CN102311690A - Waterborne exterior elastic reflective heat insulation coating and production method thereof - Google Patents
Waterborne exterior elastic reflective heat insulation coating and production method thereof Download PDFInfo
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Abstract
The invention relates to a waterborne exterior elastic reflective heat insulation coating and a production method thereof. The waterborne exterior elastic reflective heat insulation coating is prepared by the following raw materials by mass: 30-60 parts of a pure acrylic elastic emulsion, 3-10 parts of a hollow ceramic bead, 10-25 parts of a pigment, 5-20 parts of filler, 15-30 parts of water, 0.2-1.0 part of a wetting dispersant, 0.3-0.8 part of an antifoaming agent, 0.1-1.0 part of a mildew-resistant bactericide, 0.2-0.5 part of hydroxyethyl cellulose, 0.3-1.0 part of a thickening agent, 1-3 parts of an antifreezing agent, 0.4-0.8 part of a film forming auxiliary agent, 0.2-0.6 part of a levelling agent, and an amount of a neutralizer for adjusting the pH value to 8-9. The invention also includes the production method of the waterborne exterior elastic reflective heat insulation coating. The waterborne exterior elastic reflective heat insulation coating provided in the invention has good stability, good workability and heat insulation effect, sound elasticity and waterproof effect as well as satisfying environmental protection property, thus especially being suitable for application in the building industry.
Description
Technical field
The present invention relates to a kind of external paint and working method thereof, especially relate to a kind of water-based external application elasticity reflective heat-insulation paint and working method thereof.
Background technology
Sunlight brings vigor and vitality to temporal, but in extremely hot season, also brings insufferable high temperature to people; This high temperature is due to the infrared radiation in the sunshine; Therefore the high temperature season that attacks of every heat wave, people have only and are opening air-conditioning all day, have both wasted electric power; Cause Greenhouse effect again easily, cause topsoil; A large amount of outdoor storage tank and facility in industrial production, the gentle cooling of all need going bail for is handled, and its operation cost and energy consumption all are sizable.Therefore, adopt lagging material to become one of effective means that reduces room temperature.Present thermal insulating coating successful Application becomes the main effective means of thermal insulation protection at aspects such as residential building, industrial pipeline, outdoor storage tank and facilities.
The present low barrier lagging material of porousness such as the heat insulation employing woven asbesto of part, glass wool, porous plastics, these materials can only slow down but can not stop the transmission of heat energy.Daytime, sun power was through space and structure in the continuous inlet chamber of roof, wall or wall of container or in the container, in case heat energy imports into, even if external temperature reduces, heat energy still is stranded and falls into wherein.
Thermal insulating coating the typical case use on building exterior wall face and outdoor large storage tank; Metope heat preservation technology commonly used both at home and abroad as: external hanging type is incubated styrofoam and moulding of body of wall one-time-concreting and polyphenyl particle heat-insulating mortar exterior-wall heat insulation outward; All be as the insulation means with " resistance heat "; Though effect is pretty good, bigger to building influences such as load-bearing own, outer decoration, construction cost also increases many.
The popular thermal insulating coating is different from the low barrier lagging material of porousness at present; Usually adopt the reflective insulation material; Can the heat radiation that absorb be fallen with the form of loses heat; Make and indoorly feel more nice and cool, the material of reflective insulation simultaneously can reduce the influence of thermal radiation to external wall or container outer wall, is the method that fundamentally solves body of wall or container insulator insulation.Yet present reflectivity lagging material poor stability, application property and effect of heat insulation are not enough, and do not have elasticity, can not adapt to the variation that body of wall or wall of container expand with heat and contract with cold, and are prone to cracking phenomena.
Summary of the invention
The technical problem that the present invention will solve is, overcomes the deficiency of prior art, and a kind of good stability is provided, application property and good heat-insulation effect, and elasticity and good water-proof effect, not easy to crack, water-based external application elasticity reflective heat-insulation paint and working method thereof that environmental pollution is few.
The present invention solve the technical problem the technical scheme that is adopted:
The present invention's water-based external application elasticity reflective heat-insulation paint, processed by the raw material of following mass fraction: elastic pure acrylic acid emulsion 30-60 part, hollow ceramic pearl 3-10 part, pigment 10-25 part, filler 5-20 part, water 15-30 part, wetting dispersing agent 0.2-1.0 part, skimmer 0.3-0.8 part, antimildew disinfectant 0.1-1.0 part, Natvosol 0.2-0.5 part, thickening material 0.3-1.0 part, frostproofer 1-3 part, film coalescence aid 0.4-0.8 part, flow agent 0.2-0.6 deal, neutralizing agent are regulated the amount of pH value for 8-9.
