CN102429309A - Micro-capsulated germinated soybean peptide crude extract effervescent tablet and preparation method thereof - Google Patents

Micro-capsulated germinated soybean peptide crude extract effervescent tablet and preparation method thereof Download PDF

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CN102429309A
CN102429309A CN2011103696105A CN201110369610A CN102429309A CN 102429309 A CN102429309 A CN 102429309A CN 2011103696105 A CN2011103696105 A CN 2011103696105A CN 201110369610 A CN201110369610 A CN 201110369610A CN 102429309 A CN102429309 A CN 102429309A
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crude extract
soybean peptide
germinated soybean
peptide crude
microencapsulation
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CN102429309B (en
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吴金鸿
王正武
包萨日娜
金雅芳
燕霞
柳江湖
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Shanghai Rongpeng E Commerce Co ltd
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Shanghai Jiaotong University
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Abstract

The invention discloses a micro-capsulated germinated soybean peptide crude extract effervescent tablet and a preparation method thereof. The micro-capsulated germinated soybean peptide crude extract effervescent tablet comprises the following components: micro-capsulated germinated soybean peptide crude extract dry powder, citric acid, sodium bicarbonate, polyvinylpyrrolidone, isomaltooligosaccharide and polyethylene glycol 8000. The effervescent tablet has the advantages of convenience in carrying, eating and absorption of active ingredients by a human body, and stable storage, is rich in various nutritive health-care functional components, and has the characteristics of excellent color, aroma and taste of a beverage product.

Description

Microencapsulation germinated soybean peptide crude extract effervescence decoction piece and preparation method thereof
Technical field
The present invention relates to a kind of effervescence decoction piece and preparation method thereof, be specifically related to a kind of microencapsulation germinated soybean peptide crude extract effervescence decoction piece and preparation method thereof.
Background technology
Behind the soybean germination, ANFs such as phytic acid, trypsin inhibitor are degraded, and bioactie agents such as isoflavones, vitamin C, r-reanal are synthetic to be increased, and are worth thereby improve soybean nutritional.Soybean Peptide not only have free from beany flavor, no albuminous degeneration, acidity do not precipitate, do not heat solidify, excellent function character such as soluble in water, good fluidity; And has a unique biological function; Can prevent and treat thrombus, hypertension, delay senility, resisting fatigue, raising immunity of organisms etc., so Soybean Peptide is a kind of good functional food material.We have utilized germinated soybean to be raw material in previous work; Adopt zymolysis technique to prepare the Soybean Peptide crude extract, and use the germinated soybean peptide crude extract microscapsule powder product that Microencapsulation Method prepared multiple nutrients compositions such as containing polypeptide, fat, carbohydrate, mineral element, isoflavones and r-reanal and (see the patent of application for details: No.201110300437.3).This powder-product absorbability is low, and good fluidity improves the stability of functional active components in the crude extract, thereby improved germinated soybean peptide crude extract application performance.
Effervescence decoction piece is to be a kind of solid beverage tablet that disintegrant is processed with suitable bronsted lowry acids and bases bronsted lowry, drops in the water and can produce great amount of carbon dioxide gas, impels whole tablet to dissolve at short notice, is the effervesce shape.Common solid beverage is easy to carry, but active ingredient often will just can discharge through dissolving after a while; Though liquid beverage utilizes active ingredient fast, carries inconvenience, and is apt to deteriorate.The advantage that effervescence decoction piece just in time has these two kinds of products concurrently has overcome the shortcoming of these two kinds of products simultaneously, and has following advantage: (1) effervescence decoction piece volume is little, steady quality, production automation degree high, easy to carry and transport, and storage period is long; (2) effervescence decoction piece is taken facing with before being made into liquid, and its liquid is easy to swallow, bioavilability high, and is little to GI irritation property, is specially adapted to the patient of the elderly and bradymassesis; (3) the active ingredient solubility of effervescence decoction piece is high, and the disintegrant calving disaggregation is powerful, and whole tablet can dissolve rapidly at short notice; (4) effervescence decoction piece chance water just produces bubble and seethes (being effervesce) up and down, and interesting, color, smell and taste are all good, and instant-drink has especially catered to the teenager and liked new, strange, special advantage, is a kind of product that children, teenager like.
Consult relevant technical literature; Before the present invention accomplishes; All not having with microencapsulation germinated soybean peptide crude extract is the report of development of raw materials effervescent tablet solid beverage, and does not also have Related product to sell on the market, and therefore product provided by the invention will have wide market application prospect.
