CN102277110A - Aqueous sealant and preparation method thereof - Google Patents
Aqueous sealant and preparation method thereof Download PDFInfo
- Publication number
- CN102277110A CN102277110A CN 201110201884 CN201110201884A CN102277110A CN 102277110 A CN102277110 A CN 102277110A CN 201110201884 CN201110201884 CN 201110201884 CN 201110201884 A CN201110201884 A CN 201110201884A CN 102277110 A CN102277110 A CN 102277110A
- Authority
- CN
- China
- Prior art keywords
- aqueous
- sealant
- powder
- emulsion
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Sealing Material Composition (AREA)
Abstract
The invention discloses aqueous sealant and a preparation method thereof. The aqueous sealant comprises the following components in percentage by mass: 40 to 50 percent of aqueous resin emulsion, 10 to 15 percent of ethanol, 10 to 15 percent of glass fiber powder, 5 to 10 percent of glass powder, 10 to 15 percent of inorganic bonding agent, 10 to 20 percent of inorganic adhesion promoter and 0.5 to 1 percent of dispersing agent. Prepared from aqueous resin, the aqueous sealant does not pollute environment and is environment-friendly. Simultaneously, a certain quantity of ground glass fibers are added into the sealant, so that the physicochemical properties of the sealant can be improved obviously, the bonding performance is high, and the bonding is firm; and a coating is high in hardness, crack resistance, abrasive resistance and the like, and the stability of a resin bonding agent also can be improved.
Description
Technical field
The invention belongs to electric elements seal gum technical field, relate to a kind of aqueous sealant and preparation method thereof.
Background technology
Seal gum is a kind ofly to be out of shape with the trim shape, is difficult for trickling, and certain close-burning sealing material is arranged, and is to be used for filling the configuration gap to play the tackiness agent of sealing function, can rely on drying, temperature variation, solvent evaporates, progressively curing molding.In order to guarantee the reliable and stable of motor, electric elements electrical property and physical strength, need be between the conductor, use seal gum to seal between slit and outlet lead-in wire.Be widely used in being used for the bonding reinforcing of the adhering and sealing and the electronic component of class household electrical appliance.
Along with the reinforcement of environmental consciousness, the requirement of aqueous sealant has been proposed.This is because the aqueous, environmental protective formula system of aqueous sealant has guaranteed ultralow VOC quantity discharged.Safety and environmental protection, the volatilization of organic solvent-free in the use, all unharmful substance produces, and has guaranteed the environmental-protecting performance of product.
Meanwhile, along with the development of electronic enterprises, need that adhesive property is better, bonding is more firm; The seal gum that coating hardness is bigger, splitting resistance is better, wear resistance is stronger etc.
Summary of the invention
The problem that the present invention solves is to provide a kind of aqueous sealant and preparation method thereof, is the environment-friendly type seal gum, and bonding firmly can be applicable to the bonding reinforcing of the adhering and sealing and the electronic component of household electrical appliance.
The present invention is achieved through the following technical solutions:
A kind of aqueous sealant, in massfraction, comprise 40～50% resin aqueous emulsion, 10～15% ethanol, 10～15% glass fiber powder, 5～10% glass powder, 10～15% mineral binder bond, 10～20% inorganic short stick and 0.5～1% dispersion agent;
Described mineral binder bond is aluminum oxide or kaolin, and its size is 0.2～10 μ m;
Described inorganic short stick is titanium dioxide or talcum powder, and its size is 0.2～10 μ m.
Described resin aqueous emulsion is one or both of water-borne acrylic resin emulsion, aqueous polyurethane resin emulsion.
Described glass fiber powder is, its section radius is 1～10 μ m, and length is 80～110 μ m.
Described glass powder, its particle are spherical, and radius is 1～10 μ m.
Described dispersion agent is a DA type dispersion agent.
A kind of preparation method of aqueous sealant may further comprise the steps:
According to resin aqueous emulsion: ethanol: glass fiber powder: glass powder: mineral binder bond: inorganic short stick: dispersion agent=(40～50): (10～15): (10～15): (5～10): (10～15): (10～20): the mass ratio of (0.5～1), after resin aqueous emulsion, ethanol, glass fibre, glass powder, mineral binder bond, inorganic short stick and dispersant, fully stir and form uniform mixed phase;
Described mineral binder bond is aluminum oxide or kaolin, and its size is 0.2～10 μ m;
Described inorganic short stick is titanium dioxide or talcum powder, and its size is 0.2～10 μ m.
