CN102277110A - Aqueous sealant and preparation method thereof - Google Patents

Aqueous sealant and preparation method thereof Download PDF

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Publication number
CN102277110A
CN102277110A CN 201110201884 CN201110201884A CN102277110A CN 102277110 A CN102277110 A CN 102277110A CN 201110201884 CN201110201884 CN 201110201884 CN 201110201884 A CN201110201884 A CN 201110201884A CN 102277110 A CN102277110 A CN 102277110A
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aqueous
sealant
powder
emulsion
preparation
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CN102277110B (en
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姚函亮
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Irico Group Corp
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Irico Group Corp
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Abstract

The invention discloses aqueous sealant and a preparation method thereof. The aqueous sealant comprises the following components in percentage by mass: 40 to 50 percent of aqueous resin emulsion, 10 to 15 percent of ethanol, 10 to 15 percent of glass fiber powder, 5 to 10 percent of glass powder, 10 to 15 percent of inorganic bonding agent, 10 to 20 percent of inorganic adhesion promoter and 0.5 to 1 percent of dispersing agent. Prepared from aqueous resin, the aqueous sealant does not pollute environment and is environment-friendly. Simultaneously, a certain quantity of ground glass fibers are added into the sealant, so that the physicochemical properties of the sealant can be improved obviously, the bonding performance is high, and the bonding is firm; and a coating is high in hardness, crack resistance, abrasive resistance and the like, and the stability of a resin bonding agent also can be improved.

Description

A kind of aqueous sealant and preparation method thereof
Technical field
The invention belongs to electric elements seal gum technical field, relate to a kind of aqueous sealant and preparation method thereof.
Background technology
Seal gum is a kind ofly to be out of shape with the trim shape, is difficult for trickling, and certain close-burning sealing material is arranged, and is to be used for filling the configuration gap to play the tackiness agent of sealing function, can rely on drying, temperature variation, solvent evaporates, progressively curing molding.In order to guarantee the reliable and stable of motor, electric elements electrical property and physical strength, need be between the conductor, use seal gum to seal between slit and outlet lead-in wire.Be widely used in being used for the bonding reinforcing of the adhering and sealing and the electronic component of class household electrical appliance.
Along with the reinforcement of environmental consciousness, the requirement of aqueous sealant has been proposed.This is because the aqueous, environmental protective formula system of aqueous sealant has guaranteed ultralow VOC quantity discharged.Safety and environmental protection, the volatilization of organic solvent-free in the use, all unharmful substance produces, and has guaranteed the environmental-protecting performance of product.
Meanwhile, along with the development of electronic enterprises, need that adhesive property is better, bonding is more firm; The seal gum that coating hardness is bigger, splitting resistance is better, wear resistance is stronger etc.
Summary of the invention
The problem that the present invention solves is to provide a kind of aqueous sealant and preparation method thereof, is the environment-friendly type seal gum, and bonding firmly can be applicable to the bonding reinforcing of the adhering and sealing and the electronic component of household electrical appliance.
The present invention is achieved through the following technical solutions:
A kind of aqueous sealant, in massfraction, comprise 40~50% resin aqueous emulsion, 10~15% ethanol, 10~15% glass fiber powder, 5~10% glass powder, 10~15% mineral binder bond, 10~20% inorganic short stick and 0.5~1% dispersion agent;
Described mineral binder bond is aluminum oxide or kaolin, and its size is 0.2~10 μ m;
Described inorganic short stick is titanium dioxide or talcum powder, and its size is 0.2~10 μ m.
Described resin aqueous emulsion is one or both of water-borne acrylic resin emulsion, aqueous polyurethane resin emulsion.
Described glass fiber powder is, its section radius is 1~10 μ m, and length is 80~110 μ m.
Described glass powder, its particle are spherical, and radius is 1~10 μ m.
Described dispersion agent is a DA type dispersion agent.
A kind of preparation method of aqueous sealant may further comprise the steps:
According to resin aqueous emulsion: ethanol: glass fiber powder: glass powder: mineral binder bond: inorganic short stick: dispersion agent=(40~50): (10~15): (10~15): (5~10): (10~15): (10~20): the mass ratio of (0.5~1), after resin aqueous emulsion, ethanol, glass fibre, glass powder, mineral binder bond, inorganic short stick and dispersant, fully stir and form uniform mixed phase;
Described mineral binder bond is aluminum oxide or kaolin, and its size is 0.2~10 μ m;
Described inorganic short stick is titanium dioxide or talcum powder, and its size is 0.2~10 μ m.
Described resin aqueous emulsion is one or both of water-borne acrylic resin emulsion, aqueous polyurethane resin emulsion.
Its section radius of described glass fibre is 1~10 μ m, and length is 80~110 μ m.
Its particle of described glass powder is spherical, and radius is for being 1~10 μ m.
Described dispersion agent is a DA type dispersion agent.
Compared with prior art, the present invention has following beneficial technical effects:
Aqueous sealant provided by the invention is by the water-base resin preparation, and environmentally safe is the environment-friendly type seal gum.Simultaneously, add a certain amount of milled glass fiber in seal gum, can obviously improve the physicochemical property of seal gum, the knot performance is better, and it is more firm to bond; Coating hardness is bigger, and splitting resistance is better, and wear resistance is stronger etc., also can improve the stability of resin glue.
Embodiment
The present invention is described in further detail below in conjunction with specific embodiment, and the explanation of the invention is not limited.
Embodiment 1
In massfraction, the each component proportioning of aqueous sealant is:
The material thorough mixing that water-borne acrylic resin emulsion, ethanol, glass fiber powder (Hangzhou matrix material company limited of high section), glass powder (Asahi Glass), aluminum oxide, titanium dioxide and the weighing of DA type dispersion agent are finished, thorough mixing in stirrer forms uniform mixed phase.
Embodiment 2
In massfraction, the each component proportioning of aqueous sealant is:
Figure BDA0000076846870000032
The material thorough mixing that aqueous polyurethane resin emulsion, ethanol, glass fiber powder (Hangzhou matrix material company limited of high section), glass powder (Asahi Glass), kaolin, titanium dioxide and the weighing of DA type dispersion agent are finished, thorough mixing in stirrer forms uniform mixed phase.
Embodiment 3
In massfraction, the each component proportioning of aqueous sealant is:
Figure BDA0000076846870000041
The material thorough mixing that water-borne acrylic resin emulsion, aqueous polyurethane resin emulsion, ethanol, glass fiber powder (Hangzhou matrix material company limited of high section), glass powder (Asahi Glass), aluminum oxide, talcum powder and the weighing of DA type dispersion agent are finished, thorough mixing in stirrer forms uniform mixed phase.
Embodiment 4
In massfraction, the each component proportioning of aqueous sealant is:
Figure BDA0000076846870000042
With the material thorough mixing that aqueous polyurethane resin emulsion, ethanol, glass fiber powder, glass powder, kaolin, talcum powder and the weighing of DA type dispersion agent are finished, thorough mixing in stirrer forms uniform mixed phase.
Embodiment 5
In massfraction, the each component proportioning of aqueous sealant is:
With the material thorough mixing that water-borne acrylic resin emulsion, aqueous polyurethane resin emulsion, ethanol, glass fiber powder, glass powder, kaolin, titanium dioxide and the weighing of DA type dispersion agent are finished, thorough mixing in stirrer forms uniform mixed phase.