Summary of the invention
The object of the invention is to overcome the deficiency of above-mentioned prior art; Providing a kind of is primary raw material with microencapsulation germinated soybean peptide crude extract; Utilize the effervescence decoction piece method to process to carry and the microencapsulation germinated soybean peptide crude extract effervescence decoction piece of instant and preparation method thereof, said effervescence decoction piece sweet and sour taste, have certain nutritive value and promote health benefit, be easy to carry.
The objective of the invention is to realize through following technical scheme:
A kind of microencapsulation germinated soybean peptide crude extract effervescence decoction piece comprises following component by mass percent:
Microencapsulation germinated soybean peptide crude extract dry powder 5~30%,
Citric acid 20~60%,
Sodium acid carbonate 15~50%,
Polyvinylpyrrolidone 0.24~0.6%,
Oligoisomaltose 0.5~1%,
Polyethylene glycol 8000 (PEG8000) 0.5~3%.
Among the present invention, said microencapsulation germinated soybean peptide crude extract dry powder contains peptide, isoflavones, r-reanal, soybean polyoses and fat.
In the present invention's one preferred embodiments, said microencapsulation germinated soybean peptide crude extract effervescence decoction piece also comprises following component by mass percent:
Sucralose 0.1~1%,
Stevioside 0.1~1%,
Orange juice powdered flavor 0.0~0.5%,
Vitamin C 0.0~2.0%,
Strawberry powder 1~3%,
Perilla leaf extract 1~3%.
The germinated soybean of microencapsulation described in the present invention peptide crude extract dry powder is the main raw material of product; Citric acid was acid effervescent agent described in auxiliary material was formed, and said sodium acid carbonate is alkaline effervescent agent, after the two mixes, meets water chemical effervesce reaction takes place, and produced great amount of carbon dioxide gas at once; Said citric acid also can be adjusted the tart flavour of effervescent tablet solid beverage, improves mouthfeel; Said oligoisomaltose has certain viscosity, and its ratio of viscosities sucrose is high, plays bonding and keeps stablizing and filling effect of tablet configuration; Said polyvinylpyrrolidone (PVP) is as the adhesive of effervescent tablet, and bonding effect is good, is dissolvable in water in the absolute ethyl alcohol, joins in former, the auxiliary material mixture as bonding, wetting agent with the solution form and makes softwood; Said polyethylene glycol (PEG) 8000 is a lubricant, and lubricity is strong, and anti-adhesive property is good, makes effervescent tablet in pressing process, smoothly slice.
In addition; The present invention has designed and developed multiple beverage mouthfeel and local flavor effervescence decoction piece; Added some at the prescription composition and had the food additives of nutrition and health care function, having comprised: added said Sucralose of high-intensity sweeteners and said stevioside that suitable food tablet uses, its sugariness is about 600 and 200 times of sucrose respectively; Therefore use amount is few, can be fit to diabetes patient; Added the orange juice powdered flavor, it can make fresher, true to nature, the full and delicate fragrance of fragrance as flavouring agent fully dissolving in the aqueous solution; Added said vitamin C, it is a water soluble vitamin, not only can enhance immunity power, and anti-oxidant especially, protection cell, even the nutritional labeling of function such as effective antitumor; Add the fruits and vegetables inspissated juice and extracted powder; Like said strawberry powder or said perilla leaf extract, strawberry powder has increased the local flavor of beverage, makes beverage mouthfeel have the fruity of natural faint scent; And perilla leaf extract; Not only contain multivitamin and mineral matter, also contain multiple bioactivators such as Rosmarinic acid, polyphenol, flavones, perillaldehyde, perilla alcohol, perillene, alpha linolenic acid, have multiple functions such as antiallergy, anti-oxidant, anticancer, reducing blood lipid.