Described resin aqueous emulsion is one or both of water-borne acrylic resin emulsion, aqueous polyurethane resin emulsion.
Its section radius of described glass fibre is 1～10 μ m, and length is 80～110 μ m.
Its particle of described glass powder is spherical, and radius is for being 1～10 μ m.
Described dispersion agent is a DA type dispersion agent.
Compared with prior art, the present invention has following beneficial technical effects:
Aqueous sealant provided by the invention is by the water-base resin preparation, and environmentally safe is the environment-friendly type seal gum.Simultaneously, add a certain amount of milled glass fiber in seal gum, can obviously improve the physicochemical property of seal gum, the knot performance is better, and it is more firm to bond; Coating hardness is bigger, and splitting resistance is better, and wear resistance is stronger etc., also can improve the stability of resin glue.
Embodiment
The present invention is described in further detail below in conjunction with specific embodiment, and the explanation of the invention is not limited.
Embodiment 1
In massfraction, the each component proportioning of aqueous sealant is:
The material thorough mixing that water-borne acrylic resin emulsion, ethanol, glass fiber powder (Hangzhou matrix material company limited of high section), glass powder (Asahi Glass), aluminum oxide, titanium dioxide and the weighing of DA type dispersion agent are finished, thorough mixing in stirrer forms uniform mixed phase.
Embodiment 2
In massfraction, the each component proportioning of aqueous sealant is:
The material thorough mixing that aqueous polyurethane resin emulsion, ethanol, glass fiber powder (Hangzhou matrix material company limited of high section), glass powder (Asahi Glass), kaolin, titanium dioxide and the weighing of DA type dispersion agent are finished, thorough mixing in stirrer forms uniform mixed phase.
Embodiment 3
In massfraction, the each component proportioning of aqueous sealant is:
The material thorough mixing that water-borne acrylic resin emulsion, aqueous polyurethane resin emulsion, ethanol, glass fiber powder (Hangzhou matrix material company limited of high section), glass powder (Asahi Glass), aluminum oxide, talcum powder and the weighing of DA type dispersion agent are finished, thorough mixing in stirrer forms uniform mixed phase.
Embodiment 4
In massfraction, the each component proportioning of aqueous sealant is:
With the material thorough mixing that aqueous polyurethane resin emulsion, ethanol, glass fiber powder, glass powder, kaolin, talcum powder and the weighing of DA type dispersion agent are finished, thorough mixing in stirrer forms uniform mixed phase.
Embodiment 5
In massfraction, the each component proportioning of aqueous sealant is:
With the material thorough mixing that water-borne acrylic resin emulsion, aqueous polyurethane resin emulsion, ethanol, glass fiber powder, glass powder, kaolin, titanium dioxide and the weighing of DA type dispersion agent are finished, thorough mixing in stirrer forms uniform mixed phase.
Claims (10)
1. aqueous sealant, it is characterized in that, in massfraction, comprise 40～50% resin aqueous emulsion, 10～15% ethanol, 10～15% glass fiber powder, 5～10% glass powder, 10～15% mineral binder bond, 10～20% inorganic short stick and 0.5～1% dispersion agent;
Described mineral binder bond is aluminum oxide or kaolin, and its size is 0.2～10 μ m;
Described inorganic short stick is titanium dioxide or talcum powder, and its size is 0.2～10 μ m.
2. aqueous sealant as claimed in claim 1 is characterized in that, described resin aqueous emulsion is one or both of water-borne acrylic resin emulsion, aqueous polyurethane resin emulsion.
3. aqueous sealant as claimed in claim 1 is characterized in that, its section radius of described glass fiber powder is 1～10 μ m, and length is 80～110 μ m.
4. aqueous sealant as claimed in claim 1 is characterized in that, its particle of described glass powder is spherical, and radius is 1～10 μ m.
5. aqueous sealant as claimed in claim 1 is characterized in that, described dispersion agent is a DA type dispersion agent.
