CN102429835A - Keratin hairspray for hair and modeling products for hair - Google Patents
Keratin hairspray for hair and modeling products for hair Download PDFInfo
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- CN102429835A CN102429835A CN201110390600XA CN201110390600A CN102429835A CN 102429835 A CN102429835 A CN 102429835A CN 201110390600X A CN201110390600X A CN 201110390600XA CN 201110390600 A CN201110390600 A CN 201110390600A CN 102429835 A CN102429835 A CN 102429835A
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Abstract
The invention discloses a keratin hairspray for hair, which consists of a keratin extracted from human hair or animal hair and having a molecular weight of 60,000-150,000 daltons and a vinyl pyrrolidone/vinyl acetate copolymer. The weight ratio of the keratin to the vinyl pyrrolidone/vinyl acetate copolymer is 0.2-3: 1. Modeling products for the hair, which are provided by the invention, comprise gel water, fixature and mousse, and the gel water, the fixature and the mousse all comprise the keratin hairspray for the hair.
Description
Technical field
The invention belongs to the hair-dressing article field, particularly be used for the setting agent and the product of hair fixing.
Background technology
Along with the raising day by day of living standard, people require increasingly highly to U.S.A, more pursue natural beauty, require it more natural to hair-dressing article.Many researcheres have also been carried out many researchs, hope to obtain more near the beauty of nature hair care product.Hou Huiyu (Guangzhou chemical industry; 2 (38), 2010 :) studied the character of vinyl pyrrolidone, the synthetic and character of homopolymer, and the film forming in the hair conditioning style series products, lubricated in the skin type product, preserve moisture and film forming in application.Patent ZL200510007990.2 discloses a kind of method and composition of shaping of keratin fibers; Preferred human keratin fiber; The method of hair particularly, it comprises following two key steps: use the cosmetic composition that comprises at least a anionic shaped polymer and at least a non-ionic compound to keratin fiber, described non-ionic compound is selected from aliphatic alcohol; Polyhydric alcohol and siloxanes are so that the ratio of anionic shaped polymer/non-ionic compound is greater than 1; And after one period optional action time, keratin fiber is contacted with the heater of the said keratin fiber of can finalizing the design; This patent application also relates to employed compositions.CN101955566A discloses a kind of ternary amphoteric ion type hair styling polymer and preparation method thereof; Said hair styling polymer is acrylic acid (salt) type monomer and 15～30% nitrogenous types of reactive monomers that anionic function is provided by 40～70% vinyl pyrrolidone main body reactive monomers, 15～30%; With hydroxyl micromolecule polar compound is reaction medium; With azo-bis-isobutyl cyanide or organic peroxide is catalyst; Through the polymerisation in solution of free radical, and polymer is carried out the season ammonification handle and form.CN1391882A discloses a kind of natural keratin hair shaping liquid, said style keeping liquid by hydrolysis of keratin, siloxanes, glycerol, carbamide, fruit acid, pure water through mixing.Though above-mentioned hair styling agent, approved product respectively have its characteristics, but still remain further to be improved its performance, to satisfy the demand of people's hair caring and protection hair.
Summary of the invention
The object of the present invention is to provide a kind of hair keratin setting agent and use the hair styling product of its preparation; So that make human hair at aspects such as gloss, elasticity, feels more near natural kenel; And to because of the hair-waving; Hair dyeing, ultraviolet light, the damage that air pollution etc. cause human hair has certain repair function.
Hair keratin setting agent according to the invention; By the molecular weight that extracts in Crinis Carbonisatus or the animal hair is that the daltonian keratin of 60000-150000 and vinyl pyrrolidone/vinyl acetate copolymer are formed, and the weight ratio of said keratin and vinyl pyrrolidone/vinyl acetate copolymer is 0.2～3: 1.Said keratin both can be bought through market, also can prepare voluntarily; Said vinyl pyrrolidone/vinyl acetate copolymer is bought through market.
Hair styling article according to the invention comprise gel water, hair jelly and mousse, and are formulated by above-mentioned hair keratin setting agent and other component.
