Kg, triethanolamine 1Kg, methylchloroisothiazandnone 0.5Kg and be stirred to equal Uniform, essence 4Kg is dissolved in the 20Kg ethanol adds again in the ingredients pot, continue after continuation stirred 1 hour, after mixing time expires, filter with 300 mesh filter screens, filtrate is hair gel.
Embodiment 3: the preparation hair gel
In the present embodiment, hair gel is prepared from by hair keratin setting agent, triethanolamine, lauryl glucoside, castor oil hydrogenated, ethanol and distilled water, and the percetage by weight of above-mentioned each component is as follows
Preparation method:
1, the preparation of hair keratin setting agent
Keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 1: 1 (weight ratio), under room temperature, normal pressure, with described keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously, namely form hair keratin setting agent;
2, the preparation of hair gel
Under room temperature, normal pressure 859.5Kg being distilled sub-water joins in the ingredients pot, then add ethanol 50Kg, hair keratin setting agent 80Kg, lauryl glucoside 5Kg, castor oil hydrogenated 5Kg, triethanolamine 0.5Kg and be stirred to equal Uniform, filter with 300 mesh filter screens, filtrate is hair gel.
Embodiment 4: the preparation hair gel
In the present embodiment, hair gel is prepared from by hair keratin setting agent, triethanolamine, nonyl phenol polyethers-10, sodium laureth sulfate, ethanol, essence, methylchloroisothiazandnone and deionized water, and the percetage by weight of above-mentioned each component is as follows:
Preparation method:
1, the preparation of hair keratin setting agent
Keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 2: 1 (weight ratio), under room temperature, normal pressure, with described keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously, namely form hair keratin setting agent;
2, the preparation of hair gel
Under room temperature, normal pressure, the 771.5Kg deionized water is joined in the ingredients pot, then add ethanol 60Kg, hair keratin setting agent 120Kg, nonyl phenol polyethers-10 10Kg, sodium laureth sulfate 8Kg, triethanolamine 1.5Kg, methylchloroisothiazandnone 1Kg and be stirred to equal Uniform, essence 8Kg is dissolved in the 20Kg ethanol adds again in the ingredients pot, continue after continuation stirred 1 hour, after mixing time expires, filter with 300 mesh filter screens, filtrate is hair gel.
Embodiment 5: the preparation hair gel
In the present embodiment, hair gel is prepared from by hair keratin setting agent, triethanolamine, laureth-9, ethanol, essence, methylchloroisothiazandnone and distilled water, and the percetage by weight of above-mentioned each component is as follows:
1, the preparation of hair keratin setting agent
Keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 3: 1 (weight ratio), under room temperature, normal pressure, with described keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously, namely form hair keratin setting agent;
2, the preparation of hair gel
Under room temperature, normal pressure, the 730.3Kg distilled water is joined in the ingredients pot, then add ethanol 80Kg, hair keratin setting agent 150Kg, laureth-9 15Kg, triethanolamine 1Kg, methylchloroisothiazandnone 0.7Kg and be stirred to equal Uniform, essence 3Kg is dissolved in the 20Kg ethanol adds again in the ingredients pot, continue after continuation stirred 1 hour, after mixing time expires, filter with 300 mesh filter screens, filtrate is hair gel.
Embodiment 6: the preparation hair jelly
In the present embodiment, hair jelly is prepared from by hair keratin setting agent, ethanol and essence, and the percetage by weight of above-mentioned each component is as follows:
Hair keratin setting agent 5%
Alcohol 95 %
Essence is 1% of ethanol weight;
Preparation method:
1, the preparation of hair keratin setting agent
Keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 3: 1 (weight ratio), under room temperature, normal pressure, with described keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously, namely form hair keratin setting agent;
2, the preparation of hair jelly
Under room temperature, normal pressure, hair keratin setting agent 50Kg, alcohol 95 0Kg are added in the ingredients pot, be stirred to hair keratin setting agent and dissolve rear adding essence 9.5Kg fully, continue again stirring and namely formed hair jelly in 30 minutes.
