CN102397488A - Method for preparing submicron powder for legehenne at normal temperature, and two-way air flow screening machine special for method - Google Patents

Method for preparing submicron powder for legehenne at normal temperature, and two-way air flow screening machine special for method Download PDF

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CN102397488A
CN102397488A CN2011103829484A CN201110382948A CN102397488A CN 102397488 A CN102397488 A CN 102397488A CN 2011103829484 A CN2011103829484 A CN 2011103829484A CN 201110382948 A CN201110382948 A CN 201110382948A CN 102397488 A CN102397488 A CN 102397488A
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powder
screen drum
air
screening machine
normal temperature
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CN102397488B (en
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王伟伟
刘永录
张朝霞
王巧红
郭艳丽
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Henan Health Star Pharmaceutical Co., Ltd.
Henan Kang Xing Biotechnology Co., Ltd.
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Henan Kangxing Pharmaceutical Co Ltd
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Abstract

The invention discloses a method for preparing submicron powder for legehenne at normal temperature. The method comprises the following steps of: cleaning Chinese herbal medicinal decoction slices such as codonopsis pilosula, astragalus, tuckahoe, bighead atractylodes rhizome, malt, hawthorn, medicated leaven, south dodder seed, common cnidium fruit, and epimedium herb, and drying until the water content is less than and equal to 10 percent; crushing Chinese herbal medicines at room temperature to obtain coarse powder of which the granularity is 60 to 120 meshes; uniformly mixing the obtained coarse powder in a ratio; placing the obtained coarse powder in a rod mill and crushing, feeding into a two-way air flow screening machine special for the method by wind and screening to obtain powder of which the grain size is less than and equal to 25 microns, conveying the powder to a cyclone material collection device by air flow which is produced by a draught fan and collecting; and collecting powder which does not pass through a 500-mesh screen by using a funnel, conveying to the rod mill by a pipeline, and circulating and crushing again. The invention has the advantages that: the powder is prepared at normal temperature, the grain side of a finished medicine is less than and equal to 25 microns, the cell-wall breaking ratio and bioavailability are improved, and the used two-way air flow screening machine simplifies the method for preparing submicron powder for legehenne.

