CN102352575A - Filter candle paper added with adsorbent filling material, paper-based filter candle and preparation method - Google Patents
Filter candle paper added with adsorbent filling material, paper-based filter candle and preparation method Download PDFInfo
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- CN102352575A CN102352575A CN201110183853XA CN201110183853A CN102352575A CN 102352575 A CN102352575 A CN 102352575A CN 201110183853X A CN201110183853X A CN 201110183853XA CN 201110183853 A CN201110183853 A CN 201110183853A CN 102352575 A CN102352575 A CN 102352575A
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Abstract
A filter candle paper added with an adsorbent filling material, a paper-based filter candle and a preparation method. The filter candle paper contains cellulose diacetate, which is prepared by adding an adsorbent filling material into cellulose diacetate slurry from spinning and accounts for 1-99wt% in the paper; the filter candle paper also contains one or more of wood pulp fiber, cotton pulp fiber, bamboo pulp fiber and jute pulp fiber. The paper-based filter candle is processed by embossing, slitting and moulding the filter candle paper. A preparation method of the filter candle paper comprises steps of: adding the adsorbent filling material into spinning slurry from cellulose diacetate spinning and mixing well with the slurry; spinning cellulose diacetate by a dry method spinning technology; then milling the cellulose diacetate to short fibered pulp, mixing with one or more of the milled wood pulp fiber, cotton pulp fiber, bamboo pulp fiber and jute pulp fiber, and processing into paper. The filter candle paper of the invention has strong adsorptivity and can effectively reduce tar, solid particulate matter, nicotine and various other harmful components in cigarette flue gas and mitigate influenced of common paper-based filter candle on cigarette flavour.
Description
Technical field
The invention belongs to the cigarette filter technical field.
Background technology
Filter stick for cigarettes is the main cigarette supplementary of tobacco business, in the reducing cigarette tar and reducing harm reduction, plays important effect.It is good that the paper filter stick of processing with strings such as pure wood pulp, cotton pulp, bamboo pulp or jute pulps has a strainability; Fall burnt remarkably productive; Advantages of cheap price; But aspect elasticity, outward appearance, water imbibition, exist not enoughly, burn and suck to exist in the process at cigarette and produce that heat is subsided, flue gas is dry, shortcoming such as paper flavor is arranged significantly.Present widely used diacetate fiber fiber tow filter rods has overcome the shortcoming of common paper filter stick at aspects such as outward appearance, suction flavors, but also there is the not good enough deficiency of reducing tar and reducing harm effect in paper filter stick relatively.
Publication number is the one Chinese patent application of CN101032347; Proposed to make the method for the required paper of paper filter stick with the slurries that contain diacetate fiber; For novel paper filter stick provides new approaches with the research of paper, but the paper that contains acetate fiber of its preparation does not show the performance of more desirable reducing tar and reducing harm.
Summary of the invention
The object of the invention is intended to solve the deficiency of prior art; Provide a kind of cigarette filter rod to use paper with strong adsorptivity; With the tar in effective reduction cigarette smoke, solid granule phase substance, nicotine and other multiple harmful components, improve of the influence of common paper filter stick simultaneously to cigarette odor-absorbing.
Another object of the present invention provides the preparation method of above-mentioned cigarette filter rod with paper.
The 3rd purpose of the present invention is to provide and adopts above-mentioned cigarette filter rod with the paper filter stick that is equipped with made of paper.
The object of the invention is realized through following technical scheme.
A kind of filter stick that adds the adsorptivity packing material is used paper, and it is the paper that contains diacetate fiber that filter stick uses paper; Said diacetate fiber is in the diacetate fiber slurries of spinning, to add the fiber that the adsorptivity packing material prepares; The mass content of diacetate fiber in paper is 1%～99%, and all the other are in wood pulp fibre, cotton pulp fiber, bamboo pulp fiber, the ramie pulp fiber one or more;
Filter stick of the present invention is used paper, and its adsorptivity packing material total addition level is 0.2%～5% of a diacetate fiber weight.Described adsorptivity packing material is one or more in active carbon, imvite, zeolite, molecular sieve, attapulgite, medical stone, diatomite, sepiolite, the nano silicon.The particle diameter of adsorptivity packing material is 0.02 μ m～10 μ m.The quantitative of the paper that contains diacetate fiber for preparing is 12g/m
2～100g/ m
2
The filter stick of using interpolation adsorptivity packing material is that the filter stick that contains diacetate fiber that adds the adsorptivity packing material is carried out embossing, cuts with paper with the paper filter stick of doing made of paper, uses filter-stick forming device machine-shaping to be paper filter stick.
