CN102266120A - Reaction product prepared from sun-cured tobacco with strings - Google Patents
Reaction product prepared from sun-cured tobacco with strings Download PDFInfo
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- CN102266120A CN102266120A CN201110205011XA CN201110205011A CN102266120A CN 102266120 A CN102266120 A CN 102266120A CN 201110205011X A CN201110205011X A CN 201110205011XA CN 201110205011 A CN201110205011 A CN 201110205011A CN 102266120 A CN102266120 A CN 102266120A
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Abstract
The invention relates to a reaction product prepared from sun-cured tobacco with strings, which belongs to the technical field of processing of tobacco flavor. The reaction product is prepared by the following steps: a) preparing raw material, namely ninth-grade tobacco leaves of the sun-cured tobacco with strings or crushed powder of the sun-cured tobacco with strings; b) leaching the raw material with 70% ethanol which is 20 times of the mass of the raw material for 3-5 days for fully dissolving polar components in the raw material; c) concentrating leach liquor till one half of solvent is left, adding 1mol of NaOH solution in the proportion of 10:1 by volume, refluxing in a water bath at the temperature of 60 DEG C for 30 minutes-50 minutes for full hydrolysis, further adding jujube tincture in the proportion of 4:1 in by mass, adding glucose in the proportion of 10:1 by mass, adding 1,3-propanediol in the proportion of 3:1 by mass, performing electromagnetic stirring for having Maillard reaction, heating the reaction mixture to 110 DEG C-120 DEG C and keeping the temperature for continuing the reaction for 2.5-3 hours, thereby getting the Maillard reaction product. The flavor-enhancing effect of the product is closer to the characteristic flavor of the natural tobacco and the compatibility with note of the tobacco is also better. More perfume raw materials are provided for enriching the styles of cigarettes and improving the quality of the cigarettes.
Description
Technical field:
The present invention relates to a kind ofly, belong to tobacco aromatics using production and processing technical field with rope suncured tabacco product as feedstock production.
Background technology:
Sichuan rope suncured tabacco belongs to the red cigarette series of solarization, rope suncured tabacco has abundant resin perfume (or spice), acid is fragrant and like imperial saliva sample cream perfume (or spice), in cigarette composition, use and to enrich note, remedy the fragrance style of the Zimbabwe's tobacco leaf that lacks in the homemade tobacco leaf, but because rope suncured tabacco in Sichuan has clearly red cigarette of solarization and tobacco characteristic perfume, nicotine content and protein content are higher, directly in production of cigarettes, use consumption big can cover the fine odor of other tobacco leaves, and assorted gas of band and high nicotine, consumption is little and have to mix and join inequality, causes the fragrant whole inharmonic problem of cigarette.According to routine chemical components detect data as can be known the protein of rope suncured tabacco between 25%-27%, the amino acid that can utilize tobacco oneself protein matter to be hydrolyzed into adds the higher juice extraction thing of some sugar contents and carries out Maillard reaction, and it is fragrant but also better with the harmony meeting of tobacco that its product not only can increase cigarette.
By literature search, the preparation of useful flue-cured tobacco medicinal extract, fireworks medicinal extract report in the prior art, and do not see specially routine chemical components characteristics at rope suncured tabacco, utilize himself protein hydrolysate to add some fruit juice and monose again and carry out Maillard reaction and give birth to, with the open report of the product that obtains special note feature.
Summary of the invention:
The object of the present invention is to provide a kind of flavouring effect more near tobacco feature perfume (or spice), also better with the harmony of tobacco note, what production cost was low suncures tabacco as the product of feedstock production with rope, and horn of plenty cigarette style provides more perfume material.
The present invention adopts protein in the immersion liquid of first hydrolysis rope suncured tabacco as the ammonia source of Maillard reaction, utilizes the sugar in the jujube tincture and adds glucose as the carbonyl source of reaction, add 1 again, and ammediol carries out the prepared in reaction maillard reaction product as solvent.