1, gel water
The component of gel water according to the invention comprises keratin setting agent, triethanolamine, surfactant, ethanol and pure water, and the percetage by weight of each component is following:
Gel water according to the invention, its component also comprises antiseptic and essence, the percetage by weight of each component is following:
In the gel water according to the invention, said keratin setting agent is above-mentioned hair keratin setting agent; Said surfactant is at least a in laureth-9, nonyl phenol polyethers-10, castor oil hydrogenated, sodium laureth sulfate, the lauryl glucoside; Said pure water is deionized water or distilled water.
The preparation method of gel water according to the invention: pure water is joined in the ingredients pot; Under agitation add ethanol, surfactant, triethanolamine, keratin setting agent and anticorrisive agent then in room temperature, normal pressure; After mixing; Essence is added in the ingredients pot with ethanol dissolving back, continue to stir at least 1 hour, bottle with 300 mesh filter screens filtration discharging continue the back.
2, hair jelly
Hair jelly according to the invention, its component comprises keratin setting agent and ethanol, and the percetage by weight of keratin setting agent is 5%～15%, and alcoholic acid percetage by weight is 85%～95%.
Hair jelly according to the invention also comprises essence, and said essence is 0.5%～1% of ethanol weight.。
In the hair jelly according to the invention, said keratin setting agent is above-mentioned hair keratin setting agent.
Hair jelly method for preparing according to the invention is: keratin setting agent and ethanol are added in the ingredients pot, under room temperature, normal pressure, be stirred to dissolving, add essence then, continue to stir again and can bottle at least 30 minutes.
3, mousse
The component of mousse according to the invention comprises keratin setting agent, triethanolamine, surfactant and pure water, and the percetage by weight of each component is following:
Mousse according to the invention, its component also comprises antiseptic and essence, the percetage by weight of each component is following:
In the mousse according to the invention, said keratin setting agent is above-mentioned hair keratin setting agent; Said surfactant is at least a in laureth-9, nonyl phenol polyethers-10, castor oil hydrogenated, sodium laureth sulfate, the lauryl glucoside; Said pure water is deionized water or distilled water.
The method for preparing of mousse according to the invention is: pure water is joined in the ingredients pot, under agitation add keratin setting agent, triethanolamine, surfactant, essence and antiseptic in room temperature, normal pressure then, stir bottling after at least 2 hours.
The present invention has following beneficial effect:
1, hair keratin setting agent according to the invention and approved product thereof can keep the hair natural torsion; Make hair have gloss and keep suitable moisture and (contain hydroxyl owing in the keratin; Hydrone there is certain affinity; Thereby make the hair after its typing keep certain moisture, more near natural hair quality).
2, because approved product according to the invention all contains hair keratin setting agent according to the invention; Thereby approved product according to the invention can be in the hair surface film forming, and the human hair damage that hair-waving, hair dyeing, ultraviolet light, air pollution etc. are caused has the certain repairing effect.
3, use approved product according to the invention to hair fixing, not only shaping time is longer, and hair hardness is moderate, and is easy to cleaned by shampoo.
4, through check, approved product according to the invention meets sanitary index, and concrete data see the following form:
Sanitary index
Gel talent for swimming official index, physical and chemical index
Mousse sense organ, physical and chemical index
Hair jelly sense organ, physical and chemical index
The specific embodiment
Through embodiment hair keratin setting agent according to the invention and approved product are described further below.Among following each embodiment, vinyl pyrrolidone/vinyl acetate copolymer is available from ISP (international special article company).
Embodiment 1: the preparation keratin
Human hair's (or Pilus Caprae seu Ovis) is cleaned up the back pulverize, use that pH value is 11, the TGA sodium solution (sodium hydroxide is regulated pH) of concentration 0.5mol/L normal pressure, room temperature (20 ℃～30 ℃) pretreatment 3 hours, adds carbamide then in solution; The addition of carbamide reaches 7mol/L for concentration in solution, continue after normal pressure, room temperature (20 ℃～30 ℃) reduction reaction 25 hours, after the response time expires; Splash into pH value to 6～8 of acetic acid conditioned reaction liquid, then aerating oxygen in solution reacted 0.5 hour in room temperature (20 ℃～30 ℃); After response time expires; Normal pressure filters, and filtrating is carried out dialysis with the dialysis bag of holding back relative molecular weight 20～80kD, and it is 60000～150000 daltonian keratin solution first products that centrifugalize obtains molecular weight; The keratin solution first product saltoutd obtain the keratin solid; Drying at room temperature is 6 hours under vacuum (5-10mmHg post) condition, and promptly obtaining molecular weight is 60000～150000 daltonian keratin, yield 42%.
