CN102995497A - Filter paper for air filter and preparation method of filter paper - Google Patents
Filter paper for air filter and preparation method of filter paper Download PDFInfo
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- CN102995497A CN102995497A CN2012104268316A CN201210426831A CN102995497A CN 102995497 A CN102995497 A CN 102995497A CN 2012104268316 A CN2012104268316 A CN 2012104268316A CN 201210426831 A CN201210426831 A CN 201210426831A CN 102995497 A CN102995497 A CN 102995497A
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Abstract
The invention discloses a filter paper for an air filter and a preparation method of the filter paper. The filter paper comprises a composition A and a composition B in parts by weight, wherein the composition A consists of slag slurry, polystyrene fiber, bamboo charcoal, modified water-soluble phenol-formaldehyde resin, tetra-isopropyl bi(dioctyl phosphorous acid acyloxy) titanate, epoxidized soybean oil, magnesium hydrate, citric acid, diphenylamine, polycaprolactone, sodium polymethacrylate, alkylbenzene sulfonate, and modified straw powder; and the composition B consists of waste paper pulp, acetate fiber, gelatin, modified diatomite, ammonium polyacrylate, aluminium silicate, bis-tetradecene alcohol ester, nano calcium carbonate, sodium pentachlorophenate, poly-4-methyl-1-amylene, and Peregal O. By using the slag slurry, the polystyrene fiber, the waste paper pulp and the acetate fiber synchronously as the main materials, the filter paper is environment-friendly and scientific, the formula of raw materials is reasonable, the compatibility among various components is excellent, the strength, the toughness and the corrosion resistance are improved, the surface gloss is excellent, the filter paper has stable property indexes under the working conditions at normal temperature and high temperature, and has relatively good temperature resistance and filtering effects, the maximal aperture is 44micron to 52micron, the average aperture is 31micron to 37micron, and the air permeability of the formed paper is between 86L.m<2>.S and 90L.m<2>.S.
Description
Technical field
The present invention relates to the automobile filter field, specifically a kind of air filter filter paper and preparation method thereof.
Background technology
Cleaner is the important spare part of engine, it act as the particulates such as dust in air that filtering enters engine, diesel oil, the machine oil and mechanical admixture, to reduce the wearing and tearing of Cylinder Liner Piston Ring in Engine, crankshaft link rod motion pair and high-pressure oil pump plunger matching parts, optimize the combustion process of engine, reduce the discharging of the organic pollutions such as carbon monoxide.
As a kind of effective filter medium, filter paper has been widely used in every field.Different according to the kinds of fibers that forms filter paper, the performance of filter paper, purposes are also different, are useful on the common filter paper of general occasion, be used under the high temperature glass fiber filter paper, also have ultra-clean with polypropylene filter paper etc.According to filter paper impregnation whether, can be divided into two large classes, i.e. impregnation filter paper and non-impregnation filter paper.Impregnation filter paper is divided into again curing filter paper and non-curing filter paper.
Along with filtering improving constantly of requiring, anyly plant fibrous filter paper and all more and more be difficult to satisfy requirement on using by single, so the filter paper that is formed by multiple fiber combinations arises at the historic moment, fiber commonly used in the filter paper production has wood fibre, chemical fibre, glass fibre etc.
Summary of the invention
The object of the present invention is to provide a kind of air filter filter paper and preparation method thereof, the present invention adopts slag slurry, styroflex, secondary stock and acetate fiber simultaneously as main material, the environmental protection science, composition of raw materials is reasonable, each group partition inter-capacitive is good, intensity, toughness, corrosion resistance improve, surface gloss is good, stable performance indications are arranged under normal temperature and worst hot case, have preferably heatproof and filter effect, its maximum diameter of hole 44-52 μ m, average pore size 31-37 μ m becomes the paper air permeability at 86-90L/m
2.S between.