Description

Precious normal temperature preparation method of superfine powder laying hen and special-purpose two-way airflow screening machine thereof
Technical field
The present invention relates to the veterinary drug preparation field, especially relate to the precious normal temperature preparation method of superfine powder laying hen; The invention still further relates to the special-purpose two-way airflow screening machine that is used for this method.
Background technology
The laying hen treasured that is used to improve laying rate of laying hen at present is the powder of processing by after crude drug Radix Codonopsis, the Radix Astragali, Poria, the Rhizoma Atractylodis Macrocephalae, Fructus Hordei Germinatus, Fructus Crataegi, Massa Medicata Fermentata, Semen Cuscutae, Fructus Cnidii, the Herba Epimedii coarse pulverization; Have that dosage is big, dosage form is thick, appearance poor; Effective ingredient can not fully discharge; The low deficiency that waits of bioavailability has had a strong impact on Chinese medicine quality and therapeutic effect.
The broken technology of Chinese medicine ultra-fine powder is renewal and the development to traditional crushing technology; It had both kept the advantage of Chinese medicine technology of preparing; Injected new vitality for the modern production of Chinese medicine again; Have a extensive future, but in actual production, remain in some problems and a difficult problem: (1) production efficiency is low, the power consumption height is the principal element of restriction Chinese medicine ultra-fine powder large-scale production for animals.Rod mill is in traditional closed circuit method crushing process; When most of material has reached fineness requirement, always there is few part coarse powder to be mixed in wherein, make this part coarse powder further be crushed to the granularity that requires need prolong the pulverizing time significantly; Make crush efficiency reduce, power consumption significantly increases; (2) it is poor that there are the material particular diameter uniformity after the classification in selecting crude drugs with winnower classification and grading wheel classification; Influenced the quality of production of herbal medicine compound recipe superfine powder greatly; Especially when being applied to the use of animal drinking-water, because a small amount of not existence of breaking cellular wall cell is difficult to reach instructions for use.(3) traditional one-way gas flow is sieved, because Chinese medicine is when carrying out micronizing, along with reducing of particle diameter; Material particles surface area and surface energy increase; Adsorptivity increases, and mobile variation is prone to be gathered into bulky grain etc. and causes the sieve classification of crossing that surpasses 200 order fineness medicated powder to be difficult to carry out.The existence of above-mentioned factor has had a strong impact on standardization, the large-scale production of herbal medicine superfine powder, and popularization on veterinary clinic and use.
Summary of the invention
The object of the invention is to provide a kind of superfine powder laying hen precious normal temperature preparation method; Efficiently solve that the energy consumption that exists in the present production is big, the medicine maximum particle diameter is difficult to accurate control, can't continuous production, difficult problems such as dust is many in the production process, make the finished medicines of preparation have rapid-action, good effect, bioavailability is high, the clinical application amount is few effect.
Another purpose of the present invention is to provide a kind of special-purpose two-way airflow screening machine that is applied to the precious normal temperature preparation method of superfine powder laying hen.
The precious normal temperature preparation method of superfine powder laying hen of the present invention comprises the steps:
The first step, choose crude drug decoction pieces Radix Codonopsis, the Radix Astragali, Poria, the Rhizoma Atractylodis Macrocephalae, Fructus Hordei Germinatus, Fructus Crataegi, Massa Medicata Fermentata, Semen Cuscutae, Fructus Cnidii, Herba Epimedii respectively; Clean, dry or dry to moisture≤10%;
In second step, respectively that above-mentioned raw materials medicated powder is broken under 20 ℃~25 ℃ temperature, obtaining granularity is 60~120 purpose coarse powder;
The 3rd step, with the second step gained coarse powder in Radix Codonopsis: the weight portion ratio mix homogeneously of the Radix Astragali: Poria: the Rhizoma Atractylodis Macrocephalae: Fructus Hordei Germinatus: Fructus Crataegi: Massa Medicata Fermentata: Semen Cuscutae: Fructus Cnidii: Herba Epimedii=1:2:1:1:1:1:1:1:1:1;
The 4th step, with the 3rd step gained coarse powder place pulverize in the rod mill after; Be fed into special-purpose two-way airflow screening machine through wind and cross 500 mesh sieves, the air-flow that the powder that obtains particle diameter≤25 micron of sieving is produced by air-introduced machine is transported to collect in the tornado feeder set and promptly get superfine powder laying hen treasured finished product; The powder of not crossing 500 mesh sieves arrives circulation pulverizing once more in the said rod mill through the funnel collection and through line transportation.
Special-purpose two-way airflow screening machine of the present invention comprises JIKE and sets within it the downward screen drum of chamber intermediate openings, the order number of said screen drum >=500 orders; The nozzle of screen drum is connected with the funnel upper shed that is arranged on the JIKE bottom mutually; Chassis cavity is connected with air-introduced machine through the negative pressure chamber on top; Be provided with the door font rotating spraying trachea that constitutes by transverse tube and standpipe in the zone between screen drum and JIKE; The puff prot of said door font rotating spraying trachea is for axially being opened in the groove on its tube wall along said transverse tube and standpipe respectively; Said groove is offered towards the screen drum direction respectively; The groove width 0.5-2 millimeter of groove, the middle part of transverse tube and drive motors driving coupling; Be provided with blast pipe in the screen drum centre position, the air outlet of said blast pipe passes screen drum and is connected with the transverse tube middle part of door font rotating spraying trachea and is connected through the rolling bearing rolling; The air inlet of blast pipe extends outside the said hopper side walls and is connected with the blast orifice of aerator; In screen drum, be provided with feed pipe, above the discharging opening of said feed pipe, be provided with the buffering umbrella, the charging aperture of feed pipe extends outside the hopper side walls and is communicated with powder conveying fan air outlet through wind stopping device.