Said elastic pure acrylic acid emulsion is commercially available chemical self-cross linking type PEMULEN TR2 water dispersion; Its minimum film-forming temperature＜5 ℃, solid content is 45-55% (preferred 50%), median size is 0.1 ± 0.01 micron; Elongation is 500 ± 10%, and tensile strength is 10 ± 1N/ ㎜
2
Said hollow ceramic pearl preferred density is 0.12-0.50g/ ㎝
3, wall thickness is the 1-2 micron, particle diameter 15-100 micron;
Said pigment optimization Rutile type Titanium Dioxide;
The mixture of the preferred kaolin of said filler, sericite, wherein the mass ratio of kaolin and sericite is 1:1;
Said wetting dispersing agent is commercially available ammonium acrylate dipersant;
The preferred mildew-resistant stable form of said Natvosol;
The mixture of one or more in the preferred terepthaloyl moietie of said frostproofer, the Ucar 35;
The preferred termil of said antimildew disinfectant,, one or more the mixture in 2-n-octyl-4-isothiazoline-3-ketone;
The excellent commercial polyurethane association type of said flow agent compound;
The mixture of one or more in the preferred ethylene glycol monobutyl ether of said film coalescence aid, ester alcohol 12, dipropylene glycol butyl ether, terepthaloyl moietie, propylene-glycol ethyl ether, the Ucar 35 butyl ether;
The mixture of one or more in the preferred commercially available modified polyacrylic acid sodium of said thickening material, modified polypropene acid amide, the non-ionic polyurethane compound;
The mixture of one or more in the preferred dimethylethanolamine of said neutralizing agent, thanomin, ammoniacal liquor, the 2-amino-2-methyl-1-propanol (AMP-95);
Said skimmer is modified dimethyl polysiloxane solution or MO, or their mixture;
The working method of the present invention's water-based external application elasticity reflective heat-insulation paint may further comprise the steps:
(1) water is added mixer, under 600-800 rev/min stirring, add Natvosol, stirring to Natvosol is the transparent granular liquid that do not have;
(2) skimmer of adding wetting dispersing agent, antimildew disinfectant, 1/2 formula ratio after stirring, adds pigment, filler again, improves mixing speed to 1000-1600 rev/min, stirs;
(3) compound that step (2) is stirred is dispersed to fineness through grinding and reaches the 40-60 micron, and the limit is stirred the limit with 300-500 rev/min rotating speed and added film coalescence aid, frostproofer, elastic pure acrylic acid emulsion in the paint pot, stirs;
(4) the compound pH value that stirs with neutralizing agent regulating step (3) reaches 8-9, adds skimmer, the flow agent of thickening material, residue 1/2 formula ratio again, stirs;
(5) in step (4) gained compound, add the hollow ceramic pearl, stir, fully evenly sneak in the paint vehicle until the hollow ceramic pearl; Use 10-20 purpose screen filtration then.
The present invention's water-based external application elasticity reflective heat-insulation paint; Have following characteristics: 1) thermal insulation is good: heat is completely cut off in the outside; Thereby suppress buildings or the heating of tank body own, outdoor temperature is high more, and its heat insulation and heat control effect is obvious more; Compare with common coating, its actual indoor/outdoor temperature-difference can reach 10-15 ℃; 2) good endurance: can completely cut off the solar ray more than 85%, prevent the aging of buildings that ultraviolet ray causes or tank body; 3) water resistance is good: outside surface is smeared the coating of ceramic hollow packing material, can resist the erosion of ultraviolet ray, wind and rain, and waterproof effect and coiled material are suitable; 4) uphold excellent performance, elongation is higher than 300%, to the strong adhesion and the high resilience on surfaces such as most of material of construction, metal, reduces surface stress and retractility crackle; 5) feature of environmental protection: water-based, nontoxic, tasteless, pollution-free, meet the Green Product standard.
Embodiment
Below in conjunction with specific embodiment the present invention is done further explain.
Embodiment 1
The water-based external application elasticity reflective heat-insulation paint of present embodiment is processed by the raw material of following quality: elastic pure acrylic acid emulsion (solid content 50%) 45kg, hollow ceramic pearl (density 0.42g/ ㎝
3) 4 kg, Rutile type Titanium Dioxide 20 kg, kaolin 50 kg; Sericite 50 kg, water 20.6 kg, 1124 dispersion agents, 0.6 kg; X-405 wetting agent 0.2 kg, Defoamer334 skimmer 0.5kg, antimildew disinfectant Skane M-8 0.5kg; Natvosol 250HBR 0.4kg, thickening material SN-612 0.6kg, frostproofer Ucar 35 2kg; Film coalescence aid ester alcohol 12 Texanol0.5kg, DSX3220 flow agent 0.4 kg, neutralizing agent 2-amino-2-methyl-1-propanol (AMP-95) 1.0 kg.
