CN102399600A - Illegal cooking oil composite renewable fuel and its preparation method - Google Patents
Illegal cooking oil composite renewable fuel and its preparation method Download PDFInfo
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- CN102399600A CN102399600A CN2011103018037A CN201110301803A CN102399600A CN 102399600 A CN102399600 A CN 102399600A CN 2011103018037 A CN2011103018037 A CN 2011103018037A CN 201110301803 A CN201110301803 A CN 201110301803A CN 102399600 A CN102399600 A CN 102399600A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
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Abstract
Relating to the technical field of illegal cooking oil renewable fuels, the invention specifically discloses an illegal cooking oil composite renewable fuel and its preparation method. The composite fuel is prepared by mixing 35-60 parts by weight of methanol, 0.1-0.8 part by weight of ferrocene, 6-15 parts by weight of a cosolvent, 5-10 parts by weight of biodiesel, 5-10 parts by weight of an aromatic hydrocarbon, 1-5 parts by weight of an emulsifier, and 24-45 parts by weight of illegal cooking oil. And the obtained product has a high calorific value. As methanol and illegal cooking oil adopted in the invention are both renewable resources, the renewable fuel provided in the invention has low production cost and saves nonrenewable resources. Meanwhile, application fields of illegal cooking oil are expanded and the calorific value is raised, thus the renewable fuel of the invention boasts good social and economic benefits.
Description
Technical field
The present invention relates to sewer oil regenerated fuel technical field, be specifically related to composite regenerated fuel of a kind of sewer oil and preparation method thereof.
Background technology
Because world petroleum resource exhaustion and price rise steadily, international petroleum market is extremely unstable.Oil in all parts of the country station has valency not have oil.The tense situation of fuel supply, huge market demand, national environmental protection policy support that energetically exploitation substitute energy cheap, cleaning is extremely urgent.
Sewer oil general reference is human at all kinds of poor quality oils of producing, producing in the life, long-term edible may cause cancer, very harmful to human body.Owing to there is no small economic temptation, still have people's sale sewer oil of making a desperate move.To the sewer oil problem that the common people have strong complaints, the General Office of the State Council's in July, 2010 file publishing, trench wet goods city kitchen castoff recycling and harmless treatment pilot work are organized in decision.
If can be the raw material production regenerated fuel with the sewer oil, to alleviate prior fuel oil situation in short supply, then be to achieve many things at one stroke, will produce important social and economic benefit, not seeing as yet at present has the correlation technique report.
Summary of the invention
To the deficiency that exists in the prior art; The invention provides composite regenerated fuel of a kind of sewer oil and preparation method thereof, the purpose of this method be with from the restaurant, the sewer oil that reclaims of hotel is used for the preparation of methanol fuel, because methyl alcohol and sewer oil among the present invention are renewable resources; So production cost of the present invention is lower and practiced thrift Nonrenewable resources; Also expand simultaneously the Application Areas of sewer oil, improved calorific value, had good society and economic benefit.
To achieve these goals, the present invention has taked following technical measures:
The composite regenerated fuel of a kind of sewer oil is got by the preparation of following weight parts proportion raw material:
Methyl alcohol 35-60 part,
Ferrocene 0.1-0.8 part,
Solubility promoter 6-15 part,
Biofuel 5-10 part,
Aromatic hydrocarbons 5-10 part,
Emulsifying agent 1-5 part,
Sewer oil 24-45 part;
Described methyl alcohol is industrial methanol;
Described solubility promoter is one or more the mixture in ETHYLE ACETATE, butylacetate, EGME, ethylene glycol ethyl ether, butyl glycol ether, diethylene glycol dimethyl ether, diethylene glycol ether, Diethylene Glycol butyl ether, propylene glycol monomethyl ether, propylene-glycol ethyl ether, Ucar 35 butyl ether, dipropylene glycol methyl ether, dipropylene glycol ether, the dipropylene glycol butyl ether;
Described biofuel meets Chinese biological diesel oil national standard: diesel-fuel is concocted with biofuel (BD100), and GB/T 20828-2007, this raw material also have been the effects of solubility promoter;
Described aromatic hydrocarbons is one or more mixture of benzene,toluene,xylene, is the calorific value toughener;
Wherein YLENE is grade solvent YLENE;
Described emulsifying agent is a non-ionics, like one or more the mixture in Nonyl pheno (polymerization degree 9-40) ether, octyl phenol polyoxy ethene (polymerization degree 10-40) ether, lauryl alcohol polyethylene glycol oxide (polymerization degree 10-40) ether;
Described sewer oil is meant the oil that the waste grease that food and drink class enterprise such as restaurant produces (be the mixture of vegetables oil and animal oil, wash away the grease, the grease in the residue food of frying pan, grease that wash dishes produces when comprising cooking, repeatedly fry second-hand wet goods after the food) extracts through processing in the production and operation process.