6. the preparation method of an aqueous sealant is characterized in that, may further comprise the steps:
According to resin aqueous emulsion: ethanol: glass fiber powder: glass powder: mineral binder bond: inorganic short stick: dispersion agent=(40～50): (10～15): (10～15): (5～10): (10～15): (10～20): the mass ratio of (0.5～1), after resin aqueous emulsion, ethanol, glass fibre, glass powder, mineral binder bond, inorganic short stick and dispersant, fully stir and form uniform mixed phase;
Described mineral binder bond is aluminum oxide or kaolin, and its size is 0.2～10 μ m;
Described inorganic short stick is titanium dioxide or talcum powder, and its size is 0.2～10 μ m.
7. the preparation method of aqueous sealant as claimed in claim 6 is characterized in that, described resin aqueous emulsion is one or both of water-borne acrylic resin emulsion, aqueous polyurethane resin emulsion.
8. the preparation method of aqueous sealant as claimed in claim 6 is characterized in that, its section radius of described glass fiber powder is 1～10 μ m, and length is 80～110 μ m.
9. the preparation method of aqueous sealant as claimed in claim 6 is characterized in that, its particle of described glass powder is spherical, and radius is 1～10 μ m.
10. the preparation method of aqueous sealant as claimed in claim 6 is characterized in that, described dispersion agent is a DA type dispersion agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110201884A CN102277110B (en) | 2011-07-19 | 2011-07-19 | Aqueous sealant and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110201884A CN102277110B (en) | 2011-07-19 | 2011-07-19 | Aqueous sealant and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102277110A true CN102277110A (en) | 2011-12-14 |
| CN102277110B CN102277110B (en) | 2012-09-19 |
Family
ID=45102856
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201110201884A Expired - Fee Related CN102277110B (en) | 2011-07-19 | 2011-07-19 | Aqueous sealant and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102277110B (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104387992A (en) * | 2014-11-28 | 2015-03-04 | 苏州伊埃夫化学材料科技有限公司 | Environment-friendly adhesive for artificial board and preparation method of environment-friendly adhesive |
| CN104448637A (en) * | 2014-12-01 | 2015-03-25 | 湖州绿净环保科技有限公司 | Preparation method of PTFE (polytetrafluoroethylene) film for air filtration |
| CN106554733A (en) * | 2016-10-28 | 2017-04-05 | 天长市永泰密封材料有限公司 | Ageing-resistant container aqueous sealant of a kind of uvioresistant and preparation method thereof |
| CN106554734A (en) * | 2016-10-28 | 2017-04-05 | 天长市永泰密封材料有限公司 | A kind of deodorant and smell removing container aqueous sealant and preparation method thereof |
| CN108165215A (en) * | 2018-02-07 | 2018-06-15 | 合肥嘉仕诚能源科技有限公司 | A kind of anti-oxidant heat-resisting waterproof gasket cement of high viscosity |
| CN108867065A (en) * | 2018-07-03 | 2018-11-23 | 成都海蓉特种纺织品有限公司 | A kind of antiwear assistant and preparation method thereof for textile |
| CN110357447A (en) * | 2019-07-16 | 2019-10-22 | 常德市宏辉建星家具有限公司 | A kind of formula and preparation method thereof of the scratch resistant coating material of glass surface |
| CN110539538A (en) * | 2019-09-16 | 2019-12-06 | 福建立邦包装有限公司 | Cast CPE (chlorinated polyethylene) inflatable automatic packaging composite film and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2008038041A (en) * | 2006-08-08 | 2008-02-21 | Ceramic Coat Kk | Coating composition |
| CN101525525A (en) * | 2008-03-04 | 2009-09-09 | 金朝绪 | Acrylic ester waterproof gasket cement |
| CN101967256A (en) * | 2010-06-11 | 2011-02-09 | 广州市安泰化学有限公司 | Environment-friendly aqueous sealant for container |
-
2011
- 2011-07-19 CN CN201110201884A patent/CN102277110B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2008038041A (en) * | 2006-08-08 | 2008-02-21 | Ceramic Coat Kk | Coating composition |
| CN101525525A (en) * | 2008-03-04 | 2009-09-09 | 金朝绪 | Acrylic ester waterproof gasket cement |
