CN102305767A - Microcontroller-based terahertz time-domain spectroscopy automatic sample testing device - Google Patents

Microcontroller-based terahertz time-domain spectroscopy automatic sample testing device Download PDF

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CN102305767A
CN102305767A CN201110127570A CN201110127570A CN102305767A CN 102305767 A CN102305767 A CN 102305767A CN 201110127570 A CN201110127570 A CN 201110127570A CN 201110127570 A CN201110127570 A CN 201110127570A CN 102305767 A CN102305767 A CN 102305767A
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port
chip
links
resistance
ground connection
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CN102305767B (en
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王强
肖琨
王孝伟
王花丽
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China Jiliang University
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China Jiliang University
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Abstract

The invention discloses a microcontroller-based terahertz time-domain spectroscopy automatic sample testing device. The device comprises a terahertz sample testing device and a control system, wherein the terahertz sample testing device comprises a sample disk, a sample pool, a positioning hole, a stepping motor, a photoelectronic device, a testing platform, a terahertz testing hole, a leveling nut, a level instrument, a pressure spring fixation device, a pressure spring, a metal dome, a sample pool inner hole and a sample pool outer hole; and the control system comprises a microcontroller, a power supply circuit, a keypress circuit, a voice circuit, an alarm circuit, a liquid crystal display circuit, a light-emitting diode (LED) indicator circuit, a stepping motor driving circuit and a photoelectric positioning circuit. The reliability and a human engineering principle are fully considered, the experimental error is furthest reduced, the misoperation probability is reduced, and the experimental efficiency is improved.

Description

Terahertz time-domain spectroscopy sample automatic testing equipment based on microcontroller
Technical field
The present invention relates to a kind of sample automatic testing equipment that utilizes the terahertz time-domain spectroscopy measuring system of microprocessor controls.
Background technology
Terahertz time-domain spectroscopic technology is a kind of new technology that adopts femto-second laser to excite THz wave that gallium arsenide gives off that material etc. is surveyed.In the terahertz time-domain spectroscopy system, the acquisition of the terahertz time-domain waveform of sample is that the pump light that utilizes deferred mount to pass the different terahertz pulse electric field intensity constantly of sample through change is measured with the optical path difference of surveying light.Main source of error in experimentation has pump light, sample refraction and reflection and human factor.Pump light is subjected to the influence of fluctuations meeting of environment temperature and humidity to produce bigger amplitude and phase change; The refraction of sample and reflection are very responsive to the collimation of sample face and THz wave; It is directly related with measuring accuracy to vary the time length of article and the quality of placement sample etc.; These factors to difference constantly the repeatability of measurement data and the Terahertz wave intensity etc. that sees through sample considerable influence is arranged, produce bigger measuring error thus.
In the existing terahertz time-domain spectroscopy measurement mechanism, the most frequently used is a sample to be put into sample cell to measure at every turn.At every turn pack into about 1min of time of sample of this measuring method; Efficient is lower; The samples vertical precision of sample cell of packing into also is difficult to be guaranteed; And tend to cause that factors such as ambient humidity and temperature change in the case when packing sample into; This variation all has influence in various degree to the result of sample test; This influence can cause measurement result to exist certain distortion, even seriously influences test result.For the measurement that the minute differences sample is arranged; In order to make its effective information be unlikely to be seriously influenced; In test process, just must guarantee sample constant basically with respect to environment in the vertical precision of Terahertz light and the case, therefore traditional method of at every turn only measuring a sample is can not be adopted.
In order to address the above problem; Improve the terahertz time-domain spectroscopy efficiency of measurement; Improve the vertical precision of sample with respect to Terahertz light, the basically identical of environment in the guard box, the present invention proposes a kind of terahertz time-domain spectroscopy sample automatic testing equipment based on microcontroller.This device can be before putting into sample the water article precision of manual adjusting sample stage, thereby improve the vertical precision of sample with respect to Terahertz light.This device provides more than one sample cell, thereby can disposablely put into more than one sample, thereby has guaranteed the continuity of sample test, has reduced the change of environment in the case that brings when packing sample repeatedly into.The operation of this device after putting into sample reduced to load the shared time of sample repeatedly, thereby improved the efficient of sample test almost all by microprocessor controls.In addition; This terahertz time-domain spectroscopy sample automatic testing equipment based on microcontroller also provides initial position self-adjusting zeroing function; The liquid crystal display circuit that this device adopts can be real-time current system running status and when the sample cell numbering of Pretesting; Mistake such as reduced the omission that the artificial memory brings, obscure, the raising of maximum possible measuring reliability.
Though the similar sample rack device is also arranged at present; But present device difficult guarantees the vertical precision of sample with respect to Terahertz light; And after putting into sample, can not regulate the initial position of specimen holder automatically; There is not corresponding display device; Need the artificial current sample cell numbering of going to remember; Also do not have control circuits such as corresponding button input, it is very inconvenient to operate, and measuring accuracy is difficult to guarantee.Along with the increase of experiment number and put into the sample number and increase, use existing apparatus to be easy to cause the omission of sample test step and obscure, be difficult to guarantee the reliability of sample test.
Summary of the invention
The objective of the invention is to overcome the deficiency of prior art, a kind of terahertz time-domain spectroscopy sample automatic testing equipment based on microcontroller is provided.
