JP5559193B2 - 粗製エステルの後処理法 - Google Patents

粗製エステルの後処理法 Download PDF

Info

Publication number
JP5559193B2
JP5559193B2 JP2011541390A JP2011541390A JP5559193B2 JP 5559193 B2 JP5559193 B2 JP 5559193B2 JP 2011541390 A JP2011541390 A JP 2011541390A JP 2011541390 A JP2011541390 A JP 2011541390A JP 5559193 B2 JP5559193 B2 JP 5559193B2
Authority
JP
Japan
Prior art keywords
acid
water
ester
pressure
crude ester
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2011541390A
Other languages
English (en)
Japanese (ja)
Other versions
JP2012512230A (ja
JP2012512230A5 (https=
Inventor
フリーゼ カトリン
ディステルドルフ ヴァルター
ペータース ヤレン
ゴルフィア ギュンター
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of JP2012512230A publication Critical patent/JP2012512230A/ja
Publication of JP2012512230A5 publication Critical patent/JP2012512230A5/ja
Application granted granted Critical
Publication of JP5559193B2 publication Critical patent/JP5559193B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/58—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B41/00—Formation or introduction of functional groups containing oxygen
    • C07B41/12—Formation or introduction of functional groups containing oxygen of carboxylic acid ester groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/60—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
    • C07C69/80—Phthalic acid esters
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Fats And Perfumes (AREA)
JP2011541390A 2008-12-16 2009-12-15 粗製エステルの後処理法 Expired - Fee Related JP5559193B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP08171800 2008-12-16
EP08171800.9 2008-12-16
PCT/EP2009/067178 WO2010076193A1 (de) 2008-12-16 2009-12-15 Verfahren zur aufarbeitung eines rohen esters

Publications (3)

Publication Number Publication Date
JP2012512230A JP2012512230A (ja) 2012-05-31
JP2012512230A5 JP2012512230A5 (https=) 2013-12-26
JP5559193B2 true JP5559193B2 (ja) 2014-07-23

Family

ID=42167495

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2011541390A Expired - Fee Related JP5559193B2 (ja) 2008-12-16 2009-12-15 粗製エステルの後処理法

Country Status (9)

Country Link
US (1) US8729292B2 (https=)
EP (1) EP2379483B1 (https=)
JP (1) JP5559193B2 (https=)
KR (1) KR101346396B1 (https=)
CN (1) CN102256925B (https=)
CA (1) CA2744130C (https=)
ES (1) ES2422262T3 (https=)
MY (1) MY156371A (https=)
WO (1) WO2010076193A1 (https=)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102010048311A1 (de) 2010-10-14 2012-04-19 Continental Automotive Gmbh Verfahren und Vorrichtung zum Betreiben einer Brennkraftmaschine
CN102351692B (zh) * 2011-10-10 2013-08-21 山东天兴生物科技有限公司 癸二酸二甲酯的制备方法
DE102013015289A1 (de) * 2013-09-14 2015-03-19 Oxea Gmbh Verfahren zur Nachbehandlung von Polyolestern
BR112017001912A2 (pt) * 2014-08-01 2017-11-28 Basf Se ?processo para elaboração de um éster em bruto?
CN107074720B (zh) 2014-09-24 2021-01-08 巴斯夫欧洲公司 以反应混合物的循环制备对苯二甲酸二酯的方法
EP3197860A1 (de) 2014-09-24 2017-08-02 Basf Se Verfahren zur herstellung von terephthalsäurediestern mit rückalkohol-anreicherung
MX2017003927A (es) 2014-09-24 2017-06-30 Basf Se Proceso para producir diesteres de acido tereftalico.
MX2017003920A (es) 2014-09-24 2017-06-28 Basf Se Metodo para producir diesteres de acido tereftalico con deshidratacion de alcohol recirculado.
CN107540621B (zh) * 2017-09-27 2020-07-31 山西北化关铝化工有限公司 奥克托今合成产品抽滤效率提高的方法
KR102528326B1 (ko) * 2020-02-14 2023-05-02 한화솔루션 주식회사 에스테르계 화합물의 제조방법

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1945359B2 (de) 1969-09-08 1973-05-10 Verfahren zur gewinnung von estern
DE2330435C3 (de) 1973-06-15 1978-08-17 Chemische Werke Huels Ag, 4370 Marl Verfahren zur Aufarbeitung von rohen Estern
DE4002949A1 (de) 1990-02-01 1991-08-08 Rwe Dea Ag Verfahren zur aufarbeitung von rohem veresterungsgemisch
DE19721347B9 (de) * 1997-05-22 2005-09-29 Celanese Chemicals Europe Gmbh Verfahren zur Herstellung von Esterweichmachern
DE10043545A1 (de) * 2000-09-05 2002-03-14 Oxeno Olefinchemie Gmbh Verfahren zur Herstellung von Carbonsäureestern
DE10149350A1 (de) 2001-10-06 2003-04-17 Oxeno Olefinchemie Gmbh Verfahren zur Herstellung von Carbonsäureestern
DE10236279A1 (de) * 2002-08-08 2004-02-19 Basf Ag Verfahren zur Abtrennung von Veresterungskatalysator
US7919649B2 (en) * 2005-05-27 2011-04-05 Exxonmobile Chemical Patents Inc. Plasticiser esters
US7291748B2 (en) * 2005-07-28 2007-11-06 Basf Corporation C10/C7 ester mixtures based on 2-propylheptanol

Also Published As

Publication number Publication date
CA2744130A1 (en) 2010-07-08
ES2422262T3 (es) 2013-09-10
JP2012512230A (ja) 2012-05-31
EP2379483A1 (de) 2011-10-26
CN102256925A (zh) 2011-11-23
CA2744130C (en) 2013-11-26
US20110251419A1 (en) 2011-10-13
CN102256925B (zh) 2014-01-22
WO2010076193A1 (de) 2010-07-08
MY156371A (en) 2016-02-15
EP2379483B1 (de) 2013-06-26
US8729292B2 (en) 2014-05-20
KR20110094351A (ko) 2011-08-23
KR101346396B1 (ko) 2014-01-02

Similar Documents

Publication Publication Date Title
JP5559193B2 (ja) 粗製エステルの後処理法
KR101733814B1 (ko) 알콜 증기를 사용하는 스트립핑에 의한 카르복실산 에스테르의 제조
JP5780967B2 (ja) カルボン酸エステルの製造方法
TWI297681B (en) Process for preparing carboxylic esters
US20080245996A1 (en) Method for producing benzoic acid esters
CN105658613B (zh) 多元醇酯的后处理方法
CN105555750B (zh) 从多元醇酯制备中的侧流得到富含多元醇酯的产物流的方法
CA2956306C (en) Process comprising emulsification and agglomeration in the workup of crude esters
RU2424224C2 (ru) Способ введения и регенерации кобальта в процессе гидроформилирования пропилена

Legal Events

Date Code Title Description
A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20130502

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20130513

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20130812

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20130819

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20130911

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20130919

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20131011

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20131021

A524 Written submission of copy of amendment under article 19 pct

Free format text: JAPANESE INTERMEDIATE CODE: A524

Effective date: 20131111

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20140507

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20140605

R150 Certificate of patent or registration of utility model

Ref document number: 5559193

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

LAPS Cancellation because of no payment of annual fees