Embodiment 2: preparation gel water
In the present embodiment, gel water is prepared from hair keratin setting agent, triethanolamine, laureth-9, castor oil hydrogenated, ethanol, essence, methylchloroisothiazandnone and deionized water, and the percetage by weight of above-mentioned each component is following:
Method for preparing:
1, the preparation of hair keratin setting agent
The keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 1: 4 (weight ratio); Under room temperature, normal pressure,, promptly form hair keratin setting agent with said keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously;
2, the preparation of gel water
Under room temperature, normal pressure, the 824.5Kg deionized water is joined in the ingredients pot; Add ethanol 80Kg, hair keratin setting agent 50Kg, laureth-9 10Kg, rilanit special 10Kg, triethanolamine 1Kg, methylchloroisothiazandnone 0.5Kg then and be stirred to even; Essence 4Kg is dissolved in the 20Kg ethanol adds in the ingredients pot again, the continued that continues stirred 1 hour, mixing time at the expiration after; Filter with 300 mesh filter screens, filtrating is gel water.
Embodiment 3: preparation gel water
In the present embodiment, gel water is prepared from hair keratin setting agent, triethanolamine, lauryl glucoside, castor oil hydrogenated, ethanol and distilled water, and the percetage by weight of above-mentioned each component is following
Method for preparing:
1, the preparation of hair keratin setting agent
The keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 1: 1 (weight ratio); Under room temperature, normal pressure,, promptly form hair keratin setting agent with said keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously;
2, the preparation of gel water
Under room temperature, normal pressure, 859.5Kg being distilled sub-water joins in the ingredients pot; Add ethanol 50Kg, hair keratin setting agent 80Kg, lauryl glucoside 5Kg, rilanit special 5Kg, triethanolamine 0.5Kg then and be stirred to even; Filter with 300 mesh filter screens, filtrating is gel water.
Embodiment 4: preparation gel water
In the present embodiment, gel water is prepared from hair keratin setting agent, triethanolamine, nonyl phenol polyethers-10, sodium laureth sulfate, ethanol, essence, methylchloroisothiazandnone and deionized water, and the percetage by weight of above-mentioned each component is following:
Method for preparing:
1, the preparation of hair keratin setting agent
The keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 2: 1 (weight ratio); Under room temperature, normal pressure,, promptly form hair keratin setting agent with said keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously;
2, the preparation of gel water
Under room temperature, normal pressure, the 771.5Kg deionized water is joined in the ingredients pot; Add ethanol 60Kg, hair keratin setting agent 120Kg, nonyl phenol polyethers-10 10Kg, laureth sodium sulphate 8Kg, triethanolamine 1.5Kg, methylchloroisothiazandnone 1Kg then and be stirred to even; Essence 8Kg is dissolved in the 20Kg ethanol adds in the ingredients pot again, the continued that continues stirred 1 hour, mixing time at the expiration after; Filter with 300 mesh filter screens, filtrating is gel water.
Embodiment 5: preparation gel water
In the present embodiment, gel water is prepared from hair keratin setting agent, triethanolamine, laureth-9, ethanol, essence, methylchloroisothiazandnone and distilled water, and the percetage by weight of above-mentioned each component is following:
1, the preparation of hair keratin setting agent
The keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 3: 1 (weight ratio); Under room temperature, normal pressure,, promptly form hair keratin setting agent with said keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously;
2, the preparation of gel water
Under room temperature, normal pressure, 730.3Kg distilled water is joined in the ingredients pot; Add ethanol 80Kg, hair keratin setting agent 150Kg, laureth-9 15Kg, triethanolamine 1Kg, methylchloroisothiazandnone 0.7Kg then and be stirred to even; Essence 3Kg is dissolved in the 20Kg ethanol adds in the ingredients pot again, the continued that continues stirred 1 hour, mixing time at the expiration after; Filter with 300 mesh filter screens, filtrating is gel water.