The composite regenerated fuel preparation method of above-mentioned sewer oil is following:
At first in methyl alcohol, add ferrocene; Add solubility promoter, biofuel, aromatic hydrocarbons, emulsifying agent and sewer oil (carrying out next step operation again after all need mixing behind a kind of material of every adding) after the stirring and dissolving more successively; The mixed solution that obtains is filtered, and gained filtrating is compound fuel of the present invention.
Compared with prior art, advantage of the present invention and beneficial effect are:
Sewer oil is used for the production of composite fuel of methanol, has expanded the Application Areas of sewer oil, and raw material and preparation technology are simple, need not complicated procedures of forming such as heating and pressurizing, the calorific value of products obtained therefrom is higher, and comprehensive cost is low, is easy to promote.
Embodiment
Below in conjunction with concrete embodiment the inventive method is done further elaboration in detail, but following examples are not done any restriction to protection scope of the present invention.
Embodiment 1
The composite regenerated fuel of a kind of sewer oil is got by the preparation of following weight parts proportion raw material:
Industrial methanol: 60 parts,
Ferrocene: 0.5 part,
ETHYLE ACETATE: 10 parts,
Biofuel: 5 parts,
YLENE: 5 parts,
Nonyl pheno (polymerization degree 10) ether: 1 part,
Sewer oil: 24 parts.
The composite regenerated fuel preparation method of above-mentioned sewer oil, step is following:
1. methyl alcohol is added in the mixing tank;
2. adding ferrocene, stirring and dissolving;
3. add solubility promoter ETHYLE ACETATE again, mix;
4. add biofuel again, mix;
5. add YLENE again, mix;
6. add emulsifying agent Nonyl pheno (polymerization degree 10) ether again, mix;
7. add sewer oil again, mix;
8. the mixed solution that step 7 is obtained filters, and gained filtrating is product.
The calorific value of products obtained therefrom is 7500 kilocalorie/kilograms, 1100 ℃ of flame of centre temperature, and formolite test: magenta is not blue, can substitute culinary diesel oil, liquefied gas fully, can be used as the diesel oil alternative fuel of steam boiler, industrial baking heating installation yet.
Embodiment 2
The composite regenerated fuel of a kind of sewer oil is got by the preparation of following weight parts proportion raw material:
Industrial methanol: 35 parts,
Ferrocene: 0.8 part,
ETHYLE ACETATE: 10 parts,
Butylacetate: 5 parts,
Biofuel: 10 parts,
Toluene: 10 parts,
Octyl phenol polyoxy ethene (polymerization degree 20) ether: 5 parts,
Sewer oil: 45 parts.
The preparation method is referring to embodiment 1.
The calorific value of products obtained therefrom is 7800 kilocalorie/kilograms, 1150 ℃ of flame of centre temperature, and formolite test: magenta is not blue, can substitute culinary diesel oil, liquefied gas fully, can be used as the diesel oil alternative fuel of steam boiler, industrial baking heating installation yet.
Embodiment 3
The composite regenerated fuel of a kind of sewer oil is got by the preparation of following weight parts proportion raw material:
Industrial methanol: 50 parts,
Ferrocene: 0.3 part,
Ethylene glycol ethyl ether: 10 parts,
Biofuel: 8 parts,
YLENE: 6 parts,
Toluene: 2 parts,
Lauryl alcohol polyethylene glycol oxide (polymerization degree 40) ether: 3 parts,
Sewer oil: 30 parts.
The preparation method is referring to embodiment 1.
The calorific value of products obtained therefrom is 6900 kilocalorie/kilograms, 1120 ℃ of flame of centre temperature, and formolite test: magenta is not blue, can substitute culinary diesel oil, liquefied gas fully, can be used as the diesel oil alternative fuel of steam boiler, industrial baking heating installation yet.
Embodiment 4
The composite regenerated fuel of a kind of sewer oil is got by the preparation of following weight parts proportion raw material:
Industrial methanol: 45 parts,
Ferrocene: 0.6 part,
ETHYLE ACETATE: 7 parts,
Propylene glycol monomethyl ether: 5 parts,
Biofuel: 7 parts,
Toluene: 4 parts,
Benzene: 2 parts,
Lauryl alcohol polyethylene glycol oxide (polymerization degree 10) ether: 3 parts,
Sewer oil: 30 parts.
The preparation method is referring to embodiment 1.
The calorific value of products obtained therefrom is 8100 kilocalorie/kilograms, 1200 ℃ of flame of centre temperature, and formolite test: magenta is not blue, can substitute culinary diesel oil, liquefied gas fully, can be used as the diesel oil alternative fuel of steam boiler, industrial baking heating installation yet.