The working method of the water-based external application elasticity reflective heat-insulation paint of present embodiment may further comprise the steps:
(1) water is added mixer, under 600 rev/mins stirring, add Natvosol, stirring to Natvosol is the transparent granular liquid that do not have;
(2) add the skimmer of wetting dispersing agent, antimildew disinfectant, 0.25kg, after stirring, add pigment, filler again, improve mixing speed to 1200 rev/min, stir;
(3) compound that step (2) is stirred is dispersed to fineness through grinding and reaches the 40-60 micron, and the limit is stirred the limit with 400 rev/mins rotating speed and added film coalescence aid, frostproofer, elastic pure acrylic acid emulsion in the paint pot, stirs;
(4) the compound pH value that stirs with neutralizing agent regulating step (3) reaches 8.5, adds skimmer, the flow agent of thickening material, residue 0.25kg again, stirs;
(5) in step (4) gained compound, add the hollow ceramic pearl, stir, fully evenly sneak in the paint vehicle until the hollow ceramic pearl; Use 20 purpose screen filtrations then, the viscosity that promptly gets coating products is 116-120KU.
The technical indicator of the salient features of the water-based external application elasticity reflective heat-insulation paint of present embodiment and the building trade standard JG/T235-2008 of the People's Republic of China " architectural reflective heat-insulation paint " and the building trade standard JG/T172-2005 of the People's Republic of China " elasticity Building Heat coating " is relatively seen table 1.
Can know by table 1; The present invention's water-based external application elasticity reflective heat-insulation paint; Can reach the technical indicator of architectural reflective heat-insulation paint; Can reach the technical indicator of elasticity Building Heat coating again,, be particularly suitable for being applied in building trade so it possesses the performance of reflective heat-insulation paint and elasticity Building Heat coating simultaneously.
Claims (3)
1. water-based external application elasticity reflective heat-insulation paint; It is characterized in that, processed by the raw material of following mass fraction: elastic pure acrylic acid emulsion 30-60 part, hollow ceramic pearl 3-10 part, pigment 10-25 part, filler 5-20 part, water 15-30 part, wetting dispersing agent 0.2-1.0 part, skimmer 0.3-0.8 part, antimildew disinfectant 0.1-1.0 part, Natvosol 0.2-0.5 part, thickening material 0.3-1.0 part, frostproofer 1-3 part, film coalescence aid 0.4-0.8 part, flow agent 0.2-0.6 part, neutralizing agent are regulated the amount of pH value for 8-9.
2. water-based external application elasticity reflective heat-insulation paint according to claim 1; It is characterized in that said elastic pure acrylic acid emulsion is chemical self-cross linking type PEMULEN TR2 water dispersion, its minimum film-forming temperature＜5 ℃; Solid content is 45-55%; Median size is 0.1 ± 0.01 micron, and elongation is 500 ± 10%, and tensile strength is 10 ± 1N/ ㎜
2
The density of said hollow ceramic pearl is 0.12-0.50g/cm
3, wall thickness is the 1-2 micron, particle diameter 15-100 micron;
Said pigment is Rutile type Titanium Dioxide;
Said filler is the mixture of kaolin and sericite, and wherein the mass ratio of kaolin and sericite is 1:1;
Said wetting dispersing agent is commercially available ammonium acrylate dipersant;
Said Natvosol is the mildew-resistant stable form;
Said frostproofer is terepthaloyl moietie or Ucar 35, or the mixture of terepthaloyl moietie and Ucar 35;
Said antimildew disinfectant is one or more the mixture in termil, the 2-n-octyl-4-isothiazoline-3-ketone;
Said flow agent is commercially available urethane association type compound;
Said film coalescence aid is one or more the mixture that is selected from ethylene glycol monobutyl ether, ester alcohol 12, dipropylene glycol butyl ether, terepthaloyl moietie, propylene-glycol ethyl ether, the Ucar 35 butyl ether;
Said thickening material is one or more the mixture in commercially available modified polyacrylic acid sodium, modified polypropene acid amide, the non-ionic polyurethane compound;
Said skimmer is a kind of in modified dimethyl polysiloxane solution, the MO or their mixture;
Said neutralizing agent is for being selected from one or more the mixture in dimethylethanolamine, thanomin, ammoniacal liquor, the 2-amino-2-methyl-1-propanol (AMP-95).