A kind of preparation method who adds the filter stick of adsorptivity packing material with paper comprises following method step:
1) in the spinning slurry of spinning diacetate fiber, adds the adsorptivity packing material, mix with slurries;
2) spin the diacetate fiber that contains the adsorptivity packing material with dry-spinning process;
The diacetate fiber mill that 3) will contain the adsorptivity packing material becomes short fibered pulp, mixes with in wood pulp, cotton pulp, bamboo pulp or the jute pulp that mill is good one or more, adopts wet method or dry method of paper-making prepared to become paper again.
The inventive method adsorptivity packing material total addition level is 0.2%～5% of a diacetate fiber weight.Described adsorptivity packing material is one or more in active carbon, imvite, zeolite, molecular sieve, attapulgite, medical stone, diatomite, sepiolite, the nano silicon; The particle diameter of adsorptivity packing material is 0.02 μ m～10 μ m.The inventive method starches diacetate fiber with wood pulp, cotton pulp, bamboo pulp or the jute pulp of mill mix by weight 1: 0.05～5.
The present invention also can be with the filter stick that contains diacetate fiber that has added the adsorptivity packing material with paper carries out embossing, cuts, moulding obtains paper filter stick and compound binary or the composite filter more than the binary processed of other type filter stick.
Sorptive material joins as packing material can improve the Filtration Adsorption effect of diacetate fiber to tar, nicotine and other harmful components in the flue gas greatly in the diacetate fiber.The present invention has added the paper of the diacetate fiber preparation of adsorptivity packing material through employing, and then the paper filter stick of preparation, not only possesses the advantage of paper filter stick; Can also significantly reduce solid granule phase substance, tar, nicotine and other harmful components in the cigarette smoke; Improve the security of cigarette, improve the suction flavor of cigarette, improve sensory evaluating smoking's quality of common paper filter stick; Overcoming paper filter stick, to burn and suck in the process flue gas at cigarette dry; Shortcomings such as tangible paper flavor are arranged, and manufacturing technique is simple, cost is low, practicality is stronger.
The specific embodiment
Following examples are intended to further specify the present invention, but the present invention is not limited thereto.
Embodiment 1
Selecting distribute diatomite and the medical stone of 1 μ m～10 μ m of particle diameter is the adsorptivity packing material; It is even in the spinning slurry of spinning diacetate fiber, to add the adsorptivity packing material and the abundant mixed and dispersed that account for diacetate fiber quality 0.2%, adopts the dry-spinning process spinning to obtain long filament, and this long filament mill is dissociated obtains the diacetate fiber slurry; According to weight ratio 1: 0.05; The diacetate fiber slurry is mixed with the good wood pulp of mill, adopt dry method of paper-making technology system paper, obtain quantitatively being 12g/m
2Contain the diacetate fiber paper that adds the adsorptivity packing material.The paper of processing through embossing, is cut into 30cm in a narrow margin, be made into filter stick with filter-stick forming device, carry out compoundly with the diacetate fiber filter stick again, making becomes the binary compound filter candle that compositely proportional is 10mm: 15mm.Through test, adopt this filter stick to greatly reduce solid granule phase substance, tar and other multiple harmful components in the cigarette smoke.
Embodiment 2
In the spinning slurry of spinning diacetate fiber, add and account for the active carbon that diacetate fiber mass percent 2% and particle diameter are distributed as 0.2 μ m～5 μ m; Fully mixed and dispersed is even, and the dry-spinning process spinning that accordings to diacetate fiber is spun into long filament, and dissociating this long filament mill obtains the diacetate fiber slurry; According to weight ratio 1: 0.1; Diacetate fiber slurry is mixed with cotton pulp through mill, employing dry method of paper-making technology system paper, obtaining quantitatively is 60g/m
2Contain the diacetate fiber paper that adds the adsorptivity packing material.The diacetate fiber paper of processing through embossing, is cut into 19cm in a narrow margin, be made into filter stick with filter-stick forming device.Carry out compoundly with spices center line filter stick, making becomes the binary compound filter candle that compositely proportional is 15mm: 10mm.Through test, adopt this filter stick to greatly reduce solid granule phase substance, tar and other multiple harmful components in the cigarette smoke.