Embodiment 6: the preparation hair jelly
In the present embodiment, hair jelly is prepared from hair keratin setting agent, ethanol and essence, and the percetage by weight of above-mentioned each component is following:
Hair keratin setting agent 5%
Alcohol 95 %
Essence is 1% of ethanol weight;
Method for preparing:
1, the preparation of hair keratin setting agent
The keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 3: 1 (weight ratio); Under room temperature, normal pressure,, promptly form hair keratin setting agent with said keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously;
2, the preparation of hair jelly
Under room temperature, normal pressure, hair keratin setting agent 50Kg, alcohol 95 0Kg are added in the ingredients pot, be stirred to hair keratin setting agent and dissolve back adding essence 9.5Kg fully, continue stirring again and promptly formed hair jelly in 30 minutes.
Embodiment 7: the preparation hair jelly
In the present embodiment, hair jelly is prepared from hair keratin setting agent, ethanol and essence, and the percetage by weight of above-mentioned each component is following:
Hair keratin setting agent 7%
Ethanol 93%
Essence is 0.8% of ethanol weight;
Method for preparing:
1, the preparation of hair keratin setting agent
The keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 2: 5 (weight ratio); Under room temperature, normal pressure,, promptly form hair keratin setting agent with said keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously;
2, the preparation of hair jelly
Under room temperature, normal pressure, hair keratin setting agent 70Kg, ethanol 930Kg are added in the ingredients pot, be stirred to hair keratin setting agent and dissolve back adding essence 7.4Kg fully, continue stirring again and promptly formed hair jelly in 30 minutes.
Embodiment 8: the preparation hair jelly
In the present embodiment, hair jelly is prepared from hair keratin setting agent, ethanol and essence, and the percetage by weight of above-mentioned each component is following:
Hair keratin setting agent 11%
Ethanol 89%
Essence is 0.5% of ethanol weight;
Method for preparing:
1, the preparation of hair keratin setting agent
The keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 1: 1 (weight ratio); Under room temperature, normal pressure,, promptly form hair keratin setting agent with said keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously;
2, the preparation of hair jelly
Under room temperature, normal pressure, hair keratin setting agent 110Kg, ethanol 890Kg are added in the ingredients pot, be stirred to hair keratin setting agent and dissolve back adding essence 4.5Kg fully, continue stirring again and promptly formed hair jelly in 30 minutes.
Embodiment 9: the preparation hair jelly
In the present embodiment, hair jelly is formed by hair keratin setting agent and ethanol preparation, and the percetage by weight of above-mentioned each component is following:
Hair keratin setting agent 15%
Ethanol 85%;
Method for preparing:
1, the preparation of hair keratin setting agent
The keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 0.2: 1 (weight ratio); Under room temperature, normal pressure,, promptly form hair keratin setting agent with said keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously;
2, the preparation of hair jelly
Under room temperature, normal pressure, hair keratin setting agent 150Kg, ethanol 850Kg are added in the ingredients pot, continue again to stir after being stirred to hair keratin setting agent and dissolving fully and promptly formed hair jelly in 30 minutes.
Embodiment 10: the preparation mousse
In the present embodiment, mousse is prepared from hair keratin setting agent, triethanolamine, lauryl glucoside, sodium laureth sulfate, essence, methylchloroisothiazandnone and distilled water, and the percetage by weight of above-mentioned each component is following:
Method for preparing:
1, the preparation of hair keratin setting agent
The keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 0.2: 1 (weight ratio); Under room temperature, normal pressure,, promptly form hair keratin setting agent with said keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously;
2, the preparation of mousse
Under room temperature, normal pressure, the 865.5Kg distilled water is joined in the ingredients pot; Add hair keratin setting agent 100Kg, triethanolamine 10Kg, lauryl glucoside 10Kg, sodium laureth sulfate 10Kg, essence 4Kg, methylchloroisothiazandnone 0.5Kg then, stir and promptly formed mousse in 2 hours.