3. the working method of water-based external application elasticity reflective heat-insulation paint according to claim 1 and 2 is characterized in that, may further comprise the steps:
(1) water is added mixer, under 600-800 rev/min stirring, add Natvosol, stirring to Natvosol is the transparent liquid that does not have the particulate state solid substance;
(2) skimmer of adding wetting dispersing agent, antimildew disinfectant, 1/2 formula ratio after stirring, adds pigment, filler again, improves mixing speed to 1000-1600 rev/min, stirs;
(3) compound that step (2) is stirred reaches the 40-60 micron through the solid substance fineness that grinding is dispersed to wherein; In the paint pot, stir on one side on one side and add film coalescence aid, frostproofer, elastic pure acrylic acid emulsion, stir with 300-500 rev/min rotating speed;
(4) the compound pH value that stirs with neutralizing agent regulating step (3) reaches 8-9, adds skimmer, the flow agent of thickening material, residue 1/2 formula ratio again, stirs;
(5) in step (4) gained compound, add the hollow ceramic pearl, stir, fully evenly sneak in the paint vehicle until the hollow ceramic pearl; Use 10-20 purpose screen filtration then.
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| CN 201110218715 CN102311690B (en) | 2011-08-02 | 2011-08-02 | Waterborne exterior elastic reflective heat insulation coating and production method thereof |
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| CN 201110218715 CN102311690B (en) | 2011-08-02 | 2011-08-02 | Waterborne exterior elastic reflective heat insulation coating and production method thereof |
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| CN102311690B CN102311690B (en) | 2013-06-12 |
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| CN102745948A (en) * | 2012-07-20 | 2012-10-24 | 无锡立德涂料有限公司 | Novel environment-friendly radiation-free pottery sand wall decoration material and preparation method thereof |
| CN103173075A (en) * | 2013-02-26 | 2013-06-26 | 安徽真信涂料有限公司 | Aqueous paint and preparation method thereof |
| CN103788787A (en) * | 2013-10-21 | 2014-05-14 | 广州擎天材料科技有限公司 | Single-component water-based natural drying finishing coat for construction crane and preparation method thereof |
| CN104446127A (en) * | 2014-11-27 | 2015-03-25 | 韦棋 | Heat-insulating coating for outer walls |
| CN105153855A (en) * | 2015-09-17 | 2015-12-16 | 河北晨阳工贸集团有限公司 | Moistureproof mildewproof water-based paint and preparation method thereof |
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| CN102745948A (en) * | 2012-07-20 | 2012-10-24 | 无锡立德涂料有限公司 | Novel environment-friendly radiation-free pottery sand wall decoration material and preparation method thereof |
| CN102745948B (en) * | 2012-07-20 | 2013-12-18 | 无锡立德涂料有限公司 | Environment-friendly radiation-free pottery sand wall decoration material and preparation method thereof |
| CN103173075A (en) * | 2013-02-26 | 2013-06-26 | 安徽真信涂料有限公司 | Aqueous paint and preparation method thereof |
| CN103788787A (en) * | 2013-10-21 | 2014-05-14 | 广州擎天材料科技有限公司 | Single-component water-based natural drying finishing coat for construction crane and preparation method thereof |
| CN104446127A (en) * | 2014-11-27 | 2015-03-25 | 韦棋 | Heat-insulating coating for outer walls |
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| CN106147441B (en) * | 2015-04-27 | 2019-07-05 | 广东华润涂料有限公司 | Resistance to soiling water-based paint compositions |
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| CN105238122A (en) * | 2015-10-29 | 2016-01-13 | 江门市蓬江区慧邦涂料有限公司 | Heat reflective heat-insulating seaweed mud paint for external wall |
| CN105271927A (en) * | 2015-11-05 | 2016-01-27 | 苏州明轩地坪涂料有限公司 | Stain-resistant elastic coating |
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| CN107419846B (en) * | 2017-08-28 | 2023-01-03 | 河南永威安防股份有限公司 | Galvanized steel sheet assembled heat insulation wall material |
| CN108587254A (en) * | 2018-04-10 | 2018-09-28 | 米格（浙江）创新科技有限公司 | Infrared reflecting paint and application thereof |
| CN110284338A (en) * | 2019-05-23 | 2019-09-27 | 吴江市鑫淼喷织有限公司 | A kind of heat-barrier material and preparation method thereof and coating processes |
| CN111073417A (en) * | 2019-12-17 | 2020-04-28 | 中华制漆（深圳）有限公司 | Reflective heat-insulating coating and preparation method thereof |
| CN111073417B (en) * | 2019-12-17 | 2022-01-07 | 中华制漆（深圳）有限公司 | Reflective heat-insulating coating and preparation method thereof |
| CN113930103A (en) * | 2021-10-12 | 2022-01-14 | 湘江涂料科技有限公司 | Water-based sand-containing heat-insulating coating for steel-structured portable house and preparation method thereof |
| CN114716866A (en) * | 2022-05-05 | 2022-07-08 | 天津渤海望亚涂料有限公司 | Preparation method of waterproof coating |
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