Terahertz time-domain spectroscopy sample automatic testing equipment based on microcontroller comprises Terahertz Sample testing device and control system; The Terahertz Sample testing device comprises sample disc; Sample cell; Pilot hole; Stepper motor; Electrooptical device; Test platform; The Terahertz instrument connection; The leveling nut; Level meter; The holddown spring stationary installation; Holddown spring; Metal clips; The outer hole of sample cell endoporus and sample cell; The leveling nut is installed in four jiaos of test platform bottom; Level meter is installed in the upper surface of test platform; Electrooptical device and stepper motor are fixed on the groove of the upper surface of test platform; The Terahertz instrument connection runs through the front and rear surfaces of test platform; Sample disc is fixed on the output shaft of stepper motor; More than one sample cell; The holddown spring stationary installation; Holddown spring; Metal clips be evenly distributed in sample disc around; Holddown spring one end is fixed on the sample disc through the holddown spring stationary installation; Metal clips is connected the other end of holddown spring; Pilot hole is distributed in the outer rim of sample disc, and near sample cell; Control system comprises microcontroller, power circuit, key circuit, sound circuit, warning circuit, liquid crystal display circuit, LED indicating circuit, stepper motor driving circuit, photoelectricity positioning circuit, and microcontroller links to each other with power circuit, key circuit, sound circuit, warning circuit, liquid crystal display circuit, LED indicating circuit, stepper motor driving circuit, photoelectricity positioning circuit respectively.
Described power circuit is: the port one of power interface J1 is connected with the port 2 of keyswitch S1; Power interface J1 port 2 links to each other with the port 5 of keyswitch S1; Port 6 ground connection of keyswitch S1; The port 2 of keyswitch S1 links to each other with the anode of diode D1; The positive pole of the negative electrode of diode D1 and capacitor C 1; One end of capacitor C 2 and the port one of chip U6 link to each other; The minus earth of capacitor C 1; The other end ground connection of capacitor C 2; The port 3 of chip U6 and port 5 ground connection of chip U6; The port 2 of chip U6 links to each other with an end of the negative electrode of diode D4 and inductance L 1; The port 4 of chip U6 and the other end of inductance L 1; The positive pole of capacitor C 3; One end of capacitor C 10 and the port one of chip U5 link to each other; The anode of diode D4; The other end ground connection of the negative pole of capacitor C 3 and capacitor C 10; The port 3 of chip U5 links to each other with an end of resistance R 1; The other end of resistance R 1 links to each other with the anode of light emitting diode D3; The plus earth of light emitting diode D3; Port 2 ground connection of chip U5; The port 5 of chip U5 is not connected with any device with the port 6 of chip U5; Chip U5 port 4 links to each other with the grid of N-channel MOS pipe Q1; The source electrode of N-channel MOS pipe Q1 is connected with the port one of power supply with chip U5; The drain electrode of N-channel MOS pipe Q1 links to each other with the negative electrode of the port one of power supply chip U5 and diode D2; The anode of diode D2 links to each other with power supply; The anode of diode D14 links to each other with an end of resistance R 11; The plus earth of diode D14; The other end of resistance R 11; One end of capacitor C 4 and an end of capacitor C 11 link to each other with power supply, the other end ground connection of the other end of capacitor C 4 and capacitor C 11.
Described LED indicating circuit is: port 5 ground connection of the port 4 of chip U7 and chip U7; The port 6 of chip U7 links to each other with an end of an end of resistance R 12 and capacitor C 12; The other end of resistance R 12 is connected with power supply; The other end ground connection of capacitor C 12; Port 9 ground connection of chip U7; The port one 0 of chip U7 links to each other with an end of resistance R 5; The other end of resistance R 5 links to each other with the negative electrode of light emitting diode D8; The anode of diode D8 links to each other with power supply; The port one 1 of chip U7 links to each other with an end of resistance R 6; The other end of resistance R 6 links to each other with the negative electrode of light emitting diode D9; The anode of diode D9 links to each other with power supply; The port one 2 of chip U7 links to each other with an end of resistance R 7; The other end of resistance R 7 links to each other with the negative electrode of light emitting diode D10; The anode of diode D10 links to each other with power supply; The port one 3 of chip U7 links to each other with an end of resistance R 8; The other end of resistance R 8 links to each other with the negative electrode of light emitting diode D11; The anode of diode D11 links to each other with power supply; The port one 4 of chip U7 links to each other with an end of resistance R 9; The other end of resistance R 9 links to each other with the negative electrode of light emitting diode D12; The anode of diode D12 links to each other with power supply; The port one 5 of chip U7 links to each other with an end of resistance R 10; The other end of resistance R 10 links to each other with the negative electrode of light emitting diode D13; The anode of diode D13 links to each other with power supply; The port one 6 of chip U7, the port 7 of chip U7 are not connected with any device, and the port one 8 of chip U7 is connected with power supply.
Described key circuit is: port 5 ground connection of the port 4 of chip U9 and chip U9; The port 6 of chip U9 links to each other with an end of an end of resistance R 27 and capacitor C 19; The other end of resistance R 27 is connected with power supply; The other end ground connection of capacitor C 19; Port 9 ground connection of chip U9; The port one 0 of chip U9 links to each other with the end of an end of resistance R 35 and button K10; The other end of resistance R 35 links to each other with power supply; The other end ground connection of button K10; The port one 1 of chip U9 links to each other with the end of an end of resistance R 34 and button K9; The other end of resistance R 34 links to each other with power supply; The other end ground connection of button K9; The port one 2 of chip U9 links to each other with the end of an end of resistance R 33 and button K8; The other end of resistance R 33 links to each other with power supply; The other end ground connection of button K8; The port one 3 of chip U9 links to each other with the end of an end of resistance R 32 and button K7; The other end of resistance R 32 links to each other with power supply; The other end ground connection of button K7; The port one 4 of chip U9 links to each other with the end of an end of resistance R 31 and button K6; The other end of resistance R 31 links to each other with power supply; The other end ground connection of button K6; The port one 5 of chip U9 links to each other with the end of an end of resistance R 30 and button K5; The other end of resistance R 30 links to each other with power supply; The other end ground connection of button K5; The port one 6 of chip U9 links to each other with the end of an end of resistance R 29 and button K4; The other end of resistance R 29 links to each other with power supply; The other end ground connection of button K4; The port one 7 of chip U9 links to each other with the end of an end of resistance R 28 and button K3; The other end of resistance R 28 links to each other with power supply; The other end ground connection of button K3, the port one 8 of chip U9 links to each other with power supply.