Claims (10)

1. aqueous sealant, it is characterized in that, in massfraction, comprise 40~50% resin aqueous emulsion, 10~15% ethanol, 10~15% glass fiber powder, 5~10% glass powder, 10~15% mineral binder bond, 10~20% inorganic short stick and 0.5~1% dispersion agent;
Described mineral binder bond is aluminum oxide or kaolin, and its size is 0.2~10 μ m;
Described inorganic short stick is titanium dioxide or talcum powder, and its size is 0.2~10 μ m.
2. aqueous sealant as claimed in claim 1 is characterized in that, described resin aqueous emulsion is one or both of water-borne acrylic resin emulsion, aqueous polyurethane resin emulsion.
3. aqueous sealant as claimed in claim 1 is characterized in that, its section radius of described glass fiber powder is 1~10 μ m, and length is 80~110 μ m.
4. aqueous sealant as claimed in claim 1 is characterized in that, its particle of described glass powder is spherical, and radius is 1~10 μ m.
5. aqueous sealant as claimed in claim 1 is characterized in that, described dispersion agent is a DA type dispersion agent.
6. the preparation method of an aqueous sealant is characterized in that, may further comprise the steps:
According to resin aqueous emulsion: ethanol: glass fiber powder: glass powder: mineral binder bond: inorganic short stick: dispersion agent=(40~50): (10~15): (10~15): (5~10): (10~15): (10~20): the mass ratio of (0.5~1), after resin aqueous emulsion, ethanol, glass fibre, glass powder, mineral binder bond, inorganic short stick and dispersant, fully stir and form uniform mixed phase;
Described mineral binder bond is aluminum oxide or kaolin, and its size is 0.2~10 μ m;
Described inorganic short stick is titanium dioxide or talcum powder, and its size is 0.2~10 μ m.
7. the preparation method of aqueous sealant as claimed in claim 6 is characterized in that, described resin aqueous emulsion is one or both of water-borne acrylic resin emulsion, aqueous polyurethane resin emulsion.
8. the preparation method of aqueous sealant as claimed in claim 6 is characterized in that, its section radius of described glass fiber powder is 1~10 μ m, and length is 80~110 μ m.
9. the preparation method of aqueous sealant as claimed in claim 6 is characterized in that, its particle of described glass powder is spherical, and radius is 1~10 μ m.
10. the preparation method of aqueous sealant as claimed in claim 6 is characterized in that, described dispersion agent is a DA type dispersion agent.
CN201110201884A 2011-07-19 2011-07-19 Aqueous sealant and preparation method thereof Expired - Fee Related CN102277110B (en)