Embodiment 3
In the spinning slurry of diacetate fiber, add and account for the sepiolite that diacetate fiber mass percent 2.5%, particle diameter are distributed as 5 μ m～10 μ m, fully mixed and dispersed is even, is spun into long filament according to the dry-spinning process spinning of diacetate fiber; Dissociating this long filament mill obtains diacetate fiber slurry, according to weight ratio 1: 2, the diacetate fiber slurry that has added the adsorptivity packing material is mixed with the bamboo pulp through mill, and employing dry method system paper, obtaining quantitatively is 100g/m
2Contain the diacetate fiber paper that adds the adsorptivity packing material.The diacetate fiber paper of processing through embossing, is cut into 10cm in a narrow margin, be made into filter stick with filter-stick forming device.Carry out compoundly with the coaxial core filter stick, making becomes the binary compound filter candle that compositely proportional is 12mm: 10mm.Through test, adopt this filter stick to greatly reduce solid granule phase substance, tar and other multiple harmful components in the cigarette smoke.
Embodiment 4
In the spinning slurry of diacetate fiber, add and account for molecular sieve and the nano silicon that diacetate fiber mass percent 5%, particle diameter are distributed as 0.02 μ m～1 μ m; Press 1 to molecular sieve, nano silicon; The abundant mixed and dispersed of 1 mass fraction and diacetate fiber is even, and the dry-spinning process spinning that accordings to diacetate fiber is spun into long filament; Dissociate this long filament mill, according to weight ratio 1: 5, the diacetate fiber that has added the adsorptivity packing material is mixed with jute pulp through mill, adopt wet method system paper, obtaining quantitatively is 40g/m
2The paper that contains the diacetate fiber that adds the adsorptivity packing material.The paper of processing through embossing, is cut into 20cm in a narrow margin, be made into filter stick with filter-stick forming device.To carry out ternary compound with the diacetate fiber filter stick, and making becomes the diacetate fiber filter stick that compositely proportional is 5mm: 10mm:10mm, the paper filter stick that adds the diacetate fiber of adsorptivity packing material, the ternary composite filter of diacetate fiber filter stick.Through test, adopt this filter stick to greatly reduce solid granule phase substance, tar and other multiple harmful components in the cigarette smoke.
Embodiment 5
In the spinning slurry of diacetate fiber, add and respectively account for imvite and the attapulgite that diacetate fiber mass percent 1% and particle diameter are distributed as 1 μ m～5 μ m; Even imvite and attapulgite and the abundant mixed and dispersed of diacetate fiber, be spun into long filament according to the dry-spinning process spinning of diacetate fiber; Dissociate this long filament mill, according to weight ratio 1: 0.1: 0.1, the diacetate fiber that has added the adsorptivity packing material is mixed with wood pulp, bamboo pulp through mill, adopt wet method system paper, obtaining quantitatively is 75g/m
2The paper that contains the diacetate fiber that adds the adsorptivity packing material.The paper of processing through embossing, is cut into 22cm in a narrow margin, be made into filter stick with filter-stick forming device.Cut into the long paper filter stick of 22mm, be hinged with into cigarette.Through test, adopt this filter stick to greatly reduce solid granule phase substance, tar and other multiple harmful components in the cigarette smoke.