| CN101967256A (en) * | 2010-06-11 | 2011-02-09 | 广州市安泰化学有限公司 | Environment-friendly aqueous sealant for container |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104387992A (en) * | 2014-11-28 | 2015-03-04 | 苏州伊埃夫化学材料科技有限公司 | Environment-friendly adhesive for artificial board and preparation method of environment-friendly adhesive |
| CN104448637A (en) * | 2014-12-01 | 2015-03-25 | 湖州绿净环保科技有限公司 | Preparation method of PTFE (polytetrafluoroethylene) film for air filtration |
| CN106554733A (en) * | 2016-10-28 | 2017-04-05 | 天长市永泰密封材料有限公司 | Ageing-resistant container aqueous sealant of a kind of uvioresistant and preparation method thereof |
| CN106554734A (en) * | 2016-10-28 | 2017-04-05 | 天长市永泰密封材料有限公司 | A kind of deodorant and smell removing container aqueous sealant and preparation method thereof |
| CN108165215A (en) * | 2018-02-07 | 2018-06-15 | 合肥嘉仕诚能源科技有限公司 | A kind of anti-oxidant heat-resisting waterproof gasket cement of high viscosity |
| CN108867065A (en) * | 2018-07-03 | 2018-11-23 | 成都海蓉特种纺织品有限公司 | A kind of antiwear assistant and preparation method thereof for textile |
| CN110357447A (en) * | 2019-07-16 | 2019-10-22 | 常德市宏辉建星家具有限公司 | A kind of formula and preparation method thereof of the scratch resistant coating material of glass surface |
| CN110539538A (en) * | 2019-09-16 | 2019-12-06 | 福建立邦包装有限公司 | Cast CPE (chlorinated polyethylene) inflatable automatic packaging composite film and preparation method thereof |
| CN110539538B (en) * | 2019-09-16 | 2021-06-15 | 福建立邦包装有限公司 | Cast CPE (chlorinated polyethylene) inflatable automatic packaging composite film and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102277110B (en) | 2012-09-19 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102277110B (en) | Aqueous sealant and preparation method thereof | |
| CN104262953B (en) | A kind of Graphene coated glass fiber strengthens polymer matrix composites and preparation method | |
| CN100558842C (en) | Cementation type polysulfide sealant | |
| CN105505166A (en) | High-performance and single-component white waterborne adhesion primer and preparation method thereof | |
| CN107963830B (en) | Anti-cracking additive and preparation method and application thereof | |
| CN104045244B (en) | Alkali-free direct roving impregnating compound for continuous fiber reinforced polyolefin | |
| CN102675981A (en) | White ink suitable for solvent-free glue compositing and preparation method thereof | |
| CN103897636A (en) | High-strength and low-temperature-resistant composite nail-free glue and preparation method thereof | |
| CN103483993A (en) | Low-temperature curing powder paint | |
| EP2562224A1 (en) | One-pack type unhardening adhesive film waterproofing material using waste rubber and method for manufacturing same | |
| CN103923587A (en) | Preparation method of bicomponent stone dry-hanging glue capable of being cured at normal temperature | |
| CN101613539B (en) | Compound modification method of microcrystalline white mica with boric acid ester and aminosilane | |
| CN107033751A (en) | A kind of low temperature cured powder coating and preparation method thereof | |
| CN107353785A (en) | A kind of normal temperature binding preparation method of powdery paints | |
| CN104559113B (en) | Delustring PC/ABS composite | |
| CN105647167A (en) | Preparation method of antistatic fiber composite material | |
| Pingkarawat et al. | An efficient healing agent for high temperature epoxy composites based upon tetra-glycidyl diamino diphenyl methane | |
| CN106633493A (en) | High-strength wood-plastic decorative sheet | |
| CN106634717A (en) | Anti-corrosive high-viscosity binder and preparation method thereof | |
| CN103805097A (en) | Environment-friendly water-based chloroprene universal rubber and preparation method thereof | |
| CN103509495A (en) | Hot melt adhesive for cable accessories | |
| CN103666094B (en) | A kind of printing-ink and its preparation method | |
| CN102585749A (en) | Unsaturated polyester resin adhesive | |
| CN110734721A (en) | aerosol spray glue and preparation method thereof | |
| CN105802519A (en) | Wood-plastic material binder for building construction |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20120919 Termination date: 20150719 |
|
| EXPY | Termination of patent right or utility model |