Of the present inventionly obtain through following steps with rope suncured tabacco product as feedstock production:
A. raw material is nine grades of tobacco leaves of rope suncured tabacco or the rope broken end of suncuring tabacco;
B. raw material fully dissolves the polar component in the raw material with 70% ethanol lixiviate of 20 times of quality multiples 3-5 days;
C. leaching liquor is concentrated half solvent, the NaOH solution that adds 1mol with 10: 1 ratio of volume multiple, backflow 30min-50min makes its abundant hydrolysis in 60 ℃ water-bath, use 4: 1 ratio of quality multiple to add jujube tincture, add glucose, add 1 again with 3: 1 ratio of quality multiple with 10: 1 ratio of quality multiple, ammediol, electromagnetic agitation is carried out Maillard reaction, make reactant mixture be heated to 110 ℃-120 ℃, maintain the temperature between 110 ℃-120 ℃ sustained response 2.5-3 hour, both handy rope suncured tabacco is as the product of feedstock production.
The invention has the advantages that: the flavouring effect of its product is more near tobacco feature perfume (or spice), and also better with the harmony of tobacco note, production cost is low, horn of plenty cigarette style, and improving cigarette quality provides more perfume material.
The specific embodiment:
Nine grades in raw material of the present invention Sichuan rope suncured tabacco or rope suncure tabacco broken end, jujube tincture, food-grade glucose, the 1-3 propane diols is is that market is bought.Preparation equipment conventional extraction equipment and normal-pressure reaction kettle.
Embodiment 1: take by weighing Sichuan rope suncured tabacco 100g, with the ethanol lixiviate 3 of 2000ml 70% or 5 days, reducing pressure with (BUCHI) R-210 Rotary Evaporators concentrated away half spirit solvent, makes the A leaching liquor.
Get the NaOH that A leaching liquor 100ml adds 10ml one molar equivalent, back flow reaction 30min in 60 ℃ of water-baths, add 25g jujube tincture, 10g glucose, 30g1-3 propane diols again, electromagnetic agitation, heating makes reactant mixture be heated to 110 ℃, maintain the temperature at 110 ℃ of sustained responses 3 hours, both got product A-1 number.
Embodiment 2: get the NaOH that A leaching liquor 100ml adds 10ml one molar equivalent, back flow reaction 50min in 60 ℃ of water-baths, add 25g jujube tincture, 10g glucose, 30g1-3 propane diols again, electromagnetic agitation, heating makes reactant mixture be heated to 120 ℃, maintain the temperature at 120 ℃ of sustained responses 3 hours, both got product A-2 number.
Sweet cream perfume (or spice), berry perfume (or spice), ageing tobacco aroma that hay is fragrant and sweet and pure and mild are arranged for product A-1 number.
There are for product A-2 number sweet cream perfume (or spice), baking perfume (or spice) and honey sample fragrant and sweet.
Be formulated in the cigarette material essence with A-1 product and A-2 product respectively, the cigarette sample of producing, through provincial judging panel it being contrasted smoking result shows: the cigarette sample that adds the A-1 reactant can increase the mellow ageing fragrance of tobacco, better set off the lively fine natural fragrance of tobacco by contrast, simultaneously can the softening flue gas, make the fragrant conglobation property of cigarette better; And the sample that adds the A-2 product can bring fragrant and sweet and some the nut notes of baking to cigarette, and it is better to be used for the blended type cigarette effect.Just on pleasant impression, can there be some residual slightly.Application test shows that such product can strengthen feature note, richness and the concentration of tobacco, can cover assorted gas effectively.To improving cigarette quality and enriching the cigarette style and get splendid effect.