Embodiment 6
In the spinning slurry of diacetate fiber, add and account for the zeolite that diacetate fiber mass percent 2% and particle diameter are distributed as 6 μ m～10 μ m; Even adsorptivity packing material zeolite and the abundant mixed and dispersed of cellulose diacetate, the dry-spinning process spinning that accordings to diacetate fiber is spun into long filament; Dissociate this long filament mill, according to weight ratio 1: 0.5: 0.5, the diacetate fiber that has added the adsorptivity packing material is mixed with cotton pulp, fiber crops through mill, adopt dry method system paper, obtaining quantitatively is 45g/m
2The paper that contains the diacetate fiber that adds the adsorptivity packing material.The paper of processing through embossing, is cut into 18cm in a narrow margin, be made into filter stick with filter-stick forming device.With the particle composite filter, that the diacetate fiber filter stick carries out ternary is compound; Making becomes paper filter stick, particle composite filter, the ternary composite filter of diacetate fiber filter stick of diacetate fiber that compositely proportional is the interpolation adsorptivity packing material of 3mm: 10mm:12mm, is hinged with into cigarette.Through test, adopt this filter stick to greatly reduce solid granule phase substance, tar and other multiple harmful components in the cigarette smoke.
Paper filter stick of the present invention has the whole good function and the external appearance characteristic of common paper filter stick; And in the filter stick formation process, can not apply triacetyl glycerine or other cellulose diacetate plasticizer, reduce processing link; Simplify production technology, reduced production cost.
Spinning technique among the present invention, paper technology, mill pulping process all can adopt prior art, and wood pulp, cotton pulp, bamboo pulp, jute pulp etc. can oneself prepare, and also can directly buy from market.
Claims (11)
1. a filter stick that adds the adsorptivity packing material is used paper, it is characterized in that, it is the paper that contains diacetate fiber that filter stick uses paper; Said diacetate fiber is in the diacetate fiber slurries of spinning, to add the fiber that the adsorptivity packing material prepares; The mass content of diacetate fiber in paper is 1%～99%, and all the other are in wood pulp fibre, cotton pulp fiber, bamboo pulp fiber, the ramie pulp fiber one or more.
2. a kind of filter stick that adds the adsorptivity packing material according to claim 1 is used paper, it is characterized in that, adsorptivity packing material total addition level is 0.2%～5% of a diacetate fiber weight.
3. a kind of filter stick that adds the adsorptivity packing material according to claim 1 and 2 is used paper; It is characterized in that described adsorptivity packing material is one or more in active carbon, imvite, zeolite, molecular sieve, attapulgite, medical stone, diatomite, sepiolite, the nano silicon.
4. a kind of filter stick that adds the adsorptivity packing material according to claim 1 and 2 is used paper, it is characterized in that, the particle diameter of said adsorptivity packing material is 0.02 μ m～10 μ m.
5. a kind of filter stick that adds the adsorptivity packing material according to claim 1 is used paper, it is characterized in that, the said quantitative 12g/m of being that contains the paper of diacetate fiber
2～100g/ m
2
6. application rights requires 1 said a kind of filter stick that adds the adsorptivity packing material with the paper filter stick of doing made of paper; It is characterized in that; The filter stick that contains diacetate fiber that adds the adsorptivity packing material is carried out embossing, cuts with paper, use filter-stick forming device machine-shaping to be paper filter stick.
7. a preparation method who adds the filter stick of adsorptivity packing material with paper is characterized in that, comprises following method step:
1) in the spinning slurry of spinning diacetate fiber, adds the adsorptivity packing material, mix with slurries;
2) spin the diacetate fiber that contains the adsorptivity packing material with dry-spinning process;
The diacetate fiber mill that 3) will contain the adsorptivity packing material becomes short fibered pulp, mixes with in wood pulp, cotton pulp, bamboo pulp or the jute pulp that mill is good one or more, adopts wet method or dry method of paper-making prepared to become paper again.
8. a kind of preparation method who adds the filter stick of adsorptivity packing material with paper according to claim 7 is characterized in that adsorptivity packing material total addition level is 0.2%～5% of a diacetate fiber weight.
9. a kind of preparation method who adds the filter stick of adsorptivity packing material with paper according to claim 7; It is characterized in that described adsorptivity packing material is one or more in active carbon, imvite, zeolite, molecular sieve, attapulgite, medical stone, diatomite, sepiolite, the nano silicon; The particle diameter of adsorptivity packing material is 0.02 μ m～10 μ m.
10. a kind of preparation method who adds the filter stick of adsorptivity packing material with paper according to claim 7 is characterized in that, diacetate fiber is starched with wood pulp, cotton pulp, bamboo pulp or the jute pulp of mill mix by weight 1: 0.05～5.