Embodiment 7: the preparation hair jelly
In the present embodiment, hair jelly is prepared from by hair keratin setting agent, ethanol and essence, and the percetage by weight of above-mentioned each component is as follows:
Hair keratin setting agent 7%
Ethanol 93%
Essence is 0.8% of ethanol weight;
Preparation method:
1, the preparation of hair keratin setting agent
Keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 2: 5 (weight ratio), under room temperature, normal pressure, with described keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously, namely form hair keratin setting agent;
2, the preparation of hair jelly
Under room temperature, normal pressure, hair keratin setting agent 70Kg, ethanol 930Kg are added in the ingredients pot, be stirred to hair keratin setting agent and dissolve rear adding essence 7.4Kg fully, continue again stirring and namely formed hair jelly in 30 minutes.
Embodiment 8: the preparation hair jelly
In the present embodiment, hair jelly is prepared from by hair keratin setting agent, ethanol and essence, and the percetage by weight of above-mentioned each component is as follows:
Hair keratin setting agent 11%
Ethanol 89%
Essence is 0.5% of ethanol weight;
Preparation method:
1, the preparation of hair keratin setting agent
Keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 1: 1 (weight ratio), under room temperature, normal pressure, with described keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously, namely form hair keratin setting agent;
2, the preparation of hair jelly
Under room temperature, normal pressure, hair keratin setting agent 110Kg, ethanol 890Kg are added in the ingredients pot, be stirred to hair keratin setting agent and dissolve rear adding essence 4.5Kg fully, continue again stirring and namely formed hair jelly in 30 minutes.
Embodiment 9: the preparation hair jelly
In the present embodiment, hair jelly is prepared from by hair keratin setting agent and ethanol, and the percetage by weight of above-mentioned each component is as follows:
Hair keratin setting agent 15%
Ethanol 85%;
Preparation method:
1, the preparation of hair keratin setting agent
Keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 0.2: 1 (weight ratio), under room temperature, normal pressure, with described keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously, namely form hair keratin setting agent;
2, the preparation of hair jelly
Under room temperature, normal pressure, hair keratin setting agent 150Kg, ethanol 850Kg are added in the ingredients pot, continue again to stir after being stirred to hair keratin setting agent and dissolving fully and namely formed hair jelly in 30 minutes.
Embodiment 10: the preparation mousse
In the present embodiment, mousse is prepared from by hair keratin setting agent, triethanolamine, lauryl glucoside, sodium laureth sulfate, essence, methylchloroisothiazandnone and distilled water, and the percetage by weight of above-mentioned each component is as follows:
Preparation method:
1, the preparation of hair keratin setting agent
Keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 0.2: 1 (weight ratio), under room temperature, normal pressure, with described keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously, namely form hair keratin setting agent;
2, the preparation of mousse
Under room temperature, normal pressure, the 865.5Kg distilled water is joined in the ingredients pot, then add hair keratin setting agent 100Kg, triethanolamine 10Kg, lauryl glucoside 10Kg, sodium laureth sulfate 10Kg, essence 4Kg, methylchloroisothiazandnone 0.5Kg, stir and namely formed mousse in 2 hours.
Embodiment 11: the preparation mousse
In the present embodiment, mousse is prepared from by hair keratin setting agent, triethanolamine, laureth-9, nonyl phenol polyethers-10, essence, methylchloroisothiazandnone and deionized water, and the percetage by weight of above-mentioned each component is as follows:
Preparation method:
1, the preparation of hair keratin setting agent
Keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 3: 1 (weight ratio), under room temperature, normal pressure, with described keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously, namely form hair keratin setting agent;
2, the preparation of mousse
Under room temperature, normal pressure, the 833.3Kg deionized water is joined in the ingredients pot, then add hair angle egg setting agent 150Kg, triethanolamine 5Kg, laureth-9 5Kg, nonyl phenol polyethers-10 5Kg, essence 1Kg, Methylisothiazolinone 0.7Kg, stir and namely formed mousse in 2 hours.