Described sound circuit is: port 4 ground connection of chip U4; The port 5 of chip U4 links to each other with the end of microphone LS2; The port 6 of chip U4 links to each other with the other end of microphone LS2; The port 7 of chip U4 links to each other with power supply; The port 8 of chip U4 links to each other with the end of loudspeaker MK1; The port 9 of chip U4 links to each other with the other end of loudspeaker MK1; The port one 0 of chip U4 links to each other with an end of resistance R 4; The other end of resistance R 4 links to each other with the end of interface J4; The other end ground connection of interface J4; The port 20 of chip U4 links to each other with the end of button K2; The other end ground connection of button K2, the positive pole of polar capacitor C8 links to each other with power supply, the minus earth of polar capacitor C8; One end of capacitor C 9 links to each other with power supply, the other end ground connection of capacitor C 9.
Described warning circuit is: an end of resistance R 24 links to each other with power supply; The other end of resistance R 24 links to each other with the emitter of positive-negative-positive triode Q9; The collector of positive-negative-positive triode Q9 links to each other with the positive pole of hummer LS1; The minus earth of hummer LS1; The base stage of positive-negative-positive triode Q9 links to each other with an end of resistance R 16, and the other end of resistance R 16 links to each other with microcontroller.
Described photoelectricity positioning circuit is: the port one of port J3 links to each other with an end of 12V power supply and resistance R 3; The port 2 of port J3 links to each other with the other end of the port 2 of optocoupler U3 and resistance R 3; Port 3 ground connection of port J3; The port one of optocoupler U3 links to each other with the 12V power supply; The port 4 of optocoupler U3 links to each other with an end of resistance R 2, another termination power of resistance R 2.
Described liquid crystal display circuit is: the port one ground connection of chip U10; The port 2 of chip U10 links to each other with power supply; The port 3 of chip U10; The port 7 of chip U10; The port 8 of chip U10; The port 9 of chip U10; The port one 0 of chip U10; The port one 1 of chip U10; The port one 2 of chip U10; The port one 3 of chip U10; The port one 4 of chip U10; The port one 6 of chip U10 does not link to each other with any device with the port one 8 of chip U10; The port one 5 of chip U10 links to each other with an end of resistance R 23; The other end ground connection of resistance R 23; The port one 7 of chip U10 links to each other with an end of an end of resistance R 25 and capacitor C 26; The other end of resistance R 25 links to each other with power supply; The other end ground connection of capacitor C 26; The port one 9 of chip U10 links to each other with power supply, port 20 ground connection of chip U10.
Described stepper motor driving circuit is: the port one of chip U8 links to each other with the port 4 of interface J5; The port 2 of chip U8 links to each other with the port 2 of interface J5; The port 3 of chip U8 and an end of resistance R 19; One end of resistance R 20 links to each other; The other end ground connection of resistance R 19; The port 4 of chip U8 links to each other with an end of the other end of resistance R 20 and capacitor C 16; The other end ground connection of capacitor C 16; The port 5 of chip U8 links to each other with the port one of interface J5; Port 6 ground connection of chip U8; Port 7 ground connection of chip U8; The port one 1 of chip U8 links to each other with the port 2 of interface J6; The port one ground connection of interface J6; The port one 2 of chip U8 and an end of resistance R 14; One end of capacitor C 13 links to each other; The other end ground connection of resistance R 14; The other end ground connection of capacitor C 13; Port one 3 ground connection of chip U8; The port one 4 of chip U8 and an end of resistance R 15; One end of capacitor C 14 links to each other; The other end ground connection of resistance R 15; The other end ground connection of capacitor C 14; The port one 5 of chip U8 links to each other with the port one 1 of chip U8; Port one 8 ground connection of chip U8; Port one 9 ground connection of chip U8; The port 21 of chip U8 links to each other with the port 3 of interface J5; The port 22 of chip U8 and an end of resistance R 17; One end of capacitor C 15 links to each other; The other end ground connection of capacitor C 15; The port 23 of chip U8 links to each other with an end of the other end of resistance R 17 and resistance R 18; The other end ground connection of resistance R 18; The port 24 of chip U8 and an end of capacitor C 17; The positive pole of polar capacitor C18 and power supply link to each other; The other end ground connection of capacitor C 17, the minus earth of polar capacitor C18.
The present invention can improve the terahertz time-domain spectroscopy efficiency of measurement, improves the vertical precision of sample with respect to Terahertz light, the basically identical of environment in the guard box, and the present invention proposes a kind of terahertz time-domain spectroscopy sample automatic testing equipment based on microcontroller.This device can be before putting into sample the water article precision of manual adjusting sample stage, thereby improve the vertical precision of sample with respect to Terahertz light.This device provides more than one sample cell, thereby can disposablely put into more than one sample, thereby has guaranteed the continuity of sample test, has reduced the change of environment in the case that brings when packing sample repeatedly into.The operation of this device after putting into sample reduced to load the shared time of sample repeatedly, thereby improved the efficient of sample test almost all by microprocessor controls.In addition; This terahertz time-domain spectroscopy sample automatic testing equipment based on microcontroller also provides initial position self-adjusting zeroing function; The liquid crystal display circuit that this device adopts can be real-time current system running status and when the sample cell numbering of Pretesting; Mistake such as reduced the omission that the artificial memory brings, obscure, the raising of maximum possible measuring reliability.
