CN102256925B - 再生粗酯的方法 - Google Patents

再生粗酯的方法 Download PDF

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Publication number
CN102256925B
CN102256925B CN200980150535.4A CN200980150535A CN102256925B CN 102256925 B CN102256925 B CN 102256925B CN 200980150535 A CN200980150535 A CN 200980150535A CN 102256925 B CN102256925 B CN 102256925B
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CN
China
Prior art keywords
acid
water
pressure
ester
alcohol
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Expired - Fee Related
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CN200980150535.4A
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English (en)
Chinese (zh)
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CN102256925A (zh
Inventor
K·弗里泽
W·迪斯特多尔夫
J·彼得斯
G·戈尔菲耶尔
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/58—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B41/00—Formation or introduction of functional groups containing oxygen
    • C07B41/12—Formation or introduction of functional groups containing oxygen of carboxylic acid ester groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/60—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
    • C07C69/80—Phthalic acid esters
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Fats And Perfumes (AREA)
CN200980150535.4A 2008-12-16 2009-12-15 再生粗酯的方法 Expired - Fee Related CN102256925B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP08171800 2008-12-16
EP08171800.9 2008-12-16
PCT/EP2009/067178 WO2010076193A1 (de) 2008-12-16 2009-12-15 Verfahren zur aufarbeitung eines rohen esters

Publications (2)

Publication Number Publication Date
CN102256925A CN102256925A (zh) 2011-11-23
CN102256925B true CN102256925B (zh) 2014-01-22

Family

ID=42167495

Family Applications (1)

Application Number Title Priority Date Filing Date
CN200980150535.4A Expired - Fee Related CN102256925B (zh) 2008-12-16 2009-12-15 再生粗酯的方法

Country Status (9)

Country Link
US (1) US8729292B2 (https=)
EP (1) EP2379483B1 (https=)
JP (1) JP5559193B2 (https=)
KR (1) KR101346396B1 (https=)
CN (1) CN102256925B (https=)
CA (1) CA2744130C (https=)
ES (1) ES2422262T3 (https=)
MY (1) MY156371A (https=)
WO (1) WO2010076193A1 (https=)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102010048311A1 (de) 2010-10-14 2012-04-19 Continental Automotive Gmbh Verfahren und Vorrichtung zum Betreiben einer Brennkraftmaschine
CN102351692B (zh) * 2011-10-10 2013-08-21 山东天兴生物科技有限公司 癸二酸二甲酯的制备方法
DE102013015289A1 (de) * 2013-09-14 2015-03-19 Oxea Gmbh Verfahren zur Nachbehandlung von Polyolestern
BR112017001912A2 (pt) * 2014-08-01 2017-11-28 Basf Se ?processo para elaboração de um éster em bruto?
CN107074720B (zh) 2014-09-24 2021-01-08 巴斯夫欧洲公司 以反应混合物的循环制备对苯二甲酸二酯的方法
EP3197860A1 (de) 2014-09-24 2017-08-02 Basf Se Verfahren zur herstellung von terephthalsäurediestern mit rückalkohol-anreicherung
MX2017003927A (es) 2014-09-24 2017-06-30 Basf Se Proceso para producir diesteres de acido tereftalico.
MX2017003920A (es) 2014-09-24 2017-06-28 Basf Se Metodo para producir diesteres de acido tereftalico con deshidratacion de alcohol recirculado.
CN107540621B (zh) * 2017-09-27 2020-07-31 山西北化关铝化工有限公司 奥克托今合成产品抽滤效率提高的方法
KR102528326B1 (ko) * 2020-02-14 2023-05-02 한화솔루션 주식회사 에스테르계 화합물의 제조방법

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1945359A1 (de) * 1969-09-08 1971-03-11 Huels Chemische Werke Ag Verfahren zur Aufarbeitung von rohen Weichmachern
DE2330435A1 (de) * 1973-06-15 1975-01-23 Huels Chemische Werke Ag Verfahren zur aufarbeitung von rohen estern
US6310235B1 (en) * 1997-05-22 2001-10-30 Celanese Gmbh Method for producing ester plasticizers
CN1675162A (zh) * 2002-08-08 2005-09-28 巴斯福股份公司 分离酯化用催化剂的方法
CN101184721A (zh) * 2005-05-27 2008-05-21 埃克森美孚化学专利公司 增塑剂酯

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4002949A1 (de) 1990-02-01 1991-08-08 Rwe Dea Ag Verfahren zur aufarbeitung von rohem veresterungsgemisch
DE10043545A1 (de) * 2000-09-05 2002-03-14 Oxeno Olefinchemie Gmbh Verfahren zur Herstellung von Carbonsäureestern
DE10149350A1 (de) 2001-10-06 2003-04-17 Oxeno Olefinchemie Gmbh Verfahren zur Herstellung von Carbonsäureestern
US7291748B2 (en) * 2005-07-28 2007-11-06 Basf Corporation C10/C7 ester mixtures based on 2-propylheptanol

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1945359A1 (de) * 1969-09-08 1971-03-11 Huels Chemische Werke Ag Verfahren zur Aufarbeitung von rohen Weichmachern
DE2330435A1 (de) * 1973-06-15 1975-01-23 Huels Chemische Werke Ag Verfahren zur aufarbeitung von rohen estern
US6310235B1 (en) * 1997-05-22 2001-10-30 Celanese Gmbh Method for producing ester plasticizers
CN1675162A (zh) * 2002-08-08 2005-09-28 巴斯福股份公司 分离酯化用催化剂的方法
CN101184721A (zh) * 2005-05-27 2008-05-21 埃克森美孚化学专利公司 增塑剂酯

Also Published As

Publication number Publication date
CA2744130A1 (en) 2010-07-08
ES2422262T3 (es) 2013-09-10
JP2012512230A (ja) 2012-05-31
EP2379483A1 (de) 2011-10-26
CN102256925A (zh) 2011-11-23
JP5559193B2 (ja) 2014-07-23
CA2744130C (en) 2013-11-26
US20110251419A1 (en) 2011-10-13
WO2010076193A1 (de) 2010-07-08
MY156371A (en) 2016-02-15
EP2379483B1 (de) 2013-06-26
US8729292B2 (en) 2014-05-20
KR20110094351A (ko) 2011-08-23
KR101346396B1 (ko) 2014-01-02

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Granted publication date: 20140122

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