The present invention also provides a kind of preparation method of said microencapsulation germinated soybean peptide crude extract effervescence decoction piece, it is characterized in that comprising operations such as non-water granulation, drying, whole grain, compressing tablet and packing, and concrete steps are following:
1, with pulverizer said component is pulverized, crossed 100 mesh sieves, subsequent use;
2, according to the said mass percent of said component; After the said component that does not comprise said polyvinylpyrrolidone and said polyethylene glycol 8000 mixed; Add the ethanol solution contain said polyvinylpyrrolidone (PVP) again and mix and process softwood, said polyvinylpyrrolidone content in absolute ethyl alcohol is 3g/100mL;
3, said softwood being crossed 14~20 mesh sieves carries out granulation and gets wet granular;
4, place baking oven to carry out drying 1~3h in 40~50 ℃ said wet granular, make ethanol volatilize fully dried particle, said dried pellet moisture content is controlled at below 2%;
5, said dried particle is crossed 14~20 mesh sieves and carry out whole grain, the dried particle after must whole grain;
6, be in the dried particle after 0.5~3% said PEG8000 joins said whole grain with mass percent, be dosed into tablet forming in the tablet press machine after mixing,, prepare said microencapsulation germinated soybean peptide crude extract effervescence decoction piece through ultraviolet sterilization.
The consumption of each component is identical with the mass percent of pairing same composition in the said microencapsulation germinated soybean peptide crude extract effervescence decoction piece among the said preparation method.
The present invention has following beneficial effect:
1, effervescence decoction piece provided by the invention contains the multiple nutrients health-care components; As containing isoflavones, vitamin C, r-reanal bioactivators such as (GABA) in the microencapsulation germinated soybean peptide crude extract, these compositions have enhancing human immune, antifatigue, hypotensive and reducing blood lipid, inhibition cholesterol, promote lipid-metabolism, Prevention of Cardiovascular systemic disease, brain tonic, abundant physiological function such as sober up; The fruits and vegetables inspissated juice extracts powder; As containing multivitamin and mineral matter in the perilla leaf extract; Also contain multiple bioactivators such as Rosmarinic acid, polyphenol, flavones, perillaldehyde, perilla alcohol, perillene, alpha linolenic acid, have multiple functions such as antiallergy, anti-oxidant, anticancer, reducing blood lipid.
2, effervescence decoction piece provided by the invention not only have be convenient for carrying, advantage that instant, active ingredient are convenient to absorption of human body, storage-stable; And be rich in multiple nutrients health care composition and have all good characteristics of beverage products color, smell and taste, be a kind of new type functional effervescence decoction piece.
3, the effervescence decoction piece main component of the present invention's preparation is a germinated soybean peptide crude extract; It combined spray drying process to process microscapsule powder through complex coacervation before the film-making agent, and (preparation method sees the patent of application for details: No.201110300437.3); Traditional soy peptide powder hygroscopicity and caking property have obviously been reduced; Improve powder flowbility and stability, overcome the technical barrier that traditional soy peptide powder is applied to tablet processing.
4, the present invention adopts non-water granulating tabletting process to prepare effervescence decoction piece; Use the PVP ethanol solution to make wetting agent, be in non-water environment after making alkaline effervescent agent and acid effervescent agent agent mixing, acid-base reaction can not take place; And the dried particle of softwood is difficult for moisture absorption, sticking phenomenon when reducing compressing tablet.
5, the production equipment of effervescence decoction piece preparation technology provided by the invention and required usefulness is simple, and easy operating helps realizing suitability for industrialized production processing.
Description of drawings
Fig. 1 is preparation technology's flow chart of microencapsulation germinated soybean peptide crude extract effervescence decoction piece.
The specific embodiment
Below all preparations as follows of used microencapsulation germinated soybean peptide crude extract dry powder among all embodiment:
1, use the mass concentration that contains 50mM glutamic acid to be soaking soybean 8h under 0.1g/L shitosan aqueous acetic acid (the acetic acid addition is 0.1mL in the every liter of solution) room temperature; Wash 2 times; Place 25 ℃ then; Germinate in the germinating box of 80% humidity, when bud is about 30mm, take out as the germinated soybean raw material that is rich in isoflavones and r-reanal.
2, take by weighing germinated soybean and put into soy bean milk making machine, the deionized water that adds 2 times of quality is pulverized making beating, and the soluble component lixiviate is come out, and 100 mesh sieves filter, and filtrating is through-52 ℃ of freeze dryings, the germinated soybean powder that obtains.The germinated soybean powder is carried out two enzyme (flavor proteases: mixed enzymolysis alkali protease=7: 3 (w/w)); Said flavor protease and alkali protease are all purchased letter (China) Bioisystech Co., Ltd in Novi; The flavor protease enzyme activity is 500LAPU/g, and the alkali protease enzyme activity is 2.4AU/g, and enzymatic hydrolysis condition is: it is 100g/L emulsion (substrate) that the germinated soybean powder is dissolved into mass concentration prior to preheating 10min in 90 ℃ of water; The consumption of enzyme is 10% of a substrate gross mass; PH is 9, and temperature is 50 ℃, and enzymolysis time is 4h.Thoroughly boil the 5min enzyme that goes out behind the enzymolysis, cooling, centrifugal 30min under the 8000rpm/min rotating speed gets supernatant suction filtration under 0.1MPa vacuum, and filtrating promptly makes germinated soybean peptide crude extract through-52 ℃ of freeze dryings.