Description of drawings
Fig. 1 is the terahertz time-domain spectroscopy sample automatic testing equipment structural representation based on microcontroller;
Fig. 2 is a Terahertz Sample testing device vertical view of the present invention;
Fig. 3 is a sample pool structure enlarged drawing of the present invention;
Fig. 4 is a control system block scheme of the present invention;
Fig. 5 is the power circuit diagram of control system of the present invention;
Fig. 6 is the sound circuit figure of control system of the present invention;
Fig. 7 is the LED indicating circuit figure of control system of the present invention;
Fig. 8 is the key circuit figure of control system of the present invention;
Fig. 9 is the stepping motor control circuit figure of control system of the present invention;
Figure 10 is the liquid crystal display circuit figure of control system of the present invention;
Figure 11 is the warning circuit figure of control system of the present invention;
Figure 12 is the photoelectricity positioning circuit figure of control system of the present invention;
Figure 13 is the inner index path of the THz-TDS device that uses among the embodiment of being of the present invention;
Among the figure, 1, sample disc, 2, sample cell; 3, pilot hole, 4, stepper motor, 5, electrooptical device; 6, test platform, 7, the Terahertz instrument connection, 8, the leveling nut; 9, level meter; 10, holddown spring stationary installation, 11, holddown spring, 12, metal clips; 13, sample cell endoporus, 14, the outer hole of sample cell.
Embodiment
Provide embodiments of the invention below in conjunction with accompanying drawing, describe technical scheme of the present invention in detail.
Shown in Fig. 1~4; Terahertz time-domain spectroscopy sample automatic testing equipment based on microcontroller comprises Terahertz Sample testing device and control system; The Terahertz Sample testing device comprises sample disc 1; Sample cell 2; Pilot hole 3; Stepper motor 4; Electrooptical device 5; Test platform 6; Terahertz instrument connection 7; Leveling nut 8; Level meter 9; Holddown spring stationary installation 10; Holddown spring 11; Metal clips 12; Sample cell endoporus 13 and the outer hole 14 of sample cell; Leveling nut 8 is installed in four jiaos of test platform 6 bottoms; Level meter 9 is installed in the upper surface of test platform 6; Electrooptical device 5 and stepper motor 4 are fixed on the groove of the upper surface of test platform 6; Terahertz instrument connection 7 runs through the front and rear surfaces of test platform 6; Sample disc 1 is fixed on the output shaft of stepper motor; More than one sample cell 2; Holddown spring stationary installation 10; Holddown spring 11; Metal clips 12 be evenly distributed in sample disc 1 around; Holddown spring 11 1 ends are fixed on the sample disc 1 through holddown spring stationary installation 10; Metal clips 12 is connected the other end of holddown spring 11; Pilot hole 3 is distributed in the outer rim of sample disc 1, and near sample cell 2; Control system comprises microcontroller, power circuit, key circuit, sound circuit, warning circuit, liquid crystal display circuit, LED indicating circuit, stepper motor driving circuit, photoelectricity positioning circuit; Microcontroller links to each other with power circuit, key circuit, sound circuit, warning circuit, liquid crystal display circuit, LED indicating circuit, stepper motor driving circuit, photoelectricity positioning circuit respectively, and the model of microcontroller is dsPIC32MX795F512L.
As shown in Figure 5; Power circuit is: the port one of power interface J1 is connected with the port 2 of keyswitch S1; Power interface J1 port 2 links to each other with the port 5 of keyswitch S1; Port 6 ground connection of keyswitch S1; The port 2 of keyswitch S1 links to each other with the anode of diode D1; The positive pole of the negative electrode of diode D1 and capacitor C 1; One end of capacitor C 2 and the port one of chip U6 link to each other; The minus earth of capacitor C 1; The other end ground connection of capacitor C 2; The port 3 of chip U6 and port 5 ground connection of chip U6; The port 2 of chip U6 links to each other with an end of the negative electrode of diode D4 and inductance L 1; The port 4 of chip U6 and the other end of inductance L 1; The positive pole of capacitor C 3; One end of capacitor C 10 and the port one of chip U5 link to each other; The anode of diode D4; The other end ground connection of the negative pole of capacitor C 3 and capacitor C 10; The port 3 of chip U5 links to each other with an end of resistance R 1; The other end of resistance R 1 links to each other with the anode of light emitting diode D3; The plus earth of light emitting diode D3; Port 2 ground connection of chip U5; The port 5 of chip U5 is not connected with any device with the port 6 of chip U5; Chip U5 port 4 links to each other with the grid of N-channel MOS pipe Q1; The source electrode of N-channel MOS pipe Q1 is connected with the port one of power supply with chip U5; The drain electrode of N-channel MOS pipe Q1 links to each other with the negative electrode of the port one of power supply chip U5 and diode D2; The anode of diode D2 links to each other with power supply; The anode of diode D14 links to each other with an end of resistance R 11; The plus earth of diode D14; The other end of resistance R 11; One end of capacitor C 4 and an end of capacitor C 11 link to each other with power supply; The other end ground connection of the other end of capacitor C 4 and capacitor C 11; The model of chip U5 is MAX484, and the model of chip U6 is LM2576.
As shown in Figure 6; Sound circuit is: port 4 ground connection of chip U4; The port 5 of chip U4 links to each other with the end of microphone LS2; The port 6 of chip U4 links to each other with the other end of microphone LS2; The port 7 of chip U4 links to each other with power supply; The port 8 of chip U4 links to each other with the end of loudspeaker MK1; The port 9 of chip U4 links to each other with the other end of loudspeaker MK1; The port one 0 of chip U4 links to each other with an end of resistance R 4; The other end of resistance R 4 links to each other with the end of interface J4, the other end ground connection of interface J4, and the port 20 of chip U4 links to each other with the end of button K2; The other end ground connection of button K2; The positive pole of polar capacitor C8 links to each other with power supply, the minus earth of polar capacitor C8, and an end of capacitor C 9 links to each other with power supply; The other end ground connection of capacitor C 9, the model of chip U4 are ZY1730.