Embodiment 12: the preparation mousse
In the present embodiment, mousse is prepared from by hair keratin setting agent, triethanolamine, castor oil hydrogenated, lauryl glucoside, essence, methylchloroisothiazandnone and deionized water, and the percetage by weight of above-mentioned each component is as follows:
Preparation method:
1, the preparation of hair keratin setting agent
Keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 0.5: 1 (weight ratio), under room temperature, normal pressure, with described keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously, namely form hair keratin setting agent;
2, the preparation of mousse
Under room temperature, normal pressure, the 798.4Kg deionized water is joined in the ingredients pot, then add hair angle egg setting agent 160Kg, triethanolamine 15Kg, castor oil hydrogenated 15Kg, lauryl glucoside 5Kg, essence 6Kg, methylchloroisothiazandnone 0.6Kg, stir and namely formed mousse in 2 hours.
Embodiment 13 preparation mousses
In the present embodiment, mousse is prepared from by hair keratin setting agent, triethanolamine, castor oil hydrogenated, lauryl glucoside, essence, methylchloroisothiazandnone and deionized water, and the percetage by weight of above-mentioned each component is as follows:
Preparation method:
1, the preparation of hair keratin setting agent
Keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 1: 1 (weight ratio), under room temperature, normal pressure, with described keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously, namely form hair keratin setting agent;
2, the preparation of mousse
Under room temperature, normal pressure, the 780Kg deionized water is joined in the ingredients pot, then add hair angle egg setting agent 200Kg, triethanolamine 10Kg, nonyl phenol polyethers-10 10Kg, stir and namely formed mousse in 2 hours.
Embodiment 14: performance comparison test
1, test specimen
(1) hair gel of test specimen A: embodiment 3 preparations
(2) contrast of the hair gel of specimen sample B: embodiment 3 preparations, the percetage by weight of its each component is as follows:
(3) hair jelly of test specimen C: embodiment 7 preparations
(4) contrast of the hair jelly of specimen sample D: embodiment 7 preparations, the percetage by weight of its each component is as follows:
Vinyl pyrrolidone/vinyl acetate copolymer 7%
Ethanol 93%
Essence is 0.8% of ethanol weight.
(5) mousse of test specimen E: embodiment 11 preparations
(6) contrast of the mousse of test specimen F: embodiment 11 preparations, the percetage by weight of its each component is as follows:
2, method of testing
(1) topknot pretreatment: large topknot is cleaned with the sodium dodecyl sulfate solution of mass concentration 3%, then put into ether and soaked 24 hours; Large topknot after the ether processing is made the topknot of the long 23cm of multi beam, heavy 2g and the topknot of the long 15cm of multi beam, heavy 1.3g, then with the distilled water moistening of each topknot, and rub with the sodium dodecyl sulfate solution of mass concentration 3% and to wash 2～3 minutes, rinse well with tap water, naturally dry stand-by.
(2) crooked conservation degree test: on the topknot of long 23cm, heavy 2g, evenly coat respectively 0.7g test specimen A, B, C, D, E, F, then each topknot is twisted in respectively on the curly hair thick stick of 1.2cm, 50 ℃ of dryings 2 hours, after being cooled to room temperature, each topknot is taken off from the curly hair thick stick, a part is hung in 30 ℃, the constant temperature of 60%RH (relative humidity), constant humidity incubator, a part was hung in 30 ℃, the constant temperature of 90%RH, constant humidity incubator, detected respectively the length of respectively restrainting hair every 2 hours.
(3) the crooked Strong degree test of topknot: on the topknot of long 15cm, heavy 1.3g, evenly coat respectively 0.4g test specimen A, B, C, D, E, F, after the comb combing, be organized into respectively the wide tabular of 2cm that is, 50 ℃ of dryings 2 hours, then after 23 ℃, 60%RH (relative humidity) are placed 24 hours, lie on the support platform of interval 65mm, make central part crooked with 2cm/min speed, the heavy burden of when bending to 2cm, measuring it.
(4) destroy the test of Strong degree: on the angle of a right angle object, the speed of pinning with 15cm/s with hands firmly pulls with the topknot folding after the crooked Strong degree test, to the topknot fracture, measures maximum the heavy burden.