Claims (2)
1. composite regenerated fuel of sewer oil is characterized in that: said compound fuel is by the preparation of following weight parts proportion raw material and get:
Methyl alcohol 35-60 part,
Ferrocene 0.1-0.8 part,
Solubility promoter 6-15 part,
Biofuel 5-10 part,
Aromatic hydrocarbons 5-10 part,
Emulsifying agent 1-5 part,
Sewer oil 24-45 part;
Described solubility promoter is one or more the mixture in ETHYLE ACETATE, butylacetate, EGME, ethylene glycol ethyl ether, butyl glycol ether, diethylene glycol dimethyl ether, diethylene glycol ether, Diethylene Glycol butyl ether, propylene glycol monomethyl ether, propylene-glycol ethyl ether, Ucar 35 butyl ether, dipropylene glycol methyl ether, dipropylene glycol ether, the dipropylene glycol butyl ether;
Described aromatic hydrocarbons is one or more the mixture in the benzene,toluene,xylene;
Described emulsifying agent is one or more the mixture in the ethoxylated dodecyl alcohol of polyoxyethylene octylphenol ether, polymerization degree 10-40 of polyoxyethylene nonylphenol, the polymerization degree 10-40 of polymerization degree 9-40.
2. composite regenerated fuel preparation method of the described sewer oil of claim 1, its step is following:
At first in methyl alcohol, add ferrocene, add solubility promoter, biofuel, aromatic hydrocarbons, emulsifying agent and sewer oil after the stirring and dissolving more successively, the mixed solution that obtains is filtered, gained filtrating is compound fuel of the present invention.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN2011103018037A CN102399600A (en) | 2011-09-28 | 2011-09-28 | Illegal cooking oil composite renewable fuel and its preparation method |
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| CN2011103018037A CN102399600A (en) | 2011-09-28 | 2011-09-28 | Illegal cooking oil composite renewable fuel and its preparation method |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102776037A (en) * | 2012-08-08 | 2012-11-14 | 梅州市骏奇科技有限公司 | Biological tempered fuel oil using illegal cooking oil as raw material and preparation method thereof |
| CN102876395A (en) * | 2012-10-10 | 2013-01-16 | 南京友西科技有限责任公司 | Diesel-fired boiler fuel prepared by waste edible oil serving as main material and preparation method |
| CN103454267A (en) * | 2012-06-02 | 2013-12-18 | 王军 | Edible oil security detection method |
| CN103450956A (en) * | 2013-08-15 | 2013-12-18 | 陕西煤业化工集团格瑞新能源科技有限公司 | Coal-based diesel assistant |
| CN103555378A (en) * | 2013-11-05 | 2014-02-05 | 济南开发区星火科学技术研究院 | Preparation method of composite biodiesel |
| CN103642545A (en) * | 2013-12-02 | 2014-03-19 | 昆明理工大学 | Formula and preparation method for emulsified biodiesel |
| CN104804781A (en) * | 2015-04-27 | 2015-07-29 | 浙江汇能动物药品有限公司 | Methanol diesel containing illegal cooking oil and preparation method of methanol diesel |
| CN104845683A (en) * | 2015-06-03 | 2015-08-19 | 泰安华秦化工有限责任公司 | High-efficiency environment-friendly emulsifier |
| CN105400554A (en) * | 2015-12-31 | 2016-03-16 | 王丹 | Methanol gasoline efficient composite additive and preparation method thereof |
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Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103454267A (en) * | 2012-06-02 | 2013-12-18 | 王军 | Edible oil security detection method |
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| CN103642545A (en) * | 2013-12-02 | 2014-03-19 | 昆明理工大学 | Formula and preparation method for emulsified biodiesel |
| CN103642545B (en) * | 2013-12-02 | 2015-09-09 | 昆明理工大学 | A kind of emulsification formula of biodiesel and preparation method thereof |
| CN104804781A (en) * | 2015-04-27 | 2015-07-29 | 浙江汇能动物药品有限公司 | Methanol diesel containing illegal cooking oil and preparation method of methanol diesel |
| CN104804781B (en) * | 2015-04-27 | 2017-03-01 | 甘肃汇能生物工程有限公司 | Methanol diesel-oil containing waste oil and preparation method thereof |
| CN104845683A (en) * | 2015-06-03 | 2015-08-19 | 泰安华秦化工有限责任公司 | High-efficiency environment-friendly emulsifier |
| CN105400554A (en) * | 2015-12-31 | 2016-03-16 | 王丹 | Methanol gasoline efficient composite additive and preparation method thereof |
| CN105400554B (en) * | 2015-12-31 | 2017-02-01 | 太原理工大学 | Methanol gasoline efficient composite additive and preparation method thereof |
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Application publication date: 20120404 |