11. according to the said a kind of filter stick that adds the adsorptivity packing material of claim 6 with the paper filter stick of doing made of paper; It is characterized in that, with the filter stick that contains diacetate fiber that has added the adsorptivity packing material with paper carries out embossing, cuts, moulding obtains paper filter stick and compound binary or the composite filter more than the binary processed of other type filter stick.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110183853XA CN102352575A (en) | 2011-07-02 | 2011-07-02 | Filter candle paper added with adsorbent filling material, paper-based filter candle and preparation method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110183853XA CN102352575A (en) | 2011-07-02 | 2011-07-02 | Filter candle paper added with adsorbent filling material, paper-based filter candle and preparation method |
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| CN102352575A true CN102352575A (en) | 2012-02-15 |
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| CN201110183853XA Pending CN102352575A (en) | 2011-07-02 | 2011-07-02 | Filter candle paper added with adsorbent filling material, paper-based filter candle and preparation method |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102877356A (en) * | 2012-09-26 | 2013-01-16 | 南通烟滤嘴有限责任公司 | Tobacco fiber filter stick, preparation method, and composite filter tip of tobacco fiber filter stick |
| CN102987560A (en) * | 2012-11-28 | 2013-03-27 | 红塔烟草(集团)有限责任公司 | Paper filter material provided with active adsorption layer |
| CN102995497A (en) * | 2012-10-31 | 2013-03-27 | 蚌埠首创滤清器有限公司 | Filter paper for air filter and preparation method of filter paper |
| CN103054190A (en) * | 2013-02-05 | 2013-04-24 | 大亚科技股份有限公司 | Composite tobacco filter tip rod with added nanosilicon dioxide |
| CN103161097A (en) * | 2013-03-14 | 2013-06-19 | 牡丹江恒丰纸业股份有限公司 | Paper filter stick base paper containing functional additives |
| CN103638897A (en) * | 2013-12-05 | 2014-03-19 | 川渝中烟工业有限责任公司 | Metal pillared montmorillonite coated mesoporous silica composite material and preparation method thereof |
| CN105080471A (en) * | 2015-09-08 | 2015-11-25 | 江苏爱尔环保科技有限公司 | Nicotine adsorbent and preparation method thereof |
| CN105200843A (en) * | 2015-09-01 | 2015-12-30 | 云南瑞升烟草技术（集团）有限公司 | Drying groove paper for filter rod and preparation method thereof |
| CN105747264A (en) * | 2016-04-20 | 2016-07-13 | 贵州中烟工业有限责任公司 | Method for preparing heat-not-burn tobacco bases containing active carbon |
| CN106087548A (en) * | 2016-06-16 | 2016-11-09 | 铜陵锋帆彩色印务有限公司 | Anti-abnormal flavour cardboard and preparation method thereof |
| CN106894283A (en) * | 2017-03-23 | 2017-06-27 | 周佳荣 | A kind of cigarette refines paper material and preparation method and application with function |
| CN108086043A (en) * | 2017-12-28 | 2018-05-29 | 安徽宏实光机电高科有限公司 | A kind of preparation method of the cigarette filter paper with selective absorption |
| CN113957740A (en) * | 2020-07-20 | 2022-01-21 | 福建中烟工业有限责任公司 | Method for preparing activated carbon fiber composite paper, obtained paper and application thereof |
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Cited By (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102877356A (en) * | 2012-09-26 | 2013-01-16 | 南通烟滤嘴有限责任公司 | Tobacco fiber filter stick, preparation method, and composite filter tip of tobacco fiber filter stick |
| CN102995497A (en) * | 2012-10-31 | 2013-03-27 | 蚌埠首创滤清器有限公司 | Filter paper for air filter and preparation method of filter paper |
| CN102995497B (en) * | 2012-10-31 | 2015-07-22 | 蚌埠首创滤清器有限公司 | Filter paper for air filter and preparation method of filter paper |