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104387992A (en) * 2014-11-28 2015-03-04 苏州伊埃夫化学材料科技有限公司 Environment-friendly adhesive for artificial board and preparation method of environment-friendly adhesive
CN104448637A (en) * 2014-12-01 2015-03-25 湖州绿净环保科技有限公司 Preparation method of PTFE (polytetrafluoroethylene) film for air filtration
CN106554733A (en) * 2016-10-28 2017-04-05 天长市永泰密封材料有限公司 Ageing-resistant container aqueous sealant of a kind of uvioresistant and preparation method thereof
CN106554734A (en) * 2016-10-28 2017-04-05 天长市永泰密封材料有限公司 A kind of deodorant and smell removing container aqueous sealant and preparation method thereof
CN108165215A (en) * 2018-02-07 2018-06-15 合肥嘉仕诚能源科技有限公司 A kind of anti-oxidant heat-resisting waterproof gasket cement of high viscosity
CN108867065A (en) * 2018-07-03 2018-11-23 成都海蓉特种纺织品有限公司 A kind of antiwear assistant and preparation method thereof for textile
CN110357447A (en) * 2019-07-16 2019-10-22 常德市宏辉建星家具有限公司 A kind of formula and preparation method thereof of the scratch resistant coating material of glass surface
CN110539538A (en) * 2019-09-16 2019-12-06 福建立邦包装有限公司 Cast CPE (chlorinated polyethylene) inflatable automatic packaging composite film and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2008038041A (en) * 2006-08-08 2008-02-21 Ceramic Coat Kk Coating composition
CN101525525A (en) * 2008-03-04 2009-09-09 金朝绪 Acrylic ester waterproof gasket cement
CN101967256A (en) * 2010-06-11 2011-02-09 广州市安泰化学有限公司 Environment-friendly aqueous sealant for container

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2008038041A (en) * 2006-08-08 2008-02-21 Ceramic Coat Kk Coating composition
CN101525525A (en) * 2008-03-04 2009-09-09 金朝绪 Acrylic ester waterproof gasket cement
CN101967256A (en) * 2010-06-11 2011-02-09 广州市安泰化学有限公司 Environment-friendly aqueous sealant for container

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104387992A (en) * 2014-11-28 2015-03-04 苏州伊埃夫化学材料科技有限公司 Environment-friendly adhesive for artificial board and preparation method of environment-friendly adhesive
CN104448637A (en) * 2014-12-01 2015-03-25 湖州绿净环保科技有限公司 Preparation method of PTFE (polytetrafluoroethylene) film for air filtration
CN106554733A (en) * 2016-10-28 2017-04-05 天长市永泰密封材料有限公司 Ageing-resistant container aqueous sealant of a kind of uvioresistant and preparation method thereof
CN106554734A (en) * 2016-10-28 2017-04-05 天长市永泰密封材料有限公司 A kind of deodorant and smell removing container aqueous sealant and preparation method thereof
CN108165215A (en) * 2018-02-07 2018-06-15 合肥嘉仕诚能源科技有限公司 A kind of anti-oxidant heat-resisting waterproof gasket cement of high viscosity
CN108867065A (en) * 2018-07-03 2018-11-23 成都海蓉特种纺织品有限公司 A kind of antiwear assistant and preparation method thereof for textile
CN110357447A (en) * 2019-07-16 2019-10-22 常德市宏辉建星家具有限公司 A kind of formula and preparation method thereof of the scratch resistant coating material of glass surface
CN110539538A (en) * 2019-09-16 2019-12-06 福建立邦包装有限公司 Cast CPE (chlorinated polyethylene) inflatable automatic packaging composite film and preparation method thereof
CN110539538B (en) * 2019-09-16 2021-06-15 福建立邦包装有限公司 Cast CPE (chlorinated polyethylene) inflatable automatic packaging composite film and preparation method thereof

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