As shown in Figure 7; The LED indicating circuit is: port 5 ground connection of the port 4 of chip U7 and chip U7; The port 6 of chip U7 links to each other with an end of an end of resistance R 12 and capacitor C 12; The other end of resistance R 12 is connected with power supply; The other end ground connection of capacitor C 12; Port 9 ground connection of chip U7; The port one 0 of chip U7 links to each other with an end of resistance R 5; The other end of resistance R 5 links to each other with the negative electrode of light emitting diode D8; The anode of diode D8 links to each other with power supply; The port one 1 of chip U7 links to each other with an end of resistance R 6; The other end of resistance R 6 links to each other with the negative electrode of light emitting diode D9; The anode of diode D9 links to each other with power supply; The port one 2 of chip U7 links to each other with an end of resistance R 7; The other end of resistance R 7 links to each other with the negative electrode of light emitting diode D10; The anode of diode D10 links to each other with power supply; The port one 3 of chip U7 links to each other with an end of resistance R 8; The other end of resistance R 8 links to each other with the negative electrode of light emitting diode D11; The anode of diode D11 links to each other with power supply; The port one 4 of chip U7 links to each other with an end of resistance R 9; The other end of resistance R 9 links to each other with the negative electrode of light emitting diode D12; The anode of diode D12 links to each other with power supply; The port one 5 of chip U7 links to each other with an end of resistance R 10; The other end of resistance R 10 links to each other with the negative electrode of light emitting diode D13; The anode of diode D13 links to each other with power supply; The port one 6 of chip U7, the port 7 of chip U7 are not connected with any device; The port one 8 of chip U7 is connected with power supply; This circuit can show the running status of current system; The state that shows comprises start, returns to zero, tests, changes and stops, and the model of chip U7 is MCP23S08.
As shown in Figure 8; Key circuit is: port 5 ground connection of the port 4 of chip U9 and chip U9; The port 6 of chip U9 links to each other with an end of an end of resistance R 27 and capacitor C 19; The other end of resistance R 27 is connected with power supply; The other end ground connection of capacitor C 19; Port 9 ground connection of chip U9; The port one 0 of chip U9 links to each other with the end of an end of resistance R 35 and button K10; The other end of resistance R 35 links to each other with power supply; The other end ground connection of button K10; The port one 1 of chip U9 links to each other with the end of an end of resistance R 34 and button K9; The other end of resistance R 34 links to each other with power supply; The other end ground connection of button K9; The port one 2 of chip U9 links to each other with the end of an end of resistance R 33 and button K8; The other end of resistance R 33 links to each other with power supply; The other end ground connection of button K8; The port one 3 of chip U9 links to each other with the end of an end of resistance R 32 and button K7; The other end of resistance R 32 links to each other with power supply; The other end ground connection of button K7; The port one 4 of chip U9 links to each other with the end of an end of resistance R 31 and button K6; The other end of resistance R 31 links to each other with power supply; The other end ground connection of button K6; The port one 5 of chip U9 links to each other with the end of an end of resistance R 30 and button K5; The other end of resistance R 30 links to each other with power supply; The other end ground connection of button K5; The port one 6 of chip U9 links to each other with the end of an end of resistance R 29 and button K4; The other end of resistance R 29 links to each other with power supply; The other end ground connection of button K4; The port one 7 of chip U9 links to each other with the end of an end of resistance R 28 and button K3; The other end of resistance R 28 links to each other with power supply; The other end ground connection of button K3; The port one 8 of chip U9 links to each other with power supply; This circuit is used for to control system sending controling instruction; Control instruction comprise zeroing, forward, backward, finely tune forward, finely tune backward, suspend and finish, the model of chip U9 is MCP23S08.
As shown in Figure 9; Stepper motor driving circuit is: the port one of chip U8 links to each other with the port 4 of interface J5; The port 2 of chip U8 links to each other with the port 2 of interface J5; The port 3 of chip U8 and an end of resistance R 19; One end of resistance R 20 links to each other; The other end ground connection of resistance R 19; The port 4 of chip U8 links to each other with an end of the other end of resistance R 20 and capacitor C 16; The other end ground connection of capacitor C 16; The port 5 of chip U8 links to each other with the port one of interface J5; Port 6 ground connection of chip U8; Port 7 ground connection of chip U8; The port one 1 of chip U8 links to each other with the port 2 of interface J6; The port one ground connection of interface J6; The port one 2 of chip U8 and an end of resistance R 14; One end of capacitor C 13 links to each other; The other end ground connection of resistance R 14; The other end ground connection of capacitor C 13; Port one 3 ground connection of chip U8; The port one 4 of chip U8 and an end of resistance R 15; One end of capacitor C 14 links to each other; The other end ground connection of resistance R 15; The other end ground connection of capacitor C 14; The port one 5 of chip U8 links to each other with the port one 1 of chip U8; Port one 8 ground connection of chip U8; Port one 9 ground connection of chip U8; The port 21 of chip U8 links to each other with the port 3 of interface J5; The port 22 of chip U8 and an end of resistance R 17; One end of capacitor C 15 links to each other; The other end ground connection of capacitor C 15; The port 23 of chip U8 links to each other with an end of the other end of resistance R 17 and resistance R 18; The other end ground connection of resistance R 18; The port 24 of chip U8 and an end of capacitor C 17; The positive pole of polar capacitor C18 and power supply link to each other; The other end ground connection of capacitor C 17; The minus earth of polar capacitor C18, the model of chip U8 are L6219.
As shown in figure 10; Liquid crystal display circuit is: the port one ground connection of chip U10; The port 2 of chip U10 links to each other with power supply; The port 3 of chip U10; The port 7 of chip U10; The port 8 of chip U10; The port 9 of chip U10; The port one 0 of chip U10; The port one 1 of chip U10; The port one 2 of chip U10; The port one 3 of chip U10; The port one 4 of chip U10; The port one 6 of chip U10 does not link to each other with any device with the port one 8 of chip U10; The port one 5 of chip U10 links to each other with an end of resistance R 23; The other end ground connection of resistance R 23; The port one 7 of chip U10 links to each other with an end of an end of resistance R 25 and capacitor C 26; The other end of resistance R 25 links to each other with power supply; The other end ground connection of capacitor C 26; The port one 9 of chip U10 links to each other with power supply; Port 20 ground connection of chip U10, the model of chip U10 is YM12864R.