3, take by weighing above-mentioned germinated soybean peptide crude extract stirring and dissolving in the water of its 25 times of quality; Be heated to 50 ℃ then; Again the food grade emulsifier Tween-60 of volume (mL) for 0.05 times of said germinated soybean peptide crude extract quality (g) joined in the said germinated soybean peptide crude extract; In 50 ℃, high speed shear stirring and emulsifying 5min under the 13500rpm/min condition forms uniform germinated soybean peptide crude extract emulsion.
4, with addition be 2.6 times Arabic gum of said germinated soybean peptide crude extract quality; Addition is that 0.4 times lactose of said germinated soybean peptide crude extract quality adds in the said germinated soybean peptide crude extract emulsion, with electric blender stirring and dissolving 20min under the 700rpm/min rotating speed, adds mass concentration then and be 85% food-grade lactic acid regulator solution pH to 4.3; Adding quality again is the gelatin of 1 times of said germinated soybean peptide crude extract quality; With electric blender stirring and dissolving 20min under the 700rpm/min rotating speed, at 50 ℃, high-pressure homogeneous 15min under the 20MPa condition; With above solution at feed liquid flow 8mL/min; Compressed air require 536L/h, 160 ℃ of the EATs of spraying, spray-drying under 100 ℃ of conditions of outlet wind-warm syndrome degree; The gained powder is microencapsulation germinated soybean peptide crude extract dry powder, prepares the raw material of effervescence decoction piece as the present invention.
Embodiment 1
Prepare a kind of microencapsulation germinated soybean peptide crude extract effervescence decoction piece, its supplementary material is formed following by mass percentage:
Microencapsulation germinated soybean peptide crude extract dry powder 14%,
Citric acid 47%,
Sodium acid carbonate 33%,
Polyvinylpyrrolidone (PVP) 0.42%,
Oligoisomaltose 1%,
Polyethylene glycol 8000 (PEG8000) 2%,
Sucralose 1%,
Stevioside 0.5%,
Orange juice powdered flavor 0.08%,
Vitamin C 1%,
The concrete preparation method of present embodiment is following:
By above-mentioned quality proportioning; Heavy 0.6g calculates with every sheet; Take by weighing microencapsulation germinated soybean peptide crude extract dry powder, citric acid, sodium acid carbonate, Sucralose, stevioside, orange juice powdered flavor (purchase, 181018 orange juice powdered flavors, product standard is QB/T1505-2007), oligoisomaltose in Apple Flavor & Fragrance Group Co., Ltd., vitamin C is pulverized respectively and cross 100 mesh sieves; Fully mix; Add the ethanol solution 14ml that contains PVP again, the content of said PVP in absolute ethyl alcohol is 3g/100ml, mixes and processes softwood.Softwood is crossed 18 mesh sieves; Make wet granular, place drying machine in 50 ℃ of dry 2h wet granular, dried particles is crossed 16 mesh sieves carry out whole grain; Add polyethylene glycol PEG8000 2g; Be dosed into compressing tablet in the tablet press machine after mixing,, promptly get microencapsulation germinated soybean peptide crude extract effervescence decoction piece of the present invention through ultraviolet sterilization.
The effervescent tablet product sensory attributional analysis of present embodiment preparation is following:
Get two clean beakers, each adds the hot water 200ml that temperature is 37 ℃ and 50 ℃, and every cup drops into 1 of the microencapsulation germinated soybean peptide crude extract effervescence decoction piece of above-mentioned preparation; Observe its bubblement, treat the complete disintegration of effervescent tablet, when no gas is emitted; Measure its disintegration time limited; And qualitative characteristics such as the outward appearance of organoleptic analysis's tablet and effervescence tablet beverage bubblement, taste flavor, color and luster, smell, repeated test is 6 times under each water temperature, and analysis result is seen table 1.