The present invention adopts following technical scheme to achieve these goals:
Air filter filter paper, the weight portion of its constitutive material is:
Composition A: vinegar 14-18, sodium polymethacrylate 1.5-2.5, heavy alkylbenzene sulfonate 1.7-2.3, modified straw powder 1.5-3.5 in slag slurry 65-68, styroflex 13-16, bamboo charcoal 4-6, Modified Water Soluble Phenolic Resin 0.9-1.1, tetra isopropyl two (dioctyl phosphorous acid acyloxy) titanate esters 0.7-0.9, epoxidized soybean oil 0.8-1.2, magnesium hydroxide 1.4-1.6, citric acid 0.7-0.9, diphenylamines 0.4-0.6, the poly-caproic acid.
Composition B: secondary stock 23-28, acetate fiber 13-18, gelatin 1-3, modification infusorial earth 0.4-0.6, ammonium polyacrylate 0.8-1.2, alumina silicate 0.5-0.7, two ten four carbon alcohols ester 0.3-0.6, nano-calcium carbonate 1-3, penta sodium pentachlorophenate 1.5-2.5, poly--4-methyl-1-pentene 0.7-0.9 and paregal O 0.4-0.6.
Air filter filter paper, the weight portion of its constitutive material is:
Composition A: vinegar 16, sodium polymethacrylate 2, heavy alkylbenzene sulfonate 2, modified straw powder 2.5 in slag slurry 66, styroflex 14, bamboo charcoal 5, Modified Water Soluble Phenolic Resin 1, tetra isopropyl two (dioctyl phosphorous acid acyloxy) titanate esters 0.8, epoxidized soybean oil 1, magnesium hydroxide 1.5, citric acid 0.8, diphenylamines 0.5, the poly-caproic acid.
Composition B: secondary stock 25, acetate fiber 15, gelatin 2, modification infusorial earth 0.5, ammonium polyacrylate 1, alumina silicate 0.6, two ten four carbon alcohols esters 0.5, nano-calcium carbonate 2, penta sodium pentachlorophenate 2, poly--4-methyl-1-pentene 0.8 and paregal O 0.5.
The air filter preparation method of filter paper may further comprise the steps:
(1) weight portion by constitutive material takes by weighing all raw materials among composition A and the composition B, to put into the pulper size degradation behind slag slurry, the styroflex mixing respectively, obtain the slurry that solid content is 4-6%, get mixed slurry A, to put into the pulper size degradation behind secondary stock, the acetate fiber mixing, obtain the slurry that solid content is 4-6%, get mixed slurry B;
(2) add respectively other raw materials of residue of the weight portion of pressing constitutive material in the mixed slurry A of step (1) and mixed slurry B, obtain respectively composition A and composition B, then blend compositions A and composition B are heated to 70-80 ℃; After fluffer is discongested, defibrination again, the gained slurry is sized mixing through adding water behind the defibrination, copies paper according to conventional paper technology to solid content 2-3%, the moulding squeezing, is drying to obtain.
Described Modified Water Soluble Phenolic Resin preparation method adds nano-sized carbon 0.2-0.3, water soluble phenol resin 3-4,1-2 carboxymethyl cellulose, 3-4 iron oxide in water soluble phenol resin, be mixed and heated to 70-80 ℃, cooling and get final product after 30-40 minute.
The preparation method of described powder of straw is with powder of straw under 100-150 ℃ of temperature scaling loss 1-2 hour, after grind to form nanometer powder, admix the aluminate coupling agent DL-411 agitating that is equivalent to powder weight 3-5% even, oven dry is ground into powder and obtains.
The preparation method of described modification infusorial earth leaves standstill for using first 15-20% salt acid soak diatomite 1-2 hour, clarification, centrifugal, solid washes with water to neutrality, after the oven dry, add the vinyltriethoxysilane agitating that is equivalent to solid weight 3-5% even, oven dry is ground into powder.