| CN102987560A (en) * | 2012-11-28 | 2013-03-27 | 红塔烟草(集团)有限责任公司 | Paper filter material provided with active adsorption layer |
| CN103054190A (en) * | 2013-02-05 | 2013-04-24 | 大亚科技股份有限公司 | Composite tobacco filter tip rod with added nanosilicon dioxide |
| CN103161097A (en) * | 2013-03-14 | 2013-06-19 | 牡丹江恒丰纸业股份有限公司 | Paper filter stick base paper containing functional additives |
| CN103638897A (en) * | 2013-12-05 | 2014-03-19 | 川渝中烟工业有限责任公司 | Metal pillared montmorillonite coated mesoporous silica composite material and preparation method thereof |
| CN105200843A (en) * | 2015-09-01 | 2015-12-30 | 云南瑞升烟草技术（集团）有限公司 | Drying groove paper for filter rod and preparation method thereof |
| CN105080471A (en) * | 2015-09-08 | 2015-11-25 | 江苏爱尔环保科技有限公司 | Nicotine adsorbent and preparation method thereof |
| CN105080471B (en) * | 2015-09-08 | 2017-08-11 | 江苏爱尔环保科技有限公司 | Nicotine absorbent and preparation method thereof |
| CN105747264A (en) * | 2016-04-20 | 2016-07-13 | 贵州中烟工业有限责任公司 | Method for preparing heat-not-burn tobacco bases containing active carbon |
| CN105747264B (en) * | 2016-04-20 | 2020-11-20 | 贵州中烟工业有限责任公司 | Activated carbon-containing heating non-combustible tobacco substrate and preparation method and application thereof |
| CN106087548A (en) * | 2016-06-16 | 2016-11-09 | 铜陵锋帆彩色印务有限公司 | Anti-abnormal flavour cardboard and preparation method thereof |
| CN106894283A (en) * | 2017-03-23 | 2017-06-27 | 周佳荣 | A kind of cigarette refines paper material and preparation method and application with function |
| CN106894283B (en) * | 2017-03-23 | 2018-07-03 | 周佳荣 | A kind of cigarette refines paper material and preparation method and application with function |
| CN108086043A (en) * | 2017-12-28 | 2018-05-29 | 安徽宏实光机电高科有限公司 | A kind of preparation method of the cigarette filter paper with selective absorption |
| CN113957740A (en) * | 2020-07-20 | 2022-01-21 | 福建中烟工业有限责任公司 | Method for preparing activated carbon fiber composite paper, obtained paper and application thereof |
| CN113957740B (en) * | 2020-07-20 | 2023-06-09 | 福建中烟工业有限责任公司 | Method for preparing activated carbon fiber composite paper, obtained paper and application thereof |
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Inventor after: Luo Lili Inventor after: Ni Jun Inventor after: Chen Wan Inventor after: Huang Haiqun Inventor after: Sheng Peixiu Inventor after: Li Min Inventor after: Tang Rongcheng Inventor after: Yang Weizu Inventor after: Shen Jingxuan Inventor after: Ma Tao Inventor after: Yao Zhenyu Inventor after: Wen Guanghe Inventor before: Luo Lili Inventor before: Huang Haiqun Inventor before: Li Min Inventor before: Yang Weizu Inventor before: Shen Jingxuan Inventor before: Ma Tao Inventor before: Yao Zhenyu Inventor before: Wen Guanghe Inventor before: Ni Jun Inventor before: Chen Wan |
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Free format text: CORRECT: INVENTOR; FROM: LUO LILI LI MIN YANG WEIZU SHEN JINGXUAN MA TAO YAO ZHENYU WEN GUANGHE NI JUN CHEN WAN HUANG HAIQUN TO: LUO LILI SHENG PEIXIU LI MIN TANG RONGCHENG YANG WEIZU SHEN JINGXUAN MA TAO YAO ZHENYU WEN GUANGHE NI JUN CHEN WAN HUANG HAIQUN |
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Effective date of registration: 20120619 Address after: 650106 Yunnan province Haiyuan Kunming high tech Development Zone No. 1699 North Road Applicant after: Yunnan Reascend Tobacco Technology (Group) Co., Ltd. Co-applicant after: Nantong Cigarette Filter Co., Ltd. Address before: 650106 Yunnan province Haiyuan Kunming high tech Development Zone No. 1699 North Road Applicant before: Yunnan Reascend Tobacco Technology (Group) Co., Ltd. |
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Application publication date: 20120215 |