(5) play white test: on the topknot of long 23cm, heavy 2g, evenly coat respectively 0.7g test specimen A, B, C, D, E, F, 50 ℃ of dryings 2 hours, then placed 24 hours at 23 ℃, 60%RH (relative humidity), by 5 minutes code of points processed, estimated white phenomenon.1 has been divided into whitely serious, and 5 are divided into and not have in vain.
(6) brightness test: on the topknot of long 23cm, heavy 2g, evenly coat respectively 0.7g test specimen A, B, C, D, E, F, after the comb combing, be organized into respectively the wide tabular of 2cm that is, be fixed in the standard light source VERIVIDE COLOR ASSESMENT CABINET, press 5 minutes code of points processed by the evaluator, the assess sample brightness, 1 be divided into dark, 5 be divided into bright.
3 test results
Test result is seen following each table:
The crooked conservation degree test result of table 1: (30 ℃, 60%RH) unit: centimetre
| A | B | C | D | E | F | |
| 0 hour | 11 | 11 | 10.2 | 10.2 | 11.5 | 11.5 |
| 2 hours | 12.3 | 12.9 | 12.0 | 12.8 | 13.1 | 13.8 |
| 4 hours | 13.5 | 14.3 | 13.7 | 14.5 | 14.6 | 15.5 |
| 6 hours | 14.7 | 15.6 | 14.2 | 15.3 | 15.5 | 16.6 |
| 8 hours | 15.3 | 16.2 | 14.5 | 15.9 | 16.1 | 17.4 |
The crooked conservation degree test result of table 2: (30 ℃, 90%RH) unit: centimetre
| A | B | C | D | E | F | |
| 0 hour | 11.0 | 11.0 | 10.2 | 10.2 | 11.5 | 11.5 |
| 2 hours | 13.5 | 13.9 | 12.2 | 12.7 | 14.1 | 14.8 |
| 4 hours | 15.6 | 16.3 | 14.1 | 14.6 | 16.2 | 16.9 |
| 6 hours | 16.5 | 17.2 | 15.3 | 15.8 | 17.1 | 18.1 |
| 8 hours | 17.3 | 18.1 | 16.2 | 16.7 | 18.0 | 19.6 |
The crooked Strong degree of table 3 topknot test result: (23 ℃, 60%RH) unit: gram
| Sample | A | B | C | D | E | F |
| Bear a heavy burden | 6.0 | 6.5 | 8.0 | 8.7 | 5.2 | 5.9 |
Strong degree test result after table 4 destroys: unit gram
| Sample | A | B | C | D | E | F |
| Bear a heavy burden | 35 | 40 | 42 | 50 | 30 | 36 |
Table 5 a white test result
| Sample | A | B | C | D | E | F |
| Mark | 5 | 3 | 4 | 2 | 5 | 3 |
Table 6 brightness test result
| Sample | A | B | C | D | E | F |
| Mark | 5 | 3 | 5 | 4 | 5 | 3 |
Can find out from above-mentioned test result, the approved product that the approved product that adds hair keratin setting agent does not more add hair keratin setting agent at the curling conservation degree, play the aspect such as white, brightness and have more excellent performance.
Claims (8)
1. a hair gel is characterized in that component comprises keratin setting agent, triethanolamine, surfactant, ethanol and pure water, and the percetage by weight of each component is as follows:
Described keratin setting agent is that 60000 ~ 150000 daltonian keratin and vinyl pyrrolidone/vinyl acetate copolymer form by the molecular weight that extracts in Crinis Carbonisatus or the animal hair, and the weight ratio of described keratin and vinyl pyrrolidone/vinyl acetate copolymer is 0.2 ~ 3:1.
2. described hair gel according to claim 1 is characterized in that described surfactant is at least a in laureth-9, nonyl phenol polyethers-10, castor oil hydrogenated, sodium laureth sulfate, the lauryl glucoside; Described pure water is deionized water or distilled water.