Claims (1)
1. one kind with the rope suncured tabacco product as feedstock production, it is characterized in that this with the product of rope suncured tabacco as feedstock production, obtains through following steps:
A. raw material is nine grades of tobacco leaves of rope suncured tabacco or the rope broken end of suncuring tabacco;
B. raw material fully dissolves the polar component in the raw material with 70% ethanol lixiviate of 20 times of quality multiples 3-5 days;
C. leaching liquor is concentrated half solvent, the NaOH solution backflow 30min-50min in 60 ℃ water-bath that adds 1mol with 10: 1 ratio of volume multiple makes its abundant hydrolysis, use 4: 1 ratio of quality multiple to add jujube tincture, add glucose, add 1 again with 3: 1 ratio of quality multiple with 10: 1 ratio of quality multiple, ammediol, electromagnetic agitation is carried out Maillard reaction, make reactant mixture be heated to 110 ℃-120C, maintain the temperature between 110 ℃-120 ℃ sustained response 2.5-3 hour, both handy rope suncured tabacco is as the product of feedstock production.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110205011XA CN102266120A (en) | 2011-07-20 | 2011-07-20 | Reaction product prepared from sun-cured tobacco with strings |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110205011XA CN102266120A (en) | 2011-07-20 | 2011-07-20 | Reaction product prepared from sun-cured tobacco with strings |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102266120A true CN102266120A (en) | 2011-12-07 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201110205011XA Pending CN102266120A (en) | 2011-07-20 | 2011-07-20 | Reaction product prepared from sun-cured tobacco with strings |
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| CN (1) | CN102266120A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104172461A (en) * | 2014-08-20 | 2014-12-03 | 云南中烟工业有限责任公司 | Method for using red wine to promote cigarette smoking quality |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5742615B2 (en) * | 1979-09-01 | 1982-09-09 | ||
| JPS5817755B2 (en) * | 1980-11-18 | 1983-04-09 | 日本たばこ産業株式会社 | Method for producing dl-nicotine |
| JPH04207183A (en) * | 1990-11-30 | 1992-07-29 | Taiho Tsusho Kk | Aroma and taste improving combustion promoter for tobacco |
| CN101204249A (en) * | 2007-12-11 | 2008-06-25 | 广东中烟工业公司 | Preparation method for tobacco extracting |
| CN101731742A (en) * | 2008-11-10 | 2010-06-16 | 湖北中烟工业有限责任公司 | Method for catalyzing and adjusting Maillard reaction to produce tobacco flavor |
| CN102002436A (en) * | 2009-09-02 | 2011-04-06 | 湖北中烟工业有限责任公司 | Method for preparing reaction-type perfume material by using extraction residues |
-
2011
- 2011-07-20 CN CN201110205011XA patent/CN102266120A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5742615B2 (en) * | 1979-09-01 | 1982-09-09 | ||
| JPS5817755B2 (en) * | 1980-11-18 | 1983-04-09 | 日本たばこ産業株式会社 | Method for producing dl-nicotine |
| JPH04207183A (en) * | 1990-11-30 | 1992-07-29 | Taiho Tsusho Kk | Aroma and taste improving combustion promoter for tobacco |
| CN101204249A (en) * | 2007-12-11 | 2008-06-25 | 广东中烟工业公司 | Preparation method for tobacco extracting |
| CN101731742A (en) * | 2008-11-10 | 2010-06-16 | 湖北中烟工业有限责任公司 | Method for catalyzing and adjusting Maillard reaction to produce tobacco flavor |
| CN102002436A (en) * | 2009-09-02 | 2011-04-06 | 湖北中烟工业有限责任公司 | Method for preparing reaction-type perfume material by using extraction residues |
Non-Patent Citations (1)
| Title |
|---|
| 赵铭钦等: "香料烟浸膏提取工艺条件研究", 《烟草科技》, no. 3, 12 March 1999 (1999-03-12) * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104172461A (en) * | 2014-08-20 | 2014-12-03 | 云南中烟工业有限责任公司 | Method for using red wine to promote cigarette smoking quality |
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| C06 | Publication | ||
| PB01 | Publication | ||
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| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20111207 |