Embodiment 11: the preparation mousse
In the present embodiment, mousse is prepared from hair keratin setting agent, triethanolamine, laureth-9, nonyl phenol polyethers-10, essence, methylchloroisothiazandnone and deionized water, and the percetage by weight of above-mentioned each component is following:
Method for preparing:
1, the preparation of hair keratin setting agent
The keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 3: 1 (weight ratio); Under room temperature, normal pressure,, promptly form hair keratin setting agent with said keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously;
2, the preparation of mousse
Under room temperature, normal pressure, the 833.3Kg deionized water is joined in the ingredients pot; Add hair angle egg setting agent 150Kg, triethanolamine 5Kg, laureth-9 5Kg, nonyl phenol polyethers-10 5Kg, essence 1Kg, Methylisothiazolinone 0.7Kg then, stir and promptly formed mousse in 2 hours.
Embodiment 12: the preparation mousse
In the present embodiment, mousse is prepared from hair keratin setting agent, triethanolamine, castor oil hydrogenated, lauryl glucoside, essence, methylchloroisothiazandnone and deionized water, and the percetage by weight of above-mentioned each component is following:
Method for preparing:
1, the preparation of hair keratin setting agent
The keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 0.5: 1 (weight ratio); Under room temperature, normal pressure,, promptly form hair keratin setting agent with said keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously;
2, the preparation of mousse
Under room temperature, normal pressure, the 798.4Kg deionized water is joined in the ingredients pot; Add hair angle egg setting agent 160Kg, triethanolamine 15Kg, castor oil hydrogenated 15Kg, lauryl glucoside 5Kg, essence 6Kg, methylchloroisothiazandnone 0.6Kg then, stir and promptly formed mousse in 2 hours.
Embodiment 13 preparation mousses
In the present embodiment, mousse is prepared from hair keratin setting agent, triethanolamine, castor oil hydrogenated, lauryl glucoside, essence, methylchloroisothiazandnone and deionized water, and the percetage by weight of above-mentioned each component is following:
Method for preparing:
1, the preparation of hair keratin setting agent
The keratin and the vinyl pyrrolidone/vinyl acetate copolymer of embodiment 1 preparation are measured by 1: 1 (weight ratio); Under room temperature, normal pressure,, promptly form hair keratin setting agent with said keratin and vinyl pyrrolidone/vinyl acetate copolymer mix homogeneously;
2, the preparation of mousse
Under room temperature, normal pressure, the 780Kg deionized water is joined in the ingredients pot, add hair angle egg setting agent 200Kg, triethanolamine 10Kg, nonyl phenol polyethers-10 10Kg then, stir and promptly formed mousse in 2 hours.
Embodiment 14: the performance comparative test
1, test specimen
(1) the gel water of test specimen A: embodiment 3 preparations
(2) contrast of the gel water of specimen sample B: embodiment 3 preparations, the percetage by weight of its each component is following:
(3) hair jelly of test specimen C: embodiment 7 preparations
(4) contrast of the hair jelly of specimen sample D: embodiment 7 preparations, the percetage by weight of its each component is following:
Vinyl pyrrolidone/vinyl acetate copolymer 7%
Ethanol 93%
Essence is 0.8% of ethanol weight.
(5) mousse of test specimen E: embodiment 11 preparations
(6) contrast of the mousse of test specimen F: embodiment 11 preparations, the percetage by weight of its each component is following:
2, method of testing
(1) topknot pretreatment: big topknot is cleaned with the sodium dodecyl sulfate solution of mass concentration 3%, put into ether then and soaked 24 hours; Big topknot after the ether processing is processed the topknot of the long 23cm of multi beam, the topknot that weighs 2g and the long 15cm of multi beam, heavy 1.3g; Then each topknot is used the distilled water moistening; And rub with the sodium dodecyl sulfate solution of mass concentration 3% and to wash 2～3 minutes, rinse well with tap water, dry for use naturally.
(2) crooked conservation degree test: on the topknot of long 23cm, heavy 2g, evenly coat 0.7g test specimen A, B, C, D, E, F respectively; Then each topknot is twisted in respectively on the curly hair thick stick of 1.2cm, 50 ℃ of dryings 2 hours, be cooled to room temperature after; Each topknot is taken off from the curly hair thick stick; A part is hung in 30 ℃, the constant temperature of 60%RH (relative humidity), constant humidity incubator, and a part is hung in 30 ℃, the constant temperature of 90%RH, constant humidity incubator, every at a distance from 2 hours the detection length of restrainting hair respectively.