The air inducing of said air-introduced machine is pressed and is 1000pa, and the air inducing amount is 3000m 3/ h; The rotating speed of said drive motors is 155 rev/mins; The blast pressure of said aerator is 33kpa, and the blow rate required is 320m 3/ h; The wind pressure that goes out of said powder conveying fan is 24kpa, and air output is 150m 3/ h; The sidewall of said screen drum and roof respectively with corresponding standpipe and transverse tube between distance be 25 millimeters.
The invention has the advantages that whole process of preparation all carries out at normal temperatures, do not need low temperature or special additional conditions; Final drug particle diameter≤25 micron of preparation; Improve cell wall breaking rate and bioavailability greatly, strengthened pharmacological action, thereby reduced treatment disease dosage; Practiced thrift medical material; Also improve simultaneously the abnormal smells from the patient and the mouthfeel of medicine, made that directly adopting water way to take medicine to birds is achieved, changed the deficiency that Chinese powder medicine can only spice can not be drunk water and take; The two-way airflow screening machine that uses in the inventive method has been simplified the precious preparation technology of superfine powder laying hen greatly, has realized the purpose that the Chinese powder medicine quality standard is controlled, be suitable for large-scale industrial production.
The clinical therapeutic efficacy of preparation of the present invention obtains checking through following test:
1 materials and methods
1.1 experimental animal and grouping:
The I group: the precious group of superfine powder laying hen, adopt the present invention's preparation.
II group: the precious fine powder group of laying hen:, manufacture experimently at laboratory according to two ones of " Chinese veterinary drug allusion quotation " versions in 2010.
The III group: matched group, do not add the laying hen treasured
Experimental animal: select 150 of the Luo Manbai parent egg kind chickens in 43 close ages in week of raising condition, body condition, laying rate, be divided into 3 groups at random, every group each 50.
Usage and consumption are respectively: the I group is fed by 1% spice of feedstuff weight, and the II group is fed by 2% spice of feedstuff weight, III group blank group, and it is any not have interpolation; Experimental period is 42 days, and result of the test is seen table 1.
Table 1 egg laying performance leading indicator contrast table
Figure 2011103829484100002DEST_PATH_IMAGE001
Can find out from result of the test; There were significant differences on laying rate and egg counterpoise for the precious group of superfine powder laying hen, the precious fine powder group of laying hen and blank group (p 0.05); The precious group of superfine powder laying hen, the precious fine powder group of laying hen and blank group difference with insignificance on average daily feed intake; Explain and add the precious group of superfine powder laying hen and add the feed intake that the precious fine powder group of laying hen does not influence chicken that can think that superfine powder laying hen treasured is improving laying rate, increasing the egg size aspect has good effect.
Description of drawings
Fig. 1 is the production equipment system figure of the method for the invention.
Fig. 2 is the structural representation of special-purpose two-way airflow screening machine according to the invention.
The specific embodiment
Like Fig. 1, shown in 2, the precious normal temperature preparation method of superfine powder laying hen of the present invention comprises the steps:
The first step, choose crude drug decoction pieces Radix Codonopsis, the Radix Astragali, Poria, the Rhizoma Atractylodis Macrocephalae, Fructus Hordei Germinatus, Fructus Crataegi, Massa Medicata Fermentata, Semen Cuscutae, Fructus Cnidii, Herba Epimedii respectively; Clean, dry or dry to moisture≤10%;
In second step, respectively that above-mentioned raw materials medicated powder is broken under 20 ℃~25 ℃ temperature, obtaining granularity is 60~120 purpose coarse powder;
The 3rd step, with the second step gained coarse powder in Radix Codonopsis: the weight portion ratio mix homogeneously of the Radix Astragali: Poria: the Rhizoma Atractylodis Macrocephalae: Fructus Hordei Germinatus: Fructus Crataegi: Massa Medicata Fermentata: Semen Cuscutae: Fructus Cnidii: Herba Epimedii=1:2:1:1:1:1:1:1:1:1;
The 4th goes on foot, at first opens powder conveying fan 15, air-introduced machine 5, aerator 11, drive motors 8.The blow pressure of powder conveying fan 15 is 24kpa, and the blowing amount is 150m 3/ h; The air inducing of air-introduced machine 5 is pressed and is 1000pa, and the air inducing amount is 3000m 3/ h; The blast pressure of aerator 11 is 33kpa, blow rate required 320m 3/ h; The rotating speed of drive motors 8 is 155 rev/mins;
1, with the 3rd step gained coarse powder place pulverize in the rod mill 16 after; Powder body to be fractionated is arranged in the downward screen drum 2 of JIKE 1 inner chamber intermediate openings being brought into by high velocity air through wind stopping device 14, feed pipe 12 under the power of the blowing effect of powder conveying fan 15 in the rod mill 16; And, powder body to be fractionated is disperseed in screen drum 2 through the impulsive force of buffering umbrella 13 reduction powder body to be fractionated in screen drum 2; The order number of screen drum 2 is 500 orders;
2, dispersive powder body to be fractionated carries out classification through screen drum 2 in the screen drum 2 under air-introduced machine 5 effects, and fine powder negative pressure chamber 4 through JIKE 1 top under the negative-pressure air-flow effect that air-introduced machine 5 produces of passing screen drum 2 is transported to collect in the tornado feeder set 17 and promptly gets the precious finished product of superfine powder laying hen.The powder body sinking warp through screen drum 2 is collected with the funnel 3 that screen drum 2 under sheds are connected mutually and is transported in the said rod mill 16 circulation once more through pipeline 18 and pulverizes;
3, door font rotating spraying trachea rotates through rolling bearing 10 under drive motors 8 drives; The wind that aerator 11 is seen off is in blast pipe 9 gets into said transverse tube 6 and standpipe 7; And through be opened in the puff prot ejection that has the groove structure on transverse tube 6 and standpipe 7 tube walls respectively vertically towards screen drum 2 directions; Form the evenly blowback air-flow in screen drum 2 at screen drum 2 end faces and side; Powder body in the screen drum 2 is further atomized, stop powder body on screen drum 2, to lump simultaneously and stop up sieve screen apertures, make the powder body that does not pass through screen drum 2 along with the air-flow whirlpool that forms sinks to getting in the funnel 3.The groove width that is opened in groove on transverse tube 6 and standpipe 7 tube walls is respectively vertically selected between 0.5 millimeter-2 millimeters as required, between the roof of transverse tube 6 and standpipe 7 and corresponding screen drum 2 and the sidewall apart from being respectively 25 millimeters.
The precious finished product of the superfine powder laying hen of gained is sub-packed in the aluminium foil bag, every bag of 500g or 1000g storage.