As shown in figure 11; Warning circuit is: an end of resistance R 24 links to each other with power supply; The other end of resistance R 24 links to each other with the emitter of positive-negative-positive triode Q9; The collector of positive-negative-positive triode Q9 links to each other with the positive pole of hummer LS1; The minus earth of hummer LS1; The base stage of positive-negative-positive triode Q9 links to each other with an end of resistance R 16, and the other end of resistance R 16 links to each other with microcontroller, and the model of positive-negative-positive triode Q9 is 9012.
As shown in figure 12; The photoelectricity positioning circuit is: the port one of port J3 links to each other with an end of 12V power supply and resistance R 3; The port 2 of port J3 links to each other with the other end of the port 2 of optocoupler U3 and resistance R 3; Port 3 ground connection of port J3; The port one of optocoupler U3 links to each other with the 12V power supply; The port 4 of optocoupler U3 links to each other with an end of resistance R 2, another termination power of resistance R 2, and the model of optocoupler U3 is TLP521-1.
When carrying out the terahertz time-domain spectroscopy test; At first the sample that completes is put into corresponding sample cell 2 successively by certain number order; Make sample near sample endoporus 13, metal clips 12 presses hole 14 inwalls outside sample with sample, can guarantee that thus sample is parallel with sample disc 1.Regulate 4 leveling nuts 8 of test platform 6; Eye-level appearance 9; Make test platform be in horizontality; And requiring THz wave to converge hot spot is near the center of Terahertz instrument connection 7 just; To guarantee that sample face and THz wave have higher vertical precision; To reduce sample, improve measuring accuracy to Terahertz wave reflection and refraction.Build the sealing case lid, the engaging means power supply.Can prepare to carry out spectral measurement after accomplishing above procedure.
The master switch of device is pushed on-state, and this moment, voice suggestion initialization success was waited until at liquid crystal display initialization interface, and when status indicator lamp showed open state, the device initialization finished.Press the zeroing button; Initial position fix is carried out in voice suggestion; The led state indicator lamp shows the zeroing state; Thereby the automatic control step motor 4 of microcontroller rotates and drives sample disc 1 rotation; When sample 1 dish turns to certain angle; The light that electrooptical device 5 produces passes locating hole 3; This moment, a sample cell 2 of sample disc 1 just in time alignd with Terahertz instrument connection 7; Zeroing finishes; The voice suggestion initial position fix finishes to carry out the measurement of first duplicate samples; The led state indicator lamp stops to show that the zeroing state begins to show test mode, and liquid crystal display displays can be carried out the measurement of first duplicate samples.Test preliminary work this moment and finish, can carry out the spectral measurement of sample.
Carry out the terahertz time-domain spectroscopy system and carry out the spectral measurement of sample, behind to be measured the finishing, press button forward, voice suggestion please be preserved the test data of first duplicate samples.Sample disc 1 turns to next sample cell 2 under the drive of stepper motor 4 just in time and Terahertz instrument connection 7 positions aligning places, and the led state pilot lamp shows transition status in the stepper motor rotating process.The led state pilot lamp stops to show transition status when motor stops operating, and the test of second duplicate samples is carried out in voice suggestion and liquid crystal display.Repeating above step finishes up to all sample tests.Institute in steps in LCD, led state pilot lamp, and sound circuit all can the residing state of the current device of real-time prompting, and the current sample number into spectrum of testing, with handled easily personnel's operation.After all samples measurement finishes, press conclusion button, sample stage can be closed automatically.
If in the data acquisition, the sample that need test once more can be pressed button backward.If in the motor rotation process, need to suspend test, can press pause button, LED will show halted state this moment, up to stopping halted state.When sample test begins; If the positioning result to pilot hole 3 is not felt quite pleased; Can press on the control panel fine setting forward or backward fine setting carry out initial alignment; Stepper motor will rotate a very little angle forward or backward this moment; Satisfied up to operating personnel; After measurement in, control system will be carried out record to the low-angle that stepper motor rotates, and will not need the original state of manual adjustments specimen holder once more afterwards.
The terahertz time-domain spectroscopy sample automatic testing equipment based on microcontroller that the present invention proposes has the horizontality adjustment; A series of functions such as the initial position zeroing when sample is packed into; Can guarantee the constant relatively of measurement environment in continuous coverage and the whole measuring process of sample; Improve the measuring accuracy of terahertz time-domain spectroscopy, reduced experimental error.Sound prompt function, liquid crystal display function and led state Presentation Function timely the current system of alert running status and when the sample cell of Pretesting numbering; Mistake such as reduced the omission that the artificial memory brings, obscure, the raising of maximum possible measuring reliability, improved the efficiency of measurement of terahertz time-domain spectroscopy.

Claims (9)

1. terahertz time-domain spectroscopy sample automatic testing equipment based on microcontroller; It is characterized in that comprising Terahertz Sample testing device and control system; The Terahertz Sample testing device comprises sample disc (1); Sample cell (2); Pilot hole (3); Stepper motor (4); Electrooptical device (5); Test platform (6); Terahertz instrument connection (7); Leveling nut (8); Level meter (9); Holddown spring stationary installation (10); Holddown spring (11); Metal clips (12); The outer hole (14) of sample cell endoporus (13) and sample cell; Leveling nut (8) is installed in four jiaos of test platform (6) bottom; Level meter (9) is installed in the upper surface of test platform (6); Electrooptical device (5) and stepper motor (4) are fixed on the groove of the upper surface of test platform (6); Terahertz instrument connection (7) runs through the front and rear surfaces of test platform (6); Sample disc (1) is fixed on the output shaft of stepper motor; More than one sample cell (2); Holddown spring stationary installation (10); Holddown spring (11); Metal clips (12) be evenly distributed in sample disc (1) around; Holddown spring (11) one ends are fixed on the sample disc (1) through holddown spring stationary installation (10); Metal clips (12) is connected the other end of holddown spring (11); Pilot hole (3) is distributed in the outer rim of sample disc (1), and near sample cell (2); Control system comprises microcontroller, power circuit, key circuit, sound circuit, warning circuit, liquid crystal display circuit, LED indicating circuit, stepper motor driving circuit, photoelectricity positioning circuit, and microcontroller links to each other with power circuit, key circuit, sound circuit, warning circuit, liquid crystal display circuit, LED indicating circuit, stepper motor driving circuit, photoelectricity positioning circuit respectively.