Beneficial effect of the present invention:
The present invention adopts slag slurry, styroflex, secondary stock and acetate fiber simultaneously as main material, the environmental protection science, composition of raw materials is reasonable, and each group partition inter-capacitive is good, and intensity, toughness, corrosion resistance improve, surface gloss is good, stable performance indications are arranged under normal temperature and worst hot case, have preferably heatproof and filter effect, its maximum diameter of hole 44-52 μ m, average pore size 31-37 μ m becomes the paper air permeability at 86-90L/m
2.S between.
The specific embodiment
Embodiment 1: air filter filter paper, and the weight portion of its constitutive material is:
Composition A: vinegar 16, sodium polymethacrylate 2, heavy alkylbenzene sulfonate 2, modified straw powder 2.5 in slag slurry 66, styroflex 14, bamboo charcoal 5, Modified Water Soluble Phenolic Resin 1, tetra isopropyl two (dioctyl phosphorous acid acyloxy) titanate esters 0.8, epoxidized soybean oil 1, magnesium hydroxide 1.5, citric acid 0.8, diphenylamines 0.5, the poly-caproic acid.
Composition B: secondary stock 25, acetate fiber 15, gelatin 2, modification infusorial earth 0.5, ammonium polyacrylate 1, alumina silicate 0.6, two ten four carbon alcohols esters 0.5, nano-calcium carbonate 2, penta sodium pentachlorophenate 2, poly--4-methyl-1-pentene 0.8 and paregal O 0.5.
The air filter preparation method of filter paper may further comprise the steps:
(1) weight portion by constitutive material takes by weighing all raw materials among composition A and the composition B, to put into the pulper size degradation behind slag slurry, the styroflex mixing respectively, obtain the slurry that solid content is 4-6%, get mixed slurry A, to put into the pulper size degradation behind secondary stock, the acetate fiber mixing, obtain the slurry that solid content is 4-6%, get mixed slurry B;
(2) add respectively other raw materials of residue of the weight portion of pressing constitutive material in the mixed slurry A of step (1) and mixed slurry B, obtain respectively composition A and composition B, then blend compositions A and composition B are heated to 70-80 ℃; After fluffer is discongested, defibrination again, the gained slurry is sized mixing through adding water behind the defibrination, copies paper according to conventional paper technology to solid content 2-3%, the moulding squeezing, is drying to obtain.
Described Modified Water Soluble Phenolic Resin preparation method adds nano-sized carbon 0.2-0.3, water soluble phenol resin 3-4,1-2 carboxymethyl cellulose, 3-4 iron oxide in water soluble phenol resin, be mixed and heated to 70-80 ℃, cooling and get final product after 30-40 minute.
The preparation method of described powder of straw is with powder of straw under 100-150 ℃ of temperature scaling loss 1-2 hour, after grind to form nanometer powder, admix the aluminate coupling agent DL-411 agitating that is equivalent to powder weight 3-5% even, oven dry is ground into powder and obtains.
The preparation method of described modification infusorial earth leaves standstill for using first 15-20% salt acid soak diatomite 1-2 hour, clarification, centrifugal, solid washes with water to neutrality, after the oven dry, add the vinyltriethoxysilane agitating that is equivalent to solid weight 3-5% even, oven dry is ground into powder.
As follows with the performance detection data of filter paper with the air filter that above-mentioned method makes:
Grammes per square metre: 117g/cm
2Bursting strength: 316Kpa; Air permeability: 490ml/10cm
2Min; Its maximum diameter of hole 44-52 μ m, average pore size 31-37 μ m becomes the paper air permeability at 86-90L/m
2.S between.
Claims (6)
1. air filter filter paper is characterized in that the weight portion of its constitutive material is:
Composition A: vinegar 14-18, sodium polymethacrylate 1.5-2.5, heavy alkylbenzene sulfonate 1.7-2.3, modified straw powder 1.5-3.5 in slag slurry 65-68, styroflex 13-16, bamboo charcoal 4-6, Modified Water Soluble Phenolic Resin 0.9-1.1, tetra isopropyl two (dioctyl phosphorous acid acyloxy) titanate esters 0.7-0.9, epoxidized soybean oil 0.8-1.2, magnesium hydroxide 1.4-1.6, citric acid 0.7-0.9, diphenylamines 0.4-0.6, the poly-caproic acid;
Composition B: secondary stock 23-28, acetate fiber 13-18, gelatin 1-3, modification infusorial earth 0.4-0.6, ammonium polyacrylate 0.8-1.2, alumina silicate 0.5-0.7, two ten four carbon alcohols ester 0.3-0.6, nano-calcium carbonate 1-3, penta sodium pentachlorophenate 1.5-2.5, poly--4-methyl-1-pentene 0.7-0.9 and paregal O 0.4-0.6.