Claims (3)

1. the precious normal temperature preparation method of superfine powder laying hen is characterized in that: comprise the steps:
The first step, choose crude drug decoction pieces Radix Codonopsis, the Radix Astragali, Poria, the Rhizoma Atractylodis Macrocephalae, Fructus Hordei Germinatus, Fructus Crataegi, Massa Medicata Fermentata, Semen Cuscutae, Fructus Cnidii, Herba Epimedii respectively; Clean, dry or dry to moisture≤10%;
In second step, respectively that above-mentioned raw materials medicated powder is broken under 20 ℃~25 ℃ temperature, obtaining granularity is 60~120 purpose coarse powder;
The 3rd step, with the second step gained coarse powder in Radix Codonopsis: the weight portion ratio mix homogeneously of the Radix Astragali: Poria: the Rhizoma Atractylodis Macrocephalae: Fructus Hordei Germinatus: Fructus Crataegi: Massa Medicata Fermentata: Semen Cuscutae: Fructus Cnidii: Herba Epimedii=1:2:1:1:1:1:1:1:1:1;
The 4th step, with the 3rd step gained coarse powder place pulverize in the rod mill (16) after; Be fed into special-purpose two-way airflow screening machine through wind and cross 500 mesh sieves, the air-flow that the powder that obtains particle diameter≤25 micron of sieving is produced by air-introduced machine (5) is transported to collect in the tornado feeder set (17) and promptly get superfine powder laying hen treasured finished product; The powder of not crossing 500 mesh sieves is transported to circulation pulverizing once more in the said rod mill (16) through funnel (3) collection and through pipeline (18).
2. according to the special-purpose two-way airflow screening machine of the precious normal temperature preparation method of the said superfine powder laying hen of claim 1, it is characterized in that: comprise JIKE (1) and the downward screen drum of chamber intermediate openings (2) that sets within it, the order number of said screen drum (2) >=500 orders; The nozzle of screen drum (2) is connected with funnel (3) upper shed that is arranged on JIKE (1) bottom mutually; JIKE (1) inner chamber is connected with air-introduced machine (5) through the negative pressure chamber (4) on top; Zone being positioned between screen drum (2) and the JIKE (1) is provided with the door font rotating spraying trachea that is made up of transverse tube (6) and standpipe (7); The puff prot of said door font rotating spraying trachea is for axially being opened in the groove on its tube wall along said transverse tube (6) and standpipe (7) respectively; Said groove is offered towards screen drum (2) direction respectively; The groove width 0.5-2 millimeter of groove, the middle part of transverse tube (6) and drive motors (8) driving coupling; Be provided with blast pipe (9) in screen drum (2) centre position, the air outlet of said blast pipe (9) passes screen drum (2) and is connected with transverse tube (6) middle part of door font rotating spraying trachea and is connected through rolling bearing (10) rolling; The air inlet of blast pipe (9) extends outside said funnel (3) sidewall and is connected with the blast orifice of aerator (11); In screen drum (2), be provided with feed pipe (12); Be provided with buffering umbrella (13) in the discharging opening of said feed pipe (12) top, the charging aperture of feed pipe (12) extends outside funnel (3) sidewall and is communicated with powder conveying fan (15) air outlet through wind stopping device (14).
3. special-purpose two-way airflow screening machine according to claim 2 is characterized in that: the air inducing of said air-introduced machine (5) is pressed and is 1000pa, and the air inducing amount is 3000m 3/ h; The rotating speed of said drive motors (8) is 155 rev/mins; The blast pressure of said aerator (11) is 33kpa, and the blow rate required is 320m 3/ h; The wind pressure that goes out of said powder conveying fan (15) is 24kpa, and air output is 150m 3/ h; The sidewall of said screen drum (2) and roof respectively with corresponding standpipe (7) and transverse tube (6) between distance be 25 millimeters.
CN 201110382948 2011-11-28 2011-11-28 Method for preparing submicron powder for legehenne at normal temperature, and two-way air flow screening machine special for method Active CN102397488B (en)