Table 1 microencapsulation germinated soybean peptide crude extract effervescence decoction piece organoleptic quality analysis result
Embodiment 2
Prepare a kind of vitamin C strawberry flavor microencapsulation germinated soybean peptide crude extract effervescence decoction piece that is rich in, it is following that its supplementary material is formed mass percent:
Figure BDA0000109956360000062
The concrete preparation method of present embodiment is following:
By above-mentioned quality proportioning, heavy 0.7g calculates with every sheet, takes by weighing microencapsulation germinated soybean peptide crude extract dry powder, citric acid, sodium acid carbonate, Sucralose, stevioside, vitamin C, strawberry powder and (purchases the Ji Tian Food Co., Ltd in Shanghai; The FD-strawberry powder), oligoisomaltose; Pulverize and cross 100 mesh sieves respectively, fully mix then, add the ethanol solution 15mL that contains PVP again and mix and process softwood; The content of said PVP in absolute ethyl alcohol is 3g/100ml; Softwood is crossed 18 mesh sieves, make wet granular, place drying machine in 50 ℃ of dry 3h wet granular.Dried particles is crossed 16 mesh sieves carry out whole grain, add PEG8000 2g, be dosed into compressing tablet in the tablet press machine after mixing,, promptly get a kind of vitamin C strawberry flavor microencapsulation germinated soybean peptide crude extract effervescence decoction piece that is rich in of the present invention through ultraviolet sterilization.
The effervescence decoction piece product of present embodiment preparation obtains the organoleptic quality analysis result by embodiment 1 identical analytical method and sees table 2.
Table 2 rich vitamin C strawberry flavor microencapsulation germinated soybean peptide effervescence decoction piece organoleptic quality analysis result
Figure BDA0000109956360000071
Embodiment 3
Prepare a kind of purple perilla flavor microencapsulation germinated soybean peptide crude extract effervescence decoction piece, its supplementary material is formed following by mass percentage:
Microencapsulation germinated soybean peptide crude extract dry powder 12%,
Citric acid 47%,
Sodium acid carbonate 33%,
Polyvinylpyrrolidone (PVP) 0.54%,
Oligoisomaltose 1%,
Polyethylene glycol 8000 (PEG8000) 2%,
Sucralose 1%,
Stevioside 0.5%,
Perilla leaf extract 2.96%,
The concrete preparation method of present embodiment is following:
By above-mentioned quality proportioning, heavy 0.8g calculates with every sheet, takes by weighing that microencapsulation germinated soybean peptide crude extract dry powder, citric acid, sodium acid carbonate, Sucralose, stevioside, perilla leaf extract powder, oligoisomaltose was pulverized 100 mesh sieves; Fully mix; Add the ethanol solution 18mL that contains PVP again, the content of said PVP in absolute ethyl alcohol is 3g/100ml, mixes and processes softwood; Softwood is crossed 18 mesh sieves, make wet granular.Place drying machine in 50 ℃ of dry 3h wet granular.Dried particles is crossed 16 mesh sieves carry out whole grain, add PEG8000 2g, be dosed into compressing tablet in the tablet press machine after mixing,, promptly get a kind of purple perilla flavor microencapsulation germinated soybean peptide crude extract effervescent tablet of the present invention through ultraviolet sterilization.
Said perilla leaf extracts powder, preparation method thereof: be raw material with the perilla leaf, add food grade ethanolic solution (volumetric concentration is 80%), perilla leaf raw materials quality (g): food grade volumes of aqueous ethanol (ml)=1: 2; Smash to pieces with beater; Stir down at 50 ℃, lixiviate 60min, fully filter with 300 eye mesh screens the reaction back; To filtrate and concentrate in the 0.1MPa vacuum; To solid quality content is to carry out centrifugally at 5~10% o'clock, and centrifugal condition is 8000rpm/min, gets supernatant and processes the perilla leaf extract xeraphium through-52 ℃ of following freeze dryings.
The effervescence decoction piece product of present embodiment preparation obtains the organoleptic quality analysis result by embodiment 1 identical analytical method and sees table 3.
Table 3 purple perilla flavor microencapsulation germinated soybean peptide crude extract effervescence decoction piece organoleptic quality analysis result
Figure BDA0000109956360000081

Claims (5)

1. microencapsulation germinated soybean peptide crude extract effervescence decoction piece comprises following component by mass percent:
Microencapsulation germinated soybean peptide crude extract dry powder 5~30%,
Citric acid 20~60%,
Sodium acid carbonate 15~50%,
Polyvinylpyrrolidone 0.24~0.6%,
Oligoisomaltose 0.5~1%,
Polyethylene glycol 8,000 0.5~3%,
Said microencapsulation germinated soybean peptide crude extract dry powder contains peptide, isoflavones, r-reanal, soybean polyoses and fat.