2. a kind of terahertz time-domain spectroscopy sample automatic testing equipment according to claim 1 based on microcontroller; It is characterized in that described power circuit is: the port one of power interface J1 is connected with the port 2 of keyswitch S1; Power interface J1 port 2 links to each other with the port 5 of keyswitch S1; Port 6 ground connection of keyswitch S1; The port 2 of keyswitch S1 links to each other with the anode of diode D1; The positive pole of the negative electrode of diode D1 and capacitor C 1; One end of capacitor C 2 and the port one of chip U6 link to each other; The minus earth of capacitor C 1; The other end ground connection of capacitor C 2; The port 3 of chip U6 and port 5 ground connection of chip U6; The port 2 of chip U6 links to each other with an end of the negative electrode of diode D4 and inductance L 1; The port 4 of chip U6 and the other end of inductance L 1; The positive pole of capacitor C 3; One end of capacitor C 10 and the port one of chip U5 link to each other; The anode of diode D4; The other end ground connection of the negative pole of capacitor C 3 and capacitor C 10; The port 3 of chip U5 links to each other with an end of resistance R 1; The other end of resistance R 1 links to each other with the anode of light emitting diode D3; The plus earth of light emitting diode D3; Port 2 ground connection of chip U5; The port 5 of chip U5 is not connected with any device with the port 6 of chip U5; Chip U5 port 4 links to each other with the grid of N-channel MOS pipe Q1; The source electrode of N-channel MOS pipe Q1 is connected with the port one of power supply with chip U5; The drain electrode of N-channel MOS pipe Q1 links to each other with the negative electrode of the port one of power supply chip U5 and diode D2; The anode of diode D2 links to each other with power supply; The anode of diode D14 links to each other with an end of resistance R 11; The plus earth of diode D14; The other end of resistance R 11; One end of capacitor C 4 and an end of capacitor C 11 link to each other with power supply, the other end ground connection of the other end of capacitor C 4 and capacitor C 11.
3. a kind of terahertz time-domain spectroscopy sample automatic testing equipment according to claim 1 based on microcontroller; It is characterized in that described LED indicating circuit is: port 5 ground connection of the port 4 of chip U7 and chip U7; The port 6 of chip U7 links to each other with an end of an end of resistance R 12 and capacitor C 12; The other end of resistance R 12 is connected with power supply; The other end ground connection of capacitor C 12; Port 9 ground connection of chip U7; The port one 0 of chip U7 links to each other with an end of resistance R 5; The other end of resistance R 5 links to each other with the negative electrode of light emitting diode D8; The anode of diode D8 links to each other with power supply; The port one 1 of chip U7 links to each other with an end of resistance R 6; The other end of resistance R 6 links to each other with the negative electrode of light emitting diode D9; The anode of diode D9 links to each other with power supply; The port one 2 of chip U7 links to each other with an end of resistance R 7; The other end of resistance R 7 links to each other with the negative electrode of light emitting diode D10; The anode of diode D10 links to each other with power supply; The port one 3 of chip U7 links to each other with an end of resistance R 8; The other end of resistance R 8 links to each other with the negative electrode of light emitting diode D11; The anode of diode D11 links to each other with power supply; The port one 4 of chip U7 links to each other with an end of resistance R 9; The other end of resistance R 9 links to each other with the negative electrode of light emitting diode D12; The anode of diode D12 links to each other with power supply; The port one 5 of chip U7 links to each other with an end of resistance R 10; The other end of resistance R 10 links to each other with the negative electrode of light emitting diode D13; The anode of diode D13 links to each other with power supply; The port one 6 of chip U7, the port 7 of chip U7 are not connected with any device, and the port one 8 of chip U7 is connected with power supply.
4. a kind of terahertz time-domain spectroscopy sample automatic testing equipment according to claim 1 based on microcontroller; It is characterized in that described key circuit is: port 5 ground connection of the port 4 of chip U9 and chip U9; The port 6 of chip U9 links to each other with an end of an end of resistance R 27 and capacitor C 19; The other end of resistance R 27 is connected with power supply; The other end ground connection of capacitor C 19; Port 9 ground connection of chip U9; The port one 0 of chip U9 links to each other with the end of an end of resistance R 35 and button K10; The other end of resistance R 35 links to each other with power supply; The other end ground connection of button K10; The port one 1 of chip U9 links to each other with the end of an end of resistance R 34 and button K9; The other end of resistance R 34 links to each other with power supply; The other end ground connection of button K9; The port one 2 of chip U9 links to each other with the end of an end of resistance R 33 and button K8; The other end of resistance R 33 links to each other with power supply; The other end ground connection of button K8; The port one 3 of chip U9 links to each other with the end of an end of resistance R 32 and button K7; The other end of resistance R 32 links to each other with power supply; The other end ground connection of button K7; The port one 4 of chip U9 links to each other with the end of an end of resistance R 31 and button K6; The other end of resistance R 31 links to each other with power supply; The other end ground connection of button K6; The port one 5 of chip U9 links to each other with the end of an end of resistance R 30 and button K5; The other end of resistance R 30 links to each other with power supply; The other end ground connection of button K5; The port one 6 of chip U9 links to each other with the end of an end of resistance R 29 and button K4; The other end of resistance R 29 links to each other with power supply; The other end ground connection of button K4; The port one 7 of chip U9 links to each other with the end of an end of resistance R 28 and button K3; The other end of resistance R 28 links to each other with power supply; The other end ground connection of button K3, the port one 8 of chip U9 links to each other with power supply.