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Cited By (7)

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Publication number Priority date Publication date Assignee Title
CN102406688A (en) * 2011-11-28 2012-04-11 河南省康星药业有限公司 Normal-temperature preparation method of codonopsis pilosula submicron powder and special bidirectional airflow sieving machine used by same
CN103070972A (en) * 2012-12-11 2013-05-01 河南省康星药业股份有限公司 Normal temperature preparation method of Radix Scrophulariae and licorice submicron powder, and special bidirectional airflow screener therefor
CN103071011A (en) * 2012-12-11 2013-05-01 河南省康星药业股份有限公司 Normal temperature preparation method of chicken sexual maturity promotion ultrafine powder, and special bidirectional airflow screener therefor
CN103404696A (en) * 2013-07-18 2013-11-27 北京农业职业学院 Environmentally-friendly compound Chinese herbal medicinal feed additive for enhancing immunities of broilers, and application thereof
CN103960758A (en) * 2014-04-30 2014-08-06 程礼华 Production equipment for nutrition food for promoting health of sperm and eggs, and operating process of production equipment
CN104381702A (en) * 2014-12-09 2015-03-04 河南省惠民禽业有限公司 Chinese herbal medicine additive used for laying hen and used for increasing yield and resisting stress
CN104689160A (en) * 2013-12-04 2015-06-10 天津嘉瑞生物科技有限公司 Traditional Chinese medicine composition for improving egg laying rate of poultry and preparation method thereof

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102406688A (en) * 2011-11-28 2012-04-11 河南省康星药业有限公司 Normal-temperature preparation method of codonopsis pilosula submicron powder and special bidirectional airflow sieving machine used by same
CN102406688B (en) * 2011-11-28 2013-12-04 河南省康星药业股份有限公司 Normal-temperature preparation method of codonopsis pilosula submicron powder
CN103070972A (en) * 2012-12-11 2013-05-01 河南省康星药业股份有限公司 Normal temperature preparation method of Radix Scrophulariae and licorice submicron powder, and special bidirectional airflow screener therefor
CN103071011A (en) * 2012-12-11 2013-05-01 河南省康星药业股份有限公司 Normal temperature preparation method of chicken sexual maturity promotion ultrafine powder, and special bidirectional airflow screener therefor
CN103404696A (en) * 2013-07-18 2013-11-27 北京农业职业学院 Environmentally-friendly compound Chinese herbal medicinal feed additive for enhancing immunities of broilers, and application thereof
CN104689160A (en) * 2013-12-04 2015-06-10 天津嘉瑞生物科技有限公司 Traditional Chinese medicine composition for improving egg laying rate of poultry and preparation method thereof
CN103960758A (en) * 2014-04-30 2014-08-06 程礼华 Production equipment for nutrition food for promoting health of sperm and eggs, and operating process of production equipment
CN104381702A (en) * 2014-12-09 2015-03-04 河南省惠民禽业有限公司 Chinese herbal medicine additive used for laying hen and used for increasing yield and resisting stress

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