3. described hair gel according to claim 1 and 2 characterized by further comprising antiseptic and essence, and the percetage by weight of antiseptic is 0.05% ~ 0.1%, and the percetage by weight of essence is 0.1% ~ 0.8%.
4. hair jelly, it is characterized in that component comprises keratin setting agent and ethanol, the percetage by weight of keratin setting agent is 5%～15%, the percetage by weight of ethanol is 85%～95%, described keratin setting agent is that 60000 ~ 150000 daltonian keratin and vinyl pyrrolidone/vinyl acetate copolymer form by the molecular weight that extracts in Crinis Carbonisatus or the animal hair, and the weight ratio of described keratin and vinyl pyrrolidone/vinyl acetate copolymer is 0.2 ~ 3:1.
5. hair jelly according to claim 4 characterized by further comprising essence, and essence is 0.5% ~ 1% of ethanol weight.
6. a mousse is characterized in that component comprises keratin setting agent, triethanolamine, surfactant and pure water, and the percetage by weight of each component is as follows:
Keratin setting agent 10% ~ 20%
Triethanolamine 0.5 ~ 1.5%
Surfactant 1% ~ 2%
Pure water 78% ~ 88%;
Described keratin setting agent is that 60000 ~ 150000 daltonian keratin and vinyl pyrrolidone/vinyl acetate copolymer form by the molecular weight that extracts in Crinis Carbonisatus or the animal hair, and the weight ratio of described keratin and vinyl pyrrolidone/vinyl acetate copolymer is 0.2 ~ 3:1.
7. described mousse according to claim 6 is characterized in that described surfactant is at least a in laureth-9, nonyl phenol polyethers-10, castor oil hydrogenated, sodium laureth sulfate, the lauryl glucoside; Described pure water is deionized water or distilled water.
8. according to claim 6 or 7 described mousses, characterized by further comprising antiseptic and essence, the percetage by weight of antiseptic is 0.05% ~ 0.1%, and the percetage by weight of essence is 0.1% ~ 0.8%.
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| CN106619173A (en) * | 2016-12-28 | 2017-05-10 | 安徽紫檀科技有限公司 | Hair styling agent and preparation method thereof |
| CN107519053A (en) * | 2017-09-11 | 2017-12-29 | 陈磊 | A kind of hair gel containing Composition of Meteorite and preparation method thereof |
| US20200270316A1 (en) * | 2017-11-10 | 2020-08-27 | Givaudan Sa | Silk Alcohol Formulations |
| WO2020117239A1 (en) * | 2018-12-06 | 2020-06-11 | Colgate-Palmolive Company | Personal care compositions |
| CN111643391A (en) * | 2020-07-22 | 2020-09-11 | 广州市圣莎拉化妆品有限公司 | Hair care product of hydrolyzed wheat protein and processing technology |
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| US4895722A (en) * | 1981-03-03 | 1990-01-23 | Kao Soap Co., Ltd. | Hair treatments |
| CN1241402A (en) * | 1998-07-14 | 2000-01-19 | 中山市田妃化妆品有限公司 | Hair conditioning gel |
| CN1391882A (en) * | 2002-06-25 | 2003-01-22 | 武乾鹰 | Natural keratin hair shaping liquid |
| CN101332159A (en) * | 2007-06-25 | 2008-12-31 | 陈丽妹 | Clear type gel |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003192546A (en) * | 2001-12-25 | 2003-07-09 | Lion Corp | Hair cosmetic |
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|---|---|---|---|---|
| US4895722A (en) * | 1981-03-03 | 1990-01-23 | Kao Soap Co., Ltd. | Hair treatments |
| CN1241402A (en) * | 1998-07-14 | 2000-01-19 | 中山市田妃化妆品有限公司 | Hair conditioning gel |
| CN1391882A (en) * | 2002-06-25 | 2003-01-22 | 武乾鹰 | Natural keratin hair shaping liquid |
| CN101332159A (en) * | 2007-06-25 | 2008-12-31 | 陈丽妹 | Clear type gel |
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| 第[0003]段，第[0005]段 |
| 第[0017]段第1-8行 |
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|---|---|
| CN102429835A (en) | 2012-05-02 |
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