5. a kind of terahertz time-domain spectroscopy sample automatic testing equipment according to claim 1 based on microcontroller; It is characterized in that described sound circuit is: port 4 ground connection of chip U4; The port 5 of chip U4 links to each other with the end of microphone LS2; The port 6 of chip U4 links to each other with the other end of microphone LS2; The port 7 of chip U4 links to each other with power supply; The port 8 of chip U4 links to each other with the end of loudspeaker MK1; The port 9 of chip U4 links to each other with the other end of loudspeaker MK1; The port one 0 of chip U4 links to each other with an end of resistance R 4; The other end of resistance R 4 links to each other with the end of interface J4; The other end ground connection of interface J4; The port 20 of chip U4 links to each other with the end of button K2; The other end ground connection of button K2; The positive pole of polar capacitor C8 links to each other with power supply; The minus earth of polar capacitor C8, an end of capacitor C 9 links to each other with power supply, the other end ground connection of capacitor C 9.
6. a kind of terahertz time-domain spectroscopy sample automatic testing equipment according to claim 1; It is characterized in that described warning circuit is: an end of resistance R 24 links to each other with power supply; The other end of resistance R 24 links to each other with the emitter of positive-negative-positive triode Q9; The collector of positive-negative-positive triode Q9 links to each other with the positive pole of hummer LS1; The minus earth of hummer LS1; The base stage of positive-negative-positive triode Q9 links to each other with an end of resistance R 16, and the other end of resistance R 16 links to each other with microcontroller.
7. a kind of terahertz time-domain spectroscopy sample automatic testing equipment according to claim 1 based on microcontroller; It is characterized in that described photoelectricity positioning circuit is: the port one of port J3 links to each other with an end of 12V power supply and resistance R 3; The port 2 of port J3 links to each other with the other end of the port 2 of optocoupler U3 and resistance R 3; Port 3 ground connection of port J3; The port one of optocoupler U3 links to each other with the 12V power supply; The port 4 of optocoupler U3 links to each other with an end of resistance R 2, another termination power of resistance R 2.
8. a kind of terahertz time-domain spectroscopy sample automatic testing equipment according to claim 1 based on microcontroller; It is characterized in that described liquid crystal display circuit is: the port one ground connection of chip U10; The port 2 of chip U10 links to each other with power supply; The port 3 of chip U10; The port 7 of chip U10; The port 8 of chip U10; The port 9 of chip U10; The port one 0 of chip U10; The port one 1 of chip U10; The port one 2 of chip U10; The port one 3 of chip U10; The port one 4 of chip U10; The port one 6 of chip U10 does not link to each other with any device with the port one 8 of chip U10; The port one 5 of chip U10 links to each other with an end of resistance R 23; The other end ground connection of resistance R 23; The port one 7 of chip U10 links to each other with an end of an end of resistance R 25 and capacitor C 26; The other end of resistance R 25 links to each other with power supply; The other end ground connection of capacitor C 26; The port one 9 of chip U10 links to each other with power supply, port 20 ground connection of chip U10.
9. a kind of terahertz time-domain spectroscopy sample automatic testing equipment according to claim 1 based on microcontroller; It is characterized in that described stepper motor driving circuit is: the port one of chip U8 links to each other with the port 4 of interface J5; The port 2 of chip U8 links to each other with the port 2 of interface J5; The port 3 of chip U8 and an end of resistance R 19; One end of resistance R 20 links to each other; The other end ground connection of resistance R 19; The port 4 of chip U8 links to each other with an end of the other end of resistance R 20 and capacitor C 16; The other end ground connection of capacitor C 16; The port 5 of chip U8 links to each other with the port one of interface J5; Port 6 ground connection of chip U8; Port 7 ground connection of chip U8; The port one 1 of chip U8 links to each other with the port 2 of interface J6; The port one ground connection of interface J6; The port one 2 of chip U8 and an end of resistance R 14; One end of capacitor C 13 links to each other; The other end ground connection of resistance R 14; The other end ground connection of capacitor C 13; Port one 3 ground connection of chip U8; The port one 4 of chip U8 and an end of resistance R 15; One end of capacitor C 14 links to each other; The other end ground connection of resistance R 15; The other end ground connection of capacitor C 14; The port one 5 of chip U8 links to each other with the port one 1 of chip U8; Port one 8 ground connection of chip U8; Port one 9 ground connection of chip U8; The port 21 of chip U8 links to each other with the port 3 of interface J5; The port 22 of chip U8 and an end of resistance R 17; One end of capacitor C 15 links to each other; The other end ground connection of capacitor C 15; The port 23 of chip U8 links to each other with an end of the other end of resistance R 17 and resistance R 18; The other end ground connection of resistance R 18; The port 24 of chip U8 and an end of capacitor C 17; The positive pole of polar capacitor C18 and power supply link to each other; The other end ground connection of capacitor C 17, the minus earth of polar capacitor C18.
CN2011101275703A 2011-05-17 2011-05-17 Microcontroller-based terahertz time-domain spectroscopy automatic sample testing device Expired - Fee Related CN102305767B (en)

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CN103616333A (en) * 2013-12-18 2014-03-05 重庆绿色智能技术研究院 Liquid sample pool device for continuous detection by adopting terahertz spectrum
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CN106475158B (en) * 2016-10-17 2019-06-04 首都师范大学 Micro-fluidic chip and manufacturing method for transmission-type terahertz time-domain spectroscopy system
CN107144546A (en) * 2017-06-05 2017-09-08 吉林大学 Terahertz imaging method based on reflection time domain waveform adding window
CN107144546B (en) * 2017-06-05 2021-10-01 吉林大学 Terahertz imaging method based on reflected time domain waveform windowing
CN109580531A (en) * 2018-12-13 2019-04-05 浙江大学 A kind of automatic sampling for terahertz light spectrometer and vary device

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