2. air filter filter paper according to claim 1 is characterized in that the weight portion of its constitutive material is:
Composition A: vinegar 16, sodium polymethacrylate 2, heavy alkylbenzene sulfonate 2, modified straw powder 2.5 in slag slurry 66, styroflex 14, bamboo charcoal 5, Modified Water Soluble Phenolic Resin 1, tetra isopropyl two (dioctyl phosphorous acid acyloxy) titanate esters 0.8, epoxidized soybean oil 1, magnesium hydroxide 1.5, citric acid 0.8, diphenylamines 0.5, the poly-caproic acid;
Composition B: secondary stock 25, acetate fiber 15, gelatin 2, modification infusorial earth 0.5, ammonium polyacrylate 1, alumina silicate 0.6, two ten four carbon alcohols esters 0.5, nano-calcium carbonate 2, penta sodium pentachlorophenate 2, poly--4-methyl-1-pentene 0.8 and paregal O 0.5.
3. an air filter as claimed in claim 1 is characterized in that may further comprise the steps with the preparation method of filter paper:
(1) weight portion by constitutive material takes by weighing all raw materials among composition A and the composition B, to put into the pulper size degradation behind slag slurry, the styroflex mixing respectively, obtain the slurry that solid content is 4-6%, get mixed slurry A, to put into the pulper size degradation behind secondary stock, the acetate fiber mixing, obtain the slurry that solid content is 4-6%, get mixed slurry B;
(2) add respectively other raw materials of residue of the weight portion of pressing constitutive material in the mixed slurry A of step (1) and mixed slurry B, obtain respectively composition A and composition B, then blend compositions A and composition B are heated to 70-80 ℃; After fluffer is discongested, defibrination again, the gained slurry is sized mixing through adding water behind the defibrination, copies paper according to conventional paper technology to solid content 2-3%, the moulding squeezing, is drying to obtain.
4. air filter filter paper according to claim 1, it is characterized in that: described Modified Water Soluble Phenolic Resin preparation method is for adding nano-sized carbon 0.2-0.3, water soluble phenol resin 3-4,1-2 carboxymethyl cellulose, 3-4 iron oxide in water soluble phenol resin, be mixed and heated to 70-80 ℃, after 30-40 minute the cooling and get final product.
5. air filter filter paper according to claim 1, it is characterized in that: the preparation method of described powder of straw is for powder of straw under 100-150 ℃ of temperature scaling loss 1-2 hour, after grind to form nanometer powder, admix the aluminate coupling agent DL-411 agitating that is equivalent to powder weight 3-5% even, oven dry is ground into powder and obtains.