2. microencapsulation germinated soybean peptide crude extract effervescence decoction piece according to claim 1 is characterized in that said effervescence decoction piece also comprises following component by mass percent:
Sucralose 0.1~1%,
Stevioside 0.1~1%,
Orange juice powdered flavor 0.0~0.5%,
Vitamin C 0.0~2.0%,
Strawberry powder 1~3%,
Perilla leaf extract 1~3%.
3. the preparation method of claim 1 or 2 said microencapsulation germinated soybean peptide crude extract effervescence decoction pieces may further comprise the steps:
A. with pulverizer said component is pulverized, crossed 100 mesh sieves, subsequent use;
B. according to the said mass percent of said component, after the said component that does not comprise said polyvinylpyrrolidone and said polyethylene glycol 8000 mixed, add the ethanol solution that contains said polyvinylpyrrolidone again and mix and process softwood;
C. said softwood being crossed 14~20 mesh sieves carries out granulation and gets wet granular;
D. place baking oven dry said wet granular, make ethanol volatilize fully dried particle;
E. said dried particle is crossed 14~20 mesh sieves and carry out whole grain, the dried particle after must whole grain;
F. be in the dried particle after 0.5~3% said polyethylene glycol 8000 joins said whole grain with mass percent, be dosed into tablet forming in the tablet press machine after mixing,, prepare said microencapsulation germinated soybean peptide crude extract effervescence decoction piece through ultraviolet sterilization.
4. preparation method according to claim 3 is characterized in that, drying condition is 40~50 ℃ of drying 1~3h in the said steps d.
5. according to claim 3 or 4 described preparation methods, it is characterized in that the content in absolute ethyl alcohol of polyvinylpyrrolidone described in the said step b is 3g/100mL.
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CN103251111A (en) * 2013-05-27 2013-08-21 吉林大学 Soybean peptide effervescent tablets and preparation method thereof
CN104799273A (en) * 2014-01-27 2015-07-29 中粮营养健康研究院有限公司 Soybean peptide particle preparation method, soybean peptide particle and soybean peptide particle drink
CN105192841A (en) * 2015-08-17 2015-12-30 吉林大学 Multifunctional Korean pine seed peptide microcapsule effervescent tablets and preparation method thereof
CN107156307A (en) * 2017-07-11 2017-09-15 济源市能力源生物饮品有限公司 A kind of soy-bean peptide and its preparation technology
CN107569708A (en) * 2017-09-15 2018-01-12 南通香佳纺织科技有限公司 A kind of Peppermint essential oil microcapsules automobile inner air freshener and preparation method thereof
CN111887371A (en) * 2020-08-24 2020-11-06 深圳宝硒生物科技有限公司 Selenium-rich ferment peptide effervescent tablet

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CN102132819A (en) * 2011-03-30 2011-07-27 苏州先阔生物科技有限公司 Oligosaccharide-contained effervescent tablet

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CN101104866A (en) * 2006-07-14 2008-01-16 敦化市华力对外经贸有限责任公司 Technique for producing protein peptide and isoflavone extracted from bean sprout
JP4547015B2 (en) * 2008-04-02 2010-09-22 新田ゼラチン株式会社 Effervescent beverage and foaming agent for beverage
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103251111A (en) * 2013-05-27 2013-08-21 吉林大学 Soybean peptide effervescent tablets and preparation method thereof
CN104799273A (en) * 2014-01-27 2015-07-29 中粮营养健康研究院有限公司 Soybean peptide particle preparation method, soybean peptide particle and soybean peptide particle drink
CN105192841A (en) * 2015-08-17 2015-12-30 吉林大学 Multifunctional Korean pine seed peptide microcapsule effervescent tablets and preparation method thereof
CN107156307A (en) * 2017-07-11 2017-09-15 济源市能力源生物饮品有限公司 A kind of soy-bean peptide and its preparation technology
CN107569708A (en) * 2017-09-15 2018-01-12 南通香佳纺织科技有限公司 A kind of Peppermint essential oil microcapsules automobile inner air freshener and preparation method thereof
CN111887371A (en) * 2020-08-24 2020-11-06 深圳宝硒生物科技有限公司 Selenium-rich ferment peptide effervescent tablet

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