(3) topknot bending strength test: on the topknot of long 15cm, heavy 1.3g, evenly coat 0.4g test specimen A, B, C, D, E, F respectively; With after the comb combing, be organized into the wide tabular of 2cm that is respectively, 50 ℃ of dryings 2 hours; Then after 23 ℃, 60%RH (relative humidity) are placed 24 hours; Lie on the support platform of interval 65mm, make central part crooked with 2cm/min speed, the heavy burden of when bending to 2cm, measuring it.
(4) breaking strength test: flexural strength test after the beam off the object at a right angle corner, hand hold to 15cm / s speeds pull hard to break into the hair bundle, measure the maximum load.
(5) play white test: on the topknot of long 23cm, heavy 2g, evenly coat 0.7g test specimen A, B, C, D, E, F respectively; 50 ℃ of dryings 2 hours; Placed 24 hours at 23 ℃, 60%RH (relative humidity) then,, estimated white phenomenon by 5 fens system code of points.1 has been divided into whitely serious, and 5 are divided into and not have in vain.
(6) brightness test: on the topknot of long 23cm, heavy 2g, evenly coat 0.7g test specimen A, B, C, D, E, F respectively; After the comb combing, be organized into the wide tabular of 2cm that is respectively, be fixed in the standard light source VERIVIDE COLOR ASSESMENT CABINET; Press 5 fens system code of points by the evaluator; The assess sample brightness, 1 be divided into dark, 5 be divided into bright.
3 test results
Test result is stated each table as follows:
The crooked conservation degree test result of table 1: (30 ℃, 60%RH) unit: centimetre
| A | B | C | D | E | F | |
| 0 hour | 11 | 11 | 10.2 | 10.2 | 11.5 | 11.5 |
| 2 hours | 12.3 | 12.9 | 12.0 | 12.8 | 13.1 | 13.8 |
| 4 hours | 13.5 | 14.3 | 13.7 | 14.5 | 14.6 | 15.5 |
| 6 hours | 14.7 | 15.6 | 14.2 | 15.3 | 15.5 | 16.6 |
| 8 hours | 15.3 | 16.2 | 14.5 | 15.9 | 16.1 | 17.4 |
The crooked conservation degree test result of table 2: (30 ℃, 90%RH) unit: centimetre
| A | B | C | D | E | F | |
| 0 hour | 11.0 | 11.0 | 10.2 | 10.2 | 11.5 | 11.5 |
| 2 hours | 13.5 | 13.9 | 12.2 | 12.7 | 14.1 | 14.8 |
| 4 hours | 15.6 | 16.3 | 14.1 | 14.6 | 16.2 | 16.9 |
| 6 hours | 16.5 | 17.2 | 15.3 | 15.8 | 17.1 | 18.1 |
| 8 hours | 17.3 | 18.1 | 16.2 | 16.7 | 18.0 | 19.6 |
Table 3 topknot bending strength test result: (23 ℃, 60%RH) unit: gram
| Sample | A | B | C | D | E | F |
| Bear a heavy burden | 6.0 | 6.5 | 8.0 | 8.7 | 5.2 | 5.9 |
Table 4 destroys back strength test result: the unit gram
| Sample | A | B | C | D | E | F |
| Bear a heavy burden | 35 | 40 | 42 | 50 | 30 | 36 |
Table 5 a white test result
| Sample | ?A | B | C | D | E | F |
| Mark | ?5 | 3 | 4 | 2 | 5 | 3 |
Table 6 brightness test result
| Sample | ?A | B | C | D | E | F |
| Mark | ?5 | 3 | 5 | 4 | 5 | 3 |
Can find out from above-mentioned test result, the approved product that the approved product that adds hair keratin setting agent does not more add hair keratin setting agent at the curling conservation degree, play aspect such as white, brightness and have more excellent performance.
Claims (9)
1. hair keratin setting agent; It is characterized in that by the molecular weight that extracts in Crinis Carbonisatus or the animal hair being that 60000～150000 daltonian keratin and vinyl pyrrolidone/vinyl acetate copolymer are formed, the weight ratio of said keratin and vinyl pyrrolidone/vinyl acetate copolymer is 0.2～3: 1.