6. air filter filter paper according to claim 1, it is characterized in that: the preparation method of described modification infusorial earth is for using first 15-20% salt acid soak diatomite 1-2 hour, leave standstill, clarification, centrifugal, solid washes with water to neutrality, after the oven dry, add the vinyltriethoxysilane agitating that is equivalent to solid weight 3-5% even, oven dry is ground into powder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201210426831.6A CN102995497B (en) | 2012-10-31 | 2012-10-31 | Filter paper for air filter and preparation method of filter paper |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210426831.6A CN102995497B (en) | 2012-10-31 | 2012-10-31 | Filter paper for air filter and preparation method of filter paper |
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| CN102995497A true CN102995497A (en) | 2013-03-27 |
| CN102995497B CN102995497B (en) | 2015-07-22 |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103382678A (en) * | 2013-06-26 | 2013-11-06 | 蚌埠首创滤清器有限公司 | Anticorrosive filter paper and preparation method thereof |
| CN103446999A (en) * | 2013-06-20 | 2013-12-18 | 天长市天乐电器厂 | Carbon rod filter element and preparation method thereof |
| CN103966918A (en) * | 2014-04-09 | 2014-08-06 | 蚌埠市风驰滤清器有限公司 | Filter paper resistant to high temperature and corrosion and used for filter cleaner and preparation method of filter paper |
| CN103966916A (en) * | 2014-04-09 | 2014-08-06 | 蚌埠市风驰滤清器有限公司 | Energy-saving and environment-friendlyfilter paper for filter and preparation method of filter paper |
| CN103993520A (en) * | 2014-04-25 | 2014-08-20 | 蚌埠凤凰滤清器有限责任公司 | Composite fuel oil filter paper with high filtration efficiency and preparation method thereof |
| CN104420400A (en) * | 2013-08-30 | 2015-03-18 | 珠海市红旌发展有限公司 | Preparation method of air filtering paper containing nanocellulose |
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| US5866669A (en) * | 1996-01-09 | 1999-02-02 | Meisel Chemical Works, Ltd. | Sulfonated phenol-formaldehyde resin for paper-making |
| CN102352575A (en) * | 2011-07-02 | 2012-02-15 | 云南瑞升烟草技术（集团）有限公司 | Filter candle paper added with adsorbent filling material, paper-based filter candle and preparation method |
| CN102505571A (en) * | 2011-12-21 | 2012-06-20 | 中材科技股份有限公司 | No-baffle high-temperature-resistant air filter paper and preparation method thereof |
-
2012
- 2012-10-31 CN CN201210426831.6A patent/CN102995497B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| US5866669A (en) * | 1996-01-09 | 1999-02-02 | Meisel Chemical Works, Ltd. | Sulfonated phenol-formaldehyde resin for paper-making |
| CN102352575A (en) * | 2011-07-02 | 2012-02-15 | 云南瑞升烟草技术（集团）有限公司 | Filter candle paper added with adsorbent filling material, paper-based filter candle and preparation method |
| CN102505571A (en) * | 2011-12-21 | 2012-06-20 | 中材科技股份有限公司 | No-baffle high-temperature-resistant air filter paper and preparation method thereof |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103446999A (en) * | 2013-06-20 | 2013-12-18 | 天长市天乐电器厂 | Carbon rod filter element and preparation method thereof |
| CN103382678A (en) * | 2013-06-26 | 2013-11-06 | 蚌埠首创滤清器有限公司 | Anticorrosive filter paper and preparation method thereof |
| CN104420400A (en) * | 2013-08-30 | 2015-03-18 | 珠海市红旌发展有限公司 | Preparation method of air filtering paper containing nanocellulose |
| CN103966918A (en) * | 2014-04-09 | 2014-08-06 | 蚌埠市风驰滤清器有限公司 | Filter paper resistant to high temperature and corrosion and used for filter cleaner and preparation method of filter paper |
| CN103966916A (en) * | 2014-04-09 | 2014-08-06 | 蚌埠市风驰滤清器有限公司 | Energy-saving and environment-friendlyfilter paper for filter and preparation method of filter paper |
| CN103966918B (en) * | 2014-04-09 | 2016-01-20 | 蚌埠市风驰滤清器有限公司 | Filter paper of filter of a kind of corrosion-and high-temp-resistant and preparation method thereof |
| CN103966916B (en) * | 2014-04-09 | 2016-01-20 | 蚌埠市风驰滤清器有限公司 | A kind of energy saving and environment friendly cleaner filter paper and preparation method thereof |
| CN103993520A (en) * | 2014-04-25 | 2014-08-20 | 蚌埠凤凰滤清器有限责任公司 | Composite fuel oil filter paper with high filtration efficiency and preparation method thereof |
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| CN102995497B (en) | 2015-07-22 |
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