2. a gel water is characterized in that component comprises keratin setting agent, triethanolamine, surfactant, ethanol and pure water, and the percetage by weight of each component is following:
Said keratin setting agent is the said hair keratin of claim 1 setting agent.
3. according to the said gel water of claim 2, it is characterized in that said surfactant is at least a in laureth-9, nonyl phenol polyethers-10, castor oil hydrogenated, sodium laureth sulfate, the lauryl glucoside; Said pure water is deionized water or distilled water.
4. according to claim 1 or 2 said gel water, it is characterized in that also comprising antiseptic and essence, the percetage by weight of antiseptic is 0.05%～0.1%, and the percetage by weight of essence is 0.1%～0.8%.
5. hair jelly; It is characterized in that component comprises keratin setting agent and ethanol; The percetage by weight of keratin setting agent is 5%～15%, and alcoholic acid percetage by weight is 85%～95%, and said keratin setting agent is the said hair keratin of claim 1 setting agent.
6. hair jelly according to claim 5 is characterized in that also comprising essence, and essence is 0.5%～1% of ethanol weight.
7. a mousse is characterized in that component comprises keratin setting agent, triethanolamine, surfactant and pure water, and the percetage by weight of each component is following:
Said keratin setting agent is the said hair keratin of claim 1 setting agent.
8. according to the said mousse of claim 7, it is characterized in that said surfactant is at least a in laureth-9, nonyl phenol polyethers-10, castor oil hydrogenated, sodium laureth sulfate, the lauryl glucoside; Said pure water is deionized water or distilled water.
9. according to claim 7 or 8 said mousses, it is characterized in that also comprising antiseptic and essence, the percetage by weight of antiseptic is 0.05%～0.1%, and the percetage by weight of essence is 0.1%～0.8%.
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| CN 201110390600 CN102429835B (en) | 2011-11-30 | 2011-11-30 | Keratin hairspray for hair and modeling products for hair |
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|---|---|---|---|
| CN 201110390600 CN102429835B (en) | 2011-11-30 | 2011-11-30 | Keratin hairspray for hair and modeling products for hair |
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| CN102429835B CN102429835B (en) | 2013-05-01 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106619173A (en) * | 2016-12-28 | 2017-05-10 | 安徽紫檀科技有限公司 | Hair styling agent and preparation method thereof |
| CN107519053A (en) * | 2017-09-11 | 2017-12-29 | 陈磊 | A kind of hair gel containing Composition of Meteorite and preparation method thereof |
| WO2020117239A1 (en) * | 2018-12-06 | 2020-06-11 | Colgate-Palmolive Company | Personal care compositions |
| US20200270316A1 (en) * | 2017-11-10 | 2020-08-27 | Givaudan Sa | Silk Alcohol Formulations |
| CN111643391A (en) * | 2020-07-22 | 2020-09-11 | 广州市圣莎拉化妆品有限公司 | Hair care product of hydrolyzed wheat protein and processing technology |
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| CN106619173A (en) * | 2016-12-28 | 2017-05-10 | 安徽紫檀科技有限公司 | Hair styling agent and preparation method thereof |
| CN107519053A (en) * | 2017-09-11 | 2017-12-29 | 陈磊 | A kind of hair gel containing Composition of Meteorite and preparation method thereof |
| US20200270316A1 (en) * | 2017-11-10 | 2020-08-27 | Givaudan Sa | Silk Alcohol Formulations |
| WO2020117239A1 (en) * | 2018-12-06 | 2020-06-11 | Colgate-Palmolive Company | Personal care compositions |
| CN113710329A (en) * | 2018-12-06 | 2021-11-26 | 高露洁-棕榄公司 | Personal care compositions |
| AU2018452265B2 (en) * | 2018-12-06 | 2022-09-08 | Colgate-Palmolive Company | Personal care compositions |
| CN113710329B (en) * | 2018-12-06 | 2024-04-05 | 高露洁-棕榄公司 | Personal care compositions |
| CN111643391A (en) * | 2020-07-22 | 2020-09-11 | 广州市圣莎拉化妆品有限公司 | Hair care product of hydrolyzed wheat protein and processing technology |
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